Supporting information
Crystallographic Information File (CIF) https://doi.org/10.1107/S2052519213024378/dk5011sup1.cif | |
Structure factor file (CIF format) https://doi.org/10.1107/S2052519213024378/dk5011Isup2.hkl |
Crystal data, data collection and structure refinement details are summarized in Table 1.
Data collection: CrysAlis CCD (Oxford Diffraction, 2004); cell refinement: CrysAlis CCD (Oxford Diffraction, 2004); data reduction: CrysAlis RED (Oxford Diffraction, 2005); program(s) used to solve structure: SHELXS97 (Sheldrick, 1997); program(s) used to refine structure: SHELXL97 (Sheldrick, 1997); molecular graphics: Diamond (Brandenburg, 1999); software used to prepare material for publication: SHELX97 (Sheldrick, 1997).
Sn6.97Tb3 | F(000) = 1087.0 |
Mr = 1304.2 | Dx = 8.456 Mg m−3 |
Orthorhombic, Pmmm | Mo Kα radiation, λ = 0.71073 Å |
Hall symbol: -P 2 2 | Cell parameters from 508 reflections |
a = 4.3352 (1) Å | θ = 2.3–27.4° |
b = 4.4251 (1) Å | µ = 37.01 mm−1 |
c = 26.7006 (9) Å | T = 293 K |
V = 512.22 (2) Å3 | Irregularly shaped, metallic dark grey |
Z = 2 | 0.08 × 0.07 × 0.01 mm |
Xcalibur Oxford Diffraction diffractometer | 762 independent reflections |
Radiation source: fine-focus sealed tube | 508 reflections with I > 2σ(I) |
Graphite monochromator | Rint = 0.051 |
Detector resolution: 0 pixels mm-1 | θmax = 27.4°, θmin = 2.3° |
ω scans | h = −5→5 |
Absorption correction: analytical CrysAlis RED (Oxford Diffraction, 2005) | k = −5→5 |
Tmin = 0.089, Tmax = 0.598 | l = −34→34 |
4684 measured reflections |
Refinement on F2 | 0 restraints |
Least-squares matrix: full | Primary atom site location: structure-invariant direct methods |
R[F2 > 2σ(F2)] = 0.028 | Secondary atom site location: difference Fourier map |
wR(F2) = 0.088 | w = 1/[σ2(Fo2) + (0.0215P)2] where P = (Fo2 + 2Fc2)/3 |
S = 1.07 | (Δ/σ)max < 0.001 |
762 reflections | Δρmax = 1.93 e Å−3 |
49 parameters | Δρmin = −2.19 e Å−3 |
Sn6.97Tb3 | V = 512.22 (2) Å3 |
Mr = 1304.2 | Z = 2 |
Orthorhombic, Pmmm | Mo Kα radiation |
a = 4.3352 (1) Å | µ = 37.01 mm−1 |
b = 4.4251 (1) Å | T = 293 K |
c = 26.7006 (9) Å | 0.08 × 0.07 × 0.01 mm |
Xcalibur Oxford Diffraction diffractometer | 762 independent reflections |
Absorption correction: analytical CrysAlis RED (Oxford Diffraction, 2005) | 508 reflections with I > 2σ(I) |
Tmin = 0.089, Tmax = 0.598 | Rint = 0.051 |
4684 measured reflections |
R[F2 > 2σ(F2)] = 0.028 | 49 parameters |
wR(F2) = 0.088 | 0 restraints |
S = 1.07 | Δρmax = 1.93 e Å−3 |
762 reflections | Δρmin = −2.19 e Å−3 |
Geometry. All e.s.d.'s (except the e.s.d. in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell e.s.d.'s are taken into account individually in the estimation of e.s.d.'s in distances, angles and torsion angles; correlations between e.s.d.'s in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell e.s.d.'s is used for estimating e.s.d.'s involving l.s. planes. |
Refinement. Refinement of F2 against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F2, conventional R-factors R are based on F, with F set to zero for negative F2. The threshold expression of F2 > σ(F2) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F2 are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger. |
x | y | z | Uiso*/Ueq | Occ. (<1) | |
Tb1 | 0.5000 | 0.5000 | 0.0000 | 0.0228 (6) | |
Tb2 | 0.0000 | 0.5000 | 0.5000 | 0.0209 (5) | |
Tb3 | 0.5000 | 0.5000 | 0.39449 (6) | 0.0219 (4) | |
Tb4 | 0.0000 | 0.0000 | 0.19732 (6) | 0.0248 (4) | |
