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The title complex, [Ni(C30H22N4O2)], has a square-planar geometry at the Ni atom.

Supporting information

cif

Crystallographic Information File (CIF) https://doi.org/10.1107/S1600536806051038/ng2132sup1.cif
Contains datablocks global, I

hkl

Structure factor file (CIF format) https://doi.org/10.1107/S1600536806051038/ng2132Isup2.hkl
Contains datablock I

CCDC reference: 633928

Key indicators

  • Single-crystal X-ray study
  • T = 294 K
  • Mean [sigma](C-C) = 0.003 Å
  • R factor = 0.039
  • wR factor = 0.091
  • Data-to-parameter ratio = 16.0

checkCIF/PLATON results

No syntax errors found



Alert level C PLAT042_ALERT_1_C Calc. and Rep. MoietyFormula Strings Differ .... ? PLAT066_ALERT_1_C Predicted and Reported Transmissions Identical . ? PLAT125_ALERT_4_C No _symmetry_space_group_name_Hall Given ....... ? PLAT369_ALERT_2_C Long C(sp2)-C(sp2) Bond C1 - C2 ... 1.54 Ang. PLAT710_ALERT_4_C Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 3 N3 -NI1 -N1 -C1 59.50 0.40 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_C Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 6 N3 -NI1 -N1 -C18 -116.00 0.40 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_C Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 8 N4 -NI1 -N2 -C2 123.10 0.80 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_C Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 11 N4 -NI1 -N2 -C3 -58.60 0.80 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_C Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 14 N1 -NI1 -N3 -C9 -99.00 0.40 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_C Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 17 N1 -NI1 -N3 -C10 74.90 0.40 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_C Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 19 N2 -NI1 -N4 -C12 -84.30 0.80 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_C Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 22 N2 -NI1 -N4 -C11 89.30 0.80 1.555 1.555 1.555 1.555
0 ALERT level A = In general: serious problem 0 ALERT level B = Potentially serious problem 12 ALERT level C = Check and explain 0 ALERT level G = General alerts; check 2 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 1 ALERT type 2 Indicator that the structure model may be wrong or deficient 0 ALERT type 3 Indicator that the structure quality may be low 9 ALERT type 4 Improvement, methodology, query or suggestion 0 ALERT type 5 Informative message, check

Computing details top

Data collection: CrystalClear (Rigaku/MSC, 2005); cell refinement: CrystalClear; data reduction: CrystalClear; program(s) used to solve structure: SHELXS97 (Sheldrick, 1997); program(s) used to refine structure: SHELXL97 (Sheldrick, 1997); molecular graphics: CrystalStructure (Rigaku/MSC, 2005); software used to prepare material for publication: CrystalStructure.

(7,12-Diphenyl-5,6:13,14-dibenzo-8,11-diazonia-1,4-diazacyclopentadeca- 7,12-diene-2,3-dione)nickel(II) top
Crystal data top
[Ni(C30H22N4O2)]F(000) = 1096
Mr = 529.23Dx = 1.496 Mg m3
Monoclinic, P21/cMo Kα radiation, λ = 0.71070 Å
a = 15.817 (5) ÅCell parameters from 5597 reflections
b = 10.363 (3) Åθ = 3.2–27.5°
c = 16.321 (5) ŵ = 0.86 mm1
β = 118.561 (3)°T = 294 K
V = 2349.7 (11) Å3Block, red
Z = 40.06 × 0.04 × 0.04 mm
Data collection top
Rigaku Saturn
diffractometer
5373 independent reflections
Radiation source: rotating anode4318 reflections with I > 2σ(I)
Confocal monochromatorRint = 0.057
Detector resolution: 7.31 pixels mm-1θmax = 27.5°, θmin = 3.2°
ω scansh = 1620
Absorption correction: multi-scan
(Jacobson, 1998)
k = 139
Tmin = 0.950, Tmax = 0.966l = 2114
14754 measured reflections
Refinement top
Refinement on F2Primary atom site location: structure-invariant direct methods
Least-squares matrix: fullSecondary atom site location: difference Fourier map
R[F2 > 2σ(F2)] = 0.039Hydrogen site location: inferred from neighbouring sites
wR(F2) = 0.091H-atom parameters constrained
S = 1.06 w = 1/[σ2(Fo2) + (0.0342P)2 + 0.3465P]
where P = (Fo2 + 2Fc2)/3
5373 reflections(Δ/σ)max = 0.001
335 parametersΔρmax = 0.36 e Å3
0 restraintsΔρmin = 0.31 e Å3
Special details top

