Supporting information
Crystallographic Information File (CIF) https://doi.org/10.1107/S1600536804018112/lh6228sup1.cif | |
Structure factor file (CIF format) https://doi.org/10.1107/S1600536804018112/lh6228Isup2.hkl |
CCDC reference: 248757
Data collection: SMART (Siemens, 1996); cell refinement: SMART and SAINT (Siemens, 1994); data reduction: XPREP (Siemens, 1994); program(s) used to solve structure: SHELXTL (Siemens, 1994); program(s) used to refine structure: SHELXTL; molecular graphics: SHELXTL; software used to prepare material for publication: SHELXTL.
[Ag3Cl2(C25H22P2)3][SbF6]·2CH2Cl2 | F(000) = 3880 |
Mr = 1953.21 | Dx = 1.575 Mg m−3 |
Monoclinic, P21/n | Mo Kα radiation, λ = 0.71073 Å |
Hall symbol: -P 2yn | Cell parameters from 6217 reflections |
a = 16.0613 (4) Å | θ = 1.3–25.6° |
b = 18.1719 (5) Å | µ = 1.39 mm−1 |
c = 28.3500 (7) Å | T = 293 K |
β = 95.303 (1)° | Prism, pale yellow |
V = 8238.9 (4) Å3 | 0.60 × 0.50 × 0.32 mm |
Z = 4 |
Siemens SMART CCD diffractometer | 14352 independent reflections |
Radiation source: fine-focus sealed tube | 10131 reflections with I > 2σ(I) |
Graphite monochromator | Rint = 0.057 |
ω scans | θmax = 25.6°, θmin = 1.3° |
Absorption correction: multi-scan (SADABS; Sheldrick, 1996) | h = −19→9 |
Tmin = 0.438, Tmax = 0.641 | k = −16→21 |
28476 measured reflections | l = −32→34 |
Refinement on F2 | Primary atom site location: structure-invariant direct methods |
Least-squares matrix: full | Secondary atom site location: difference Fourier map |
R[F2 > 2σ(F2)] = 0.072 | Hydrogen site location: inferred from neighbouring sites |
wR(F2) = 0.171 | H-atom parameters constrained |
S = 1.22 | w = 1/[σ2(Fo2) + (0.0294P)2 + 55.193P] where P = (Fo2 + 2Fc2)/3 |
14352 reflections | (Δ/σ)max = 0.094 |
892 parameters | Δρmax = 1.54 e Å−3 |
6 restraints | Δρmin = −1.06 e Å−3 |
Geometry. All e.s.d.'s (except the e.s.d. in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell e.s.d.'s are taken into account individually in the estimation of e.s.d.'s in distances, angles and torsion angles; correlations between e.s.d.'s in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell e.s.d.'s is used for estimating e.s.d.'s involving l.s. planes. |
Refinement. Refinement of F2 against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F2, conventional R-factors R are based on F, with F set to zero for negative F2. The threshold expression of F2 > σ(F2) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F2 are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger. |
x | y | z | Uiso*/Ueq | ||
Ag3 | 0.85375 (4) | 0.82543 (4) | 0.75825 (2) | 0.04721 (18) | |
Ag2 | 0.95918 (4) | 0.82398 (5) | 0.66148 (2) | 0.0528 (2) | |
Ag1 | 1.06488 (4) | 0.78071 (4) | 0.76999 (2) | 0.0528 (2) | |
Sb1 | 0.43565 (4) | 0.77895 (5) | 0.55432 (3) | 0.0693 (2) | |
P2 | 0.86252 (13) | 0.82303 (13) | 0.84630 (7) | 0.0386 (5) | |
C01 | 0.7404 (5) | 0.7847 (5) | 0.6417 (3) | 0.0394 (19) | |
H01A | 0.7551 | 0.7330 | 0.6414 | 0.047* | |
H01B | 0.6879 | 0.7907 | 0.6223 | 0.047* | |
Cl2 | 0.93667 (13) | 0.70478 (12) | 0.72449 (8) | 0.0482 (5) | |
P5 | 1.09321 (13) | 0.80082 (13) | 0.62819 (8) | 0.0414 (5) | |
Cl1 | 0.98756 (14) | 0.91145 (12) | 0.73781 (8) | 0.0483 (5) | |
P6 | 1.19248 (13) | 0.77800 (13) | 0.72676 (8) | 0.0421 (5) | |
P4 | 0.82170 (14) | 0.83775 (14) | 0.61517 (8) | 0.0463 (6) | |
P3 | 0.72575 (13) | 0.81242 (12) | 0.70306 (7) | 0.0390 (5) | |
P1 | 1.04450 (13) | 0.75886 (13) | 0.85544 (8) | 0.0407 (5) | |
C211 | 0.7655 (5) | 0.7949 (5) | 0.8715 (3) | 0.046 (2) | |
C621 | 1.2830 (6) | 0.8242 (5) | 0.7595 (3) | 0.049 (2) | |
C121 | 1.0952 (5) | 0.8284 (5) | 0.8955 (3) | 0.047 (2) | |
C521 | 1.1126 (5) | 0.7059 (5) | 0.6089 (3) | 0.048 (2) | |
C421 | 0.7746 (6) | 0.9294 (5) | 0.6046 (3) | 0.055 (2) | |
C321 | 0.6642 (5) | 0.7332 (5) | 0.7220 (3) | 0.043 (2) | |
C511 | 1.1044 (6) | 0.8547 (5) | 0.5740 (3) | 0.049 (2) | |
C221 | 0.8912 (6) | 0.9103 (5) | 0.8775 (3) | 0.047 (2) | |
C212 | 0.7627 (6) | 0.7709 (6) | 0.9181 (3) | 0.060 (3) | |
H21A | 0.8120 | 0.7678 | 0.9380 | 0.072* | |