Sn1 | 0.0000 | 0.0000 | 0.40015 (8) | 0.0369 (9) | |
Sn2 | 0.5000 | 0.5000 | 0.20214 (11) | 0.0403 (8) | |
Sn3 | 0.5000 | 0.0000 | 0.29131 (10) | 0.0391 (8) | |
Sn4 | 0.0000 | 0.5000 | 0.09758 (9) | 0.0391 (9) | |
Sn5 | 0.0000 | 0.5000 | 0.28940 (11) | 0.0462 (8) | |
Sn6 | 0.5000 | 0.0000 | 0.10357 (9) | 0.0337 (7) | |
Sn7 | 0.0000 | 0.0000 | 0.0000 | 0.023 (13)* | 0.12 (4) |
Sn7A | 0.0000 | 0.0000 | 0.0180 (5) | 0.042 (3)* | 0.43 (3) |
Sn8A | 0.5000 | 0.0000 | 0.4841 (9) | 0.041 (4)* | 0.36 (4) |
Sn8 | 0.5000 | 0.0000 | 0.5000 | 0.049 (9)* | 0.24 (8) |
U11 | U22 | U33 | U12 | U13 | U23 | |
Tb1 | 0.0218 (12) | 0.0218 (12) | 0.0249 (10) | 0.000 | 0.000 | 0.000 |
Tb2 | 0.0184 (10) | 0.0184 (10) | 0.0258 (10) | 0.000 | 0.000 | 0.000 |
Tb3 | 0.0207 (8) | 0.0205 (8) | 0.0245 (6) | 0.000 | 0.000 | 0.000 |
Tb4 | 0.0219 (8) | 0.0215 (8) | 0.0310 (7) | 0.000 | 0.000 | 0.000 |
Sn1 | 0.0324 (17) | 0.0315 (17) | 0.0469 (17) | 0.000 | 0.000 | 0.000 |
Sn2 | 0.0405 (17) | 0.0397 (17) | 0.0408 (13) | 0.000 | 0.000 | 0.000 |
Sn3 | 0.0409 (18) | 0.0404 (18) | 0.0359 (13) | 0.000 | 0.000 | 0.000 |
Sn4 | 0.033 (2) | 0.032 (2) | 0.0521 (18) | 0.000 | 0.000 | 0.000 |
Sn5 | 0.0429 (17) | 0.0419 (16) | 0.0537 (15) | 0.000 | 0.000 | 0.000 |
Sn6 | 0.0332 (15) | 0.0325 (14) | 0.0353 (11) | 0.000 | 0.000 | 0.000 |
Tb1—Sn7i | 3.0974 | Sn2—Sn5iii | 3.182 (3) |
Tb1—Sn7 | 3.0974 | Sn2—Sn5 | 3.182 (3) |
Tb1—Sn7ii | 3.0974 | Sn2—Sn3ii | 3.250 (3) |
Tb1—Sn7iii | 3.0974 | Sn2—Sn3 | 3.250 (3) |
Tb1—Sn7Ai | 3.134 (2) | Sn3—Sn5xv | 3.0978 (1) |
Tb1—Sn7Aiv | 3.134 (2) | Sn3—Sn5iii | 3.0978 (1) |
Tb1—Sn7A | 3.134 (2) | Sn3—Sn5xvi | 3.0978 (1) |
Tb1—Sn7Av | 3.134 (2) | Sn3—Sn5 | 3.0978 (1) |
Tb1—Sn7Aii | 3.134 (2) | Sn3—Sn2xv | 3.250 (3) |
Tb1—Sn7Aiii | 3.134 (2) | Sn3—Tb4iii | 3.316 (2) |
Tb1—Sn7Avi | 3.134 (2) | Sn3—Tb3xv | 3.534 (2) |
Tb1—Sn7Avii | 3.134 (2) | Sn4—Sn7A | 3.068 (10) |
Tb2—Sn8ii | 3.0974 | Sn4—Sn7Aii | 3.068 (10) |
Tb2—Sn8viii | 3.0974 | Sn4—Sn6ii | 3.1015 (2) |
Tb2—Sn8ix | 3.0974 | Sn4—Sn6viii | 3.1015 (2) |
Tb2—Sn8 | 3.0974 | Sn4—Sn6 | 3.1015 (2) |
Tb2—Sn8Ax | 3.126 (3) | Sn4—Sn6ix | 3.1015 (2) |
Tb2—Sn8Aviii | 3.126 (3) | Sn4—Tb1viii | 3.3892 (18) |
Tb2—Sn8Axi | 3.126 (3) | Sn4—Tb4ii | 3.462 (3) |
Tb2—Sn8Aii | 3.126 (3) | Sn5—Sn3ii | 3.0978 (1) |
Tb2—Sn8Axii | 3.126 (3) | Sn5—Sn3viii | 3.0978 (10) |
Tb2—Sn8Axiii | 3.126 (3) | Sn5—Sn3ix | 3.0978 (10) |
Tb2—Sn8A | 3.126 (3) | Sn5—Sn2viii | 3.182 (3) |
Tb2—Sn8Aix | 3.126 (3) | Sn5—Tb4ii | 3.308 (3) |
Tb3—Sn1i | 3.1011 (2) | Sn5—Tb3viii | 3.546 (3) |
Tb3—Sn1 | 3.1011 (2) | Sn6—Sn4xv | 3.1015 (2) |
Tb3—Sn1ii | 3.1011 (2) | Sn6—Sn4iii | 3.1015 (2) |
Tb3—Sn1iii | 3.1011 (2) | Sn6—Sn4xvi | 3.1015 (2) |
Tb3—Sn8Aii | 3.259 (17) | Sn6—Sn7A | 3.150 (10) |
Tb3—Sn8A | 3.259 (17) | Sn6—Sn7Aiii | 3.150 (10) |
Tb3—Sn3 | 3.534 (2) | Sn6—Tb4iii | 3.3111 (19) |
Tb3—Sn3ii | 3.534 (2) | Sn6—Tb1xv | 3.5416 (18) |
Tb3—Sn5 | 3.546 (3) | Sn7—Sn7Aiv | 0.480 (14) |
Tb3—Sn5iii | 3.546 (3) | Sn7—Tb1xiv | 3.0974 |
Tb3—Tb2iii | 3.5545 (12) | Sn7—Tb1xv | 3.0974 |
Tb4—Sn2 | 3.1001 (2) | Sn7—Tb1viii | 3.0974 |
Tb4—Sn2xiv | 3.1001 (2) | Sn7A—Sn7Aiv | 0.96 (3) |
Tb4—Sn2viii | 3.1001 (2) | Sn7A—Sn4xv | 3.068 (10) |
Tb4—Sn2xv | 3.1001 (2) | Sn7A—Tb1xiv | 3.134 (2) |
Tb4—Sn5 | 3.308 (3) | Sn7A—Tb1xv | 3.134 (2) |
Tb4—Sn5xv | 3.308 (3) | Sn7A—Tb1viii | 3.134 (2) |
Tb4—Sn6viii | 3.3111 (19) | Sn7A—Sn6viii | 3.150 (10) |
Tb4—Sn6 | 3.3111 (19) | Sn8A—Sn8Axiii | 0.85 (5) |
Tb4—Sn3 | 3.316 (2) | Sn8A—Sn1iii | 3.118 (17) |
