metal-organic compounds
A redetermination of the structure of the title compound, [Ni(C4H13N3)2]Cl2.H2O, from diffractometer data leads to considerably more accurate geometric parameters than those obtained in a previous determination using film data. The coordination geometry around the NiII atom in the [Ni(C4H13N3)2]2+ cation is distorted octahedron, with the Ni-N distances in the range 2.083 (4)-2.166 (4) Å and the trans- N-Ni-N 161.9 (2)-177.5 (2)°
Supporting information
Crystallographic Information File (CIF) | |
Structure factor file (CIF format) |
CCDC reference: 127086