C03 | 1.1882 (5) | 0.8239 (5) | 0.6677 (3) | 0.045 (2) | |
H03A | 1.1903 | 0.8768 | 0.6724 | 0.054* | |
H03B | 1.2372 | 0.8098 | 0.6522 | 0.054* | |
C611 | 1.2324 (5) | 0.6845 (5) | 0.7178 (3) | 0.047 (2) | |
C126 | 1.1075 (6) | 0.8990 (6) | 0.8781 (4) | 0.063 (3) | |
H12A | 1.0898 | 0.9099 | 0.8467 | 0.076* | |
C522 | 1.1775 (7) | 0.6893 (6) | 0.5819 (4) | 0.070 (3) | |
H52A | 1.2113 | 0.7267 | 0.5720 | 0.084* | |
C216 | 0.6918 (5) | 0.7975 (6) | 0.8425 (4) | 0.062 (3) | |
H21B | 0.6920 | 0.8133 | 0.8113 | 0.074* | |
C02 | 0.9366 (5) | 0.7538 (5) | 0.8724 (3) | 0.043 (2) | |
H02A | 0.9145 | 0.7055 | 0.8639 | 0.052* | |
H02B | 0.9387 | 0.7579 | 0.9066 | 0.052* | |
C622 | 1.2801 (6) | 0.8371 (6) | 0.8082 (3) | 0.060 (3) | |
H62A | 1.2320 | 0.8243 | 0.8223 | 0.072* | |
C411 | 0.8261 (6) | 0.7963 (6) | 0.5567 (3) | 0.061 (3) | |
C111 | 1.0872 (5) | 0.6711 (5) | 0.8797 (3) | 0.049 (2) | |
C226 | 0.9066 (6) | 0.9136 (6) | 0.9267 (3) | 0.062 (3) | |
H22A | 0.9048 | 0.8707 | 0.9445 | 0.075* | |
C626 | 1.3539 (6) | 0.8459 (6) | 0.7392 (4) | 0.063 (3) | |
H62B | 1.3577 | 0.8393 | 0.7070 | 0.076* | |
C311 | 0.6542 (5) | 0.8913 (5) | 0.6992 (3) | 0.045 (2) | |
C326 | 0.5797 (6) | 0.7341 (6) | 0.7240 (4) | 0.066 (3) | |
H32A | 0.5491 | 0.7761 | 0.7149 | 0.079* | |
C215 | 0.6172 (6) | 0.7765 (7) | 0.8596 (4) | 0.078 (3) | |
H21C | 0.5681 | 0.7774 | 0.8395 | 0.093* | |
C526 | 1.0634 (7) | 0.6487 (5) | 0.6228 (4) | 0.063 (3) | |
H52B | 1.0194 | 0.6587 | 0.6410 | 0.075* | |
C612 | 1.3038 (7) | 0.6698 (6) | 0.6960 (4) | 0.071 (3) | |
H61A | 1.3317 | 0.7081 | 0.6825 | 0.086* | |
C125 | 1.1460 (8) | 0.9535 (7) | 0.9070 (5) | 0.084 (4) | |
H12B | 1.1541 | 1.0001 | 0.8948 | 0.100* | |
C322 | 0.7083 (6) | 0.6697 (5) | 0.7361 (4) | 0.061 (3) | |
H32B | 0.7661 | 0.6685 | 0.7360 | 0.074* | |
C625 | 1.4204 (7) | 0.8780 (6) | 0.7677 (5) | 0.078 (3) | |
H62C | 1.4684 | 0.8922 | 0.7542 | 0.094* | |
C514 | 1.1074 (8) | 0.9349 (7) | 0.4902 (4) | 0.080 (3) | |
H51A | 1.1078 | 0.9640 | 0.4632 | 0.096* | |
C116 | 1.0557 (7) | 0.6317 (6) | 0.9168 (4) | 0.071 (3) | |
H11A | 1.0114 | 0.6512 | 0.9318 | 0.085* | |
C122 | 1.1224 (7) | 0.8143 (6) | 0.9434 (3) | 0.066 (3) | |
H12C | 1.1145 | 0.7680 | 0.9562 | 0.080* | |
C312 | 0.5855 (6) | 0.8975 (7) | 0.6658 (4) | 0.070 (3) | |
H31A | 0.5750 | 0.8604 | 0.6434 | 0.083* | |
C416 | 0.8559 (8) | 0.7250 (7) | 0.5548 (4) | 0.082 (3) | |
H41A | 0.8653 | 0.6986 | 0.5829 | 0.098* | |
C325 | 0.5387 (7) | 0.6715 (7) | 0.7398 (5) | 0.086 (4) | |
H32C | 0.4814 | 0.6730 | 0.7423 | 0.103* | |
C213 | 0.6877 (7) | 0.7516 (7) | 0.9354 (4) | 0.074 (3) | |
H21D | 0.6867 | 0.7368 | 0.9667 | 0.089* | |
C512 | 1.0359 (7) | 0.8601 (7) | 0.5415 (4) | 0.082 (4) | |
H51B | 0.9867 | 0.8364 | 0.5476 | 0.099* | |
C112 | 1.1526 (7) | 0.6395 (7) | 0.8587 (4) | 0.078 (3) | |
H11B | 1.1750 | 0.6633 | 0.8338 | 0.093* | |
C316 | 0.6691 (6) | 0.9476 (5) | 0.7319 (4) | 0.062 (3) | |
H31B | 0.7142 | 0.9449 | 0.7549 | 0.074* | |
C222 | 0.8971 (7) | 0.9738 (5) | 0.8509 (4) | 0.063 (3) | |
H22B | 0.8879 | 0.9723 | 0.8181 | 0.076* | |
C422 | 0.6987 (7) | 0.9383 (7) | 0.5768 (4) | 0.075 (3) | |
H42A | 0.6711 | 0.8975 | 0.5631 | 0.090* | |
F5 | 0.5366 (7) | 0.7532 (8) | 0.5817 (5) | 0.227 (7) | |
C516 | 1.1750 (7) | 0.8887 (7) | 0.5621 (4) | 0.079 (4) | |
H51C | 1.2235 | 0.8858 | 0.5826 | 0.095* | |
C423 | 0.6641 (9) | 1.0084 (9) | 0.5697 (6) | 0.099 (4) | |
H42B | 0.6149 | 1.0148 | 0.5501 | 0.118* | |
C323 | 0.6662 (7) | 0.6085 (6) | 0.7503 (4) | 0.074 (3) | |
H32D | 0.6963 | 0.5663 | 0.7593 | 0.089* | |
C114 | 1.1523 (9) | 0.5337 (7) | 0.9106 (6) | 0.094 (4) | |
H11C | 1.1728 | 0.4877 | 0.9201 | 0.113* | |
C123 | 1.1610 (8) | 0.8698 (8) | 0.9714 (4) | 0.089 (4) | |
H12D | 1.1796 | 0.8598 | 1.0028 | 0.106* | |
C525 | 1.0788 (8) | 0.5769 (7) | 0.6100 (5) | 0.089 (4) | |
H52C | 1.0454 | 0.5394 | 0.6202 | 0.106* | |
C624 | 1.4153 (7) | 0.8887 (6) | 0.8153 (5) | 0.078 (3) | |
H62D | 1.4598 | 0.9103 | 0.8336 | 0.094* | |
F4 | 0.4649 (6) | 0.7510 (8) | 0.4961 (3) | 0.185 (6) | |
C214 | 0.6145 (7) | 0.7545 (7) | 0.9056 (4) | 0.078 (3) | |
