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The title compound [systematic name: bis(η5-cyclo­penta­dien­yl)hexa­kis(μ-diethyl phosphito)-1:2κ6P:O;2:3κ6O:P-tricobalt(II,III,III)], [Co3(C5H5)2(C4H10O3P)6], is a well known mixed-valence CoII/CoIII cluster, with inversion symmetry. Each CoIII atom is bonded to three P atoms and a η5-cyclo­penta­dienyl ring; the central CoII atom, lying on an inversion center, has six O-atom neighbors in an octa­hedral arrangement.

Supporting information

cif

Crystallographic Information File (CIF) https://doi.org/10.1107/S1600536807013001/hb2322sup1.cif
Contains datablocks I, global

hkl

Structure factor file (CIF format) https://doi.org/10.1107/S1600536807013001/hb2322Isup2.hkl
Contains datablock I

CCDC reference: 643012

Key indicators

  • Single-crystal X-ray study
  • T = 100 K
  • Mean [sigma](C-C) = 0.003 Å
  • Disorder in main residue
  • R factor = 0.024
  • wR factor = 0.065
  • Data-to-parameter ratio = 19.6

checkCIF/PLATON results

No syntax errors found



Alert level C PLAT153_ALERT_1_C The su's on the Cell Axes are Equal (x 100000) . 80 Ang. PLAT154_ALERT_1_C The su's on the Cell Angles are Equal (x 10000) 100 Deg. PLAT180_ALERT_3_C Check Cell Rounding: # of Values Ending with 0 = 3 PLAT301_ALERT_3_C Main Residue Disorder ......................... 16.00 Perc.
0 ALERT level A = In general: serious problem 0 ALERT level B = Potentially serious problem 4 ALERT level C = Check and explain 0 ALERT level G = General alerts; check 2 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 0 ALERT type 2 Indicator that the structure model may be wrong or deficient 2 ALERT type 3 Indicator that the structure quality may be low 0 ALERT type 4 Improvement, methodology, query or suggestion 0 ALERT type 5 Informative message, check

Computing details top

Data collection: SMART (Bruker, 2002); cell refinement: SAINT-Plus (Bruker, 2003); data reduction: SAINT-Plus; program(s) used to solve structure: SHELXS97 (Sheldrick, 1997); program(s) used to refine structure: SHELXL97 (Sheldrick, 1997); molecular graphics: SHELXP97 (Sheldrick, 1997); software used to prepare material for publication: publCIF (Westrip, 2007).

Bis[1,3(η5)-cyclopentadienyl]hexakis(µ-diethyl phosphito)-1:2κ6P:O;2:3κ6O:P-tricobalt(II) top
Crystal data top
[Co3(C5H5)2(C4H10O3P)6]Z = 1
Mr = 1129.51F(000) = 589
Triclinic, P1Dx = 1.535 Mg m3
Hall symbol: -P 1Melting point: decomp > 559 K
a = 11.6355 (8) ÅMo Kα radiation, λ = 0.71073 Å
b = 11.6433 (8) ÅCell parameters from 6247 reflections
c = 12.1363 (8) Åθ = 2.5–30.5°
α = 116.529 (1)°µ = 1.27 mm1
β = 91.982 (1)°T = 100 K
γ = 118.802 (1)°Block, orange
V = 1221.90 (14) Å30.58 × 0.55 × 0.38 mm
Data collection top
Bruker SMART APEX CCD
diffractometer
6038 independent reflections
Radiation source: fine-focus sealed tube5710 reflections with I > 2σ(I)
Graphite monochromatorRint = 0.012
ω scansθmax = 28.3°, θmin = 2.0°
Absorption correction: multi-scan
(SADABS in SAINT-Plus; Bruker, 2003)
h = 1515
Tmin = 0.516, Tmax = 0.617k = 1515
12593 measured reflectionsl = 1616
Refinement top
Refinement on F2Primary atom site location: structure-invariant direct methods
Least-squares matrix: fullSecondary atom site location: difference Fourier map
R[F2 > 2σ(F2)] = 0.024Hydrogen site location: inferred from neighbouring sites
wR(F2) = 0.065H-atom parameters constrained
S = 1.06 w = 1/[σ2(Fo2) + (0.0362P)2 + 0.5433P]
where P = (Fo2 + 2Fc2)/3
6038 reflections(Δ/σ)max = 0.001
308 parametersΔρmax = 0.68 e Å3
0 restraintsΔρmin = 0.41 e Å3
Special details top

Geometry. All e.s.d.'s (except the e.s.d. in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell e.s.d.'s are taken into account individually in the estimation of e.s.d.'s in distances, angles and torsion angles; correlations between e.s.d.'s in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell e.s.d.'s is used for estimating e.s.d.'s involving l.s. planes.

Refinement. Refinement of F2 against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F2, conventional R-factors R are based on F, with F set to zero for negative F2. The threshold expression of F2 > σ(F2) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F2 are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger.

The P=O bonds exhibit a 95:5 disorder. This disorder was elected to be modeled after signifcant increases in the reliability indices.

