Supporting information
Crystallographic Information File (CIF) https://doi.org/10.1107/S1600536806009421/br2001sup1.cif | |
Structure factor file (CIF format) https://doi.org/10.1107/S1600536806009421/br2001Isup2.hkl |
Data collection: COLLECT (Nonius, 2000); cell refinement: SCALEPACK (Otwinowski & Minor, 1997); data reduction: DENZO and SCALEPACK (Otwinowski & Minor, 1997); program(s) used to solve structure: SIR97 (Altomare et al., 1999); program(s) used to refine structure: SHELXL97 (Sheldrick, 1997); molecular graphics: CrystalMaker (Palmer, 2003); software used to prepare material for publication: SHELXL97 and enCIFer (Allen et al., 2004).
LaPdSb3 | F(000) = 2048 |
Mr = 610.56 | Dx = 7.913 Mg m−3 |
Orthorhombic, Pbcm | Mo Kα radiation, λ = 0.71073 Å |
Hall symbol: -P 2c 2b | Cell parameters from 1722 reflections |
a = 12.9210 (4) Å | θ = 1.0–30.0° |
b = 6.3450 (9) Å | µ = 27.02 mm−1 |
c = 12.5030 (9) Å | T = 298 K |
V = 1025.04 (17) Å3 | Plate-shaped fragment, silver |
Z = 8 | 0.10 × 0.10 × 0.08 mm |
Nonius KappaCCD area-detector diffractometer | 1557 independent reflections |
Radiation source: fine-focus sealed tube | 1016 reflections with I > 2σ(I) |
Graphite monochromator | Rint = 0.063 |
ω scans with κ offsets | θmax = 30.0°, θmin = 3.2° |
Absorption correction: multi-scan (SCALEPACK; Otwinowski & Minor 1997) | h = −18→18 |
Tmin = 0.092, Tmax = 0.12 | k = −8→8 |
2790 measured reflections | l = −17→17 |
Refinement on F2 | 0 restraints |
Least-squares matrix: full | Primary atom site location: structure-invariant direct methods |
R[F2 > 2σ(F2)] = 0.045 | Secondary atom site location: difference Fourier map |
wR(F2) = 0.101 | w = 1/[σ2(Fo2) + (0.0401P)2 + P] where P = (Fo2 + 2Fc2)/3 |
S = 1.08 | (Δ/σ)max < 0.001 |
1557 reflections | Δρmax = 2.98 e Å−3 |
52 parameters | Δρmin = −3.60 e Å−3 |
Geometry. All e.s.d.'s (except the e.s.d. in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell e.s.d.'s are taken into account individually in the estimation of e.s.d.'s in distances, angles and torsion angles; correlations between e.s.d.'s in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell e.s.d.'s is used for estimating e.s.d.'s involving l.s. planes. |
Refinement. Refinement of F2 against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F2, conventional R-factors R are based on F, with F set to zero for negative F2. The threshold expression of F2 > σ(F2) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F2 are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger. |