Geometry. All e.s.d.'s (except the e.s.d. in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell e.s.d.'s are taken into account individually in the estimation of e.s.d.'s in distances, angles and torsion angles; correlations between e.s.d.'s in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell e.s.d.'s is used for estimating e.s.d.'s involving l.s. planes.

Refinement. Refinement of F2 against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F2, conventional R-factors R are based on F, with F set to zero for negative F2. The threshold expression of F2 > σ(F2) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F2 are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger.

Fractional atomic coordinates and isotropic or equivalent isotropic displacement parameters (Å2) top
xyzUiso*/Ueq
Ni10.630951 (17)1.07406 (2)0.191739 (17)0.03119 (9)
O10.58010 (12)1.43631 (15)0.14277 (12)0.0527 (4)
O20.77470 (11)1.38748 (15)0.21426 (11)0.0462 (4)
N10.55597 (11)1.21335 (16)0.12454 (11)0.0330 (4)
N20.73594 (11)1.16997 (16)0.20590 (11)0.0333 (4)
N30.70881 (12)0.94942 (16)0.27729 (12)0.0342 (4)
N40.52612 (12)0.96885 (17)0.16861 (12)0.0345 (4)
C10.60862 (15)1.3251 (2)0.15118 (14)0.0366 (4)
C20.71761 (14)1.2983 (2)0.19496 (14)0.0356 (4)
C30.82564 (14)1.1183 (2)0.22797 (14)0.0327 (4)
C40.88406 (16)1.1760 (2)0.19498 (16)0.0426 (5)
H40.86391.25210.16070.051*
C50.97052 (17)1.1218 (2)0.21263 (19)0.0524 (6)
H51.00691.16040.18840.063*
C61.00433 (18)1.0110 (2)0.2656 (2)0.0549 (6)
H61.06360.97610.27840.066*
C70.94876 (16)0.9532 (2)0.29915 (18)0.0442 (5)
H70.97160.87940.33570.053*
C80.85821 (14)1.0027 (2)0.27964 (14)0.0345 (4)
C90.79976 (14)0.92919 (19)0.31139 (14)0.0335 (4)
C100.64968 (14)0.8795 (2)0.31095 (15)0.0405 (5)
H10A0.63900.93280.35400.049*
H10B0.68150.80060.34250.049*
C110.55611 (15)0.8498 (2)0.22603 (15)0.0428 (5)
H11A0.56420.77940.19120.051*
H11B0.50790.82520.24380.051*
C120.43714 (14)0.9834 (2)0.10559 (13)0.0320 (4)
C130.40096 (14)1.1003 (2)0.04828 (13)0.0325 (4)
C140.30474 (16)1.1010 (2)0.02286 (15)0.0424 (5)
H140.26741.02780.03180.051*
C150.26374 (16)1.2062 (2)0.07987 (15)0.0466 (5)
H150.19941.20450.12530.056*
C160.31980 (16)1.3148 (2)0.06860 (15)0.0423 (5)
H160.29331.38590.10740.051*
C170.41431 (15)1.3173 (2)0.00008 (14)0.0390 (5)