Fractional atomic coordinates and isotropic or equivalent isotropic displacement parameters (Å2) top
xyzUiso*/UeqOcc. (<1)
Co10.147626 (17)0.279018 (19)0.378891 (15)0.01550 (5)
Co20.00000.00000.00000.01437 (6)
O10.39111 (10)0.36641 (12)0.26111 (10)0.0240 (2)
O20.35297 (10)0.18293 (11)0.32920 (9)0.02167 (19)
O40.00693 (11)0.06400 (12)0.30835 (10)0.0247 (2)
O50.13961 (10)0.03835 (12)0.34861 (10)0.0244 (2)
O70.06704 (11)0.32045 (13)0.26910 (10)0.0259 (2)
O80.17562 (11)0.49826 (11)0.29321 (10)0.0243 (2)
P10.26585 (3)0.21829 (4)0.25748 (3)0.01521 (7)0.95
P20.02630 (3)0.03952 (4)0.27609 (3)0.01559 (7)0.95
P30.06827 (3)0.31928 (4)0.24592 (3)0.01566 (7)0.95
O30.19099 (10)0.08603 (11)0.11821 (9)0.01709 (18)0.95
O60.09368 (10)0.04723 (11)0.13172 (9)0.01716 (18)0.95
O90.03843 (10)0.22100 (11)0.10222 (9)0.01702 (18)0.95
P1A0.1576 (9)0.0886 (10)0.2758 (9)0.0321 (17)*0.05
P2A0.0699 (8)0.1519 (9)0.2574 (7)0.0244 (14)*0.05
P3A0.2159 (8)0.3487 (9)0.2382 (8)0.0273 (15)*0.05
O3A0.132 (3)0.012 (3)0.130 (2)0.034 (5)*0.05
O6A0.119 (2)0.014 (2)0.125 (2)0.025 (4)*0.05
O9A0.124 (3)0.244 (3)0.102 (2)0.029 (4)*0.05
C10.31277 (15)0.48657 (16)0.53723 (13)0.0228 (3)
H10.39460.55450.53150.027*
C20.28610 (15)0.36162 (16)0.55113 (13)0.0234 (3)
H20.34850.33500.55780.028*
C30.14898 (16)0.28507 (17)0.55303 (13)0.0247 (3)
H30.10490.19880.56020.030*
C40.08981 (15)0.36368 (17)0.54202 (13)0.0255 (3)
H40.00040.33760.54060.031*
C50.19159 (16)0.48838 (16)0.53371 (13)0.0246 (3)
H50.18090.55950.52710.030*
C60.03599 (17)0.16964 (18)0.21561 (16)0.0294 (3)
H6A0.10650.16920.26120.035*
H6B0.07140.13580.15720.035*
C70.09206 (19)0.33079 (18)0.13832 (15)0.0335 (3)
H7A0.13170.36100.19650.050*
H7B0.06840.40060.08380.050*
H7C0.15790.33380.08530.050*
C80.27134 (15)0.10439 (18)0.30162 (15)0.0274 (3)
H8A0.25980.18950.27150.033*
H8B0.33380.12530.23000.033*
C90.32856 (16)0.0861 (2)0.41344 (16)0.0307 (3)
H9A0.26730.06880.48260.046*
H9B0.41800.17820.38500.046*
H9C0.33680.00030.44400.046*
C100.20349 (15)0.19436 (19)0.17978 (16)0.0303 (3)
H10A0.26520.16340.22720.036*
H10B0.20090.10660.11990.036*
C110.2562 (2)0.2421 (2)0.10585 (19)0.0451 (5)
H11A0.25400.33220.16560.068*
H11B0.34950.15970.05040.068*
H11C0.19880.26510.05390.068*
C120.14030 (16)0.55689 (17)0.22417 (15)0.0266 (3)
H12A0.09240.60340.26800.032*
H12B0.07910.47270.13670.032*
C130.2691 (2)0.6744 (2)0.2191 (2)0.0444 (4)
H13A0.33170.75430.30570.067*
H13B0.24630.71850.17870.067*
H13C0.31220.62590.16950.067*
C140.38822 (16)0.38690 (19)0.15258 (16)0.0279 (3)
H14A0.41800.49250.18340.034*
H14B0.29440.31880.09330.034*
C150.4810 (2)0.3521 (3)0.08269 (19)0.0436 (4)
H15A0.57150.41090.14350.065*
H15B0.48730.37890.01800.065*
H15C0.44400.24390.04160.065*
C160.42667 (15)0.12044 (18)0.25878 (14)0.0252 (3)
H16A0.49370.19140.23760.030*
H16B0.36250.02290.17850.030*
C170.49896 (16)0.09681 (19)0.34381 (16)0.0283 (3)
H17A0.56540.19460.42110.042*
H17B0.54540.05110.29750.042*
H17C0.43220.02960.36710.042*
Atomic displacement parameters (Å2) top
U11U22U33U12U13U23
Co10.01682 (9)0.01577 (9)0.01138 (8)0.00872 (7)0.00338 (6)0.00584 (7)
Co20.01433 (11)0.01494 (11)0.01169 (11)0.00749 (9)0.00361 (8)0.00628 (9)
O10.0200 (5)0.0218 (5)0.0222 (5)0.0067 (4)0.0062 (4)0.0114 (4)
O20.0227 (5)0.0262 (5)0.0182 (4)0.0168 (4)0.0048 (4)0.0098 (4)
O40.0338 (5)0.0222 (5)0.0204 (5)0.0164 (4)0.0064 (4)0.0122 (4)
O50.0227 (5)0.0248 (5)0.0199 (5)0.0107 (4)0.0097 (4)0.0103 (4)