H21E | 0.5638 | 0.7415 | 0.9168 | 0.094* | |
C225 | 0.9246 (8) | 0.9803 (7) | 0.9494 (4) | 0.081 (3) | |
H22C | 0.9323 | 0.9823 | 0.9823 | 0.097* | |
C523 | 1.1923 (8) | 0.6159 (8) | 0.5693 (5) | 0.093 (4) | |
H52D | 1.2366 | 0.6050 | 0.5517 | 0.112* | |
F3 | 0.3972 (9) | 0.6862 (7) | 0.5612 (6) | 0.227 (7) | |
C115 | 1.0888 (8) | 0.5652 (7) | 0.9315 (5) | 0.087 (4) | |
H11D | 1.0671 | 0.5410 | 0.9566 | 0.105* | |
C414 | 0.8562 (12) | 0.7315 (12) | 0.4694 (5) | 0.127 (7) | |
H41B | 0.8668 | 0.7107 | 0.4405 | 0.153* | |
C412 | 0.8107 (7) | 0.8337 (8) | 0.5132 (4) | 0.085 (4) | |
H41C | 0.7902 | 0.8815 | 0.5132 | 0.102* | |
F2 | 0.4000 (7) | 0.8081 (8) | 0.6118 (4) | 0.203 (6) | |
C515 | 1.1763 (8) | 0.9276 (8) | 0.5199 (5) | 0.097 (4) | |
H51D | 1.2260 | 0.9489 | 0.5123 | 0.116* | |
C113 | 1.1853 (8) | 0.5717 (8) | 0.8748 (6) | 0.104 (5) | |
H11E | 1.2306 | 0.5519 | 0.8609 | 0.124* | |
C224 | 0.9311 (9) | 1.0433 (8) | 0.9231 (5) | 0.100 (5) | |
H22D | 0.9449 | 1.0877 | 0.9382 | 0.120* | |
C513 | 1.0376 (7) | 0.8997 (8) | 0.4997 (4) | 0.096 (4) | |
H51E | 0.9902 | 0.9019 | 0.4783 | 0.115* | |
C424 | 0.7041 (12) | 1.0686 (9) | 0.5921 (6) | 0.112 (6) | |
H42C | 0.6805 | 1.1152 | 0.5882 | 0.135* | |
F1 | 0.4766 (9) | 0.8708 (6) | 0.5494 (5) | 0.210 (6) | |
C223 | 0.9171 (9) | 1.0407 (7) | 0.8744 (5) | 0.096 (4) | |
H22E | 0.9209 | 1.0836 | 0.8568 | 0.116* | |
C315 | 0.6153 (8) | 1.0092 (7) | 0.7301 (5) | 0.087 (4) | |
H31C | 0.6259 | 1.0474 | 0.7516 | 0.104* | |
C616 | 1.1882 (8) | 0.6263 (6) | 0.7342 (4) | 0.080 (3) | |
H61B | 1.1380 | 0.6346 | 0.7472 | 0.096* | |
C314 | 0.5478 (8) | 1.0130 (8) | 0.6969 (5) | 0.087 (4) | |
H31D | 0.5125 | 1.0536 | 0.6962 | 0.104* | |
C413 | 0.8250 (10) | 0.8014 (12) | 0.4705 (5) | 0.114 (6) | |
H41D | 0.8133 | 0.8274 | 0.4424 | 0.137* | |
C313 | 0.5321 (8) | 0.9577 (8) | 0.6650 (5) | 0.090 (4) | |
H31E | 0.4859 | 0.9602 | 0.6427 | 0.108* | |
C426 | 0.8148 (8) | 0.9903 (6) | 0.6270 (4) | 0.073 (3) | |
H42D | 0.8647 | 0.9847 | 0.6461 | 0.088* | |
C524 | 1.1415 (8) | 0.5599 (7) | 0.5830 (5) | 0.090 (4) | |
H52E | 1.1502 | 0.5115 | 0.5739 | 0.108* | |
C613 | 1.3350 (8) | 0.5975 (8) | 0.6940 (5) | 0.091 (4) | |
H61C | 1.3846 | 0.5885 | 0.6805 | 0.110* | |
C614 | 1.2918 (11) | 0.5405 (8) | 0.7122 (6) | 0.104 (5) | |
H61D | 1.3124 | 0.4928 | 0.7112 | 0.125* | |
C425 | 0.7779 (12) | 1.0599 (7) | 0.6199 (5) | 0.105 (5) | |
H42E | 0.8039 | 1.1009 | 0.6343 | 0.126* | |
F6 | 0.3319 (7) | 0.7989 (10) | 0.5282 (5) | 0.232 (7) | |
C615 | 1.2197 (11) | 0.5535 (7) | 0.7313 (5) | 0.103 (5) | |
H61E | 1.1901 | 0.5144 | 0.7428 | 0.124* | |
Cl3 | 1.1078 (3) | 1.1697 (3) | 0.65989 (19) | 0.1402 (17) | |
Cl4 | 1.0704 (4) | 1.0258 (3) | 0.6221 (2) | 0.168 (2) | |
Cl6 | 1.1578 (6) | 0.4551 (7) | 0.3617 (3) | 0.305 (5) | |
C623 | 1.3460 (8) | 0.8681 (7) | 0.8359 (4) | 0.078 (3) | |
H62E | 1.3431 | 0.8747 | 0.8683 | 0.093* | |
Cl5 | 1.1211 (8) | 0.5277 (6) | 0.4460 (4) | 0.351 (7) | |
C124 | 1.1721 (8) | 0.9387 (8) | 0.9534 (5) | 0.087 (4) | |
H12E | 1.1973 | 0.9754 | 0.9727 | 0.105* | |
C324 | 0.5822 (8) | 0.6088 (7) | 0.7515 (5) | 0.084 (4) | |
H32E | 0.5545 | 0.5667 | 0.7602 | 0.101* | |
C415 | 0.8727 (11) | 0.6906 (9) | 0.5116 (6) | 0.130 (6) | |
H41E | 0.8937 | 0.6430 | 0.5112 | 0.156* | |
C04 | 1.0599 (17) | 1.0862 (7) | 0.6675 (6) | 0.269 (18) | |
H04A | 1.0837 | 1.0642 | 0.6969 | 0.323* | |
H04B | 1.0009 | 1.0944 | 0.6703 | 0.323* | |
C05 | 1.1957 (10) | 0.5113 (14) | 0.4075 (7) | 0.32 (2) | |
H05B | 1.2441 | 0.4883 | 0.4245 | 0.385* | |
H05A | 1.2134 | 0.5577 | 0.3947 | 0.385* |
U11 | U22 | U33 | U12 | U13 | U23 | |
Ag3 | 0.0410 (4) | 0.0633 (4) | 0.0365 (3) | 0.0017 (3) | −0.0006 (3) | −0.0014 (3) |
Ag2 | 0.0379 (4) | 0.0775 (5) | 0.0431 (4) | 0.0011 (3) | 0.0052 (3) | −0.0011 (4) |
Ag1 | 0.0422 (4) | 0.0733 (5) | 0.0435 (4) | 0.0014 (3) | 0.0076 (3) | 0.0041 (4) |
Sb1 | 0.0561 (4) | 0.0951 (6) | 0.0567 (4) | −0.0040 (4) | 0.0059 (3) | −0.0176 (4) |
P2 | 0.0354 (11) | 0.0485 (13) | 0.0315 (10) | 0.0034 (10) | 0.0012 (8) | 0.0011 (10) |
C01 | 0.035 (4) | 0.047 (5) | 0.036 (4) | −0.009 (4) | 0.005 (3) | 0.005 (4) |
