Supporting information
Crystallographic Information File (CIF) https://doi.org/10.1107/S1600536802004786/bt6125sup1.cif | |
Structure factor file (CIF format) https://doi.org/10.1107/S1600536802004786/bt6125Isup2.hkl |
CCDC reference: 183809
Data collection: DENZO (Otwinowski & Minor, 1997) and COLLECT (Hooft, 1998); cell refinement: DENZO and COLLECT; data reduction: DENZO and COLLECT; program(s) used to solve structure: SHELXS97 (Sheldrick, 1997); program(s) used to refine structure: SHELXL97 (Sheldrick, 1997); molecular graphics: PLATON (Spek, 1990).
C27H48 | F(000) = 840 |
Mr = 372.65 | Dx = 1.055 Mg m−3 |
Monoclinic, P21 | Mo Kα radiation, λ = 0.71073 Å |
a = 11.3936 (3) Å | Cell parameters from 6151 reflections |
b = 10.8972 (3) Å | θ = 2.9–27.5° |
c = 19.5047 (7) Å | µ = 0.06 mm−1 |
β = 104.2390 (11)° | T = 120 K |
V = 2347.27 (12) Å3 | Plate, colourless |
Z = 4 | 0.4 × 0.35 × 0.04 mm |
Nonius KappaCCD diffractometer | 5989 reflections with I > 2σ(I) |
Radiation source: Nonius FR591 rotating anode | Rint = 0.076 |
φ and ω scans | θmax = 27.5°, θmin = 3.0° |
Absorption correction: multi-scan (SORTAV; Blessing, 1997) | h = −14→14 |
Tmin = 0.977, Tmax = 0.998 | k = −14→11 |
15024 measured reflections | l = −25→25 |
9278 independent reflections |
Refinement on F2 | w = 1/[σ2(Fo2) + (0.0563P)2] where P = (Fo2 + 2Fc2)/3 |
Least-squares matrix: full | (Δ/σ)max = 0.025 |
R[F2 > 2σ(F2)] = 0.062 | Δρmax = 0.63 e Å−3 |
wR(F2) = 0.137 | Δρmin = −0.62 e Å−3 |
S = 0.99 | Extinction correction: SHELXL, Fc*=kFc[1+0.001xFc2λ3/sin(2θ)]-1/4 |
9278 reflections | Extinction coefficient: 0.047 (2) |
498 parameters | Absolute structure: (Flack, 1983) |
1 restraint | Absolute structure parameter: 2 (5) |
H-atom parameters constrained |
Geometry. All e.s.d.'s (except the e.s.d. in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell e.s.d.'s are taken into account individually in the estimation of e.s.d.'s in distances, angles and torsion angles; correlations between e.s.d.'s in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell e.s.d.'s is used for estimating e.s.d.'s involving l.s. planes. |
x | y | z | Uiso*/Ueq | ||
C1A | 0.4704 (2) | 0.5206 (2) | 0.88447 (13) | 0.0282 (6) | |
H1A1 | 0.3884 | 0.5089 | 0.8533 | 0.034* | |
H1A2 | 0.5219 | 0.4524 | 0.8753 | 0.034* | |
C2A | 0.4624 (3) | 0.5137 (3) | 0.96141 (13) | 0.0323 (7) | |
H2A1 | 0.4049 | 0.5766 | 0.9699 | 0.039* | |
H2A2 | 0.4313 | 0.4321 | 0.9706 | 0.039* | |
C3A | 0.5861 (3) | 0.5346 (3) | 1.01191 (14) | 0.0324 (7) | |
H3A1 | 0.5779 | 0.5349 | 1.0613 | 0.039* | |
H3A2 | 0.6414 | 0.4669 | 1.007 | 0.039* | |
C4A | 0.6391 (3) | 0.6565 (3) | 0.99577 (14) | 0.0320 (7) | |
H4A1 | 0.7214 | 0.6663 | 1.027 | 0.038* | |
H4A2 | 0.5883 | 0.7245 | 1.0059 | 0.038* | |
C5A | 0.6460 (3) | 0.6641 (2) | 0.91858 (13) | 0.0282 (7) | |
H5A | 0.6993 | 0.5948 | 0.9115 | 0.034* | |
C6A | 0.7070 (3) | 0.7804 (3) | 0.90200 (14) | 0.0322 (7) | |
H6A1 | 0.7858 | 0.7902 | 0.9368 | 0.039* | |
H6A2 | 0.6559 | 0.852 | 0.9064 | 0.039* | |
C7A | 0.7274 (2) | 0.7772 (3) | 0.82729 (13) | 0.0295 (7) | |
H7A1 | 0.7903 | 0.7153 | 0.8257 | 0.035* | |
H7A2 | 0.7581 | 0.8582 | 0.8166 | 0.035* | |
C8A | 0.6120 (2) | 0.7464 (2) | 0.77013 (13) | 0.0222 (6) | |
H8A | 0.5555 | 0.8179 | 0.7649 | 0.027* | |
C9A | 0.5474 (2) | 0.6326 (2) | 0.79043 (13) | 0.0230 (6) | |
H9A | 0.6052 | 0.5627 | 0.7931 | 0.028* | |
C10A | 0.5225 (2) | 0.6426 (2) | 0.86510 (13) | 0.0230 (6) | |
C11A | 0.4357 (2) | 0.6002 (3) | 0.73069 (13) | 0.0277 (7) | |
H11A | 0.3997 | 0.5231 | 0.743 | 0.033* | |
H11B | 0.3745 | 0.6659 | 0.727 | 0.033* | |
C12A | 0.4656 (3) | 0.5846 (2) | 0.65899 (14) | 0.0289 (7) | |
H12A | 0.3898 | 0.5688 | 0.6225 | 0.035* | |
H12B | 0.5187 | 0.5121 | 0.6609 | 0.035* | |
C13A | 0.5285 (2) | 0.6972 (2) | 0.63748 (13) | 0.0212 (6) | |