H170.45071.39090.00670.047*
C180.45802 (14)1.21205 (19)0.06031 (13)0.0319 (4)
C190.84872 (14)0.8253 (2)0.38215 (14)0.0356 (4)
C200.90706 (17)0.8566 (3)0.47512 (16)0.0510 (6)
H200.91740.94250.49390.061*
C210.9497 (2)0.7592 (3)0.53967 (19)0.0674 (8)
H210.98810.77970.60230.081*
C220.9358 (2)0.6316 (3)0.5122 (2)0.0662 (8)
H220.96360.56630.55620.079*
C230.88040 (19)0.6012 (2)0.4191 (2)0.0587 (7)
H230.87290.51550.40000.070*
C240.83626 (16)0.6973 (2)0.35439 (18)0.0456 (5)
H240.79790.67630.29190.055*
C250.36742 (14)0.8746 (2)0.08710 (13)0.0338 (4)
C260.37608 (18)0.7646 (2)0.04341 (16)0.0485 (6)
H260.42590.75810.02860.058*
C270.3108 (2)0.6644 (3)0.02166 (18)0.0607 (7)
H270.31650.59050.00760.073*
C280.2373 (2)0.6757 (3)0.04403 (17)0.0611 (7)
H280.19220.60980.02800.073*
C290.22977 (17)0.7828 (3)0.08952 (17)0.0537 (6)
H290.18070.78830.10540.064*
C300.29534 (15)0.8827 (2)0.11176 (16)0.0417 (5)
H300.29080.95500.14320.050*
Atomic displacement parameters (Å2) top
U11U22U33U12U13U23
Ni10.02749 (14)0.02899 (15)0.03853 (14)0.00035 (10)0.01694 (10)0.00667 (11)
O10.0476 (10)0.0293 (9)0.0704 (11)0.0035 (7)0.0196 (8)0.0012 (8)
O20.0424 (9)0.0333 (8)0.0629 (10)0.0087 (7)0.0251 (8)0.0002 (8)
N10.0306 (8)0.0292 (9)0.0407 (9)0.0003 (7)0.0182 (7)0.0053 (7)
N20.0304 (8)0.0295 (9)0.0399 (9)0.0008 (7)0.0169 (7)0.0054 (7)
N30.0314 (8)0.0330 (9)0.0397 (9)0.0007 (7)0.0182 (7)0.0075 (7)
N40.0312 (9)0.0316 (9)0.0424 (9)0.0016 (7)0.0190 (7)0.0108 (8)
C10.0395 (11)0.0313 (11)0.0403 (10)0.0012 (9)0.0202 (9)0.0034 (9)
C20.0365 (11)0.0341 (12)0.0380 (10)0.0044 (8)0.0193 (8)0.0021 (9)
C30.0298 (10)0.0312 (10)0.0392 (10)0.0044 (8)0.0183 (8)0.0035 (9)
C40.0428 (12)0.0391 (12)0.0534 (12)0.0039 (9)0.0291 (10)0.0024 (10)
C50.0500 (14)0.0479 (14)0.0803 (17)0.0057 (11)0.0481 (13)0.0021 (14)
C60.0424 (13)0.0468 (15)0.0900 (19)0.0024 (11)0.0433 (13)0.0019 (14)
C70.0385 (12)0.0338 (12)0.0647 (14)0.0025 (9)0.0283 (10)0.0007 (11)
C80.0325 (10)0.0304 (11)0.0432 (10)0.0032 (8)0.0203 (8)0.0027 (9)
C90.0329 (10)0.0285 (11)0.0392 (10)0.0008 (8)0.0175 (8)0.0001 (9)
C100.0353 (11)0.0441 (13)0.0464 (11)0.0022 (9)0.0232 (9)0.0160 (10)
C110.0351 (11)0.0374 (13)0.0540 (12)0.0017 (9)0.0199 (9)0.0142 (10)
C120.0325 (10)0.0319 (11)0.0361 (9)0.0020 (8)0.0201 (8)0.0001 (8)
C130.0323 (10)0.0325 (11)0.0346 (9)0.0009 (8)0.0176 (8)0.0027 (8)
