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The centrosymmetric title compound, Na(H)[Rh2(C2H3O2)6], consists of dirhodium(II) tetraacetate with two additional axial acetate ligands. Charges are balanced by a sodium ion and a disordered proton. The sodium coordination sphere includes O atoms bound equatorially to the rhodium as well as O atoms from the axial acetates. The Rh-Rh distance is 2.3827 (5) Å, Rh-O(axial) is 2.279 (2) Å, and the average Rh-O(equatorial) distance is 2.040 (4) Å.

Supporting information

cif

Crystallographic Information File (CIF)
Contains datablocks grnm, global

fcf

Structure factor file (CIF format)
Contains datablock grnm

CCDC reference: 129708

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