Cl2 | 0.0438 (12) | 0.0486 (12) | 0.0530 (13) | −0.0025 (10) | 0.0080 (10) | −0.0019 (10) |
P5 | 0.0358 (11) | 0.0499 (13) | 0.0393 (12) | −0.0002 (10) | 0.0075 (9) | 0.0014 (10) |
Cl1 | 0.0548 (13) | 0.0453 (12) | 0.0451 (12) | 0.0011 (10) | 0.0056 (10) | −0.0035 (10) |
P6 | 0.0340 (11) | 0.0522 (14) | 0.0405 (12) | 0.0011 (10) | 0.0048 (9) | 0.0006 (11) |
P4 | 0.0391 (12) | 0.0611 (15) | 0.0384 (12) | −0.0013 (11) | 0.0022 (9) | 0.0036 (11) |
P3 | 0.0365 (11) | 0.0456 (13) | 0.0343 (11) | −0.0021 (9) | 0.0005 (9) | 0.0009 (10) |
P1 | 0.0353 (11) | 0.0505 (13) | 0.0361 (11) | 0.0032 (10) | 0.0029 (9) | 0.0049 (10) |
C211 | 0.038 (5) | 0.053 (5) | 0.046 (5) | −0.003 (4) | 0.004 (4) | −0.006 (4) |
C621 | 0.053 (5) | 0.048 (5) | 0.045 (5) | 0.009 (4) | 0.003 (4) | −0.008 (4) |
C121 | 0.033 (4) | 0.066 (6) | 0.041 (5) | −0.002 (4) | 0.006 (4) | −0.003 (5) |
C521 | 0.039 (5) | 0.058 (6) | 0.046 (5) | 0.001 (4) | −0.001 (4) | −0.006 (4) |
C421 | 0.055 (6) | 0.058 (6) | 0.053 (6) | −0.005 (5) | 0.013 (5) | 0.015 (5) |
C321 | 0.038 (5) | 0.050 (5) | 0.040 (5) | 0.004 (4) | 0.000 (4) | −0.001 (4) |
C511 | 0.053 (5) | 0.055 (6) | 0.040 (5) | 0.004 (4) | 0.014 (4) | 0.007 (4) |
C221 | 0.052 (5) | 0.050 (5) | 0.041 (5) | −0.001 (4) | 0.009 (4) | −0.009 (4) |
C212 | 0.043 (5) | 0.085 (8) | 0.052 (6) | −0.004 (5) | 0.000 (4) | 0.019 (5) |
C03 | 0.040 (5) | 0.051 (5) | 0.045 (5) | −0.007 (4) | 0.010 (4) | −0.002 (4) |
C611 | 0.049 (5) | 0.046 (5) | 0.044 (5) | 0.004 (4) | −0.003 (4) | 0.001 (4) |
C126 | 0.058 (6) | 0.080 (8) | 0.052 (6) | −0.010 (5) | 0.008 (5) | 0.005 (6) |
C522 | 0.058 (6) | 0.075 (8) | 0.079 (7) | 0.002 (6) | 0.021 (6) | −0.013 (6) |
C216 | 0.034 (5) | 0.092 (8) | 0.059 (6) | 0.007 (5) | 0.009 (4) | −0.001 (6) |
C02 | 0.033 (4) | 0.056 (5) | 0.039 (5) | 0.013 (4) | −0.003 (4) | 0.002 (4) |
C622 | 0.059 (6) | 0.067 (7) | 0.053 (6) | −0.004 (5) | 0.006 (5) | 0.004 (5) |
C411 | 0.058 (6) | 0.079 (8) | 0.046 (6) | −0.014 (5) | 0.009 (5) | −0.015 (5) |
C111 | 0.043 (5) | 0.052 (5) | 0.051 (5) | 0.009 (4) | −0.007 (4) | 0.000 (5) |
C226 | 0.071 (7) | 0.067 (7) | 0.047 (6) | 0.003 (5) | −0.001 (5) | −0.007 (5) |
C626 | 0.050 (6) | 0.074 (7) | 0.068 (7) | −0.006 (5) | 0.017 (5) | −0.016 (6) |
C311 | 0.041 (5) | 0.050 (5) | 0.042 (5) | 0.009 (4) | 0.005 (4) | 0.008 (4) |
C326 | 0.039 (5) | 0.068 (7) | 0.090 (8) | 0.001 (5) | 0.005 (5) | 0.009 (6) |
C215 | 0.043 (6) | 0.116 (10) | 0.073 (8) | −0.008 (6) | −0.002 (5) | −0.005 (7) |
C526 | 0.073 (7) | 0.047 (6) | 0.072 (7) | −0.009 (5) | 0.025 (6) | −0.004 (5) |
C612 | 0.068 (7) | 0.054 (6) | 0.094 (8) | 0.012 (5) | 0.019 (6) | −0.001 (6) |
C125 | 0.093 (9) | 0.081 (8) | 0.080 (9) | −0.035 (7) | 0.022 (7) | −0.014 (7) |
C322 | 0.052 (6) | 0.057 (6) | 0.078 (7) | 0.002 (5) | 0.016 (5) | 0.006 (5) |
C625 | 0.049 (6) | 0.072 (8) | 0.115 (10) | −0.010 (5) | 0.006 (6) | −0.016 (7) |
C514 | 0.092 (9) | 0.094 (9) | 0.056 (7) | 0.000 (7) | 0.016 (6) | 0.028 (6) |
C116 | 0.085 (8) | 0.061 (7) | 0.067 (7) | 0.014 (6) | 0.010 (6) | 0.017 (6) |
C122 | 0.073 (7) | 0.074 (7) | 0.052 (6) | −0.007 (6) | 0.001 (5) | −0.004 (5) |
C312 | 0.060 (6) | 0.088 (8) | 0.058 (6) | 0.025 (6) | −0.007 (5) | 0.003 (6) |
C416 | 0.093 (9) | 0.094 (9) | 0.058 (7) | −0.016 (7) | 0.011 (6) | −0.018 (7) |
C325 | 0.061 (7) | 0.083 (9) | 0.117 (11) | −0.020 (7) | 0.020 (7) | 0.001 (8) |
C213 | 0.058 (7) | 0.108 (9) | 0.058 (6) | −0.002 (6) | 0.019 (5) | 0.016 (6) |
C512 | 0.060 (7) | 0.125 (11) | 0.060 (7) | −0.012 (7) | −0.004 (5) | 0.040 (7) |
C112 | 0.059 (7) | 0.079 (8) | 0.097 (9) | 0.018 (6) | 0.015 (6) | 0.004 (7) |
C316 | 0.062 (6) | 0.043 (5) | 0.080 (7) | 0.000 (5) | 0.006 (5) | −0.004 (5) |
C222 | 0.082 (7) | 0.053 (6) | 0.056 (6) | 0.001 (5) | 0.012 (5) | −0.001 (5) |
C422 | 0.054 (6) | 0.080 (8) | 0.091 (8) | 0.005 (6) | 0.006 (6) | 0.024 (7) |
F5 | 0.127 (8) | 0.269 (15) | 0.261 (15) | 0.070 (9) | −0.104 (9) | −0.113 (12) |
C516 | 0.067 (7) | 0.113 (10) | 0.056 (6) | −0.033 (7) | 0.002 (5) | 0.026 (7) |
C423 | 0.081 (9) | 0.097 (11) | 0.120 (12) | 0.018 (8) | 0.021 (8) | 0.036 (10) |