C140.0369 (11)0.0409 (13)0.0436 (11)0.0039 (9)0.0145 (9)0.0058 (10)
C150.0379 (12)0.0488 (15)0.0421 (11)0.0028 (10)0.0103 (9)0.0055 (10)
C160.0429 (12)0.0377 (12)0.0409 (11)0.0102 (9)0.0158 (9)0.0086 (10)
C170.0406 (12)0.0321 (11)0.0448 (11)0.0022 (9)0.0207 (9)0.0032 (9)
C180.0313 (10)0.0324 (11)0.0365 (9)0.0038 (8)0.0198 (8)0.0020 (8)
C190.0302 (10)0.0324 (11)0.0444 (11)0.0034 (8)0.0180 (8)0.0061 (9)
C200.0493 (14)0.0471 (15)0.0484 (13)0.0153 (11)0.0168 (10)0.0015 (11)
C210.0572 (17)0.088 (2)0.0494 (14)0.0327 (15)0.0194 (12)0.0155 (15)
C220.0601 (17)0.0625 (19)0.089 (2)0.0338 (15)0.0461 (16)0.0427 (17)
C230.0475 (14)0.0342 (14)0.104 (2)0.0075 (11)0.0441 (15)0.0138 (14)
C240.0367 (12)0.0344 (12)0.0639 (14)0.0014 (9)0.0227 (10)0.0030 (11)
C250.0327 (10)0.0310 (11)0.0365 (10)0.0008 (8)0.0156 (8)0.0039 (9)
C260.0607 (15)0.0463 (14)0.0456 (12)0.0056 (11)0.0312 (11)0.0036 (11)
C270.094 (2)0.0382 (14)0.0486 (13)0.0161 (13)0.0331 (14)0.0059 (12)
C280.0685 (18)0.0467 (15)0.0525 (14)0.0277 (13)0.0164 (12)0.0063 (12)
C290.0397 (13)0.0637 (18)0.0558 (14)0.0107 (11)0.0214 (11)0.0153 (13)
C300.0355 (11)0.0403 (12)0.0500 (12)0.0031 (9)0.0210 (9)0.0018 (10)
Geometric parameters (Å, º) top
Ni1—N21.8527 (16)C12—C251.504 (3)
Ni1—N11.8572 (17)C13—C141.405 (3)
Ni1—N41.8660 (17)C13—C181.423 (3)
Ni1—N31.8682 (17)C14—C151.378 (3)
O1—C11.221 (3)C14—H140.9300
O2—C21.224 (2)C15—C161.390 (3)
N1—C11.371 (3)C15—H150.9300
N1—C181.395 (2)C16—C171.374 (3)
N2—C21.354 (3)C16—H160.9300
N2—C31.393 (2)C17—C181.410 (3)
N3—C91.287 (3)C17—H170.9300
N3—C101.481 (2)C19—C201.386 (3)
N4—C121.295 (3)C19—C241.386 (3)
N4—C111.483 (3)C20—C211.380 (3)
C1—C21.543 (3)C20—H200.9300
C3—C41.406 (3)C21—C221.380 (4)
C3—C81.413 (3)C21—H210.9300
C4—C51.376 (3)C22—C231.379 (4)
C4—H40.9300C22—H220.9300
C5—C61.382 (3)C23—C241.374 (3)
C5—H50.9300C23—H230.9300
C6—C71.375 (3)C24—H240.9300
C6—H60.9300C25—C301.381 (3)
C7—C81.407 (3)C25—C261.385 (3)
C7—H70.9300C26—C271.385 (3)
C8—C91.470 (3)C26—H260.9300
C9—C191.496 (3)C27—C281.381 (4)
C10—C111.498 (3)C27—H270.9300
C10—H10A0.9700C28—C291.371 (4)
C10—H10B0.9700C28—H280.9300
C11—H11A0.9700C29—C301.386 (3)
C11—H11B0.9700C29—H290.9300
C12—C131.469 (3)C30—H300.9300
N2—Ni1—N186.44 (7)N4—C12—C13123.13 (18)
N2—Ni1—N4174.58 (8)N4—C12—C25119.08 (19)