O70.0267 (5)0.0357 (6)0.0227 (5)0.0230 (5)0.0098 (4)0.0144 (4)
O80.0303 (5)0.0186 (4)0.0210 (5)0.0125 (4)0.0034 (4)0.0099 (4)
P10.01410 (15)0.01606 (15)0.01339 (15)0.00780 (13)0.00305 (11)0.00706 (12)
P20.01693 (15)0.01626 (15)0.01310 (15)0.00872 (13)0.00521 (12)0.00796 (12)
P30.01721 (15)0.01564 (15)0.01362 (15)0.00968 (13)0.00420 (12)0.00683 (12)
O30.0160 (4)0.0188 (5)0.0139 (4)0.0097 (4)0.0038 (3)0.0068 (4)
O60.0168 (4)0.0172 (4)0.0138 (4)0.0076 (4)0.0046 (3)0.0077 (4)
O90.0203 (5)0.0169 (4)0.0140 (4)0.0108 (4)0.0047 (3)0.0078 (4)
C10.0229 (6)0.0181 (6)0.0138 (6)0.0074 (5)0.0004 (5)0.0034 (5)
C20.0274 (7)0.0249 (6)0.0127 (5)0.0148 (6)0.0011 (5)0.0065 (5)
C30.0320 (7)0.0238 (7)0.0123 (6)0.0127 (6)0.0059 (5)0.0085 (5)
C40.0272 (7)0.0292 (7)0.0132 (6)0.0160 (6)0.0073 (5)0.0059 (5)
C50.0332 (7)0.0219 (6)0.0141 (6)0.0173 (6)0.0044 (5)0.0042 (5)
C60.0343 (8)0.0269 (7)0.0348 (8)0.0208 (7)0.0137 (6)0.0174 (6)
C70.0469 (9)0.0262 (7)0.0235 (7)0.0188 (7)0.0105 (7)0.0123 (6)
C80.0210 (6)0.0305 (7)0.0250 (7)0.0104 (6)0.0082 (5)0.0148 (6)
C90.0288 (7)0.0404 (9)0.0353 (8)0.0213 (7)0.0177 (6)0.0260 (7)
C100.0218 (7)0.0336 (8)0.0375 (8)0.0156 (6)0.0127 (6)0.0198 (7)
C110.0442 (10)0.0425 (10)0.0355 (9)0.0275 (9)0.0070 (8)0.0092 (8)
C120.0343 (8)0.0260 (7)0.0264 (7)0.0187 (6)0.0103 (6)0.0166 (6)
C130.0371 (9)0.0374 (9)0.0664 (13)0.0167 (8)0.0120 (9)0.0377 (10)
C140.0260 (7)0.0317 (7)0.0340 (8)0.0157 (6)0.0110 (6)0.0233 (7)
C150.0447 (10)0.0667 (13)0.0357 (9)0.0353 (10)0.0231 (8)0.0331 (9)
C160.0266 (7)0.0295 (7)0.0244 (7)0.0194 (6)0.0094 (5)0.0134 (6)
C170.0283 (7)0.0342 (8)0.0395 (8)0.0220 (6)0.0163 (6)0.0261 (7)
Geometric parameters (Å, º) top
Co1—C42.0813 (13)P3A—O9A1.48 (2)
Co1—C32.0822 (13)P3A—C142.235 (8)
Co1—C12.0849 (13)C1—C51.420 (2)
Co1—C22.0901 (13)C1—C21.424 (2)
Co1—C52.0916 (13)C1—H10.9300
Co1—P32.1601 (4)C2—C31.411 (2)
Co1—P22.1698 (4)C2—H20.9300
Co1—P12.1703 (4)C3—C41.428 (2)
Co1—P1A2.068 (9)C3—H30.9300
Co1—P3A2.217 (8)C4—C51.415 (2)
Co1—P2A2.225 (8)C4—H40.9300
Co2—O32.0859 (9)C5—H50.9300
Co2—O3i2.0859 (9)C6—C71.503 (2)
Co2—O92.0884 (9)C6—H6A0.9700
Co2—O9i2.0884 (9)C6—H6B0.9700
Co2—O62.0915 (9)C7—H7A0.9600
Co2—O6i2.0915 (9)C7—H7B0.9600
Co2—O3A2.07 (2)C7—H7C0.9600
Co2—O3Ai2.07 (2)C8—C91.507 (2)
Co2—O6A2.09 (2)C8—H8A0.9700
Co2—O6Ai2.09 (2)C8—H8B0.9700
Co2—O9Ai2.11 (2)C9—H9A0.9600
Co2—O9A2.11 (2)C9—H9B0.9600
O1—C141.4416 (17)C9—H9C0.9600
O1—P11.6144 (10)C10—C111.492 (2)
O1—P3A1.944 (8)C10—H10A0.9700
O2—C161.4462 (16)C10—H10B0.9700
O2—P11.6174 (10)C11—H11A0.9600
O2—P1A1.910 (9)C11—H11B0.9600
O4—C61.4437 (18)C11—H11C0.9600
O4—P21.6174 (10)C12—C131.493 (2)
O4—P1A2.015 (9)C12—H12A0.9700
O5—C81.4405 (17)C12—H12B0.9700
O5—P21.6083 (10)C13—H13A0.9600
O5—P2A1.992 (8)C13—H13B0.9600
O7—C101.4369 (19)C13—H13C0.9600
O7—P31.6143 (10)C14—C151.493 (2)
O7—P2A1.887 (8)C14—H14A0.9700
O8—C121.4471 (17)C14—H14B0.9700
O8—P31.6144 (10)C15—H15A0.9600
O8—P3A1.862 (8)C15—H15B0.9600
P1—O31.5058 (10)C15—H15C0.9600
P2—O61.5052 (10)C16—C171.505 (2)
P3—O91.5046 (10)C16—H16A0.9700
P1A—O3A1.52 (3)C16—H16B0.9700
P1A—C62.333 (9)C17—H17A0.9600
P2A—O6A1.49 (2)C17—H17B0.9600
P2A—C102.146 (8)C17—H17C0.9600
P1A—Co1—C4134.9 (2)O9—P3—O8108.81 (6)
P1A—Co1—C398.8 (2)O7—P3—O899.95 (6)
C4—Co1—C340.12 (6)O9—P3—Co1120.17 (4)
P1A—Co1—C1122.1 (2)O7—P3—Co1110.82 (4)
C4—Co1—C167.01 (6)O8—P3—Co1106.87 (4)
C3—Co1—C167.02 (6)P1—O3—Co2127.63 (6)
P1A—Co1—C293.0 (2)P2—O6—Co2126.24 (6)
C4—Co1—C266.76 (6)P3—O9—Co2127.34 (6)