C14A | 0.6410 (2) | 0.7223 (2) | 0.69891 (13) | 0.0230 (6) | |
H14A | 0.6898 | 0.645 | 0.7051 | 0.028* | |
C15A | 0.7138 (3) | 0.8163 (2) | 0.66878 (14) | 0.0288 (7) | |
H15A | 0.8006 | 0.8133 | 0.6939 | 0.035* | |
H15B | 0.6828 | 0.9004 | 0.6722 | 0.035* | |
C16A | 0.6948 (2) | 0.7765 (2) | 0.59073 (13) | 0.0253 (6) | |
H16A | 0.7698 | 0.7392 | 0.5831 | 0.03* | |
H16B | 0.6736 | 0.8484 | 0.5591 | 0.03* | |
C17A | 0.5903 (2) | 0.6817 (2) | 0.57488 (13) | 0.0224 (6) | |
H17A | 0.6286 | 0.5986 | 0.5801 | 0.027* | |
C18A | 0.4318 (3) | 0.7463 (3) | 0.86726 (15) | 0.0323 (7) | |
H18A | 0.3524 | 0.7247 | 0.8368 | 0.048* | |
H18B | 0.4604 | 0.8227 | 0.8504 | 0.048* | |
H18C | 0.4247 | 0.7574 | 0.9159 | 0.048* | |
C19A | 0.4422 (3) | 0.8075 (2) | 0.62386 (14) | 0.0311 (7) | |
H19A | 0.4837 | 0.8784 | 0.6097 | 0.047* | |
H19B | 0.4171 | 0.8272 | 0.6672 | 0.047* | |
H19C | 0.3707 | 0.7873 | 0.586 | 0.047* | |
C20A | 0.5113 (2) | 0.6902 (2) | 0.49847 (13) | 0.0243 (6) | |
H20A | 0.4747 | 0.7741 | 0.4919 | 0.029* | |
C21A | 0.4081 (3) | 0.5977 (3) | 0.48527 (14) | 0.0349 (7) | |
H21A | 0.4409 | 0.5153 | 0.4977 | 0.052* | |
H21B | 0.3649 | 0.5995 | 0.4352 | 0.052* | |
H21C | 0.3521 | 0.6187 | 0.5144 | 0.052* | |
C22A | 0.5871 (3) | 0.6740 (3) | 0.44435 (13) | 0.0286 (7) | |
H22A | 0.6565 | 0.7315 | 0.4562 | 0.034* | |
H22B | 0.6203 | 0.5896 | 0.4485 | 0.034* | |
C23A | 0.5181 (3) | 0.6959 (3) | 0.36776 (14) | 0.0295 (7) | |
H23A | 0.4508 | 0.6361 | 0.3553 | 0.035* | |
H23B | 0.4819 | 0.779 | 0.3641 | 0.035* | |
C24A | 0.5944 (3) | 0.6851 (3) | 0.31424 (14) | 0.0321 (7) | |
H24A | 0.6284 | 0.6012 | 0.3171 | 0.039* | |
H24B | 0.6632 | 0.7429 | 0.3279 | 0.039* | |
C25A | 0.5287 (3) | 0.7106 (2) | 0.23769 (13) | 0.0283 (7) | |
H25A | 0.4886 | 0.7925 | 0.2361 | 0.034* | |
C26A | 0.4306 (3) | 0.6164 (3) | 0.20829 (16) | 0.0458 (9) | |
H26A | 0.3706 | 0.6168 | 0.2367 | 0.069* | |
H26B | 0.4671 | 0.5347 | 0.21 | 0.069* | |
H26C | 0.3908 | 0.6371 | 0.1592 | 0.069* | |
C27A | 0.6181 (3) | 0.7178 (3) | 0.19120 (15) | 0.0427 (8) | |
H27A | 0.5744 | 0.7368 | 0.1425 | 0.064* | |
H27B | 0.6597 | 0.6389 | 0.1922 | 0.064* | |
H27C | 0.6777 | 0.7824 | 0.209 | 0.064* | |
C1B | 1.1012 (3) | 0.6048 (2) | 0.90578 (13) | 0.0299 (7) | |
H1B1 | 1.1784 | 0.6182 | 0.8923 | 0.036* | |
H1B2 | 1.0479 | 0.6759 | 0.8885 | 0.036* | |
C2B | 1.1267 (3) | 0.5999 (3) | 0.98673 (13) | 0.0355 (7) | |
H2B1 | 1.1879 | 0.5357 | 1.0049 | 0.043* | |
H2B2 | 1.1604 | 0.6796 | 1.0067 | 0.043* | |
C3B | 1.0133 (3) | 0.5725 (3) | 1.01076 (15) | 0.0365 (8) | |
H3B1 | 0.9569 | 0.6429 | 0.9989 | 0.044* | |
H3B2 | 1.0344 | 0.5621 | 1.0628 | 0.044* | |
C4B | 0.9504 (3) | 0.4568 (3) | 0.97603 (14) | 0.0314 (7) | |
H4B1 | 0.873 | 0.4459 | 0.9897 | 0.038* | |
H4B2 | 1.0021 | 0.3846 | 0.9932 | 0.038* | |
C5B | 0.9257 (3) | 0.4638 (2) | 0.89549 (13) | 0.0256 (6) | |
H5B | 0.873 | 0.5374 | 0.8813 | 0.031* | |
C6B | 0.8524 (2) | 0.3550 (3) | 0.85885 (13) | 0.0283 (7) | |
H6B1 | 0.7783 | 0.3461 | 0.8764 | 0.034* | |
H6B2 | 0.9007 | 0.279 | 0.8708 | 0.034* | |
C7B | 0.8168 (2) | 0.3712 (3) | 0.77871 (13) | 0.0279 (7) | |
H7B1 | 0.757 | 0.4387 | 0.7664 | 0.033* | |
H7B2 | 0.7775 | 0.2951 | 0.7566 | 0.033* | |
C8B | 0.9258 (2) | 0.4002 (2) | 0.74852 (13) | 0.0224 (6) | |
H8B | 0.9795 | 0.3264 | 0.7549 | 0.027* | |
C9B | 0.9996 (2) | 0.5092 (2) | 0.78775 (13) | 0.0232 (6) | |
H9B | 0.9432 | 0.581 | 0.7806 | 0.028* | |
C10B | 1.0409 (2) | 0.4880 (2) | 0.86918 (13) | 0.0242 (6) | |
C11B | 1.1032 (2) | 0.5444 (3) | 0.75338 (13) | 0.0278 (7) | |
H11C | 1.1414 | 0.621 | 0.7755 | 0.033* | |
H11D | 1.1654 | 0.479 | 0.7634 | 0.033* | |
C12B | 1.0623 (3) | 0.5633 (2) | 0.67323 (13) | 0.0294 (7) | |
H12C | 1.1343 | 0.5785 | 0.6545 | 0.035* | |
H12D | 1.0099 | 0.6368 | 0.6632 | 0.035* | |
