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The channeling effect in electron-induced X-ray emission has proved useful as a method to get immediate information about the cation atom distribution between octahedral and tetrahedral positions in the recently synthesized spinels: ZnCr0.4Fe1.6O4, ZnCrFeO4 and ZnCr1.6Fe0.4O4. It is concluded that the Zn atoms are in tetrahedral positions and the Cr atoms in octahedral positions. The Fe atoms also have a strong octahedral site preference, but the analysis indicates that ~5% of them are in tetrahedral positions.

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