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(S)-1,3-Butanediol (guest), C4H10O2, was found to be resolved from the racemate by inclusion crystallization with (S, S)-(+)-trans-2,3-bis(hydroxydiphenylmethyl)-1,4-dioxaspiro[4.4]nonane (host), C33H32O4. The unit cell of the crystal contains two pairs of host and guest molecules. There are four crystallographically independent hydrogen bonds, which form a belt-like structure along the b axis of the unit cell. The inclusion complex appears to be stabilized by hydrogen bonds and van der Waals interactions.

Supporting information

cif

Crystallographic Information File (CIF)
Contains datablock RAS227

hkl

Structure factor file (CIF format)
Supplementary material

CCDC reference: 128538

-1

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