C13B | 0.9928 (2) | 0.4523 (2) | 0.63488 (13) | 0.0222 (6) | |
C14B | 0.8871 (2) | 0.4302 (2) | 0.66984 (13) | 0.0228 (6) | |
H14B | 0.8411 | 0.5091 | 0.6657 | 0.027* | |
C15B | 0.8050 (3) | 0.3390 (3) | 0.62063 (13) | 0.0296 (7) | |
H15C | 0.7203 | 0.3456 | 0.6247 | 0.035* | |
H15D | 0.8335 | 0.2537 | 0.6313 | 0.035* | |
C16B | 0.8158 (2) | 0.3783 (2) | 0.54605 (13) | 0.0266 (6) | |
H16C | 0.7395 | 0.4171 | 0.5196 | 0.032* | |
H16D | 0.8319 | 0.3059 | 0.5191 | 0.032* | |
C17B | 0.9224 (2) | 0.4713 (2) | 0.55634 (13) | 0.0238 (6) | |
H17B | 0.8864 | 0.5554 | 0.5527 | 0.029* | |
C18B | 1.1309 (2) | 0.3801 (2) | 0.88712 (13) | 0.0285 (7) | |
H18D | 1.2063 | 0.4018 | 0.8744 | 0.043* | |
H18E | 1.0955 | 0.3072 | 0.8604 | 0.043* | |
H18F | 1.1481 | 0.3627 | 0.9379 | 0.043* | |
C19B | 1.0750 (2) | 0.3399 (3) | 0.64091 (14) | 0.0324 (7) | |
H19D | 1.0287 | 0.2708 | 0.6157 | 0.049* | |
H19E | 1.1061 | 0.3183 | 0.6909 | 0.049* | |
H19F | 1.1429 | 0.3586 | 0.6201 | 0.049* | |
C20B | 0.9917 (3) | 0.4603 (3) | 0.49831 (14) | 0.0277 (7) | |
H20B | 1.0261 | 0.3756 | 0.5006 | 0.033* | |
C21B | 1.0968 (3) | 0.5508 (3) | 0.51034 (15) | 0.0502 (10) | |
H21D | 1.1577 | 0.5282 | 0.5534 | 0.075* | |
H21E | 1.067 | 0.6338 | 0.5155 | 0.075* | |
H21F | 1.1334 | 0.5484 | 0.4698 | 0.075* | |
C22B | 0.9080 (3) | 0.4782 (3) | 0.42417 (13) | 0.0286 (7) | |
H22C | 0.8371 | 0.4233 | 0.4188 | 0.034* | |
H22D | 0.878 | 0.5638 | 0.4196 | 0.034* | |
C23B | 0.9700 (3) | 0.4517 (3) | 0.36461 (14) | 0.0308 (7) | |
H23C | 1.0032 | 0.3673 | 0.3706 | 0.037* | |
H23D | 1.0389 | 0.5089 | 0.369 | 0.037* | |
C24B | 0.8867 (3) | 0.4637 (3) | 0.29021 (13) | 0.0318 (7) | |
H24C | 0.8189 | 0.4048 | 0.2855 | 0.038* | |
H24D | 0.8517 | 0.5473 | 0.2847 | 0.038* | |
C25B | 0.9489 (2) | 0.4406 (2) | 0.23059 (13) | 0.0256 (6) | |
H25B | 0.9878 | 0.3578 | 0.2381 | 0.031* | |
C26B | 1.0467 (3) | 0.5347 (3) | 0.23022 (14) | 0.0330 (7) | |
H26D | 1.01 | 0.6163 | 0.2212 | 0.05* | |
H26E | 1.0876 | 0.5142 | 0.193 | 0.05* | |
H26F | 1.1057 | 0.5345 | 0.2762 | 0.05* | |
C27B | 0.8572 (3) | 0.4402 (3) | 0.15897 (14) | 0.0379 (8) | |
H27D | 0.898 | 0.4182 | 0.1219 | 0.057* | |
H27E | 0.8212 | 0.5221 | 0.1493 | 0.057* | |
H27F | 0.7934 | 0.3802 | 0.1596 | 0.057* |
U11 | U22 | U33 | U12 | U13 | U23 | |
C1A | 0.0274 (16) | 0.0316 (15) | 0.0253 (16) | −0.0052 (13) | 0.0061 (12) | −0.0015 (12) |
C2A | 0.0370 (18) | 0.0336 (16) | 0.0269 (16) | −0.0070 (14) | 0.0089 (13) | 0.0027 (12) |
C3A | 0.0375 (18) | 0.0367 (17) | 0.0238 (16) | −0.0044 (15) | 0.0092 (14) | 0.0034 (13) |
C4A | 0.0342 (18) | 0.0362 (18) | 0.0239 (16) | −0.0057 (14) | 0.0040 (13) | 0.0000 (12) |
C5A | 0.0310 (17) | 0.0275 (16) | 0.0253 (16) | −0.0011 (13) | 0.0056 (13) | −0.0007 (11) |
C6A | 0.0346 (18) | 0.0339 (16) | 0.0254 (17) | −0.0076 (14) | 0.0023 (14) | −0.0001 (12) |
C7A | 0.0322 (17) | 0.0281 (15) | 0.0277 (17) | −0.0077 (13) | 0.0063 (13) | −0.0004 (12) |
C8A | 0.0248 (15) | 0.0195 (14) | 0.0210 (15) | 0.0001 (12) | 0.0034 (12) | −0.0009 (10) |
C9A | 0.0233 (15) | 0.0248 (14) | 0.0213 (15) | 0.0014 (12) | 0.0062 (12) | −0.0032 (11) |
C10A | 0.0217 (15) | 0.0249 (14) | 0.0227 (15) | −0.0030 (12) | 0.0056 (12) | −0.0005 (11) |
C11A | 0.0260 (16) | 0.0334 (16) | 0.0244 (16) | −0.0084 (13) | 0.0078 (13) | −0.0009 (12) |
C12A | 0.0291 (17) | 0.0333 (16) | 0.0228 (15) | −0.0068 (14) | 0.0033 (13) | −0.0017 (12) |
C13A | 0.0182 (14) | 0.0259 (14) | 0.0192 (14) | −0.0004 (12) | 0.0042 (11) | −0.0001 (11) |
C14A | 0.0211 (15) | 0.0192 (14) | 0.0272 (16) | 0.0001 (12) | 0.0032 (12) | 0.0009 (11) |
C15A | 0.0282 (16) | 0.0314 (16) | 0.0269 (16) | −0.0076 (13) | 0.0072 (13) | 0.0003 (12) |
C16A | 0.0218 (15) | 0.0288 (15) | 0.0255 (16) | 0.0010 (13) | 0.0060 (12) | 0.0033 (11) |
C17A | 0.0220 (15) | 0.0223 (14) | 0.0221 (15) | 0.0027 (12) | 0.0041 (12) | 0.0014 (11) |