N1—Ni1—N494.58 (7)C13—C12—C25117.75 (17)
N2—Ni1—N392.66 (7)C14—C13—C18118.33 (19)
N1—Ni1—N3170.18 (8)C14—C13—C12117.96 (19)
N4—Ni1—N387.23 (7)C18—C13—C12123.71 (18)
C1—N1—C18122.31 (17)C15—C14—C13122.4 (2)
C1—N1—Ni1110.49 (13)C15—C14—H14118.8
C18—N1—Ni1127.04 (14)C13—C14—H14118.8
C2—N2—C3122.62 (16)C14—C15—C16119.2 (2)
C2—N2—Ni1112.80 (13)C14—C15—H15120.4
C3—N2—Ni1124.55 (14)C16—C15—H15120.4
C9—N3—C10122.24 (17)C17—C16—C15120.0 (2)
C9—N3—Ni1129.54 (14)C17—C16—H16120.0
C10—N3—Ni1107.93 (13)C15—C16—H16120.0
C12—N4—C11119.78 (17)C16—C17—C18122.3 (2)
C12—N4—Ni1127.99 (15)C16—C17—H17118.9
C11—N4—Ni1111.92 (12)C18—C17—H17118.9
O1—C1—N1128.8 (2)N1—C18—C17121.00 (18)
O1—C1—C2119.55 (19)N1—C18—C13120.98 (18)
N1—C1—C2111.66 (18)C17—C18—C13117.81 (18)
O2—C2—N2128.5 (2)C20—C19—C24119.9 (2)
O2—C2—C1120.42 (19)C20—C19—C9120.4 (2)
N2—C2—C1111.07 (17)C24—C19—C9119.78 (19)
N2—C3—C4120.77 (19)C21—C20—C19119.5 (2)
N2—C3—C8121.07 (16)C21—C20—H20120.3
C4—C3—C8118.07 (18)C19—C20—H20120.3
C5—C4—C3121.0 (2)C22—C21—C20120.6 (3)
C5—C4—H4119.5C22—C21—H21119.7
C3—C4—H4119.5C20—C21—H21119.7
C4—C5—C6121.3 (2)C23—C22—C21119.7 (2)
C4—C5—H5119.4C23—C22—H22120.2
C6—C5—H5119.4C21—C22—H22120.2
C7—C6—C5118.7 (2)C24—C23—C22120.2 (3)
C7—C6—H6120.6C24—C23—H23119.9
C5—C6—H6120.6C22—C23—H23119.9
C6—C7—C8121.8 (2)C23—C24—C19120.1 (2)
C6—C7—H7119.1C23—C24—H24119.9
C8—C7—H7119.1C19—C24—H24119.9
C7—C8—C3119.04 (18)C30—C25—C26119.9 (2)
C7—C8—C9118.35 (19)C30—C25—C12121.62 (19)
C3—C8—C9122.58 (18)C26—C25—C12118.47 (19)
N3—C9—C8121.62 (18)C27—C26—C25120.2 (2)
N3—C9—C19120.66 (17)C27—C26—H26119.9
C8—C9—C19117.67 (17)C25—C26—H26119.9
N3—C10—C11106.09 (17)C28—C27—C26119.2 (2)
N3—C10—H10A110.5C28—C27—H27120.4
C11—C10—H10A110.5C26—C27—H27120.4
N3—C10—H10B110.5C29—C28—C27120.9 (2)
C11—C10—H10B110.5C29—C28—H28119.6
H10A—C10—H10B108.7C27—C28—H28119.6
N4—C11—C10106.84 (17)C28—C29—C30119.9 (2)
N4—C11—H11A110.4C28—C29—H29120.0
C10—C11—H11A110.4C30—C29—H29120.0
N4—C11—H11B110.4C25—C30—C29119.8 (2)
C10—C11—H11B110.4C25—C30—H30120.1
H11A—C11—H11B108.6C29—C30—H30120.1
N2—Ni1—N1—C125.51 (14)C3—C8—C9—N315.5 (3)
N4—Ni1—N1—C1159.82 (14)C7—C8—C9—C1915.0 (3)
N3—Ni1—N1—C159.5 (4)C3—C8—C9—C19167.12 (18)
N2—Ni1—N1—C18158.96 (16)C9—N3—C10—C11140.2 (2)
N4—Ni1—N1—C1815.71 (16)Ni1—N3—C10—C1145.5 (2)