C3—Co1—C239.54 (6)O3A—P1A—O297.8 (11)
C1—Co1—C239.90 (6)O3A—P1A—O4108.1 (11)
P1A—Co1—C5159.4 (3)O2—P1A—O4130.1 (5)
C4—Co1—C539.65 (6)O3A—P1A—Co1121.3 (11)
C3—Co1—C566.79 (6)O2—P1A—Co1100.7 (4)
C1—Co1—C539.75 (6)O4—P1A—Co1100.9 (4)
C2—Co1—C566.52 (6)O3A—P1A—C680.3 (11)
P1A—Co1—P3109.8 (2)O2—P1A—C6111.5 (4)
C4—Co1—P3105.48 (4)Co1—P1A—C6138.5 (4)
C3—Co1—P3145.07 (4)O6A—P2A—O7118.1 (10)
C1—Co1—P3110.72 (4)O6A—P2A—O596.8 (9)
C2—Co1—P3150.61 (4)O7—P2A—O5132.9 (4)
C5—Co1—P389.25 (4)O6A—P2A—C1088.1 (9)
P1A—Co1—P254.2 (2)O5—P2A—C10117.9 (4)
C4—Co1—P298.60 (4)O6A—P2A—Co1117.4 (9)
C3—Co1—P289.43 (4)O7—P2A—Co198.5 (3)
C1—Co1—P2155.91 (4)O5—P2A—Co191.3 (3)
C2—Co1—P2117.48 (4)C10—P2A—Co1139.4 (4)
C5—Co1—P2135.93 (4)O9A—P3A—O899.8 (10)
P3—Co1—P291.346 (15)O9A—P3A—O1113.5 (10)
P1A—Co1—P142.8 (2)O8—P3A—O1131.4 (4)
C4—Co1—P1161.22 (4)O9A—P3A—Co1117.6 (10)
C3—Co1—P1124.65 (4)O8—P3A—Co196.3 (3)
C1—Co1—P198.13 (4)O1—P3A—Co198.1 (3)
C2—Co1—P194.51 (4)O9A—P3A—C1485.1 (10)
C5—Co1—P1132.99 (4)O8—P3A—C14116.1 (4)
P3—Co1—P190.248 (15)Co1—P3A—C14137.2 (4)
P2—Co1—P191.072 (15)P1A—O3A—Co2125.6 (15)
P1A—Co1—P3A89.5 (3)P2A—O6A—Co2124.5 (12)
C4—Co1—P3A135.5 (2)P3A—O9A—Co2126.4 (14)
C3—Co1—P3A160.1 (2)C5—C1—C2107.47 (13)
C1—Co1—P3A93.3 (2)C5—C1—Co170.38 (8)
C2—Co1—P3A122.5 (2)C2—C1—Co170.25 (8)
C5—Co1—P3A99.9 (2)C5—C1—H1126.3
P3—Co1—P3A42.8 (2)C2—C1—H1126.3
P2—Co1—P3A110.0 (2)Co1—C1—H1124.7
P1—Co1—P3A53.2 (2)C3—C2—C1108.44 (13)
P1A—Co1—P2A92.2 (3)C3—C2—Co169.93 (8)
C4—Co1—P2A88.2 (2)C1—C2—Co169.85 (8)
C3—Co1—P2A109.3 (2)C3—C2—H2125.8
C1—Co1—P2A145.6 (2)C1—C2—H2125.8
C2—Co1—P2A148.9 (2)Co1—C2—H2126.0
C5—Co1—P2A106.2 (2)C2—C3—C4107.86 (13)
P3—Co1—P2A51.5 (2)C2—C3—Co170.53 (8)
P2—Co1—P2A45.7 (2)C4—C3—Co169.90 (8)
P1—Co1—P2A109.9 (2)C2—C3—H3126.1
P3A—Co1—P2A88.2 (3)C4—C3—H3126.1
O3A—Co2—O3Ai180.0 (14)Co1—C3—H3125.1
O3A—Co2—O324.5 (7)C5—C4—C3107.79 (13)
O3Ai—Co2—O3155.5 (7)C5—C4—Co170.57 (8)
O3A—Co2—O3i155.5 (7)C3—C4—Co169.97 (8)
O3Ai—Co2—O3i24.5 (7)C5—C4—H4126.1
O3—Co2—O3i180.00 (6)C3—C4—H4126.1
O3A—Co2—O9102.2 (7)Co1—C4—H4124.9
O3Ai—Co2—O977.8 (7)C4—C5—C1108.42 (13)
O3—Co2—O989.23 (4)C4—C5—Co169.78 (8)
O3i—Co2—O990.77 (4)C1—C5—Co169.87 (8)
O3A—Co2—O9i77.8 (7)C4—C5—H5125.8
O3Ai—Co2—O9i102.2 (7)C1—C5—H5125.8
O3—Co2—O9i90.77 (4)Co1—C5—H5126.1
O3i—Co2—O9i89.23 (4)O4—C6—C7110.99 (13)
O9—Co2—O9i180.00 (3)O4—C6—P1A59.0 (2)
O3A—Co2—O669.6 (7)C7—C6—P1A150.2 (2)
O3Ai—Co2—O6110.4 (7)O4—C6—H6A109.4
O3—Co2—O689.95 (4)C7—C6—H6A109.4
O3i—Co2—O690.05 (4)P1A—C6—H6A100.2
O9—Co2—O689.48 (4)O4—C6—H6B109.4
O9i—Co2—O690.52 (4)C7—C6—H6B109.4
O3A—Co2—O6i110.4 (7)P1A—C6—H6B57.0
O3Ai—Co2—O6i69.6 (7)H6A—C6—H6B108.0
O3—Co2—O6i90.05 (4)C6—C7—H7A109.5
O3i—Co2—O6i89.95 (4)C6—C7—H7B109.5
O9—Co2—O6i90.52 (4)H7A—C7—H7B109.5
O9i—Co2—O6i89.48 (4)C6—C7—H7C109.5
O6—Co2—O6i180.00 (11)H7A—C7—H7C109.5
O3A—Co2—O6A89.3 (9)H7B—C7—H7C109.5
O3Ai—Co2—O6A90.7 (9)O5—C8—C9107.07 (12)
O3—Co2—O6A104.1 (6)O5—C8—H8A110.3
O3i—Co2—O6A75.9 (6)C9—C8—H8A110.3
O9—Co2—O6A69.1 (6)O5—C8—H8B110.3
O9i—Co2—O6A110.9 (6)C9—C8—H8B110.3
O6—Co2—O6A25.4 (6)H8A—C8—H8B108.6
O6i—Co2—O6A154.6 (6)C8—C9—H9A109.5
O3A—Co2—O6Ai90.7 (9)C8—C9—H9B109.5
O3Ai—Co2—O6Ai89.3 (9)H9A—C9—H9B109.5
O3—Co2—O6Ai75.9 (6)C8—C9—H9C109.5
O3i—Co2—O6Ai104.1 (6)H9A—C9—H9C109.5
O9—Co2—O6Ai110.9 (6)H9B—C9—H9C109.5
O9i—Co2—O6Ai69.1 (6)O7—C10—C11109.91 (14)
O6—Co2—O6Ai154.6 (6)O7—C10—P2A59.7 (2)
O6i—Co2—O6Ai25.4 (6)C11—C10—P2A159.5 (2)
O6A—Co2—O6Ai180.0 (19)O7—C10—H10A109.7