C323 | 0.080 (8) | 0.051 (6) | 0.096 (9) | 0.003 (6) | 0.029 (7) | 0.008 (6) |
C114 | 0.087 (10) | 0.068 (8) | 0.122 (12) | 0.024 (7) | −0.025 (9) | 0.002 (8) |
C123 | 0.099 (10) | 0.110 (11) | 0.052 (7) | −0.013 (8) | −0.016 (6) | −0.019 (7) |
C525 | 0.100 (10) | 0.064 (8) | 0.106 (10) | −0.010 (7) | 0.027 (8) | −0.010 (7) |
C624 | 0.065 (7) | 0.066 (7) | 0.098 (10) | 0.001 (6) | −0.021 (7) | −0.026 (7) |
F4 | 0.150 (9) | 0.315 (15) | 0.099 (6) | −0.068 (9) | 0.054 (6) | −0.104 (8) |
C214 | 0.046 (6) | 0.108 (10) | 0.084 (8) | −0.011 (6) | 0.029 (6) | 0.008 (7) |
C225 | 0.096 (9) | 0.086 (9) | 0.062 (7) | −0.009 (7) | 0.010 (6) | −0.026 (7) |
C523 | 0.082 (9) | 0.098 (10) | 0.107 (10) | 0.009 (8) | 0.045 (8) | −0.026 (8) |
F3 | 0.235 (15) | 0.149 (11) | 0.303 (18) | −0.066 (10) | 0.063 (13) | 0.005 (11) |
C115 | 0.094 (9) | 0.071 (8) | 0.093 (9) | 0.013 (7) | −0.013 (7) | 0.027 (7) |
C414 | 0.148 (16) | 0.178 (19) | 0.062 (9) | −0.040 (14) | 0.038 (9) | −0.051 (12) |
C412 | 0.086 (8) | 0.126 (11) | 0.042 (6) | −0.013 (8) | 0.007 (5) | 0.009 (7) |
F2 | 0.175 (10) | 0.327 (17) | 0.116 (8) | −0.025 (10) | 0.060 (7) | −0.094 (10) |
C515 | 0.085 (9) | 0.120 (11) | 0.087 (9) | −0.035 (8) | 0.020 (7) | 0.040 (8) |
C113 | 0.071 (9) | 0.107 (12) | 0.135 (13) | 0.041 (8) | 0.021 (9) | −0.009 (10) |
C224 | 0.112 (11) | 0.097 (11) | 0.093 (10) | −0.023 (9) | 0.009 (8) | −0.058 (9) |
C513 | 0.061 (7) | 0.146 (13) | 0.080 (9) | −0.009 (8) | 0.002 (6) | 0.039 (9) |
C424 | 0.142 (15) | 0.078 (10) | 0.128 (14) | 0.042 (11) | 0.064 (12) | 0.045 (10) |
F1 | 0.286 (16) | 0.123 (9) | 0.232 (14) | −0.068 (10) | 0.072 (12) | −0.002 (9) |
C223 | 0.131 (12) | 0.062 (8) | 0.098 (11) | −0.016 (8) | 0.022 (9) | −0.006 (7) |
C315 | 0.090 (9) | 0.059 (7) | 0.115 (11) | 0.005 (7) | 0.024 (8) | −0.018 (7) |
C616 | 0.093 (9) | 0.060 (7) | 0.089 (9) | −0.007 (6) | 0.027 (7) | −0.008 (6) |
C314 | 0.078 (9) | 0.082 (9) | 0.104 (10) | 0.037 (7) | 0.025 (8) | 0.027 (8) |
C413 | 0.117 (12) | 0.182 (18) | 0.045 (7) | −0.019 (12) | 0.013 (7) | −0.016 (10) |
C313 | 0.074 (8) | 0.112 (11) | 0.085 (9) | 0.041 (8) | 0.002 (7) | 0.015 (8) |
C426 | 0.095 (9) | 0.059 (7) | 0.069 (7) | −0.013 (6) | 0.023 (6) | 0.006 (6) |
C524 | 0.094 (10) | 0.066 (8) | 0.111 (11) | 0.007 (7) | 0.012 (8) | −0.025 (8) |
C613 | 0.076 (8) | 0.082 (9) | 0.116 (11) | 0.016 (7) | 0.008 (7) | −0.028 (8) |
C614 | 0.125 (13) | 0.069 (9) | 0.114 (12) | 0.025 (9) | −0.014 (10) | −0.024 (8) |
C425 | 0.171 (16) | 0.048 (8) | 0.103 (11) | −0.007 (9) | 0.046 (11) | 0.007 (7) |
F6 | 0.113 (8) | 0.37 (2) | 0.197 (12) | 0.078 (11) | −0.051 (8) | −0.079 (13) |
C615 | 0.148 (14) | 0.055 (8) | 0.112 (12) | −0.018 (8) | 0.039 (10) | −0.003 (7) |
Cl3 | 0.141 (4) | 0.123 (4) | 0.164 (4) | −0.024 (3) | 0.049 (3) | −0.035 (3) |
Cl4 | 0.207 (6) | 0.142 (4) | 0.154 (5) | −0.023 (4) | 0.016 (4) | −0.024 (4) |
Cl6 | 0.260 (10) | 0.430 (16) | 0.226 (9) | −0.078 (10) | 0.033 (8) | 0.014 (10) |
C623 | 0.082 (8) | 0.089 (9) | 0.059 (7) | −0.005 (7) | −0.014 (6) | −0.016 (6) |
Cl5 | 0.424 (17) | 0.348 (14) | 0.278 (12) | −0.195 (13) | 0.014 (11) | 0.027 (11) |
C124 | 0.084 (9) | 0.099 (10) | 0.079 (9) | −0.031 (8) | 0.008 (7) | −0.030 (8) |
C324 | 0.090 (9) | 0.056 (7) | 0.112 (10) | −0.024 (7) | 0.037 (8) | −0.002 (7) |
C415 | 0.170 (17) | 0.113 (13) | 0.116 (14) | −0.027 (11) | 0.063 (12) | −0.048 (11) |
C04 | 0.28 (3) | 0.41 (4) | 0.143 (19) | −0.17 (3) | 0.14 (2) | −0.12 (2) |
C05 | 0.52 (6) | 0.37 (5) | 0.079 (15) | −0.23 (4) | 0.06 (3) | −0.03 (2) |
Ag3—P3 | 2.477 (2) | C322—H32B | 0.9300 |
Ag3—P2 | 2.488 (2) | C625—C624 | 1.372 (16) |
Ag3—Cl1 | 2.762 (2) | C625—H62C | 0.9300 |
Ag3—Cl2 | 2.781 (2) | C514—C515 | 1.335 (17) |
Ag3—Ag2 | 3.3544 (9) | C514—C513 | 1.339 (16) |
Ag2—P5 | 2.465 (2) | C514—H51A | 0.9300 |
Ag2—P4 | 2.475 (2) | C116—C115 | 1.369 (15) |
Ag2—Cl1 | 2.690 (2) | C116—H11A | 0.9300 |
Ag2—Cl2 | 2.852 (2) | C122—C123 | 1.393 (15) |
Ag1—P6 | 2.484 (2) | C122—H12C | 0.9300 |
Ag1—P1 | 2.506 (2) | C312—C313 | 1.388 (15) |
Ag1—Cl2 | 2.705 (2) | C312—H31A | 0.9300 |