Tb4—Sn3viii | 3.316 (2) | Sn8A—Tb2iii | 3.126 (3) |
Tb4—Sn4xv | 3.462 (3) | Sn8A—Tb2xv | 3.126 (3) |
Tb4—Sn4 | 3.462 (3) | Sn8A—Tb2xvi | 3.126 (3) |
Sn1—Tb3xiv | 3.1011 (2) | Sn8A—Tb3xv | 3.259 (17) |
Sn1—Tb3viii | 3.1011 (2) | Sn8—Sn8Axiii | 0.42 (2) |
Sn1—Tb3xv | 3.1011 (2) | Sn8—Tb2iii | 3.0974 |
Sn1—Sn8A | 3.118 (17) | Sn8—Tb2xv | 3.0974 |
Sn1—Sn8Aviii | 3.118 (17) | Sn8—Tb2xvi | 3.0974 |
Sn1—Tb2xv | 3.4645 (17) | Sn8—Tb3xv | 3.5821 (12) |
Sn2—Tb4i | 3.1001 (2) | Sn8—Tb3x | 3.5821 (12) |
Sn2—Tb4ii | 3.1001 (2) | Sn8—Tb3xiii | 3.5821 (12) |
Sn2—Tb4iii | 3.1001 (2) | ||
Sn7i—Tb1—Sn7 | 180.0 | Tb4ii—Sn2—Sn3ii | 62.91 (4) |
Sn7i—Tb1—Sn7ii | 88.824 (2) | Tb4iii—Sn2—Sn3ii | 121.08 (8) |
Sn7—Tb1—Sn7ii | 91.176 (2) | Sn5iii—Sn2—Sn3ii | 57.57 (5) |
Sn7i—Tb1—Sn7iii | 91.176 (2) | Sn5—Sn2—Sn3ii | 57.57 (5) |
Sn7—Tb1—Sn7iii | 88.824 (2) | Tb4—Sn2—Sn3 | 62.91 (4) |
Sn7ii—Tb1—Sn7iii | 180.0 | Tb4i—Sn2—Sn3 | 121.08 (8) |
Sn7i—Tb1—Sn7Ai | 8.8 (3) | Tb4ii—Sn2—Sn3 | 121.08 (8) |
Sn7—Tb1—Sn7Ai | 171.2 (3) | Tb4iii—Sn2—Sn3 | 62.91 (4) |
Sn7ii—Tb1—Sn7Ai | 88.838 (2) | Sn5iii—Sn2—Sn3 | 57.57 (5) |
Sn7iii—Tb1—Sn7Ai | 91.162 (2) | Sn5—Sn2—Sn3 | 57.57 (5) |
Sn7i—Tb1—Sn7Aiv | 171.2 (3) | Sn3ii—Sn2—Sn3 | 85.80 (11) |
Sn7—Tb1—Sn7Aiv | 8.8 (3) | Sn5xv—Sn3—Sn5iii | 178.12 (18) |
Sn7ii—Tb1—Sn7Aiv | 91.162 (2) | Sn5xv—Sn3—Sn5xvi | 88.809 (4) |
Sn7iii—Tb1—Sn7Aiv | 88.838 (2) | Sn5iii—Sn3—Sn5xvi | 91.160 (4) |
Sn7Ai—Tb1—Sn7Aiv | 180.0 | Sn5xv—Sn3—Sn5 | 91.160 (4) |
Sn7i—Tb1—Sn7A | 171.2 (3) | Sn5iii—Sn3—Sn5 | 88.809 (4) |
Sn7—Tb1—Sn7A | 8.8 (3) | Sn5xvi—Sn3—Sn5 | 178.12 (18) |
Sn7ii—Tb1—Sn7A | 91.162 (2) | Sn5xv—Sn3—Sn2xv | 60.12 (6) |
Sn7iii—Tb1—Sn7A | 88.838 (2) | Sn5iii—Sn3—Sn2xv | 118.30 (10) |
Sn7Ai—Tb1—Sn7A | 162.4 (5) | Sn5xvi—Sn3—Sn2xv | 60.12 (6) |
Sn7Aiv—Tb1—Sn7A | 17.6 (5) | Sn5—Sn3—Sn2xv | 118.30 (10) |
Sn7i—Tb1—Sn7Av | 8.8 (3) | Sn5xv—Sn3—Sn2 | 118.30 (10) |
Sn7—Tb1—Sn7Av | 171.2 (3) | Sn5iii—Sn3—Sn2 | 60.12 (6) |
Sn7ii—Tb1—Sn7Av | 88.838 (2) | Sn5xvi—Sn3—Sn2 | 118.30 (10) |
Sn7iii—Tb1—Sn7Av | 91.162 (2) | Sn5—Sn3—Sn2 | 60.12 (6) |
Sn7Ai—Tb1—Sn7Av | 17.6 (5) | Sn2xv—Sn3—Sn2 | 85.80 (11) |
Sn7Aiv—Tb1—Sn7Av | 162.4 (5) | Sn5xv—Sn3—Tb4 | 61.98 (6) |
Sn7A—Tb1—Sn7Av | 180.0 (5) | Sn5iii—Sn3—Tb4 | 116.42 (9) |
Sn7i—Tb1—Sn7Aii | 88.838 (2) | Sn5xvi—Sn3—Tb4 | 116.42 (9) |
Sn7—Tb1—Sn7Aii | 91.162 (2) | Sn5—Sn3—Tb4 | 61.98 (6) |
Sn7ii—Tb1—Sn7Aii | 8.8 (3) | Sn2xv—Sn3—Tb4 | 56.33 (5) |
Sn7iii—Tb1—Sn7Aii | 171.2 (3) | Sn2—Sn3—Tb4 | 56.33 (5) |
Sn7Ai—Tb1—Sn7Aii | 87.51 (7) | Sn5xv—Sn3—Tb4iii | 116.42 (9) |
Sn7Aiv—Tb1—Sn7Aii | 92.49 (7) | Sn5iii—Sn3—Tb4iii | 61.98 (6) |
Sn7A—Tb1—Sn7Aii | 89.81 (8) | Sn5xvi—Sn3—Tb4iii | 61.98 (6) |
Sn7Av—Tb1—Sn7Aii | 90.19 (8) | Sn5—Sn3—Tb4iii | 116.42 (9) |
Sn7i—Tb1—Sn7Aiii | 91.162 (2) | Sn2xv—Sn3—Tb4iii | 56.33 (5) |
Sn7—Tb1—Sn7Aiii | 88.838 (2) | Sn2—Sn3—Tb4iii | 56.33 (5) |
Sn7ii—Tb1—Sn7Aiii | 171.2 (3) | Tb4—Sn3—Tb4iii | 81.64 (6) |
Sn7iii—Tb1—Sn7Aiii | 8.8 (3) | Sn5xv—Sn3—Tb3 | 117.39 (9) |
Sn7Ai—Tb1—Sn7Aiii | 89.81 (8) | Sn5iii—Sn3—Tb3 | 64.25 (6) |
Sn7Aiv—Tb1—Sn7Aiii | 90.19 (8) | Sn5xvi—Sn3—Tb3 | 117.39 (9) |
Sn7A—Tb1—Sn7Aiii | 87.51 (7) | Sn5—Sn3—Tb3 | 64.25 (6) |
Sn7Av—Tb1—Sn7Aiii | 92.49 (7) | Sn2xv—Sn3—Tb3 | 175.87 (8) |
Sn7Aii—Tb1—Sn7Aiii | 162.4 (5) | Sn2—Sn3—Tb3 | 98.33 (3) |
Sn7i—Tb1—Sn7Avi | 88.838 (2) | Tb4—Sn3—Tb3 | 126.162 (17) |
Sn7—Tb1—Sn7Avi | 91.162 (2) | Tb4iii—Sn3—Tb3 | 126.162 (17) |
Sn7ii—Tb1—Sn7Avi | 8.8 (3) | Sn5xv—Sn3—Tb3xv | 64.25 (6) |
