A reaction cell for in situ studies of hydrothermal titration

Norby, P.; Cahill, C.; Koleda, C.; Parise, J.B.

doi:10.1107/S002188989701337X

A reaction cell for in situ studies of hydrothermal titration

P. Norby, C. Cahill, C. Koleda and J. B. Parise

A reaction cell for in situ studies of both ion-exchange and hydrothermal titration reactions has been designed and built. This cell allows the injection of reagents into a reaction mixture over time during X-ray data collection. A demonstration experiment followed the injection of Na₂SO₄(aq) into BaCl₂(aq) to yield a time-resolved X-ray powder diffraction pattern of the precipitation of BaSO₄(s).

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A reaction cell for in situ studies of hydrothermal titration

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