C18A | 0.0340 (18) | 0.0353 (17) | 0.0291 (17) | 0.0063 (14) | 0.0107 (14) | 0.0014 (13) |
C19A | 0.0305 (17) | 0.0356 (17) | 0.0263 (17) | 0.0064 (14) | 0.0054 (13) | −0.0004 (12) |
C20A | 0.0259 (15) | 0.0260 (15) | 0.0206 (15) | −0.0004 (13) | 0.0053 (12) | −0.0012 (11) |
C21A | 0.0347 (18) | 0.0469 (19) | 0.0226 (16) | −0.0074 (15) | 0.0062 (14) | −0.0042 (13) |
C22A | 0.0274 (16) | 0.0342 (17) | 0.0253 (16) | 0.0004 (13) | 0.0083 (13) | 0.0006 (12) |
C23A | 0.0304 (17) | 0.0340 (16) | 0.0260 (16) | 0.0040 (14) | 0.0102 (13) | 0.0042 (12) |
C24A | 0.0336 (17) | 0.0390 (17) | 0.0265 (17) | 0.0018 (14) | 0.0126 (13) | 0.0033 (13) |
C25A | 0.0363 (17) | 0.0266 (15) | 0.0241 (16) | 0.0050 (13) | 0.0111 (13) | 0.0018 (11) |
C26A | 0.058 (2) | 0.0427 (19) | 0.0331 (19) | −0.0035 (17) | 0.0037 (16) | −0.0029 (14) |
C27A | 0.054 (2) | 0.049 (2) | 0.0283 (18) | 0.0070 (17) | 0.0167 (16) | 0.0069 (14) |
C1B | 0.0345 (17) | 0.0309 (16) | 0.0243 (16) | −0.0039 (14) | 0.0075 (13) | −0.0005 (12) |
C2B | 0.047 (2) | 0.0362 (17) | 0.0228 (17) | −0.0049 (15) | 0.0064 (14) | −0.0057 (12) |
C3B | 0.051 (2) | 0.0362 (17) | 0.0244 (17) | −0.0012 (15) | 0.0125 (15) | −0.0001 (12) |
C4B | 0.0374 (18) | 0.0348 (17) | 0.0238 (16) | 0.0023 (14) | 0.0107 (13) | 0.0033 (12) |
C5B | 0.0304 (16) | 0.0271 (15) | 0.0206 (15) | 0.0016 (13) | 0.0091 (12) | 0.0030 (11) |
C6B | 0.0295 (17) | 0.0345 (16) | 0.0226 (15) | −0.0018 (14) | 0.0097 (13) | 0.0037 (12) |
C7B | 0.0263 (16) | 0.0308 (15) | 0.0279 (16) | −0.0037 (13) | 0.0092 (13) | 0.0027 (12) |
C8B | 0.0222 (15) | 0.0243 (15) | 0.0205 (15) | 0.0000 (12) | 0.0048 (12) | 0.0023 (11) |
C9B | 0.0247 (15) | 0.0221 (14) | 0.0238 (15) | 0.0021 (12) | 0.0078 (12) | 0.0014 (11) |
C10B | 0.0280 (16) | 0.0238 (15) | 0.0214 (15) | −0.0004 (12) | 0.0070 (12) | 0.0003 (11) |
C11B | 0.0297 (17) | 0.0327 (16) | 0.0208 (15) | −0.0072 (13) | 0.0063 (12) | −0.0021 (12) |
C12B | 0.0298 (17) | 0.0352 (17) | 0.0236 (16) | −0.0092 (13) | 0.0076 (13) | 0.0003 (12) |
C13B | 0.0206 (15) | 0.0289 (15) | 0.0169 (14) | 0.0007 (13) | 0.0042 (11) | 0.0005 (11) |
C14B | 0.0209 (15) | 0.0238 (14) | 0.0235 (15) | 0.0001 (12) | 0.0048 (12) | 0.0036 (11) |
C15B | 0.0278 (16) | 0.0360 (17) | 0.0235 (16) | −0.0085 (14) | 0.0038 (13) | 0.0018 (12) |
C16B | 0.0249 (15) | 0.0312 (15) | 0.0224 (15) | −0.0005 (13) | 0.0035 (12) | −0.0006 (11) |
C17B | 0.0220 (15) | 0.0247 (15) | 0.0237 (15) | −0.0007 (12) | 0.0038 (12) | 0.0001 (11) |
C18B | 0.0285 (17) | 0.0339 (16) | 0.0232 (16) | 0.0013 (13) | 0.0063 (13) | −0.0002 (12) |
C19B | 0.0261 (16) | 0.0475 (19) | 0.0231 (16) | 0.0059 (14) | 0.0050 (13) | 0.0004 (13) |
C20B | 0.0253 (16) | 0.0387 (17) | 0.0194 (15) | −0.0025 (14) | 0.0061 (12) | 0.0011 (12) |
C21B | 0.042 (2) | 0.083 (3) | 0.0259 (18) | −0.0230 (19) | 0.0092 (16) | 0.0020 (17) |
C22B | 0.0253 (16) | 0.0395 (18) | 0.0212 (16) | −0.0022 (13) | 0.0062 (13) | 0.0003 (12) |
C23B | 0.0328 (18) | 0.0354 (17) | 0.0237 (16) | 0.0033 (15) | 0.0060 (13) | 0.0031 (12) |
C24B | 0.0307 (17) | 0.0443 (18) | 0.0207 (16) | −0.0018 (14) | 0.0068 (13) | 0.0012 (13) |
C25B | 0.0320 (17) | 0.0253 (15) | 0.0193 (15) | 0.0013 (13) | 0.0059 (12) | 0.0000 (11) |
C26B | 0.0395 (19) | 0.0351 (16) | 0.0258 (16) | 0.0021 (15) | 0.0107 (14) | 0.0024 (12) |
C27B | 0.0419 (19) | 0.0496 (19) | 0.0217 (17) | −0.0045 (16) | 0.0069 (14) | −0.0013 (13) |
C1A—C2A | 1.528 (3) | C1B—C2B | 1.534 (3) |
C1A—C10A | 1.541 (3) | C1B—C10B | 1.536 (4) |
C1A—H1A1 | 0.99 | C1B—H1B1 | 0.99 |
C1A—H1A2 | 0.99 | C1B—H1B2 | 0.99 |
C2A—C3A | 1.525 (4) | C2B—C3B | 1.508 (4) |
C2A—H2A1 | 0.99 | C2B—H2B1 | 0.99 |
C2A—H2A2 | 0.99 | C2B—H2B2 | 0.99 |
C3A—C4A | 1.524 (4) | C3B—C4B | 1.524 (4) |
C3A—H3A1 | 0.99 | C3B—H3B1 | 0.99 |
C3A—H3A2 | 0.99 | C3B—H3B2 | 0.99 |