O3A—Co2—O9Ai92.0 (9)C11—C10—H10A109.7
O3Ai—Co2—O9Ai88.0 (9)P2A—C10—H10A90.8
O3—Co2—O9Ai110.7 (6)O7—C10—H10B109.7
O3i—Co2—O9Ai69.3 (6)C11—C10—H10B109.7
O9—Co2—O9Ai155.2 (7)P2A—C10—H10B62.9
O9i—Co2—O9Ai24.8 (7)H10A—C10—H10B108.2
O6—Co2—O9Ai76.4 (6)C10—C11—H11A109.5
O6i—Co2—O9Ai103.6 (6)C10—C11—H11B109.5
O6A—Co2—O9Ai91.0 (8)H11A—C11—H11B109.5
O6Ai—Co2—O9Ai89.0 (8)C10—C11—H11C109.5
O3A—Co2—O9A88.0 (9)H11A—C11—H11C109.5
O3Ai—Co2—O9A92.0 (9)H11B—C11—H11C109.5
O3—Co2—O9A69.3 (6)O8—C12—C13109.50 (13)
O3i—Co2—O9A110.7 (6)O8—C12—H12A109.8
O9—Co2—O9A24.8 (7)C13—C12—H12A109.8
O9i—Co2—O9A155.2 (7)O8—C12—H12B109.8
O6—Co2—O9A103.6 (6)C13—C12—H12B109.8
O6i—Co2—O9A76.4 (6)H12A—C12—H12B108.2
O6A—Co2—O9A89.0 (8)C12—C13—H13A109.5
O6Ai—Co2—O9A91.0 (8)C12—C13—H13B109.5
O9Ai—Co2—O9A180.0 (11)H13A—C13—H13B109.5
C14—O1—P1122.23 (9)C12—C13—H13C109.5
C14—O1—P3A81.1 (3)H13A—C13—H13C109.5
P1—O1—P3A66.2 (2)H13B—C13—H13C109.5
C16—O2—P1117.50 (9)O1—C14—C15110.50 (13)
C16—O2—P1A125.8 (3)O1—C14—P3A59.3 (2)
P1—O2—P1A51.3 (3)C15—C14—P3A158.5 (2)
C6—O4—P2121.43 (9)O1—C14—H14A109.6
C6—O4—P1A83.1 (3)C15—C14—H14A109.6
P2—O4—P1A63.1 (3)P3A—C14—H14A91.9
C8—O5—P2119.66 (9)O1—C14—H14B109.6
C8—O5—P2A126.6 (2)C15—C14—H14B109.6
P2—O5—P2A55.4 (2)P3A—C14—H14B62.3
C10—O7—P3121.71 (9)H14A—C14—H14B108.1
C10—O7—P2A79.1 (2)C14—C15—H15A109.5
P3—O7—P2A65.5 (2)C14—C15—H15B109.5
C12—O8—P3117.52 (9)H15A—C15—H15B109.5
C12—O8—P3A130.9 (3)C14—C15—H15C109.5
P3—O8—P3A54.1 (3)H15A—C15—H15C109.5
O3—P1—O1108.61 (6)H15B—C15—H15C109.5
O3—P1—O2108.37 (5)O2—C16—C17108.01 (12)
O1—P1—O2100.04 (6)O2—C16—H16A110.1
O3—P1—Co1119.19 (4)C17—C16—H16A110.1
O1—P1—Co1111.69 (4)O2—C16—H16B110.1
O2—P1—Co1107.15 (4)C17—C16—H16B110.1
O6—P2—O5109.58 (6)H16A—C16—H16B108.4
O6—P2—O4108.47 (6)C16—C17—H17A109.5
O5—P2—O499.50 (6)C16—C17—H17B109.5
O6—P2—Co1120.34 (4)H17A—C17—H17B109.5
O5—P2—Co1105.23 (4)C16—C17—H17C109.5
O4—P2—Co1111.64 (4)H17A—C17—H17C109.5
O9—P3—O7108.29 (6)H17B—C17—H17C109.5
C14—O1—P1—O325.90 (12)C3—Co1—P2A—O524.0 (3)
P3A—O1—P1—O387.4 (3)C1—Co1—P2A—O5101.3 (3)
C14—O1—P1—O2139.32 (11)C2—Co1—P2A—O523.3 (5)
P3A—O1—P1—O2159.1 (3)C5—Co1—P2A—O594.5 (2)
C14—O1—P1—Co1107.55 (10)P3—Co1—P2A—O5170.1 (4)
P3A—O1—P1—Co146.0 (3)P2—Co1—P2A—O545.12 (17)
C16—O2—P1—O342.43 (11)P1—Co1—P2A—O5116.2 (2)
P1A—O2—P1—O372.9 (3)P3A—Co1—P2A—O5165.7 (3)
C16—O2—P1—O171.17 (10)P1A—Co1—P2A—C10145.5 (6)
P1A—O2—P1—O1173.5 (3)C4—Co1—P2A—C1079.6 (5)
C16—O2—P1—Co1172.24 (9)C3—Co1—P2A—C10114.3 (5)
P1A—O2—P1—Co156.9 (3)C1—Co1—P2A—C1037.0 (8)
P1A—Co1—P1—O360.7 (4)C2—Co1—P2A—C10115.0 (5)
C4—Co1—P1—O3153.84 (14)C5—Co1—P2A—C1043.8 (6)
C3—Co1—P1—O3122.57 (7)P3—Co1—P2A—C1031.9 (4)
C1—Co1—P1—O3169.80 (6)P2—Co1—P2A—C10176.6 (7)
C2—Co1—P1—O3150.20 (6)P1—Co1—P2A—C10105.5 (5)
C5—Co1—P1—O3148.03 (7)P3A—Co1—P2A—C1056.0 (6)
P3—Co1—P1—O358.83 (5)C12—O8—P3A—O9A33.5 (11)
P2—Co1—P1—O332.53 (5)P3—O8—P3A—O9A63.8 (10)
P3A—Co1—P1—O381.8 (3)C12—O8—P3A—O1100.3 (6)
P2A—Co1—P1—O310.1 (2)P3—O8—P3A—O1162.4 (7)
P1A—Co1—P1—O1171.3 (4)C12—O8—P3A—Co1153.03 (16)
C4—Co1—P1—O178.15 (15)P3—O8—P3A—Co155.7 (2)
C3—Co1—P1—O1109.43 (6)C12—O8—P3A—C1455.7 (5)
C1—Co1—P1—O141.80 (6)P3—O8—P3A—C14153.1 (5)
C2—Co1—P1—O181.80 (6)C14—O1—P3A—O9A47.7 (11)
C5—Co1—P1—O120.03 (7)P1—O1—P3A—O9A83.5 (11)
P3—Co1—P1—O169.18 (4)C14—O1—P3A—O881.5 (5)
P2—Co1—P1—O1160.53 (4)P1—O1—P3A—O8147.3 (6)
P3A—Co1—P1—O146.2 (3)C14—O1—P3A—Co1172.6 (3)
P2A—Co1—P1—O1117.9 (2)P1—O1—P3A—Co141.37 (18)
