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The title compound, ADS {N-2-(2,4-dinitrophenylthio)phenyl]acetamide, C14H11N3O5S}, has been isolated as yellow crystals during the three-step synthesis of 3-nitrophenothiazine. To confirm the mechanism of this type of reaction, we report here the structure of ADS before the Smiles rearrangement. X-ray analysis shows the expected ortho and para dinitro compound.

Supporting information

cif

Crystallographic Information File (CIF)
Contains datablock DU1181

fcf

Structure factor file (CIF format)
Contains datablock reb2

CCDC reference: 129701

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