C4A—C5A | 1.529 (4) | C4B—C5B | 1.528 (4) |
C4A—H4A1 | 0.99 | C4B—H4B1 | 0.99 |
C4A—H4A2 | 0.99 | C4B—H4B2 | 0.99 |
C5A—C6A | 1.518 (4) | C5B—C6B | 1.523 (4) |
C5A—C10A | 1.549 (4) | C5B—C10B | 1.545 (4) |
C5A—H5A | 1.00 | C5B—H5B | 1.00 |
C6A—C7A | 1.532 (4) | C6B—C7B | 1.525 (3) |
C6A—H6A1 | 0.99 | C6B—H6B1 | 0.99 |
C6A—H6A2 | 0.99 | C6B—H6B2 | 0.99 |
C7A—C8A | 1.538 (3) | C7B—C8B | 1.533 (4) |
C7A—H7A1 | 0.99 | C7B—H7B1 | 0.99 |
C7A—H7A2 | 0.99 | C7B—H7B2 | 0.99 |
C8A—C14A | 1.528 (4) | C8B—C14B | 1.524 (3) |
C8A—C9A | 1.542 (4) | C8B—C9B | 1.545 (4) |
C8A—H8A | 1.00 | C8B—H8B | 1.00 |
C9A—C11A | 1.540 (3) | C9B—C11B | 1.542 (4) |
C9A—C10A | 1.555 (3) | C9B—C10B | 1.559 (3) |
C9A—H9A | 1.00 | C9B—H9B | 1.00 |
C10A—C18A | 1.539 (4) | C10B—C18B | 1.543 (4) |
C11A—C12A | 1.528 (3) | C11B—C12B | 1.531 (3) |
C11A—H11A | 0.99 | C11B—H11C | 0.99 |
C11A—H11B | 0.99 | C11B—H11D | 0.99 |
C12A—C13A | 1.531 (4) | C12B—C13B | 1.536 (4) |
C12A—H12A | 0.99 | C12B—H12C | 0.99 |
C12A—H12B | 0.99 | C12B—H12D | 0.99 |
C13A—C19A | 1.534 (4) | C13B—C19B | 1.528 (4) |
C13A—C14A | 1.549 (4) | C13B—C14B | 1.543 (4) |
C13A—C17A | 1.561 (4) | C13B—C17B | 1.558 (3) |
C14A—C15A | 1.523 (4) | C14B—C15B | 1.530 (4) |
C14A—H14A | 1.00 | C14B—H14B | 1.00 |
C15A—C16A | 1.546 (4) | C15B—C16B | 1.550 (3) |
C15A—H15A | 0.99 | C15B—H15C | 0.99 |
C15A—H15B | 0.99 | C15B—H15D | 0.99 |
C16A—C17A | 1.548 (4) | C16B—C17B | 1.556 (4) |
C16A—H16A | 0.99 | C16B—H16C | 0.99 |
C16A—H16B | 0.99 | C16B—H16D | 0.99 |
C17A—C20A | 1.543 (3) | C17B—C20B | 1.535 (4) |
C17A—H17A | 1.00 | C17B—H17B | 1.00 |
C18A—H18A | 0.98 | C18B—H18D | 0.98 |
C18A—H18B | 0.98 | C18B—H18E | 0.98 |
C18A—H18C | 0.98 | C18B—H18F | 0.98 |
C19A—H19A | 0.98 | C19B—H19D | 0.98 |
C19A—H19B | 0.98 | C19B—H19E | 0.98 |
C19A—H19C | 0.98 | C19B—H19F | 0.98 |
C20A—C21A | 1.521 (4) | C20B—C21B | 1.524 (4) |
C20A—C22A | 1.530 (4) | C20B—C22B | 1.536 (4) |
C20A—H20A | 1.00 | C20B—H20B | 1.00 |
C21A—H21A | 0.98 | C21B—H21D | 0.98 |
C21A—H21B | 0.98 | C21B—H21E | 0.98 |
C21A—H21C | 0.98 | C21B—H21F | 0.98 |
C22A—C23A | 1.526 (4) | C22B—C23B | 1.528 (4) |
C22A—H22A | 0.99 | C22B—H22C | 0.99 |
C22A—H22B | 0.99 | C22B—H22D | 0.99 |
C23A—C24A | 1.519 (4) | C23B—C24B | 1.532 (4) |
C23A—H23A | 0.99 | C23B—H23C | 0.99 |
C23A—H23B | 0.99 | C23B—H23D | 0.99 |
C24A—C25A | 1.522 (4) | C24B—C25B | 1.524 (4) |
C24A—H24A | 0.99 | C24B—H24C | 0.99 |
C24A—H24B | 0.99 | C24B—H24D | 0.99 |
C25A—C26A | 1.522 (4) | C25B—C26B | 1.516 (4) |
C25A—C27A | 1.523 (4) | C25B—C27B | 1.525 (4) |
C25A—H25A | 1.00 | C25B—H25B | 1.00 |
C26A—H26A | 0.98 | C26B—H26D | 0.98 |
C26A—H26B | 0.98 | C26B—H26E | 0.98 |
C26A—H26C | 0.98 | C26B—H26F | 0.98 |
C27A—H27A | 0.98 | C27B—H27D | 0.98 |
C27A—H27B | 0.98 | C27B—H27E | 0.98 |
C27A—H27C | 0.98 | C27B—H27F | 0.98 |
C2A—C1A—C10A | 113.8 (2) | C2B—C1B—C10B | 113.5 (2) |
C2A—C1A—H1A1 | 108.8 | C2B—C1B—H1B1 | 108.9 |
C10A—C1A—H1A1 | 108.8 | C10B—C1B—H1B1 | 108.9 |
C2A—C1A—H1A2 | 108.8 | C2B—C1B—H1B2 | 108.9 |
C10A—C1A—H1A2 | 108.8 | C10B—C1B—H1B2 | 108.9 |
H1A1—C1A—H1A2 | 107.7 | H1B1—C1B—H1B2 | 107.7 |
C3A—C2A—C1A | 111.0 (2) | C3B—C2B—C1B | 111.5 (2) |
C3A—C2A—H2A1 | 109.4 | C3B—C2B—H2B1 | 109.3 |
C1A—C2A—H2A1 | 109.4 | C1B—C2B—H2B1 | 109.3 |
C3A—C2A—H2A2 | 109.4 | C3B—C2B—H2B2 | 109.3 |
C1A—C2A—H2A2 | 109.4 | C1B—C2B—H2B2 | 109.3 |
H2A1—C2A—H2A2 | 108 | H2B1—C2B—H2B2 | 108 |
C4A—C3A—C2A | 110.3 (2) | C2B—C3B—C4B | 111.7 (2) |
C4A—C3A—H3A1 | 109.6 | C2B—C3B—H3B1 | 109.3 |
C2A—C3A—H3A1 | 109.6 | C4B—C3B—H3B1 | 109.3 |
C4A—C3A—H3A2 | 109.6 | C2B—C3B—H3B2 | 109.3 |
C2A—C3A—H3A2 | 109.6 | C4B—C3B—H3B2 | 109.3 |
H3A1—C3A—H3A2 | 108.1 | H3B1—C3B—H3B2 | 107.9 |
C3A—C4A—C5A | 111.7 (2) | C3B—C4B—C5B | 111.3 (2) |
C3A—C4A—H4A1 | 109.3 | C3B—C4B—H4B1 | 109.4 |
C5A—C4A—H4A1 | 109.3 | C5B—C4B—H4B1 | 109.4 |