P1A—Co1—P1—O262.7 (4)P1—O1—P3A—C14131.18 (16)
C4—Co1—P1—O230.46 (15)P1A—Co1—P3A—O9A63.3 (11)
C3—Co1—P1—O20.81 (7)C4—Co1—P3A—O9A114.5 (11)
C1—Co1—P1—O266.81 (6)C3—Co1—P3A—O9A178.7 (10)
C2—Co1—P1—O226.82 (6)C1—Co1—P3A—O9A174.5 (11)
C5—Co1—P1—O288.59 (7)C2—Co1—P3A—O9A156.5 (11)
P3—Co1—P1—O2177.79 (4)C5—Co1—P3A—O9A135.1 (11)
P2—Co1—P1—O290.86 (4)P3—Co1—P3A—O9A57.1 (11)
P3A—Co1—P1—O2154.8 (3)P2—Co1—P3A—O9A12.0 (12)
P2A—Co1—P1—O2133.5 (2)P1—Co1—P3A—O9A87.7 (11)
C8—O5—P2—O647.52 (12)P2A—Co1—P3A—O9A28.9 (11)
P2A—O5—P2—O668.7 (3)P1A—Co1—P3A—O8167.9 (4)
C8—O5—P2—O466.09 (11)C4—Co1—P3A—O810.0 (5)
P2A—O5—P2—O4177.7 (3)C3—Co1—P3A—O876.7 (7)
C8—O5—P2—Co1178.24 (9)C1—Co1—P3A—O870.0 (3)
P2A—O5—P2—Co162.1 (3)C2—Co1—P3A—O898.9 (3)
C6—O4—P2—O629.68 (12)C5—Co1—P3A—O830.5 (3)
P1A—O4—P2—O691.8 (3)P3—Co1—P3A—O847.4 (2)
C6—O4—P2—O5144.14 (11)P2—Co1—P3A—O8116.6 (3)
P1A—O4—P2—O5153.8 (3)P1—Co1—P3A—O8167.7 (4)
C6—O4—P2—Co1105.19 (11)P2A—Co1—P3A—O875.6 (3)
P1A—O4—P2—Co143.1 (3)P1A—Co1—P3A—O158.6 (4)
P1A—Co1—P2—O681.8 (3)C4—Co1—P3A—O1123.5 (2)
C4—Co1—P2—O6137.72 (6)C3—Co1—P3A—O156.8 (8)
C3—Co1—P2—O6176.93 (6)C1—Co1—P3A—O163.5 (3)
C1—Co1—P2—O6171.29 (11)C2—Co1—P3A—O134.6 (4)
C2—Co1—P2—O6154.07 (6)C5—Co1—P3A—O1103.0 (3)
C5—Co1—P2—O6122.16 (7)P3—Co1—P3A—O1179.1 (5)
P3—Co1—P2—O631.85 (5)P2—Co1—P3A—O1109.9 (3)
P1—Co1—P2—O658.42 (5)P1—Co1—P3A—O134.21 (17)
P3A—Co1—P2—O67.6 (2)P2A—Co1—P3A—O1150.9 (3)
P2A—Co1—P2—O658.7 (3)P1A—Co1—P3A—C1451.6 (6)
P1A—Co1—P2—O5154.1 (3)C4—Co1—P3A—C14130.5 (4)
C4—Co1—P2—O513.55 (6)C3—Co1—P3A—C1463.8 (9)
C3—Co1—P2—O552.75 (6)C1—Co1—P3A—C1470.5 (5)
C1—Co1—P2—O564.54 (11)C2—Co1—P3A—C1441.6 (6)
C2—Co1—P2—O581.76 (6)C5—Co1—P3A—C14110.0 (5)
C5—Co1—P2—O52.01 (7)P3—Co1—P3A—C14172.1 (8)
P3—Co1—P2—O592.32 (4)P2—Co1—P3A—C14102.9 (5)
P1—Co1—P2—O5177.40 (4)P1—Co1—P3A—C1427.2 (4)
P3A—Co1—P2—O5131.7 (2)P2A—Co1—P3A—C14143.9 (6)
P2A—Co1—P2—O565.4 (3)O2—P1A—O3A—Co2139.3 (16)
P1A—Co1—P2—O447.1 (3)O4—P1A—O3A—Co283.9 (18)
C4—Co1—P2—O493.44 (6)Co1—P1A—O3A—Co232 (2)
C3—Co1—P2—O454.24 (6)C6—P1A—O3A—Co2110.0 (17)
C1—Co1—P2—O442.45 (11)O3—Co2—O3A—P1A101 (3)
C2—Co1—P2—O425.23 (6)O3i—Co2—O3A—P1A79 (3)
C5—Co1—P2—O4109.00 (7)O9—Co2—O3A—P1A42 (2)
P3—Co1—P2—O4160.69 (4)O9i—Co2—O3A—P1A138 (2)
P1—Co1—P2—O470.41 (4)O6—Co2—O3A—P1A43.2 (17)
P3A—Co1—P2—O4121.3 (2)O6i—Co2—O3A—P1A136.8 (17)
P2A—Co1—P2—O4172.4 (3)O6A—Co2—O3A—P1A26.9 (19)
C10—O7—P3—O927.35 (12)O6Ai—Co2—O3A—P1A153.1 (19)
P2A—O7—P3—O985.7 (3)O9Ai—Co2—O3A—P1A117.9 (19)
C10—O7—P3—O8141.10 (11)O9A—Co2—O3A—P1A62.1 (19)
P2A—O7—P3—O8160.6 (3)O7—P2A—O6A—Co277.9 (15)
C10—O7—P3—Co1106.44 (11)O5—P2A—O6A—Co2134.9 (13)
P2A—O7—P3—Co148.1 (3)C10—P2A—O6A—Co2107.3 (13)
C12—O8—P3—O952.86 (11)Co1—P2A—O6A—Co239.8 (18)
P3A—O8—P3—O969.5 (3)O3A—Co2—O6A—P2A66.3 (16)
C12—O8—P3—O760.49 (11)O3Ai—Co2—O6A—P2A113.7 (16)
P3A—O8—P3—O7177.2 (3)O3—Co2—O6A—P2A46.6 (16)
C12—O8—P3—Co1175.98 (9)O3i—Co2—O6A—P2A133.4 (16)
P3A—O8—P3—Co161.7 (3)O9—Co2—O6A—P2A37.1 (13)
P1A—Co1—P3—O93.8 (3)O9i—Co2—O6A—P2A142.9 (13)
C4—Co1—P3—O9155.28 (6)O6—Co2—O6A—P2A104 (2)
C3—Co1—P3—O9146.91 (8)O6i—Co2—O6A—P2A76 (2)
C1—Co1—P3—O9133.90 (6)O9Ai—Co2—O6A—P2A158.2 (16)
C2—Co1—P3—O9134.76 (9)O9A—Co2—O6A—P2A21.8 (16)
C5—Co1—P3—O9168.10 (6)O8—P3A—O9A—Co2137.4 (14)
P2—Co1—P3—O955.97 (5)O1—P3A—O9A—Co278.8 (17)
P1—Co1—P3—O935.10 (5)Co1—P3A—O9A—Co235 (2)
P3A—Co1—P3—O962.5 (3)C14—P3A—O9A—Co2107.0 (16)
P2A—Co1—P3—O980.4 (3)O3A—Co2—O9A—P3A23.2 (18)
P1A—Co1—P3—O7123.7 (3)O3Ai—Co2—O9A—P3A156.8 (18)