Ag1—Cl1 | 2.794 (2) | C416—C415 | 1.423 (17) |
Sb1—F5 | 1.794 (10) | C416—H41A | 0.9300 |
Sb1—F6 | 1.797 (10) | C325—C324 | 1.362 (16) |
Sb1—F1 | 1.804 (11) | C325—H32C | 0.9300 |
Sb1—F3 | 1.812 (12) | C213—C214 | 1.384 (15) |
Sb1—F4 | 1.829 (8) | C213—H21D | 0.9300 |
Sb1—F2 | 1.855 (9) | C512—C513 | 1.388 (15) |
P2—C02 | 1.839 (8) | C512—H51B | 0.9300 |
P2—C211 | 1.845 (9) | C112—C113 | 1.398 (17) |
P2—C221 | 1.853 (9) | C112—H11B | 0.9300 |
C01—P4 | 1.838 (7) | C316—C315 | 1.411 (15) |
C01—P3 | 1.847 (8) | C316—H31B | 0.9300 |
C01—H01A | 0.9700 | C222—C223 | 1.408 (15) |
C01—H01B | 0.9700 | C222—H22B | 0.9300 |
P5—C511 | 1.845 (9) | C422—C423 | 1.397 (17) |
P5—C521 | 1.846 (9) | C422—H42A | 0.9300 |
P5—C03 | 1.855 (8) | C516—C515 | 1.390 (15) |
P6—C611 | 1.842 (9) | C516—H51C | 0.9300 |
P6—C621 | 1.852 (9) | C423—C424 | 1.39 (2) |
P6—C03 | 1.866 (8) | C423—H42B | 0.9300 |
P4—C411 | 1.828 (10) | C323—C324 | 1.353 (15) |
P4—C421 | 1.842 (10) | C323—H32D | 0.9300 |
P3—C311 | 1.834 (9) | C114—C115 | 1.353 (18) |
P3—C321 | 1.853 (9) | C114—C113 | 1.373 (19) |
P1—C121 | 1.839 (9) | C114—H11C | 0.9300 |
P1—C111 | 1.844 (9) | C123—C124 | 1.370 (17) |
P1—C02 | 1.843 (8) | C123—H12D | 0.9300 |
C211—C216 | 1.379 (12) | C525—C524 | 1.356 (17) |
C211—C212 | 1.398 (12) | C525—H52C | 0.9300 |
C621—C626 | 1.380 (13) | C624—C623 | 1.356 (16) |
C621—C622 | 1.406 (12) | C624—H62D | 0.9300 |
C121—C126 | 1.396 (13) | C214—H21E | 0.9300 |
C121—C122 | 1.410 (13) | C225—C224 | 1.375 (18) |
C521—C522 | 1.381 (13) | C225—H22C | 0.9300 |
C521—C526 | 1.385 (13) | C523—C524 | 1.382 (17) |
C421—C422 | 1.398 (14) | C523—H52D | 0.9300 |
C421—C426 | 1.404 (14) | C115—H11D | 0.9300 |
C321—C326 | 1.364 (12) | C414—C413 | 1.37 (2) |
C321—C322 | 1.394 (12) | C414—C415 | 1.41 (2) |
C511—C516 | 1.360 (13) | C414—H41B | 0.9300 |
C511—C512 | 1.373 (13) | C412—C413 | 1.384 (17) |
C221—C222 | 1.387 (13) | C412—H41C | 0.9300 |
C221—C226 | 1.395 (12) | C515—H51D | 0.9300 |
C212—C213 | 1.385 (13) | C113—H11E | 0.9300 |
C212—H21A | 0.9300 | C224—C223 | 1.380 (18) |
C03—H03A | 0.9700 | C224—H22D | 0.9300 |
C03—H03B | 0.9700 | C513—H51E | 0.9300 |
C611—C612 | 1.376 (13) | C424—C425 | 1.37 (2) |
C611—C616 | 1.379 (14) | C424—H42C | 0.9300 |
C126—C125 | 1.393 (15) | C223—H22E | 0.9300 |
C126—H12A | 0.9300 | C315—C314 | 1.370 (17) |
C522—C523 | 1.406 (16) | C315—H31C | 0.9300 |
C522—H52A | 0.9300 | C616—C615 | 1.421 (17) |
C216—C215 | 1.386 (14) | C616—H61B | 0.9300 |
C216—H21B | 0.9300 | C314—C313 | 1.362 (18) |
C02—H02A | 0.9700 | C314—H31D | 0.9300 |
C02—H02B | 0.9700 | C413—H41D | 0.9300 |
C622—C623 | 1.379 (14) | C313—H31E | 0.9300 |
C622—H62A | 0.9300 | C426—C425 | 1.403 (17) |
C411—C416 | 1.383 (16) | C426—H42D | 0.9300 |
C411—C412 | 1.408 (15) | C524—H52E | 0.9300 |
C111—C112 | 1.381 (13) | C613—C614 | 1.373 (19) |
C111—C116 | 1.405 (13) | C613—H61C | 0.9300 |
C226—C225 | 1.391 (15) | C614—C615 | 1.344 (19) |
C226—H22A | 0.9300 | C614—H61D | 0.9300 |
C626—C625 | 1.404 (14) | C425—H42E | 0.9300 |
C626—H62B | 0.9300 | C615—H61E | 0.9300 |
C311—C316 | 1.386 (13) | Cl3—C04 | 1.725 (5) |
C311—C312 | 1.392 (12) | Cl4—C04 | 1.713 (5) |
C326—C325 | 1.408 (15) | Cl6—C05 | 1.718 (5) |
C326—H32A | 0.9300 | C623—H62E | 0.9300 |
C215—C214 | 1.369 (15) | Cl5—C05 | 1.721 (5) |
C215—H21C | 0.9300 | C124—H12E | 0.9300 |
C526—C525 | 1.382 (15) | C324—H32E | 0.9300 |
C526—H52B | 0.9300 | C415—H41E | 0.9300 |
C612—C613 | 1.409 (15) | C04—H04A | 0.9700 |
C612—H61A | 0.9300 | C04—H04B | 0.9700 |
C125—C124 | 1.370 (17) | C05—H05B | 0.9700 |
C125—H12B | 0.9300 | C05—H05A | 0.9700 |
C322—C323 | 1.379 (14) | ||
P3—Ag3—P2 | 126.79 (7) | C525—C526—H52B | 119.6 |
P3—Ag3—Cl1 | 122.55 (7) | C521—C526—H52B | 119.6 |
P2—Ag3—Cl1 | 104.32 (7) | C611—C612—C613 | 120.9 (11) |
P3—Ag3—Cl2 | 95.93 (7) | C611—C612—H61A | 119.6 |
P2—Ag3—Cl2 | 110.31 (7) | C613—C612—H61A | 119.6 |
Cl1—Ag3—Cl2 | 88.13 (6) | C124—C125—C126 | 120.4 (12) |
P3—Ag3—Ag2 | 86.27 (5) | C124—C125—H12B | 119.8 |
P2—Ag3—Ag2 | 146.56 (5) | C126—C125—H12B | 119.8 |
Cl1—Ag3—Ag2 | 51.06 (5) | C323—C322—C321 | 120.1 (9) |
