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Colourless rhombohedral crystals of dodekakis[tris(2-aminoethyl)amine]heptacadmium(II) tetradecaperchlorate, [Cd7(tren)12](ClO4)14, form from aqueous solutions of the cellulose solvent `Cd–tren' on addition of perchloric acid. The heptanuclear cations are flat star-shaped disks and are composed of Cd(tren) moieties that are linked by further tren ligands, which exhibit the unusual μ3,κ3N,N′,N′′ mode of coordination.

Supporting information

cif

Crystallographic Information File (CIF)
Contains datablocks cdtren, cd

hkl

Structure factor file (CIF format)
Contains datablock cd

CCDC reference: 130094

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