research papers
Pd nanocrystals were produced with uniform truncated-cube shape and a narrow size distribution, yielding controlled surface area fractions from low Miller index ({100}, {110}, {111}) crystalline facets. Details on the structure and morphology of the nanocrystals were obtained by combining X-ray powder diffraction line profile analysis, high-resolution transmission electron microscopy and surface electrochemistry based on Cu underpotential deposition.
Keywords: nanocrystalline metals; catalysts; line profile analysis; surface electrochemistry; transmission electron microscopy.
Supporting information
Portable Document Format (PDF) file https://doi.org/10.1107/S1600576715015964/ks5481sup1.pdf |