Sn7iii—Tb1—Sn7Avi | 171.2 (3) | Sn5iii—Sn3—Tb3xv | 117.39 (9) |
Sn7Ai—Tb1—Sn7Avi | 90.19 (8) | Sn5xvi—Sn3—Tb3xv | 64.25 (6) |
Sn7Aiv—Tb1—Sn7Avi | 89.81 (8) | Sn5—Sn3—Tb3xv | 117.39 (9) |
Sn7A—Tb1—Sn7Avi | 92.49 (7) | Sn2xv—Sn3—Tb3xv | 98.33 (3) |
Sn7Av—Tb1—Sn7Avi | 87.51 (7) | Sn2—Sn3—Tb3xv | 175.87 (8) |
Sn7Aii—Tb1—Sn7Avi | 17.6 (5) | Tb4—Sn3—Tb3xv | 126.162 (17) |
Sn7Aiii—Tb1—Sn7Avi | 180.0 | Tb4iii—Sn3—Tb3xv | 126.162 (17) |
Sn7i—Tb1—Sn7Avii | 91.162 (2) | Tb3—Sn3—Tb3xv | 77.53 (6) |
Sn7—Tb1—Sn7Avii | 88.838 (2) | Sn7A—Sn4—Sn7Aii | 92.3 (4) |
Sn7ii—Tb1—Sn7Avii | 171.2 (3) | Sn7A—Sn4—Sn6ii | 123.38 (11) |
Sn7iii—Tb1—Sn7Avii | 8.8 (3) | Sn7Aii—Sn4—Sn6ii | 61.40 (12) |
Sn7Ai—Tb1—Sn7Avii | 92.49 (8) | Sn7A—Sn4—Sn6viii | 61.40 (12) |
Sn7Aiv—Tb1—Sn7Avii | 87.51 (7) | Sn7Aii—Sn4—Sn6viii | 123.38 (11) |
Sn7A—Tb1—Sn7Avii | 90.19 (8) | Sn6ii—Sn4—Sn6viii | 174.08 (12) |
Sn7Av—Tb1—Sn7Avii | 89.81 (8) | Sn7A—Sn4—Sn6 | 61.40 (12) |
Sn7Aii—Tb1—Sn7Avii | 180.0 | Sn7Aii—Sn4—Sn6 | 123.38 (11) |
Sn7Aiii—Tb1—Sn7Avii | 17.6 (5) | Sn6ii—Sn4—Sn6 | 91.020 (7) |
Sn7Avi—Tb1—Sn7Avii | 162.4 (5) | Sn6viii—Sn4—Sn6 | 88.675 (6) |
Sn8ii—Tb2—Sn8viii | 180.0 | Sn7A—Sn4—Sn6ix | 123.38 (11) |
Sn8ii—Tb2—Sn8ix | 88.824 (2) | Sn7Aii—Sn4—Sn6ix | 61.40 (12) |
Sn8viii—Tb2—Sn8ix | 91.176 (2) | Sn6ii—Sn4—Sn6ix | 88.675 (6) |
Sn8ii—Tb2—Sn8 | 91.176 (2) | Sn6viii—Sn4—Sn6ix | 91.020 (7) |
Sn8viii—Tb2—Sn8 | 88.824 (2) | Sn6—Sn4—Sn6ix | 174.08 (12) |
Sn8ix—Tb2—Sn8 | 180.0 | Sn7A—Sn4—Tb1viii | 57.82 (13) |
Sn8ii—Tb2—Sn8Ax | 7.8 (4) | Sn7Aii—Sn4—Tb1viii | 57.82 (13) |
Sn8viii—Tb2—Sn8Ax | 172.2 (4) | Sn6ii—Sn4—Tb1viii | 119.12 (6) |
Sn8ix—Tb2—Sn8Ax | 88.835 (3) | Sn6viii—Sn4—Tb1viii | 65.96 (4) |
Sn8—Tb2—Sn8Ax | 91.165 (3) | Sn6—Sn4—Tb1viii | 119.12 (6) |
Sn8ii—Tb2—Sn8Aviii | 172.2 (4) | Sn6ix—Sn4—Tb1viii | 65.96 (4) |
Sn8viii—Tb2—Sn8Aviii | 7.8 (4) | Sn7A—Sn4—Tb1 | 57.82 (13) |
Sn8ix—Tb2—Sn8Aviii | 91.165 (3) | Sn7Aii—Sn4—Tb1 | 57.82 (13) |
Sn8—Tb2—Sn8Aviii | 88.835 (3) | Sn6ii—Sn4—Tb1 | 65.96 (4) |
Sn8Ax—Tb2—Sn8Aviii | 180.0 | Sn6viii—Sn4—Tb1 | 119.12 (6) |
Sn8ii—Tb2—Sn8Axi | 172.2 (4) | Sn6—Sn4—Tb1 | 65.96 (4) |
Sn8viii—Tb2—Sn8Axi | 7.8 (4) | Sn6ix—Sn4—Tb1 | 119.12 (6) |
Sn8ix—Tb2—Sn8Axi | 91.165 (3) | Tb1viii—Sn4—Tb1 | 79.52 (5) |
Sn8—Tb2—Sn8Axi | 88.835 (3) | Sn7A—Sn4—Tb4ii | 173.6 (2) |
Sn8Ax—Tb2—Sn8Axi | 164.4 (9) | Sn7Aii—Sn4—Tb4ii | 94.13 (19) |
Sn8Aviii—Tb2—Sn8Axi | 15.6 (9) | Sn6ii—Sn4—Tb4ii | 60.29 (4) |
Sn8ii—Tb2—Sn8Aii | 7.8 (4) | Sn6viii—Sn4—Tb4ii | 114.59 (7) |
Sn8viii—Tb2—Sn8Aii | 172.2 (4) | Sn6—Sn4—Tb4ii | 114.59 (7) |
Sn8ix—Tb2—Sn8Aii | 88.835 (3) | Sn6ix—Sn4—Tb4ii | 60.29 (4) |
Sn8—Tb2—Sn8Aii | 91.165 (3) | Tb1viii—Sn4—Tb4ii | 126.248 (10) |
Sn8Ax—Tb2—Sn8Aii | 15.6 (9) | Tb1—Sn4—Tb4ii | 126.248 (10) |
Sn8Aviii—Tb2—Sn8Aii | 164.4 (9) | Sn7A—Sn4—Tb4 | 94.13 (19) |
Sn8Axi—Tb2—Sn8Aii | 180.0 (9) | Sn7Aii—Sn4—Tb4 | 173.6 (2) |
Sn8ii—Tb2—Sn8Axii | 88.835 (3) | Sn6ii—Sn4—Tb4 | 114.59 (7) |
Sn8viii—Tb2—Sn8Axii | 91.165 (3) | Sn6viii—Sn4—Tb4 | 60.29 (4) |
Sn8ix—Tb2—Sn8Axii | 7.8 (4) | Sn6—Sn4—Tb4 | 60.29 (4) |
Sn8—Tb2—Sn8Axii | 172.2 (4) | Sn6ix—Sn4—Tb4 | 114.59 (7) |
Sn8Ax—Tb2—Sn8Axii | 87.79 (11) | Tb1viii—Sn4—Tb4 | 126.248 (10) |
Sn8Aviii—Tb2—Sn8Axii | 92.21 (11) | Tb1—Sn4—Tb4 | 126.248 (10) |
Sn8Axi—Tb2—Sn8Axii | 90.10 (12) | Tb4ii—Sn4—Tb4 | 79.44 (7) |
Sn8Aii—Tb2—Sn8Axii | 89.90 (12) | Sn3ii—Sn5—Sn3viii | 178.12 (18) |
Sn8ii—Tb2—Sn8Axiii | 91.165 (3) | Sn3ii—Sn5—Sn3ix | 88.809 (4) |
Sn8viii—Tb2—Sn8Axiii | 88.835 (3) | Sn3viii—Sn5—Sn3ix | 91.160 (4) |