C4—Co1—P3—O727.73 (6)O3—Co2—O9A—P3A39.4 (15)
C3—Co1—P3—O719.35 (9)O3i—Co2—O9A—P3A140.6 (15)
C1—Co1—P3—O798.55 (6)O9—Co2—O9A—P3A102 (2)
C2—Co1—P3—O797.68 (10)O9i—Co2—O9A—P3A78 (2)
C5—Co1—P3—O764.35 (6)O6—Co2—O9A—P3A45.3 (18)
P2—Co1—P3—O771.58 (5)O6i—Co2—O9A—P3A134.7 (18)
P1—Co1—P3—O7162.66 (5)O6A—Co2—O9A—P3A66.1 (18)
P3A—Co1—P3—O7169.9 (3)O6Ai—Co2—O9A—P3A113.9 (18)
P2A—Co1—P3—O747.2 (3)P1A—Co1—C1—C5166.8 (3)
P1A—Co1—P3—O8128.3 (3)C4—Co1—C1—C537.07 (9)
C4—Co1—P3—O880.24 (6)C3—Co1—C1—C580.82 (9)
C3—Co1—P3—O888.62 (8)C2—Co1—C1—C5117.81 (12)
C1—Co1—P3—O89.42 (6)P3—Co1—C1—C561.52 (9)
C2—Co1—P3—O810.29 (10)P2—Co1—C1—C593.64 (12)
C5—Co1—P3—O843.62 (6)P1—Co1—C1—C5154.89 (8)
P2—Co1—P3—O8179.55 (4)P3A—Co1—C1—C5101.7 (2)
P1—Co1—P3—O889.37 (4)P2A—Co1—C1—C510.2 (4)
P3A—Co1—P3—O861.9 (3)P1A—Co1—C1—C249.0 (3)
P2A—Co1—P3—O8155.1 (3)C4—Co1—C1—C280.74 (9)
O1—P1—O3—Co2104.27 (8)C3—Co1—C1—C236.99 (9)
O2—P1—O3—Co2147.93 (7)C5—Co1—C1—C2117.81 (12)
Co1—P1—O3—Co225.14 (9)P3—Co1—C1—C2179.34 (7)
O3A—Co2—O3—P192.4 (16)P2—Co1—C1—C224.17 (15)
O3Ai—Co2—O3—P187.6 (16)P1—Co1—C1—C287.29 (8)
O9—Co2—O3—P130.22 (7)P3A—Co1—C1—C2140.5 (2)
O9i—Co2—O3—P1149.78 (7)P2A—Co1—C1—C2128.0 (4)
O6—Co2—O3—P159.26 (8)C5—C1—C2—C31.37 (15)
O6i—Co2—O3—P1120.74 (8)Co1—C1—C2—C359.49 (9)
O6A—Co2—O3—P138.0 (6)C5—C1—C2—Co160.86 (9)
O6Ai—Co2—O3—P1142.0 (6)P1A—Co1—C2—C3100.3 (3)
O9Ai—Co2—O3—P1134.6 (7)C4—Co1—C2—C338.09 (9)
O9A—Co2—O3—P145.4 (7)C1—Co1—C2—C3119.52 (12)
O5—P2—O6—Co2147.70 (6)C5—Co1—C2—C381.45 (9)
O4—P2—O6—Co2104.63 (7)P3—Co1—C2—C3118.26 (10)
Co1—P2—O6—Co225.61 (9)P2—Co1—C2—C349.62 (9)
O3A—Co2—O6—P243.6 (7)P1—Co1—C2—C3143.18 (8)
O3Ai—Co2—O6—P2136.4 (7)P3A—Co1—C2—C3168.4 (3)
O3—Co2—O6—P229.62 (7)P2A—Co1—C2—C31.0 (4)
O3i—Co2—O6—P2150.38 (7)P1A—Co1—C2—C1140.2 (3)
O9—Co2—O6—P259.61 (7)C4—Co1—C2—C181.43 (9)
O9i—Co2—O6—P2120.39 (7)C3—Co1—C2—C1119.52 (12)
O6A—Co2—O6—P295.3 (13)C5—Co1—C2—C138.07 (8)
O6Ai—Co2—O6—P284.7 (13)P3—Co1—C2—C11.26 (14)
O9Ai—Co2—O6—P2141.0 (7)P2—Co1—C2—C1169.14 (7)
O9A—Co2—O6—P239.0 (7)P1—Co1—C2—C197.30 (8)
O7—P3—O9—Co2106.42 (7)P3A—Co1—C2—C148.8 (3)
O8—P3—O9—Co2145.83 (7)P2A—Co1—C2—C1120.5 (4)
Co1—P3—O9—Co222.28 (9)C1—C2—C3—C40.77 (15)
O3A—Co2—O9—P336.7 (7)Co1—C2—C3—C460.22 (9)
O3Ai—Co2—O9—P3143.3 (7)C1—C2—C3—Co159.44 (9)
O3—Co2—O9—P357.60 (7)P1A—Co1—C3—C283.9 (3)
O3i—Co2—O9—P3122.40 (7)C4—Co1—C3—C2118.40 (12)
O6—Co2—O9—P332.36 (7)C1—Co1—C3—C237.32 (8)
O6i—Co2—O9—P3147.64 (7)C5—Co1—C3—C280.70 (9)
O6A—Co2—O9—P347.9 (6)P3—Co1—C3—C2130.98 (8)
O6Ai—Co2—O9—P3132.1 (6)P2—Co1—C3—C2137.48 (8)
O9Ai—Co2—O9—P386.8 (15)P1—Co1—C3—C246.57 (9)
O9A—Co2—O9—P393.2 (15)P3A—Co1—C3—C230.0 (6)
C16—O2—P1A—O3A33.4 (11)P2A—Co1—C3—C2179.5 (2)
P1—O2—P1A—O3A65.3 (10)P1A—Co1—C3—C4157.7 (3)
C16—O2—P1A—O488.2 (6)C1—Co1—C3—C481.08 (9)
P1—O2—P1A—O4173.1 (8)C2—Co1—C3—C4118.40 (12)
C16—O2—P1A—Co1157.47 (17)C5—Co1—C3—C437.70 (9)
P1—O2—P1A—Co158.7 (3)P3—Co1—C3—C412.58 (12)
C16—O2—P1A—C649.2 (5)P2—Co1—C3—C4104.12 (8)
P1—O2—P1A—C6147.9 (5)P1—Co1—C3—C4164.97 (7)
C6—O4—P1A—O3A45.0 (11)P3A—Co1—C3—C488.4 (6)
P2—O4—P1A—O3A85.6 (11)P2A—Co1—C3—C462.1 (2)
C6—O4—P1A—O272.5 (6)C2—C3—C4—C50.12 (15)
P2—O4—P1A—O2157.0 (7)Co1—C3—C4—C560.74 (9)
C6—O4—P1A—Co1173.3 (3)C2—C3—C4—Co160.62 (9)
P2—O4—P1A—Co142.7 (2)P1A—Co1—C4—C5150.3 (4)
P2—O4—P1A—C6130.57 (17)C3—Co1—C4—C5118.26 (12)
C4—Co1—P1A—O3A148.0 (12)C1—Co1—C4—C537.16 (8)
C3—Co1—P1A—O3A168.2 (13)C2—Co1—C4—C580.71 (9)
C1—Co1—P1A—O3A123.5 (13)P3—Co1—C4—C569.18 (8)
