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Polystyrene latex spheres of 1.011 and 0.234 μm diameter were used to observe low-angle X-ray scattering. For particles of about 1 μm in diameter the central scattering has not been observed accurately with characteristic X-rays such as Cu Kα and Mo Kα radiations, because it is strongly affected by the primary beam and the parasitic scattering of the slits. The present results show that the central scattering of particles of this size can be measured within 22′ without such influences by the use of C Kα radiation (wavelength 44.7 Å).