Sn8ix—Tb2—Sn8Axiii | 172.2 (4) | Sn3ii—Sn5—Sn3 | 91.160 (4) |
Sn8—Tb2—Sn8Axiii | 7.8 (4) | Sn3viii—Sn5—Sn3 | 88.809 (4) |
Sn8Ax—Tb2—Sn8Axiii | 90.10 (12) | Sn3ix—Sn5—Sn3 | 178.12 (18) |
Sn8Aviii—Tb2—Sn8Axiii | 89.90 (12) | Sn3ii—Sn5—Sn2viii | 119.25 (9) |
Sn8Axi—Tb2—Sn8Axiii | 87.79 (11) | Sn3viii—Sn5—Sn2viii | 62.32 (7) |
Sn8Aii—Tb2—Sn8Axiii | 92.21 (11) | Sn3ix—Sn5—Sn2viii | 62.32 (7) |
Sn8Axii—Tb2—Sn8Axiii | 164.4 (9) | Sn3—Sn5—Sn2viii | 119.25 (9) |
Sn8ii—Tb2—Sn8A | 91.165 (3) | Sn3ii—Sn5—Sn2 | 62.32 (7) |
Sn8viii—Tb2—Sn8A | 88.835 (3) | Sn3viii—Sn5—Sn2 | 119.25 (9) |
Sn8ix—Tb2—Sn8A | 172.2 (4) | Sn3ix—Sn5—Sn2 | 119.25 (9) |
Sn8—Tb2—Sn8A | 7.8 (4) | Sn3—Sn5—Sn2 | 62.32 (7) |
Sn8Ax—Tb2—Sn8A | 92.21 (11) | Sn2viii—Sn5—Sn2 | 85.86 (9) |
Sn8Aviii—Tb2—Sn8A | 87.79 (11) | Sn3ii—Sn5—Tb4 | 119.34 (10) |
Sn8Axi—Tb2—Sn8A | 89.90 (12) | Sn3viii—Sn5—Tb4 | 62.25 (6) |
Sn8Aii—Tb2—Sn8A | 90.10 (12) | Sn3ix—Sn5—Tb4 | 119.34 (10) |
Sn8Axii—Tb2—Sn8A | 180.0 | Sn3—Sn5—Tb4 | 62.25 (6) |
Sn8Axiii—Tb2—Sn8A | 15.6 (9) | Sn2viii—Sn5—Tb4 | 57.03 (4) |
Sn8ii—Tb2—Sn8Aix | 88.835 (3) | Sn2—Sn5—Tb4 | 57.03 (4) |
Sn8viii—Tb2—Sn8Aix | 91.165 (3) | Sn3ii—Sn5—Tb4ii | 62.25 (6) |
Sn8ix—Tb2—Sn8Aix | 7.8 (4) | Sn3viii—Sn5—Tb4ii | 119.34 (10) |
Sn8—Tb2—Sn8Aix | 172.2 (4) | Sn3ix—Sn5—Tb4ii | 62.25 (6) |
Sn8Ax—Tb2—Sn8Aix | 89.90 (12) | Sn3—Sn5—Tb4ii | 119.34 (10) |
Sn8Aviii—Tb2—Sn8Aix | 90.10 (12) | Sn2viii—Sn5—Tb4ii | 57.03 (4) |
Sn8Axi—Tb2—Sn8Aix | 92.21 (11) | Sn2—Sn5—Tb4ii | 57.03 (4) |
Sn8Aii—Tb2—Sn8Aix | 87.79 (11) | Tb4—Sn5—Tb4ii | 83.97 (8) |
Sn8Axii—Tb2—Sn8Aix | 15.6 (9) | Sn3ii—Sn5—Tb3 | 63.85 (6) |
Sn8Axiii—Tb2—Sn8Aix | 180.0 | Sn3viii—Sn5—Tb3 | 114.50 (9) |
Sn8A—Tb2—Sn8Aix | 164.4 (9) | Sn3ix—Sn5—Tb3 | 114.50 (9) |
Sn1i—Tb3—Sn1 | 174.41 (11) | Sn3—Sn5—Tb3 | 63.85 (6) |
Sn1i—Tb3—Sn1ii | 88.691 (6) | Sn2viii—Sn5—Tb3 | 174.75 (7) |
Sn1—Tb3—Sn1ii | 91.037 (6) | Sn2—Sn5—Tb3 | 99.38 (3) |
Sn1i—Tb3—Sn1iii | 91.037 (6) | Tb4—Sn5—Tb3 | 126.034 (19) |
Sn1—Tb3—Sn1iii | 88.691 (6) | Tb4ii—Sn5—Tb3 | 126.034 (19) |
Sn1ii—Tb3—Sn1iii | 174.41 (11) | Sn3ii—Sn5—Tb3viii | 114.50 (9) |
Sn1i—Tb3—Sn8Aii | 58.65 (17) | Sn3viii—Sn5—Tb3viii | 63.85 (6) |
Sn1—Tb3—Sn8Aii | 116.66 (18) | Sn3ix—Sn5—Tb3viii | 63.85 (6) |
Sn1ii—Tb3—Sn8Aii | 58.65 (17) | Sn3—Sn5—Tb3viii | 114.50 (9) |
Sn1iii—Tb3—Sn8Aii | 116.66 (18) | Sn2viii—Sn5—Tb3viii | 99.38 (3) |
Sn1i—Tb3—Sn8A | 116.66 (18) | Sn2—Sn5—Tb3viii | 174.75 (7) |
Sn1—Tb3—Sn8A | 58.65 (17) | Tb4—Sn5—Tb3viii | 126.034 (19) |
Sn1ii—Tb3—Sn8A | 116.66 (18) | Tb4ii—Sn5—Tb3viii | 126.034 (19) |
Sn1iii—Tb3—Sn8A | 58.65 (17) | Tb3—Sn5—Tb3viii | 75.37 (6) |
Sn8Aii—Tb3—Sn8A | 85.5 (6) | Sn4xv—Sn6—Sn4iii | 174.08 (12) |
Sn1i—Tb3—Sn3 | 119.00 (6) | Sn4xv—Sn6—Sn4xvi | 88.675 (6) |
Sn1—Tb3—Sn3 | 65.87 (4) | Sn4iii—Sn6—Sn4xvi | 91.020 (7) |
Sn1ii—Tb3—Sn3 | 119.00 (6) | Sn4xv—Sn6—Sn4 | 91.020 (7) |
Sn1iii—Tb3—Sn3 | 65.87 (4) | Sn4iii—Sn6—Sn4 | 88.675 (6) |
Sn8Aii—Tb3—Sn3 | 176.0 (3) | Sn4xvi—Sn6—Sn4 | 174.08 (12) |
Sn8A—Tb3—Sn3 | 98.5 (3) | Sn4xv—Sn6—Sn7A | 58.78 (10) |
Sn1i—Tb3—Sn3ii | 65.87 (4) | Sn4iii—Sn6—Sn7A | 116.32 (13) |
Sn1—Tb3—Sn3ii | 119.00 (6) | Sn4xvi—Sn6—Sn7A | 116.32 (13) |
Sn1ii—Tb3—Sn3ii | 65.87 (4) | Sn4—Sn6—Sn7A | 58.78 (10) |
Sn1iii—Tb3—Sn3ii | 119.00 (6) | Sn4xv—Sn6—Sn7Aiii | 116.32 (13) |
Sn8Aii—Tb3—Sn3ii | 98.5 (3) | Sn4iii—Sn6—Sn7Aiii | 58.78 (10) |
Sn8A—Tb3—Sn3ii | 176.0 (3) | Sn4xvi—Sn6—Sn7Aiii | 58.78 (10) |
Sn3—Tb3—Sn3ii | 77.53 (6) | Sn4—Sn6—Sn7Aiii | 116.32 (13) |
Sn1i—Tb3—Sn5 | 117.77 (5) | Sn7A—Sn6—Sn7Aiii | 87.0 (4) |