Cl2—Ag3—Ag2 | 54.43 (5) | C323—C322—H32B | 119.9 |
P5—Ag2—P4 | 125.59 (8) | C321—C322—H32B | 119.9 |
P5—Ag2—Cl1 | 108.65 (8) | C624—C625—C626 | 120.9 (11) |
P4—Ag2—Cl1 | 116.33 (8) | C624—C625—H62C | 119.6 |
P5—Ag2—Cl2 | 106.01 (7) | C626—C625—H62C | 119.6 |
P4—Ag2—Cl2 | 104.51 (7) | C515—C514—C513 | 119.0 (11) |
Cl1—Ag2—Cl2 | 88.10 (7) | C515—C514—H51A | 120.5 |
P5—Ag2—Ag3 | 147.05 (6) | C513—C514—H51A | 120.5 |
P4—Ag2—Ag3 | 86.56 (6) | C115—C116—C111 | 121.4 (11) |
Cl1—Ag2—Ag3 | 53.00 (5) | C115—C116—H11A | 119.3 |
Cl2—Ag2—Ag3 | 52.48 (5) | C111—C116—H11A | 119.3 |
P6—Ag1—P1 | 131.40 (8) | C123—C122—C121 | 119.9 (11) |
P6—Ag1—Cl2 | 112.40 (7) | C123—C122—H12C | 120.1 |
P1—Ag1—Cl2 | 102.62 (7) | C121—C122—H12C | 120.1 |
P6—Ag1—Cl1 | 102.58 (7) | C313—C312—C311 | 121.6 (11) |
P1—Ag1—Cl1 | 110.88 (7) | C313—C312—H31A | 119.2 |
Cl2—Ag1—Cl1 | 88.98 (7) | C311—C312—H31A | 119.2 |
F5—Sb1—F6 | 176.1 (8) | C411—C416—C415 | 122.5 (14) |
F5—Sb1—F1 | 87.3 (7) | C411—C416—H41A | 118.7 |
F6—Sb1—F1 | 96.5 (8) | C415—C416—H41A | 118.7 |
F5—Sb1—F3 | 90.8 (7) | C324—C325—C326 | 120.6 (11) |
F6—Sb1—F3 | 85.4 (8) | C324—C325—H32C | 119.7 |
F1—Sb1—F3 | 177.9 (8) | C326—C325—H32C | 119.7 |
F5—Sb1—F4 | 91.2 (6) | C212—C213—C214 | 119.5 (10) |
F6—Sb1—F4 | 89.4 (6) | C212—C213—H21D | 120.3 |
F1—Sb1—F4 | 93.5 (6) | C214—C213—H21D | 120.3 |
F3—Sb1—F4 | 87.6 (6) | C511—C512—C513 | 122.1 (10) |
F5—Sb1—F2 | 92.0 (6) | C511—C512—H51B | 118.9 |
F6—Sb1—F2 | 87.4 (6) | C513—C512—H51B | 118.9 |
F1—Sb1—F2 | 87.0 (6) | C111—C112—C113 | 120.3 (12) |
F3—Sb1—F2 | 92.0 (7) | C111—C112—H11B | 119.9 |
F4—Sb1—F2 | 176.8 (5) | C113—C112—H11B | 119.9 |
C02—P2—C211 | 101.1 (4) | C311—C316—C315 | 119.7 (11) |
C02—P2—C221 | 105.6 (4) | C311—C316—H31B | 120.2 |
C211—P2—C221 | 103.5 (4) | C315—C316—H31B | 120.2 |
C02—P2—Ag3 | 113.0 (3) | C221—C222—C223 | 119.1 (10) |
C211—P2—Ag3 | 114.9 (3) | C221—C222—H22B | 120.5 |
C221—P2—Ag3 | 116.9 (3) | C223—C222—H22B | 120.5 |
P4—C01—P3 | 113.6 (4) | C421—C422—C423 | 120.1 (12) |
P4—C01—H01A | 108.9 | C421—C422—H42A | 119.9 |
P3—C01—H01A | 108.9 | C423—C422—H42A | 119.9 |
P4—C01—H01B | 108.9 | C511—C516—C515 | 121.6 (11) |
P3—C01—H01B | 108.9 | C511—C516—H51C | 119.2 |
H01A—C01—H01B | 107.7 | C515—C516—H51C | 119.2 |
Ag1—Cl2—Ag3 | 78.54 (6) | C424—C423—C422 | 119.3 (14) |
Ag1—Cl2—Ag2 | 77.07 (6) | C424—C423—H42B | 120.4 |
Ag3—Cl2—Ag2 | 73.09 (6) | C422—C423—H42B | 120.4 |
C511—P5—C521 | 102.5 (4) | C324—C323—C322 | 121.4 (11) |
C511—P5—C03 | 104.2 (4) | C324—C323—H32D | 119.3 |
C521—P5—C03 | 103.8 (4) | C322—C323—H32D | 119.3 |
C511—P5—Ag2 | 112.6 (3) | C115—C114—C113 | 118.0 (12) |
C521—P5—Ag2 | 116.8 (3) | C115—C114—H11C | 121.0 |
C03—P5—Ag2 | 115.4 (3) | C113—C114—H11C | 121.0 |
Ag2—Cl1—Ag3 | 75.94 (6) | C124—C123—C122 | 121.1 (11) |
Ag2—Cl1—Ag1 | 78.31 (6) | C124—C123—H12D | 119.5 |
Ag3—Cl1—Ag1 | 77.37 (6) | C122—C123—H12D | 119.5 |
C611—P6—C621 | 102.7 (4) | C524—C525—C526 | 121.6 (12) |
C611—P6—C03 | 105.8 (4) | C524—C525—H52C | 119.2 |
C621—P6—C03 | 102.1 (4) | C526—C525—H52C | 119.2 |
C611—P6—Ag1 | 113.6 (3) | C623—C624—C625 | 120.7 (11) |
C621—P6—Ag1 | 112.9 (3) | C623—C624—H62D | 119.7 |
C03—P6—Ag1 | 118.0 (3) | C625—C624—H62D | 119.7 |
C411—P4—C01 | 104.1 (4) | C215—C214—C213 | 119.5 (9) |
C411—P4—C421 | 105.9 (5) | C215—C214—H21E | 120.3 |
C01—P4—C421 | 104.1 (4) | C213—C214—H21E | 120.3 |
C411—P4—Ag2 | 109.4 (3) | C224—C225—C226 | 119.8 (11) |
C01—P4—Ag2 | 111.3 (3) | C224—C225—H22C | 120.1 |
C421—P4—Ag2 | 120.7 (3) | C226—C225—H22C | 120.1 |
C311—P3—C01 | 106.9 (4) | C524—C523—C522 | 120.7 (11) |
C311—P3—C321 | 106.0 (4) | C524—C523—H52D | 119.6 |
C01—P3—C321 | 100.3 (4) | C522—C523—H52D | 119.6 |
C311—P3—Ag3 | 116.2 (3) | C114—C115—C116 | 121.8 (13) |
C01—P3—Ag3 | 116.8 (3) | C114—C115—H11D | 119.1 |
C321—P3—Ag3 | 109.0 (3) | C116—C115—H11D | 119.1 |
C121—P1—C111 | 103.6 (4) | C413—C414—C415 | 120.5 (14) |
C121—P1—C02 | 104.3 (4) | C413—C414—H41B | 119.7 |
C111—P1—C02 | 100.7 (4) | C415—C414—H41B | 119.7 |
C121—P1—Ag1 | 113.5 (3) | C413—C412—C411 | 122.1 (14) |