C3A—C4A—H4A2 | 109.3 | C3B—C4B—H4B2 | 109.4 |
C5A—C4A—H4A2 | 109.3 | C5B—C4B—H4B2 | 109.4 |
H4A1—C4A—H4A2 | 107.9 | H4B1—C4B—H4B2 | 108 |
C6A—C5A—C4A | 113.1 (2) | C6B—C5B—C4B | 112.6 (2) |
C6A—C5A—C10A | 111.7 (2) | C6B—C5B—C10B | 113.0 (2) |
C4A—C5A—C10A | 113.4 (2) | C4B—C5B—C10B | 113.1 (2) |
C6A—C5A—H5A | 106 | C6B—C5B—H5B | 105.8 |
C4A—C5A—H5A | 106 | C4B—C5B—H5B | 105.8 |
C10A—C5A—H5A | 106 | C10B—C5B—H5B | 105.8 |
C5A—C6A—C7A | 111.6 (2) | C5B—C6B—C7B | 111.6 (2) |
C5A—C6A—H6A1 | 109.3 | C5B—C6B—H6B1 | 109.3 |
C7A—C6A—H6A1 | 109.3 | C7B—C6B—H6B1 | 109.3 |
C5A—C6A—H6A2 | 109.3 | C5B—C6B—H6B2 | 109.3 |
C7A—C6A—H6A2 | 109.3 | C7B—C6B—H6B2 | 109.3 |
H6A1—C6A—H6A2 | 108 | H6B1—C6B—H6B2 | 108 |
C6A—C7A—C8A | 113.1 (2) | C6B—C7B—C8B | 112.4 (2) |
C6A—C7A—H7A1 | 109 | C6B—C7B—H7B1 | 109.1 |
C8A—C7A—H7A1 | 109 | C8B—C7B—H7B1 | 109.1 |
C6A—C7A—H7A2 | 109 | C6B—C7B—H7B2 | 109.1 |
C8A—C7A—H7A2 | 109 | C8B—C7B—H7B2 | 109.1 |
H7A1—C7A—H7A2 | 107.8 | H7B1—C7B—H7B2 | 107.9 |
C14A—C8A—C7A | 111.0 (2) | C14B—C8B—C7B | 111.7 (2) |
C14A—C8A—C9A | 108.63 (19) | C14B—C8B—C9B | 108.78 (19) |
C7A—C8A—C9A | 111.5 (2) | C7B—C8B—C9B | 111.2 (2) |
C14A—C8A—H8A | 108.5 | C14B—C8B—H8B | 108.3 |
C7A—C8A—H8A | 108.5 | C7B—C8B—H8B | 108.3 |
C9A—C8A—H8A | 108.5 | C9B—C8B—H8B | 108.3 |
C11A—C9A—C8A | 110.3 (2) | C11B—C9B—C8B | 110.9 (2) |
C11A—C9A—C10A | 114.7 (2) | C11B—C9B—C10B | 114.1 (2) |
C8A—C9A—C10A | 113.1 (2) | C8B—C9B—C10B | 112.5 (2) |
C11A—C9A—H9A | 106 | C11B—C9B—H9B | 106.2 |
C8A—C9A—H9A | 106 | C8B—C9B—H9B | 106.2 |
C10A—C9A—H9A | 106 | C10B—C9B—H9B | 106.2 |
C18A—C10A—C1A | 109.0 (2) | C1B—C10B—C18B | 109.3 (2) |
C18A—C10A—C5A | 112.1 (2) | C1B—C10B—C5B | 107.8 (2) |
C1A—C10A—C5A | 107.8 (2) | C18B—C10B—C5B | 111.5 (2) |
C18A—C10A—C9A | 110.8 (2) | C1B—C10B—C9B | 109.8 (2) |
C1A—C10A—C9A | 109.8 (2) | C18B—C10B—C9B | 111.2 (2) |
C5A—C10A—C9A | 107.3 (2) | C5B—C10B—C9B | 107.2 (2) |
C12A—C11A—C9A | 112.9 (2) | C12B—C11B—C9B | 113.8 (2) |
C12A—C11A—H11A | 109 | C12B—C11B—H11C | 108.8 |
C9A—C11A—H11A | 109 | C9B—C11B—H11C | 108.8 |
C12A—C11A—H11B | 109 | C12B—C11B—H11D | 108.8 |
C9A—C11A—H11B | 109 | C9B—C11B—H11D | 108.8 |
H11A—C11A—H11B | 107.8 | H11C—C11B—H11D | 107.7 |
C11A—C12A—C13A | 112.7 (2) | C11B—C12B—C13B | 112.5 (2) |
C11A—C12A—H12A | 109 | C11B—C12B—H12C | 109.1 |
C13A—C12A—H12A | 109 | C13B—C12B—H12C | 109.1 |
C11A—C12A—H12B | 109 | C11B—C12B—H12D | 109.1 |
C13A—C12A—H12B | 109 | C13B—C12B—H12D | 109.1 |
H12A—C12A—H12B | 107.8 | H12C—C12B—H12D | 107.8 |
C12A—C13A—C19A | 110.6 (2) | C19B—C13B—C12B | 111.1 (2) |
C12A—C13A—C14A | 106.5 (2) | C19B—C13B—C14B | 111.8 (2) |
C19A—C13A—C14A | 111.6 (2) | C12B—C13B—C14B | 105.8 (2) |
C12A—C13A—C17A | 117.3 (2) | C19B—C13B—C17B | 109.9 (2) |
C19A—C13A—C17A | 110.0 (2) | C12B—C13B—C17B | 117.0 (2) |
C14A—C13A—C17A | 100.2 (2) | C14B—C13B—C17B | 100.7 (2) |
C15A—C14A—C8A | 119.7 (2) | C8B—C14B—C15B | 118.3 (2) |
C15A—C14A—C13A | 104.2 (2) | C8B—C14B—C13B | 114.5 (2) |
C8A—C14A—C13A | 114.2 (2) | C15B—C14B—C13B | 104.3 (2) |
C15A—C14A—H14A | 105.9 | C8B—C14B—H14B | 106.3 |
C8A—C14A—H14A | 105.9 | C15B—C14B—H14B | 106.3 |
C13A—C14A—H14A | 105.9 | C13B—C14B—H14B | 106.3 |
C14A—C15A—C16A | 103.5 (2) | C14B—C15B—C16B | 103.4 (2) |
C14A—C15A—H15A | 111.1 | C14B—C15B—H15C | 111.1 |
C16A—C15A—H15A | 111.1 | C16B—C15B—H15C | 111.1 |
C14A—C15A—H15B | 111.1 | C14B—C15B—H15D | 111.1 |
C16A—C15A—H15B | 111.1 | C16B—C15B—H15D | 111.1 |
H15A—C15A—H15B | 109 | H15C—C15B—H15D | 109 |
C15A—C16A—C17A | 107.4 (2) | C15B—C16B—C17B | 107.3 (2) |
C15A—C16A—H16A | 110.2 | C15B—C16B—H16C | 110.2 |
C17A—C16A—H16A | 110.2 | C17B—C16B—H16C | 110.2 |
C15A—C16A—H16B | 110.2 | C15B—C16B—H16D | 110.2 |
C17A—C16A—H16B | 110.2 | C17B—C16B—H16D | 110.2 |
H16A—C16A—H16B | 108.5 | H16C—C16B—H16D | 108.5 |
C20A—C17A—C16A | 113.0 (2) | C20B—C17B—C16B | 112.4 (2) |