Sn1—Tb3—Sn5 | 67.12 (5) | Sn4xv—Sn6—Tb4iii | 119.77 (6) |
Sn1ii—Tb3—Sn5 | 67.12 (5) | Sn4iii—Sn6—Tb4iii | 65.26 (5) |
Sn1iii—Tb3—Sn5 | 117.77 (5) | Sn4xvi—Sn6—Tb4iii | 65.26 (5) |
Sn8Aii—Tb3—Sn5 | 125.52 (18) | Sn4—Sn6—Tb4iii | 119.77 (6) |
Sn8A—Tb3—Sn5 | 125.52 (19) | Sn7A—Sn6—Tb4iii | 177.41 (19) |
Sn3—Tb3—Sn5 | 51.90 (3) | Sn7Aiii—Sn6—Tb4iii | 95.63 (18) |
Sn3ii—Tb3—Sn5 | 51.90 (3) | Sn4xv—Sn6—Tb4 | 65.26 (5) |
Sn1i—Tb3—Sn5iii | 67.12 (5) | Sn4iii—Sn6—Tb4 | 119.77 (6) |
Sn1—Tb3—Sn5iii | 117.77 (5) | Sn4xvi—Sn6—Tb4 | 119.77 (6) |
Sn1ii—Tb3—Sn5iii | 117.77 (5) | Sn4—Sn6—Tb4 | 65.26 (5) |
Sn1iii—Tb3—Sn5iii | 67.12 (5) | Sn7A—Sn6—Tb4 | 95.63 (18) |
Sn8Aii—Tb3—Sn5iii | 125.52 (19) | Sn7Aiii—Sn6—Tb4 | 177.41 (19) |
Sn8A—Tb3—Sn5iii | 125.52 (19) | Tb4iii—Sn6—Tb4 | 81.79 (6) |
Sn3—Tb3—Sn5iii | 51.90 (3) | Sn4xv—Sn6—Tb1xv | 60.93 (4) |
Sn3ii—Tb3—Sn5iii | 51.90 (3) | Sn4iii—Sn6—Tb1xv | 113.91 (6) |
Sn5—Tb3—Sn5iii | 75.37 (6) | Sn4xvi—Sn6—Tb1xv | 60.93 (4) |
Sn1i—Tb3—Tb2iii | 62.30 (4) | Sn4—Sn6—Tb1xv | 113.91 (6) |
Sn1—Tb3—Tb2iii | 112.81 (6) | Sn7A—Sn6—Tb1xv | 55.49 (12) |
Sn1ii—Tb3—Tb2iii | 112.81 (6) | Sn7Aiii—Sn6—Tb1xv | 55.49 (12) |
Sn1iii—Tb3—Tb2iii | 62.30 (4) | Tb4iii—Sn6—Tb1xv | 126.176 (11) |
Sn8Aii—Tb3—Tb2iii | 54.42 (18) | Tb4—Sn6—Tb1xv | 126.176 (11) |
Sn8A—Tb3—Tb2iii | 54.42 (18) | Sn4xv—Sn6—Tb1 | 113.91 (6) |
Sn3—Tb3—Tb2iii | 128.166 (17) | Sn4iii—Sn6—Tb1 | 60.93 (4) |
Sn3ii—Tb3—Tb2iii | 128.166 (17) | Sn4xvi—Sn6—Tb1 | 113.91 (6) |
Sn5—Tb3—Tb2iii | 179.89 (4) | Sn4—Sn6—Tb1 | 60.93 (4) |
Sn5iii—Tb3—Tb2iii | 104.74 (3) | Sn7A—Sn6—Tb1 | 55.49 (12) |
Sn1i—Tb3—Tb2 | 112.81 (6) | Sn7Aiii—Sn6—Tb1 | 55.49 (12) |
Sn1—Tb3—Tb2 | 62.30 (4) | Tb4iii—Sn6—Tb1 | 126.176 (11) |
Sn1ii—Tb3—Tb2 | 62.30 (4) | Tb4—Sn6—Tb1 | 126.176 (11) |
Sn1iii—Tb3—Tb2 | 112.81 (6) | Tb1xv—Sn6—Tb1 | 77.32 (5) |
Sn8Aii—Tb3—Tb2 | 54.42 (18) | Sn7Aiv—Sn7—Tb1 | 90.0 |
Sn8A—Tb3—Tb2 | 54.42 (18) | Sn7Aiv—Sn7—Tb1xiv | 90.0 |
Sn3—Tb3—Tb2 | 128.166 (17) | Tb1—Sn7—Tb1xiv | 180.0 |
Sn3ii—Tb3—Tb2 | 128.166 (17) | Sn7Aiv—Sn7—Tb1xv | 90.0 |
Sn5—Tb3—Tb2 | 104.74 (3) | Tb1—Sn7—Tb1xv | 91.176 (2) |
Sn5iii—Tb3—Tb2 | 179.89 (4) | Tb1xiv—Sn7—Tb1xv | 88.824 (2) |
Tb2iii—Tb3—Tb2 | 75.15 (3) | Sn7Aiv—Sn7—Tb1viii | 90.0 |
Sn2—Tb4—Sn2xiv | 175.24 (13) | Tb1—Sn7—Tb1viii | 88.824 (2) |
Sn2—Tb4—Sn2viii | 88.727 (6) | Tb1xiv—Sn7—Tb1viii | 91.176 (2) |
Sn2xiv—Tb4—Sn2viii | 91.075 (6) | Tb1xv—Sn7—Tb1viii | 180.0 |
Sn2—Tb4—Sn2xv | 91.075 (6) | Sn7Aiv—Sn7A—Sn4 | 133.86 (19) |
Sn2xiv—Tb4—Sn2xv | 88.727 (6) | Sn7Aiv—Sn7A—Sn4xv | 133.86 (19) |
Sn2viii—Tb4—Sn2xv | 175.24 (13) | Sn4—Sn7A—Sn4xv | 92.3 (4) |
Sn2—Tb4—Sn5 | 59.45 (5) | Sn7Aiv—Sn7A—Tb1xiv | 81.2 (3) |
Sn2xiv—Tb4—Sn5 | 116.52 (7) | Sn4—Sn7A—Tb1xiv | 128.0 (3) |
Sn2viii—Tb4—Sn5 | 59.45 (5) | Sn4xv—Sn7A—Tb1xiv | 66.23 (9) |
Sn2xv—Tb4—Sn5 | 116.52 (7) | Sn7Aiv—Sn7A—Tb1 | 81.2 (3) |
Sn2—Tb4—Sn5xv | 116.52 (7) | Sn4—Sn7A—Tb1 | 66.23 (9) |
Sn2xiv—Tb4—Sn5xv | 59.45 (5) | Sn4xv—Sn7A—Tb1 | 128.0 (3) |
Sn2viii—Tb4—Sn5xv | 116.52 (7) | Tb1xiv—Sn7A—Tb1 | 162.4 (5) |
Sn2xv—Tb4—Sn5xv | 59.45 (5) | Sn7Aiv—Sn7A—Tb1xv | 81.2 (3) |
Sn5—Tb4—Sn5xv | 83.97 (8) | Sn4—Sn7A—Tb1xv | 128.0 (3) |
Sn2—Tb4—Sn6viii | 119.28 (6) | Sn4xv—Sn7A—Tb1xv | 66.23 (9) |
Sn2xiv—Tb4—Sn6viii | 64.76 (6) | Tb1xiv—Sn7A—Tb1xv | 87.51 (8) |
Sn2viii—Tb4—Sn6viii | 64.76 (6) | Tb1—Sn7A—Tb1xv | 89.81 (8) |
Sn2xv—Tb4—Sn6viii | 119.28 (6) | Sn7Aiv—Sn7A—Tb1viii | 81.2 (3) |
Sn5—Tb4—Sn6viii | 124.19 (3) | Sn4—Sn7A—Tb1viii | 66.23 (9) |