N3—Ni1—N1—C18116.0 (4)C12—N4—C11—C10160.81 (18)
N1—Ni1—N2—C222.04 (14)Ni1—N4—C11—C1025.0 (2)
N4—Ni1—N2—C2123.1 (8)N3—C10—C11—N444.7 (2)
N3—Ni1—N2—C2148.16 (15)C11—N4—C12—C13177.68 (18)
N1—Ni1—N2—C3159.64 (16)Ni1—N4—C12—C139.2 (3)
N4—Ni1—N2—C358.6 (8)C11—N4—C12—C254.5 (3)
N3—Ni1—N2—C330.15 (16)Ni1—N4—C12—C25168.60 (14)
N2—Ni1—N3—C914.48 (19)N4—C12—C13—C14175.1 (2)
N1—Ni1—N3—C999.0 (4)C25—C12—C13—C142.7 (3)
N4—Ni1—N3—C9160.10 (19)N4—C12—C13—C184.4 (3)
N2—Ni1—N3—C10159.36 (14)C25—C12—C13—C18177.78 (18)
N1—Ni1—N3—C1074.9 (4)C18—C13—C14—C151.1 (3)
N4—Ni1—N3—C1026.07 (14)C12—C13—C14—C15179.43 (19)
N2—Ni1—N4—C1284.3 (8)C13—C14—C15—C161.6 (4)
N1—Ni1—N4—C1216.42 (19)C14—C15—C16—C171.2 (3)
N3—Ni1—N4—C12173.25 (19)C15—C16—C17—C180.3 (3)
N2—Ni1—N4—C1189.3 (8)C1—N1—C18—C1718.5 (3)
N1—Ni1—N4—C11170.02 (14)Ni1—N1—C18—C17166.46 (14)
N3—Ni1—N4—C110.31 (15)C1—N1—C18—C13166.88 (18)
C18—N1—C1—O117.6 (3)Ni1—N1—C18—C138.2 (3)
Ni1—N1—C1—O1158.2 (2)C16—C17—C18—N1175.1 (2)
C18—N1—C1—C2160.89 (16)C16—C17—C18—C130.3 (3)
Ni1—N1—C1—C223.34 (19)C14—C13—C18—N1174.71 (18)
C3—N2—C2—O211.2 (3)C12—C13—C18—N14.8 (3)
Ni1—N2—C2—O2167.15 (18)C14—C13—C18—C170.1 (3)
C3—N2—C2—C1168.16 (17)C12—C13—C18—C17179.56 (17)
Ni1—N2—C2—C113.5 (2)N3—C9—C19—C20105.6 (2)
O1—C1—C2—O25.9 (3)C8—C9—C19—C2077.0 (3)
N1—C1—C2—O2172.76 (19)N3—C9—C19—C2475.0 (3)
O1—C1—C2—N2174.69 (19)C8—C9—C19—C24102.4 (2)
N1—C1—C2—N26.7 (2)C24—C19—C20—C212.1 (3)
C2—N2—C3—C433.2 (3)C9—C19—C20—C21178.4 (2)
Ni1—N2—C3—C4148.64 (17)C19—C20—C21—C220.9 (4)
C2—N2—C3—C8150.3 (2)C20—C21—C22—C231.4 (4)
Ni1—N2—C3—C827.8 (3)C21—C22—C23—C242.5 (4)
N2—C3—C4—C5176.7 (2)C22—C23—C24—C191.3 (3)
C8—C3—C4—C50.1 (3)C20—C19—C24—C231.0 (3)
C3—C4—C5—C62.0 (4)C9—C19—C24—C23179.5 (2)
C4—C5—C6—C71.5 (4)N4—C12—C25—C30110.1 (2)
C5—C6—C7—C81.0 (4)C13—C12—C25—C3072.0 (3)
C6—C7—C8—C33.1 (3)N4—C12—C25—C2670.5 (3)
C6—C7—C8—C9174.9 (2)C13—C12—C25—C26107.4 (2)
N2—C3—C8—C7179.12 (19)C30—C25—C26—C272.1 (3)
C4—C3—C8—C72.5 (3)C12—C25—C26—C27177.3 (2)
N2—C3—C8—C91.3 (3)C25—C26—C27—C280.0 (4)
C4—C3—C8—C9175.3 (2)C26—C27—C28—C291.8 (4)
C10—N3—C9—C8177.72 (19)C27—C28—C29—C301.4 (4)
Ni1—N3—C9—C84.7 (3)C26—C25—C30—C292.4 (3)
C10—N3—C9—C195.0 (3)C12—C25—C30—C29176.9 (2)
Ni1—N3—C9—C19178.03 (14)C28—C29—C30—C250.7 (4)
C7—C8—C9—N3162.4 (2)
 

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