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The crystal structure of [Co(NO2)(NH3)5](SiF6) has been determined at 293 and 150K. The complex cations in the structure are linked by N—H...F hydrogen bonds to the (SiF6)2− anions and by N—H...O hydrogen bonds to other cations. The role of these hydrogen bonds and of the repulsive O...F interactions in the anisotropy of the structural distortion on cooling is discussed.

Supporting information

cif

Crystallographic Information File (CIF)
Contains datablocks 1, 2, global

hkl

Structure factor file (CIF format)
Contains datablock 1

hkl

Structure factor file (CIF format)
Contains datablock 2

-1

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