Sn5xv—Tb4—Sn6viii | 124.19 (3) | Sn4xv—Sn7A—Tb1viii | 128.0 (3) |
Sn2—Tb4—Sn6 | 64.76 (6) | Tb1xiv—Sn7A—Tb1viii | 89.81 (8) |
Sn2xiv—Tb4—Sn6 | 119.28 (6) | Tb1—Sn7A—Tb1viii | 87.51 (8) |
Sn2viii—Tb4—Sn6 | 119.28 (6) | Tb1xv—Sn7A—Tb1viii | 162.4 (5) |
Sn2xv—Tb4—Sn6 | 64.76 (6) | Sn7Aiv—Sn7A—Sn6 | 136.52 (18) |
Sn5—Tb4—Sn6 | 124.19 (3) | Sn4—Sn7A—Sn6 | 59.8 (2) |
Sn5xv—Tb4—Sn6 | 124.19 (3) | Sn4xv—Sn7A—Sn6 | 59.8 (2) |
Sn6viii—Tb4—Sn6 | 81.79 (6) | Tb1xiv—Sn7A—Sn6 | 125.9 (3) |
Sn2—Tb4—Sn3 | 60.76 (6) | Tb1—Sn7A—Sn6 | 68.60 (10) |
Sn2xiv—Tb4—Sn3 | 115.19 (6) | Tb1xv—Sn7A—Sn6 | 68.60 (10) |
Sn2viii—Tb4—Sn3 | 115.19 (6) | Tb1viii—Sn7A—Sn6 | 125.9 (3) |
Sn2xv—Tb4—Sn3 | 60.76 (6) | Sn7Aiv—Sn7A—Sn6viii | 136.52 (18) |
Sn5—Tb4—Sn3 | 55.77 (3) | Sn4—Sn7A—Sn6viii | 59.8 (2) |
Sn5xv—Tb4—Sn3 | 55.77 (3) | Sn4xv—Sn7A—Sn6viii | 59.8 (2) |
Sn6viii—Tb4—Sn3 | 179.93 (5) | Tb1xiv—Sn7A—Sn6viii | 68.60 (10) |
Sn6—Tb4—Sn3 | 98.29 (3) | Tb1—Sn7A—Sn6viii | 125.9 (3) |
Sn2—Tb4—Sn3viii | 115.19 (6) | Tb1xv—Sn7A—Sn6viii | 125.9 (3) |
Sn2xiv—Tb4—Sn3viii | 60.76 (6) | Tb1viii—Sn7A—Sn6viii | 68.60 (10) |
Sn2viii—Tb4—Sn3viii | 60.76 (6) | Sn6—Sn7A—Sn6viii | 87.0 (4) |
Sn2xv—Tb4—Sn3viii | 115.19 (6) | Sn8Axiii—Sn8A—Sn1 | 136.0 (3) |
Sn5—Tb4—Sn3viii | 55.77 (3) | Sn8Axiii—Sn8A—Sn1iii | 136.0 (3) |
Sn5xv—Tb4—Sn3viii | 55.77 (3) | Sn1—Sn8A—Sn1iii | 88.1 (6) |
Sn6viii—Tb4—Sn3viii | 98.29 (3) | Sn8Axiii—Sn8A—Tb2iii | 82.2 (4) |
Sn6—Tb4—Sn3viii | 179.93 (5) | Sn1—Sn8A—Tb2iii | 125.4 (5) |
Sn3—Tb4—Sn3viii | 81.64 (6) | Sn1iii—Sn8A—Tb2iii | 67.40 (17) |
Sn2—Tb4—Sn4xv | 119.21 (7) | Sn8Axiii—Sn8A—Tb2xv | 82.2 (4) |
Sn2xiv—Tb4—Sn4xv | 64.90 (5) | Sn1—Sn8A—Tb2xv | 67.40 (17) |
Sn2viii—Tb4—Sn4xv | 119.21 (7) | Sn1iii—Sn8A—Tb2xv | 125.4 (5) |
Sn2xv—Tb4—Sn4xv | 64.90 (5) | Tb2iii—Sn8A—Tb2xv | 164.4 (9) |
Sn5—Tb4—Sn4xv | 177.74 (7) | Sn8Axiii—Sn8A—Tb2 | 82.2 (4) |
Sn5xv—Tb4—Sn4xv | 98.30 (3) | Sn1—Sn8A—Tb2 | 67.40 (17) |
Sn6viii—Tb4—Sn4xv | 54.45 (3) | Sn1iii—Sn8A—Tb2 | 125.4 (5) |
Sn6—Tb4—Sn4xv | 54.45 (3) | Tb2iii—Sn8A—Tb2 | 87.79 (11) |
Sn3—Tb4—Sn4xv | 125.60 (3) | Tb2xv—Sn8A—Tb2 | 90.10 (12) |
Sn3viii—Tb4—Sn4xv | 125.60 (3) | Sn8Axiii—Sn8A—Tb2xvi | 82.2 (4) |
Sn2—Tb4—Sn4 | 64.90 (5) | Sn1—Sn8A—Tb2xvi | 125.4 (5) |
Sn2xiv—Tb4—Sn4 | 119.21 (7) | Sn1iii—Sn8A—Tb2xvi | 67.40 (17) |
Sn2viii—Tb4—Sn4 | 64.90 (5) | Tb2iii—Sn8A—Tb2xvi | 90.10 (12) |
Sn2xv—Tb4—Sn4 | 119.21 (7) | Tb2xv—Sn8A—Tb2xvi | 87.79 (11) |
Sn5—Tb4—Sn4 | 98.30 (3) | Tb2—Sn8A—Tb2xvi | 164.4 (9) |
Sn5xv—Tb4—Sn4 | 177.74 (7) | Sn8Axiii—Sn8A—Tb3xv | 137.2 (3) |
Sn6viii—Tb4—Sn4 | 54.45 (3) | Sn1—Sn8A—Tb3xv | 58.1 (3) |
Sn6—Tb4—Sn4 | 54.45 (3) | Sn1iii—Sn8A—Tb3xv | 58.1 (3) |
Sn3—Tb4—Sn4 | 125.60 (3) | Tb2iii—Sn8A—Tb3xv | 125.5 (5) |
Sn3viii—Tb4—Sn4 | 125.60 (3) | Tb2xv—Sn8A—Tb3xv | 67.62 (18) |
Sn4xv—Tb4—Sn4 | 79.44 (7) | Tb2—Sn8A—Tb3xv | 125.5 (5) |
Tb3xiv—Sn1—Tb3 | 174.41 (11) | Tb2xvi—Sn8A—Tb3xv | 67.62 (18) |
Tb3xiv—Sn1—Tb3viii | 91.037 (6) | Sn8Axiii—Sn8A—Tb3 | 137.2 (3) |
Tb3—Sn1—Tb3viii | 88.691 (6) | Sn1—Sn8A—Tb3 | 58.1 (3) |
Tb3xiv—Sn1—Tb3xv | 88.691 (6) | Sn1iii—Sn8A—Tb3 | 58.1 (3) |
Tb3—Sn1—Tb3xv | 91.037 (6) | Tb2iii—Sn8A—Tb3 | 67.62 (18) |
Tb3viii—Sn1—Tb3xv | 174.41 (11) | Tb2xv—Sn8A—Tb3 | 125.5 (5) |
Tb3xiv—Sn1—Sn8A | 121.40 (18) | Tb2—Sn8A—Tb3 | 67.62 (18) |
Tb3—Sn1—Sn8A | 63.20 (18) | Tb2xvi—Sn8A—Tb3 | 125.5 (5) |
Tb3viii—Sn1—Sn8A | 121.40 (18) | Tb3xv—Sn8A—Tb3 | 85.5 (6) |
Tb3xv—Sn1—Sn8A | 63.20 (18) | Sn8Axiii—Sn8—Tb2iii | 90.000 (8) |
Tb3xiv—Sn1—Sn8Aviii | 63.20 (18) | Sn8Axiii—Sn8—Tb2xv | 90.000 (8) |