C2—Co1—P1A—O3A152.5 (13)P2—Co1—C4—C5163.00 (8)
C5—Co1—P1A—O3A147.9 (12)P1—Co1—C4—C576.76 (17)
P3—Co1—P1A—O3A8.6 (13)P3A—Co1—C4—C532.8 (3)
P2—Co1—P1A—O3A85.4 (13)P2A—Co1—C4—C5118.3 (2)
P1—Co1—P1A—O3A59.0 (13)P1A—Co1—C4—C332.0 (4)
P3A—Co1—P1A—O3A29.9 (13)C1—Co1—C4—C381.10 (9)
P2A—Co1—P1A—O3A58.2 (13)C2—Co1—C4—C337.55 (8)
C4—Co1—P1A—O2106.0 (4)C5—Co1—C4—C3118.26 (12)
C3—Co1—P1A—O285.7 (3)P3—Co1—C4—C3172.56 (7)
C1—Co1—P1A—O217.4 (5)P2—Co1—C4—C378.75 (8)
C2—Co1—P1A—O246.4 (3)P1—Co1—C4—C341.50 (18)
C5—Co1—P1A—O241.9 (9)P3A—Co1—C4—C3151.0 (3)
P3—Co1—P1A—O2114.6 (3)P2A—Co1—C4—C3123.4 (2)
P2—Co1—P1A—O2168.6 (5)C3—C4—C5—C10.97 (15)
P1—Co1—P1A—O247.0 (2)Co1—C4—C5—C159.39 (9)
P3A—Co1—P1A—O276.1 (4)C3—C4—C5—Co160.36 (9)
P2A—Co1—P1A—O2164.3 (4)C2—C1—C5—C41.44 (15)
C4—Co1—P1A—O428.8 (5)Co1—C1—C5—C459.33 (9)
C3—Co1—P1A—O449.0 (3)C2—C1—C5—Co160.77 (9)
C1—Co1—P1A—O4117.4 (3)P1A—Co1—C5—C486.3 (7)
C2—Co1—P1A—O488.4 (3)C3—Co1—C5—C438.14 (9)
C5—Co1—P1A—O492.9 (7)C1—Co1—C5—C4119.58 (12)
P3—Co1—P1A—O4110.6 (3)C2—Co1—C5—C481.37 (9)
P2—Co1—P1A—O433.82 (19)P3—Co1—C5—C4115.73 (8)
P1—Co1—P1A—O4178.2 (6)P2—Co1—C5—C424.57 (11)
P3A—Co1—P1A—O4149.1 (4)P1—Co1—C5—C4154.64 (7)
P2A—Co1—P1A—O460.9 (4)P3A—Co1—C5—C4157.3 (2)
C4—Co1—P1A—C635.0 (8)P2A—Co1—C5—C466.4 (2)
C3—Co1—P1A—C655.2 (6)P1A—Co1—C5—C133.3 (7)
C1—Co1—P1A—C6123.6 (5)C4—Co1—C5—C1119.58 (12)
C2—Co1—P1A—C694.6 (6)C3—Co1—C5—C181.44 (9)
C5—Co1—P1A—C699.1 (8)C2—Co1—C5—C138.21 (8)
P3—Co1—P1A—C6104.4 (6)P3—Co1—C5—C1124.69 (8)
P2—Co1—P1A—C627.6 (5)P2—Co1—C5—C1144.15 (7)
P1—Co1—P1A—C6172.0 (9)P1—Co1—C5—C135.05 (10)
P3A—Co1—P1A—C6142.9 (6)P3A—Co1—C5—C183.1 (2)
P2A—Co1—P1A—C654.7 (6)P2A—Co1—C5—C1174.0 (2)
C10—O7—P2A—O6A48.2 (10)P2—O4—C6—C796.06 (14)
P3—O7—P2A—O6A84.3 (10)P1A—O4—C6—C7148.6 (3)
C10—O7—P2A—O584.6 (5)P2—O4—C6—P1A52.6 (3)
P3—O7—P2A—O5142.9 (6)O3A—P1A—C6—O4137.0 (10)
P3—O7—P2A—C10132.50 (17)O2—P1A—C6—O4128.4 (5)
C10—O7—P2A—Co1175.6 (3)Co1—P1A—C6—O49.9 (5)
P3—O7—P2A—Co143.06 (17)O3A—P1A—C6—C759.0 (11)
C8—O5—P2A—O6A42.1 (9)O2—P1A—C6—C7153.6 (3)
P2—O5—P2A—O6A61.6 (9)O4—P1A—C6—C778.0 (5)
C8—O5—P2A—O797.2 (5)Co1—P1A—C6—C768.0 (9)
P2—O5—P2A—O7159.1 (7)P2—O5—C8—C9157.09 (10)
C8—O5—P2A—C1049.4 (5)P2A—O5—C8—C9135.9 (3)
P2—O5—P2A—C10153.1 (5)P3—O7—C10—C11108.38 (14)
C8—O5—P2A—Co1159.91 (13)P2A—O7—C10—C11160.4 (3)
P2—O5—P2A—Co156.24 (17)P3—O7—C10—P2A52.1 (2)
P1A—Co1—P2A—O6A22.2 (11)O6A—P2A—C10—O7138.9 (9)
C4—Co1—P2A—O6A157.1 (10)O5—P2A—C10—O7124.4 (4)
C3—Co1—P2A—O6A122.3 (10)Co1—P2A—C10—O76.8 (4)
C1—Co1—P2A—O6A160.4 (9)O6A—P2A—C10—C1174.7 (11)
C2—Co1—P2A—O6A121.6 (10)O7—P2A—C10—C1164.2 (7)
C5—Co1—P2A—O6A167.1 (10)O5—P2A—C10—C11171.4 (4)
P3—Co1—P2A—O6A91.5 (10)Co1—P2A—C10—C1157.4 (10)
P2—Co1—P2A—O6A53.2 (10)P3—O8—C12—C13145.87 (13)
P1—Co1—P2A—O6A17.8 (11)P3A—O8—C12—C1380.9 (4)
P3A—Co1—P2A—O6A67.3 (10)P1—O1—C14—C15104.46 (14)
P1A—Co1—P2A—O7150.0 (4)P3A—O1—C14—C15159.0 (3)
C4—Co1—P2A—O775.1 (3)P1—O1—C14—P3A54.5 (3)
C3—Co1—P2A—O7109.8 (3)O9A—P3A—C14—O1137.1 (10)
C1—Co1—P2A—O732.5 (5)O8—P3A—C14—O1124.4 (5)
C2—Co1—P2A—O7110.5 (3)Co1—P3A—C14—O110.9 (4)
C5—Co1—P2A—O739.3 (3)O9A—P3A—C14—C1570.6 (12)
P3—Co1—P2A—O736.36 (17)O8—P3A—C14—C15169.1 (4)
P2—Co1—P2A—O7178.9 (5)O1—P3A—C14—C1566.5 (7)
P1—Co1—P2A—O7110.0 (3)Co1—P3A—C14—C1555.6 (10)
P3A—Co1—P2A—O760.5 (3)P1—O2—C16—C17179.83 (9)
P1A—Co1—P2A—O576.2 (3)P1A—O2—C16—C17119.4 (3)
C4—Co1—P2A—O558.7 (2)
Symmetry code: (i) x, y, z.
 

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