C111—P1—Ag1 | 114.9 (3) | C413—C412—H41C | 119.0 |
C02—P1—Ag1 | 118.1 (3) | C411—C412—H41C | 119.0 |
C216—C211—C212 | 118.3 (8) | C514—C515—C516 | 121.0 (11) |
C216—C211—P2 | 118.0 (7) | C514—C515—H51D | 119.5 |
C212—C211—P2 | 123.7 (7) | C516—C515—H51D | 119.5 |
C626—C621—C622 | 117.7 (9) | C114—C113—C112 | 121.6 (12) |
C626—C621—P6 | 124.1 (7) | C114—C113—H11E | 119.2 |
C622—C621—P6 | 118.2 (7) | C112—C113—H11E | 119.2 |
C126—C121—C122 | 117.9 (9) | C223—C224—C225 | 120.1 (12) |
C126—C121—P1 | 118.8 (7) | C223—C224—H22D | 120.0 |
C122—C121—P1 | 123.3 (8) | C225—C224—H22D | 120.0 |
C522—C521—C526 | 118.3 (9) | C514—C513—C512 | 120.2 (12) |
C522—C521—P5 | 121.6 (8) | C514—C513—H51E | 119.9 |
C526—C521—P5 | 120.0 (7) | C512—C513—H51E | 119.9 |
C422—C421—C426 | 120.2 (10) | C425—C424—C423 | 120.7 (14) |
C422—C421—P4 | 121.4 (8) | C425—C424—H42C | 119.6 |
C426—C421—P4 | 118.3 (8) | C423—C424—H42C | 119.6 |
C326—C321—C322 | 118.6 (9) | C224—C223—C222 | 120.7 (12) |
C326—C321—P3 | 124.3 (7) | C224—C223—H22E | 119.6 |
C322—C321—P3 | 117.1 (7) | C222—C223—H22E | 119.6 |
C516—C511—C512 | 115.8 (9) | C314—C315—C316 | 120.5 (12) |
C516—C511—P5 | 126.6 (8) | C314—C315—H31C | 119.7 |
C512—C511—P5 | 117.6 (7) | C316—C315—H31C | 119.7 |
C222—C221—C226 | 119.5 (9) | C611—C616—C615 | 119.9 (11) |
C222—C221—P2 | 118.6 (7) | C611—C616—H61B | 120.1 |
C226—C221—P2 | 121.8 (7) | C615—C616—H61B | 120.1 |
C213—C212—C211 | 121.2 (9) | C313—C314—C315 | 120.3 (11) |
C213—C212—H21A | 119.4 | C313—C314—H31D | 119.8 |
C211—C212—H21A | 119.4 | C315—C314—H31D | 119.8 |
P5—C03—P6 | 113.6 (4) | C414—C413—C412 | 120.4 (15) |
P5—C03—H03A | 108.8 | C414—C413—H41D | 119.8 |
P6—C03—H03A | 108.8 | C412—C413—H41D | 119.8 |
P5—C03—H03B | 108.8 | C314—C313—C312 | 119.7 (12) |
P6—C03—H03B | 108.8 | C314—C313—H31E | 120.2 |
H03A—C03—H03B | 107.7 | C312—C313—H31E | 120.2 |
C612—C611—C616 | 118.6 (9) | C425—C426—C421 | 118.4 (13) |
C612—C611—P6 | 123.8 (8) | C425—C426—H42D | 120.8 |
C616—C611—P6 | 117.6 (8) | C421—C426—H42D | 120.8 |
C121—C126—C125 | 120.9 (10) | C525—C524—C523 | 118.5 (12) |
C121—C126—H12A | 119.6 | C525—C524—H52E | 120.7 |
C125—C126—H12A | 119.6 | C523—C524—H52E | 120.7 |
C521—C522—C523 | 120.0 (11) | C614—C613—C612 | 119.6 (12) |
C521—C522—H52A | 120.0 | C614—C613—H61C | 120.2 |
C523—C522—H52A | 120.0 | C612—C613—H61C | 120.2 |
C211—C216—C215 | 120.3 (10) | C615—C614—C613 | 120.2 (13) |
C211—C216—H21B | 119.9 | C615—C614—H61D | 119.9 |
C215—C216—H21B | 119.9 | C613—C614—H61D | 119.9 |
P2—C02—P1 | 116.7 (5) | C424—C425—C426 | 121.1 (14) |
P2—C02—H02A | 108.1 | C424—C425—H42E | 119.4 |
P1—C02—H02A | 108.1 | C426—C425—H42E | 119.4 |
P2—C02—H02B | 108.1 | C614—C615—C616 | 120.6 (13) |
P1—C02—H02B | 108.1 | C614—C615—H61E | 119.7 |
H02A—C02—H02B | 107.3 | C616—C615—H61E | 119.7 |
C623—C622—C621 | 122.3 (10) | C624—C623—C622 | 119.0 (11) |
C623—C622—H62A | 118.9 | C624—C623—H62E | 120.5 |
C621—C622—H62A | 118.9 | C622—C623—H62E | 120.5 |
C416—C411—C412 | 116.8 (10) | C125—C124—C123 | 119.8 (11) |
C416—C411—P4 | 117.6 (8) | C125—C124—H12E | 120.1 |
C412—C411—P4 | 125.2 (10) | C123—C124—H12E | 120.1 |
C112—C111—C116 | 116.8 (9) | C323—C324—C325 | 119.2 (11) |
C112—C111—P1 | 118.1 (8) | C323—C324—H32E | 120.4 |
C116—C111—P1 | 125.0 (7) | C325—C324—H32E | 120.4 |
C225—C226—C221 | 120.7 (10) | C416—C415—C414 | 117.6 (16) |
C225—C226—H22A | 119.7 | C416—C415—H41E | 121.2 |
C221—C226—H22A | 119.7 | C414—C415—H41E | 121.2 |
C621—C626—C625 | 119.5 (10) | Cl4—C04—Cl3 | 113.2 (5) |
C621—C626—H62B | 120.3 | Cl4—C04—H04A | 108.9 |
C625—C626—H62B | 120.3 | Cl3—C04—H04A | 108.9 |
C316—C311—C312 | 118.2 (9) | Cl4—C04—H04B | 108.9 |
C316—C311—P3 | 118.0 (7) | Cl3—C04—H04B | 108.9 |
C312—C311—P3 | 123.8 (8) | H04A—C04—H04B | 107.8 |
C321—C326—C325 | 120.0 (10) | Cl5—C05—Cl6 | 111.3 (6) |
C321—C326—H32A | 120.0 | Cl5—C05—H05B | 109.4 |
C325—C326—H32A | 120.0 | Cl6—C05—H05B | 109.4 |
C214—C215—C216 | 121.3 (10) | Cl5—C05—H05A | 109.3 |
C214—C215—H21C | 119.4 | Cl6—C05—H05A | 109.3 |
C216—C215—H21C | 119.4 | H05B—C05—H05A | 108.0 |
C525—C526—C521 | 120.8 (10) |