Tb3—Sn1—Sn8Aviii | 121.40 (18) | Tb2iii—Sn8—Tb2xv | 180.0 |
Tb3viii—Sn1—Sn8Aviii | 63.20 (18) | Sn8Axiii—Sn8—Tb2 | 90.0 |
Tb3xv—Sn1—Sn8Aviii | 121.40 (18) | Tb2iii—Sn8—Tb2 | 88.824 (2) |
Sn8A—Sn1—Sn8Aviii | 88.1 (6) | Tb2xv—Sn8—Tb2 | 91.176 (2) |
Tb3xiv—Sn1—Tb2 | 119.55 (6) | Sn8Axiii—Sn8—Tb2xvi | 90.0 |
Tb3—Sn1—Tb2 | 65.28 (4) | Tb2iii—Sn8—Tb2xvi | 91.176 (2) |
Tb3viii—Sn1—Tb2 | 65.28 (4) | Tb2xv—Sn8—Tb2xvi | 88.824 (2) |
Tb3xv—Sn1—Tb2 | 119.55 (6) | Tb2—Sn8—Tb2xvi | 180.0 |
Sn8A—Sn1—Tb2 | 56.4 (2) | Sn8Axiii—Sn8—Tb3xv | 141.854 (16) |
Sn8Aviii—Sn1—Tb2 | 56.4 (2) | Tb2iii—Sn8—Tb3xv | 116.181 (9) |
Tb3xiv—Sn1—Tb2xv | 65.28 (4) | Tb2xv—Sn8—Tb3xv | 63.819 (9) |
Tb3—Sn1—Tb2xv | 119.55 (6) | Tb2—Sn8—Tb3xv | 116.181 (9) |
Tb3viii—Sn1—Tb2xv | 119.55 (6) | Tb2xvi—Sn8—Tb3xv | 63.819 (9) |
Tb3xv—Sn1—Tb2xv | 65.28 (4) | Sn8Axiii—Sn8—Tb3x | 38.146 (16) |
Sn8A—Sn1—Tb2xv | 56.4 (2) | Tb2iii—Sn8—Tb3x | 63.819 (10) |
Sn8Aviii—Sn1—Tb2xv | 56.4 (2) | Tb2xv—Sn8—Tb3x | 116.181 (10) |
Tb2—Sn1—Tb2xv | 79.38 (5) | Tb2—Sn8—Tb3x | 63.819 (9) |
Tb4—Sn2—Tb4i | 175.24 (13) | Tb2xvi—Sn8—Tb3x | 116.181 (9) |
Tb4—Sn2—Tb4ii | 91.075 (6) | Tb3xv—Sn8—Tb3x | 180.00 (3) |
Tb4i—Sn2—Tb4ii | 88.727 (6) | Sn8Axiii—Sn8—Tb3 | 141.854 (17) |
Tb4—Sn2—Tb4iii | 88.727 (6) | Tb2iii—Sn8—Tb3 | 63.819 (10) |
Tb4i—Sn2—Tb4iii | 91.075 (6) | Tb2xv—Sn8—Tb3 | 116.181 (9) |
Tb4ii—Sn2—Tb4iii | 175.24 (13) | Tb2—Sn8—Tb3 | 63.819 (9) |
Tb4—Sn2—Sn5iii | 120.44 (7) | Tb2xvi—Sn8—Tb3 | 116.181 (9) |
Tb4i—Sn2—Sn5iii | 63.52 (5) | Tb3xv—Sn8—Tb3 | 76.29 (3) |
Tb4ii—Sn2—Sn5iii | 120.44 (7) | Tb3x—Sn8—Tb3 | 103.71 (3) |
Tb4iii—Sn2—Sn5iii | 63.52 (5) | Sn8Axiii—Sn8—Tb3xiii | 38.146 (17) |
Tb4—Sn2—Sn5 | 63.52 (5) | Tb2iii—Sn8—Tb3xiii | 116.181 (9) |
Tb4i—Sn2—Sn5 | 120.44 (7) | Tb2xv—Sn8—Tb3xiii | 63.819 (9) |
Tb4ii—Sn2—Sn5 | 63.52 (5) | Tb2—Sn8—Tb3xiii | 116.181 (9) |
Tb4iii—Sn2—Sn5 | 120.44 (7) | Tb2xvi—Sn8—Tb3xiii | 63.819 (9) |
Sn5iii—Sn2—Sn5 | 85.86 (9) | Tb3xv—Sn8—Tb3xiii | 103.71 (3) |
Tb4—Sn2—Sn3ii | 121.08 (8) | Tb3x—Sn8—Tb3xiii | 76.29 (3) |
Tb4i—Sn2—Sn3ii | 62.91 (4) | Tb3—Sn8—Tb3xiii | 180.0 |
Symmetry codes: (i) x+1, y+1, z; (ii) x, y+1, z; (iii) x+1, y, z; (iv) −x, −y, −z; (v) −x+1, −y+1, −z; (vi) −x, −y+1, −z; (vii) −x+1, −y, −z; (viii) x−1, y, z; (ix) x−1, y+1, z; (x) −x+1, −y+1, −z+1; (xi) −x, −y, −z+1; (xii) −x, −y+1, −z+1; (xiii) −x+1, −y, −z+1; (xiv) x−1, y−1, z; (xv) x, y−1, z; (xvi) x+1, y−1, z. |
Experimental details
Crystal data | |
Chemical formula | Sn6.97Tb3 |
Mr | 1304.2 |
Crystal system, space group | Orthorhombic, Pmmm |
Temperature (K) | 293 |
a, b, c (Å) | 4.3352 (1), 4.4251 (1), 26.7006 (9) |
V (Å3) | 512.22 (2) |
Z | 2 |
Radiation type | Mo Kα |
µ (mm−1) | 37.01 |
Crystal size (mm) | 0.08 × 0.07 × 0.01 |
Data collection | |
Diffractometer | Xcalibur Oxford Diffraction diffractometer |
Absorption correction | Analytical CrysAlis RED (Oxford Diffraction, 2005) |
Tmin, Tmax | 0.089, 0.598 |
No. of measured, independent and observed [I > 2σ(I)] reflections | 4684, 762, 508 |
Rint | 0.051 |
(sin θ/λ)max (Å−1) | 0.648 |
Refinement | |
R[F2 > 2σ(F2)], wR(F2), S | 0.028, 0.088, 1.07 |
No. of reflections | 762 |
No. of parameters | 49 |
Δρmax, Δρmin (e Å−3) | 1.93, −2.19 |
Computer programs: CrysAlis CCD (Oxford Diffraction, 2004), CrysAlis RED (Oxford Diffraction, 2005), SHELXS97 (Sheldrick, 1997), SHELXL97 (Sheldrick, 1997), Diamond (Brandenburg, 1999), SHELX97 (Sheldrick, 1997).
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