C20A—C17A—C13A | 118.7 (2) | C20B—C17B—C13B | 118.7 (2) |
C16A—C17A—C13A | 104.1 (2) | C16B—C17B—C13B | 103.7 (2) |
C20A—C17A—H17A | 106.8 | C20B—C17B—H17B | 107.1 |
C16A—C17A—H17A | 106.8 | C16B—C17B—H17B | 107.1 |
C13A—C17A—H17A | 106.8 | C13B—C17B—H17B | 107.1 |
C10A—C18A—H18A | 109.5 | C10B—C18B—H18D | 109.5 |
C10A—C18A—H18B | 109.5 | C10B—C18B—H18E | 109.5 |
H18A—C18A—H18B | 109.5 | H18D—C18B—H18E | 109.5 |
C10A—C18A—H18C | 109.5 | C10B—C18B—H18F | 109.5 |
H18A—C18A—H18C | 109.5 | H18D—C18B—H18F | 109.5 |
H18B—C18A—H18C | 109.5 | H18E—C18B—H18F | 109.5 |
C13A—C19A—H19A | 109.5 | C13B—C19B—H19D | 109.5 |
C13A—C19A—H19B | 109.5 | C13B—C19B—H19E | 109.5 |
H19A—C19A—H19B | 109.5 | H19D—C19B—H19E | 109.5 |
C13A—C19A—H19C | 109.5 | C13B—C19B—H19F | 109.5 |
H19A—C19A—H19C | 109.5 | H19D—C19B—H19F | 109.5 |
H19B—C19A—H19C | 109.5 | H19E—C19B—H19F | 109.5 |
C21A—C20A—C22A | 110.5 (2) | C21B—C20B—C22B | 110.2 (2) |
C21A—C20A—C17A | 111.5 (2) | C21B—C20B—C17B | 111.3 (2) |
C22A—C20A—C17A | 111.4 (2) | C22B—C20B—C17B | 111.8 (2) |
C21A—C20A—H20A | 107.7 | C21B—C20B—H20B | 107.8 |
C22A—C20A—H20A | 107.7 | C22B—C20B—H20B | 107.8 |
C17A—C20A—H20A | 107.7 | C17B—C20B—H20B | 107.8 |
C20A—C21A—H21A | 109.5 | C20B—C21B—H21D | 109.5 |
C20A—C21A—H21B | 109.5 | C20B—C21B—H21E | 109.5 |
H21A—C21A—H21B | 109.5 | H21D—C21B—H21E | 109.5 |
C20A—C21A—H21C | 109.5 | C20B—C21B—H21F | 109.5 |
H21A—C21A—H21C | 109.5 | H21D—C21B—H21F | 109.5 |
H21B—C21A—H21C | 109.5 | H21E—C21B—H21F | 109.5 |
C23A—C22A—C20A | 114.5 (2) | C23B—C22B—C20B | 113.3 (2) |
C23A—C22A—H22A | 108.6 | C23B—C22B—H22C | 108.9 |
C20A—C22A—H22A | 108.6 | C20B—C22B—H22C | 108.9 |
C23A—C22A—H22B | 108.6 | C23B—C22B—H22D | 108.9 |
C20A—C22A—H22B | 108.6 | C20B—C22B—H22D | 108.9 |
H22A—C22A—H22B | 107.6 | H22C—C22B—H22D | 107.7 |
C24A—C23A—C22A | 114.6 (2) | C22B—C23B—C24B | 114.2 (2) |
C24A—C23A—H23A | 108.6 | C22B—C23B—H23C | 108.7 |
C22A—C23A—H23A | 108.6 | C24B—C23B—H23C | 108.7 |
C24A—C23A—H23B | 108.6 | C22B—C23B—H23D | 108.7 |
C22A—C23A—H23B | 108.6 | C24B—C23B—H23D | 108.7 |
H23A—C23A—H23B | 107.6 | H23C—C23B—H23D | 107.6 |
C23A—C24A—C25A | 115.7 (2) | C25B—C24B—C23B | 114.4 (2) |
C23A—C24A—H24A | 108.4 | C25B—C24B—H24C | 108.7 |
C25A—C24A—H24A | 108.4 | C23B—C24B—H24C | 108.7 |
C23A—C24A—H24B | 108.4 | C25B—C24B—H24D | 108.7 |
C25A—C24A—H24B | 108.4 | C23B—C24B—H24D | 108.7 |
H24A—C24A—H24B | 107.4 | H24C—C24B—H24D | 107.6 |
C26A—C25A—C24A | 112.7 (2) | C26B—C25B—C27B | 109.7 (2) |
C26A—C25A—C27A | 110.3 (2) | C26B—C25B—C24B | 111.9 (2) |
C24A—C25A—C27A | 110.7 (2) | C27B—C25B—C24B | 110.9 (2) |
C26A—C25A—H25A | 107.6 | C26B—C25B—H25B | 108.1 |
C24A—C25A—H25A | 107.6 | C27B—C25B—H25B | 108.1 |
C27A—C25A—H25A | 107.6 | C24B—C25B—H25B | 108.1 |
C25A—C26A—H26A | 109.5 | C25B—C26B—H26D | 109.5 |
C25A—C26A—H26B | 109.5 | C25B—C26B—H26E | 109.5 |
H26A—C26A—H26B | 109.5 | H26D—C26B—H26E | 109.5 |
C25A—C26A—H26C | 109.5 | C25B—C26B—H26F | 109.5 |
H26A—C26A—H26C | 109.5 | H26D—C26B—H26F | 109.5 |
H26B—C26A—H26C | 109.5 | H26E—C26B—H26F | 109.5 |
C25A—C27A—H27A | 109.5 | C25B—C27B—H27D | 109.5 |
C25A—C27A—H27B | 109.5 | C25B—C27B—H27E | 109.5 |
H27A—C27A—H27B | 109.5 | H27D—C27B—H27E | 109.5 |
C25A—C27A—H27C | 109.5 | C25B—C27B—H27F | 109.5 |
H27A—C27A—H27C | 109.5 | H27D—C27B—H27F | 109.5 |
H27B—C27A—H27C | 109.5 | H27E—C27B—H27F | 109.5 |
C10A—C1A—C2A—C3A | −57.0 (3) | C10B—C1B—C2B—C3B | −55.4 (3) |
C1A—C2A—C3A—C4A | 55.8 (3) | C1B—C2B—C3B—C4B | 53.5 (3) |
C2A—C3A—C4A—C5A | −55.5 (3) | C2B—C3B—C4B—C5B | −54.0 (3) |
C3A—C4A—C5A—C6A | −175.7 (2) | C3B—C4B—C5B—C6B | −174.5 (2) |
C3A—C4A—C5A—C10A | 55.8 (3) | C3B—C4B—C5B—C10B | 55.8 (3) |
C4A—C5A—C6A—C7A | 172.4 (2) | C4B—C5B—C6B—C7B | 173.6 (2) |
C10A—C5A—C6A—C7A | −58.2 (3) | C10B—C5B—C6B—C7B | −56.7 (3) |
C5A—C6A—C7A—C8A | 52.0 (3) | C5B—C6B—C7B—C8B | 52.5 (3) |
C6A—C7A—C8A—C14A | −170.1 (2) | C6B—C7B—C8B—C14B | −173.6 (2) |
C6A—C7A—C8A—C9A | −48.8 (3) | C6B—C7B—C8B—C9B | −51.9 (3) |
C14A—C8A—C9A—C11A | −54.6 (3) | C14B—C8B—C9B—C11B | −52.1 (3) |
C7A—C8A—C9A—C11A | −177.3 (2) | C7B—C8B—C9B—C11B | −175.6 (2) |
C14A—C8A—C9A—C10A | 175.4 (2) | C14B—C8B—C9B—C10B | 178.7 (2) |
C7A—C8A—C9A—C10A | 52.7 (3) | C7B—C8B—C9B—C10B | 55.3 (3) |
C2A—C1A—C10A—C18A | −68.0 (3) | C2B—C1B—C10B—C18B | −67.0 (3) |
C2A—C1A—C10A—C5A | 53.9 (3) | C2B—C1B—C10B—C5B | 54.4 (3) |
C2A—C1A—C10A—C9A | 170.4 (2) | C2B—C1B—C10B—C9B | 170.8 (2) |
C6A—C5A—C10A—C18A | −62.3 (3) | C6B—C5B—C10B—C1B | 175.8 (2) |
C4A—C5A—C10A—C18A | 66.9 (3) | C4B—C5B—C10B—C1B | −54.7 (3) |
C6A—C5A—C10A—C1A | 177.8 (2) | C6B—C5B—C10B—C18B | −64.3 (3) |
C4A—C5A—C10A—C1A | −53.0 (3) | C4B—C5B—C10B—C18B | 65.2 (3) |
C6A—C5A—C10A—C9A | 59.6 (3) | C6B—C5B—C10B—C9B | 57.6 (3) |
C4A—C5A—C10A—C9A | −171.2 (2) | C4B—C5B—C10B—C9B | −172.9 (2) |
C11A—C9A—C10A—C18A | −62.3 (3) | C11B—C9B—C10B—C1B | 58.8 (3) |
C8A—C9A—C10A—C18A | 65.5 (3) | C8B—C9B—C10B—C1B | −173.7 (2) |
C11A—C9A—C10A—C1A | 58.2 (3) | C11B—C9B—C10B—C18B | −62.3 (3) |
C8A—C9A—C10A—C1A | −174.0 (2) | C8B—C9B—C10B—C18B | 65.2 (3) |
C11A—C9A—C10A—C5A | 175.1 (2) | C11B—C9B—C10B—C5B | 175.7 (2) |
C8A—C9A—C10A—C5A | −57.1 (3) | C8B—C9B—C10B—C5B | −56.8 (3) |
C8A—C9A—C11A—C12A | 53.9 (3) | C8B—C9B—C11B—C12B | 50.9 (3) |
C10A—C9A—C11A—C12A | −176.9 (2) | C10B—C9B—C11B—C12B | 179.2 (2) |
C9A—C11A—C12A—C13A | −55.4 (3) | C9B—C11B—C12B—C13B | −54.0 (3) |
C11A—C12A—C13A—C19A | −66.7 (3) | C11B—C12B—C13B—C19B | −66.0 (3) |
C11A—C12A—C13A—C14A | 54.8 (3) | C11B—C12B—C13B—C14B | 55.6 (3) |
C11A—C12A—C13A—C17A | 166.1 (2) | C11B—C12B—C13B—C17B | 166.8 (2) |
C7A—C8A—C14A—C15A | −52.4 (3) | C7B—C8B—C14B—C15B | −52.7 (3) |
C9A—C8A—C14A—C15A | −175.4 (2) | C9B—C8B—C14B—C15B | −175.8 (2) |
C7A—C8A—C14A—C13A | −177.0 (2) | C7B—C8B—C14B—C13B | −176.3 (2) |
C9A—C8A—C14A—C13A | 60.1 (3) | C9B—C8B—C14B—C13B | 60.5 (3) |
C12A—C13A—C14A—C15A | 168.4 (2) | C19B—C13B—C14B—C8B | 60.0 (3) |
C19A—C13A—C14A—C15A | −70.7 (3) | C12B—C13B—C14B—C8B | −61.2 (3) |
C17A—C13A—C14A—C15A | 45.7 (2) | C17B—C13B—C14B—C8B | 176.6 (2) |
C12A—C13A—C14A—C8A | −59.1 (3) | C19B—C13B—C14B—C15B | −70.8 (3) |
C19A—C13A—C14A—C8A | 61.7 (3) | C12B—C13B—C14B—C15B | 168.0 (2) |
C17A—C13A—C14A—C8A | 178.2 (2) | C17B—C13B—C14B—C15B | 45.8 (2) |
C8A—C14A—C15A—C16A | −165.7 (2) | C8B—C14B—C15B—C16B | −164.1 (2) |
C13A—C14A—C15A—C16A | −36.5 (3) | C13B—C14B—C15B—C16B | −35.6 (3) |
C14A—C15A—C16A—C17A | 12.7 (3) | C14B—C15B—C16B—C17B | 11.4 (3) |
C15A—C16A—C17A—C20A | 145.6 (2) | C15B—C16B—C17B—C20B | 145.9 (2) |
C15A—C16A—C17A—C13A | 15.4 (3) | C15B—C16B—C17B—C13B | 16.4 (3) |
C12A—C13A—C17A—C20A | 81.9 (3) | C19B—C13B—C17B—C20B | −44.9 (3) |
C19A—C13A—C17A—C20A | −45.7 (3) | C12B—C13B—C17B—C20B | 83.0 (3) |
C14A—C13A—C17A—C20A | −163.4 (2) | C14B—C13B—C17B—C20B | −162.9 (2) |
C12A—C13A—C17A—C16A | −151.4 (2) | C19B—C13B—C17B—C16B | 80.7 (3) |
C19A—C13A—C17A—C16A | 81.0 (2) | C12B—C13B—C17B—C16B | −151.4 (2) |
C14A—C13A—C17A—C16A | −36.7 (2) | C14B—C13B—C17B—C16B | −37.4 (2) |
C16A—C17A—C20A—C21A | −178.8 (2) | C16B—C17B—C20B—C21B | −179.0 (2) |
C13A—C17A—C20A—C21A | −56.5 (3) | C13B—C17B—C20B—C21B | −57.8 (3) |
C16A—C17A—C20A—C22A | 57.2 (3) | C16B—C17B—C20B—C22B | 57.2 (3) |
C13A—C17A—C20A—C22A | 179.5 (2) | C13B—C17B—C20B—C22B | 178.5 (2) |
C21A—C20A—C22A—C23A | 62.1 (3) | C21B—C20B—C22B—C23B | 63.1 (3) |
C17A—C20A—C22A—C23A | −173.3 (2) | C17B—C20B—C22B—C23B | −172.5 (2) |
C20A—C22A—C23A—C24A | 177.6 (2) | C20B—C22B—C23B—C24B | 177.6 (2) |
C22A—C23A—C24A—C25A | −178.1 (2) | C22B—C23B—C24B—C25B | 178.5 (2) |
C23A—C24A—C25A—C26A | −65.3 (3) | C23B—C24B—C25B—C26B | −63.6 (3) |
C23A—C24A—C25A—C27A | 170.6 (2) |