x | y | z | Uiso*/Ueq | ||
La1 | 0.69911 (8) | 0.2500 | 0.0000 | 0.0135 (2) | |
La2 | 0.30822 (8) | 0.27465 (17) | 0.7500 | 0.0142 (2) | |
Pd1 | 0.10190 (7) | 0.04698 (16) | 0.86576 (8) | 0.0180 (2) | |
Sb1 | 0.97485 (9) | 0.2500 | 0.0000 | 0.0168 (3) | |
Sb2 | 0.77702 (9) | 0.26349 (19) | 0.7500 | 0.0155 (3) | |
Sb3 | 0.50307 (6) | 0.51265 (13) | 0.87810 (6) | 0.0156 (2) | |
Sb4 | 0.23292 (9) | 0.2500 | 0.0000 | 0.0150 (3) | |
Sb5 | 0.93811 (9) | 0.92186 (19) | 0.7500 | 0.0164 (3) |
U11 | U22 | U33 | U12 | U13 | U23 | |
La1 | 0.0113 (5) | 0.0151 (5) | 0.0140 (5) | 0.000 | 0.000 | −0.0002 (4) |
La2 | 0.0116 (5) | 0.0158 (6) | 0.0153 (5) | −0.0001 (4) | 0.000 | 0.000 |
Pd1 | 0.0148 (5) | 0.0218 (6) | 0.0172 (5) | −0.0012 (4) | −0.0003 (4) | −0.0013 (4) |
Sb1 | 0.0169 (6) | 0.0154 (7) | 0.0181 (6) | 0.000 | 0.000 | 0.0006 (5) |
Sb2 | 0.0155 (6) | 0.0160 (7) | 0.0151 (6) | −0.0003 (5) | 0.000 | 0.000 |
Sb3 | 0.0121 (4) | 0.0183 (5) | 0.0166 (4) | 0.0000 (3) | 0.0000 (3) | −0.0001 (3) |
Sb4 | 0.0146 (6) | 0.0153 (6) | 0.0150 (6) | 0.000 | 0.000 | 0.0000 (5) |
Sb5 | 0.0122 (6) | 0.0172 (7) | 0.0199 (6) | 0.0003 (5) | 0.000 | 0.000 |
La1—Sb2i | 3.2850 (5) | Sb1—Pd1xviii | 2.6779 (12) |
La1—Sb2ii | 3.2850 (5) | Sb1—Pd1vii | 2.7113 (11) |
La1—Sb4iii | 3.2918 (6) | Sb1—Pd1viii | 2.7113 (11) |
La1—Sb4iv | 3.2919 (6) | Sb1—Sb1xix | 3.2384 (7) |
La1—Sb3v | 3.3787 (11) | Sb1—Sb1xx | 3.2384 (7) |
La1—Sb3vi | 3.3787 (11) | Sb2—Pd1xi | 2.7889 (14) |
La1—Sb3i | 3.3936 (11) | Sb2—Pd1xxi | 2.7889 (14) |
La1—Sb3ii | 3.3936 (11) | Sb2—Sb5xxii | 3.0052 (17) |
La1—Sb1 | 3.5629 (15) | Sb2—La1ix | 3.2850 (5) |
La1—Pd1vii | 3.6026 (12) | Sb2—La1x | 3.2850 (5) |
La1—Pd1viii | 3.6026 (12) | Sb2—La2xii | 3.2915 (17) |
La2—Sb4ix | 3.2774 (5) | Sb2—La2xi | 3.4252 (17) |
La2—Sb4x | 3.2774 (5) | Sb3—Sb3xxiii | 3.0535 (16) |
La2—Sb2xi | 3.2915 (17) | Sb3—Sb3xii | 3.1735 (13) |
La2—Sb5xii | 3.3170 (15) | Sb3—Sb3xi | 3.1735 (13) |
La2—Sb3xiii | 3.3443 (12) | Sb3—Sb3xiii | 3.2032 (16) |
La2—Sb3 | 3.3443 (12) | Sb3—La2xi | 3.3577 (12) |
La2—Sb3xii | 3.3576 (12) | Sb3—La1vi | 3.3787 (11) |
La2—Sb3xiv | 3.3576 (12) | Sb3—La1x | 3.3935 (11) |
La2—Pd1 | 3.3598 (13) | Sb4—Pd1i | 2.7097 (12) |
La2—Pd1xiii | 3.3598 (13) | Sb4—Pd1ii | 2.7097 (12) |
La2—Sb2xii | 3.4252 (17) | Sb4—La2i | 3.2774 (5) |
Pd1—Sb1xv | 2.6779 (12) | Sb4—La2ii | 3.2774 (5) |
Pd1—Sb5xvi | 2.6840 (14) | Sb4—La1iii | 3.2918 (6) |
Pd1—Sb4x | 2.7097 (13) | Sb4—La1iv | 3.2918 (6) |
Pd1—Sb1viii | 2.7113 (11) | Sb5—Pd1xxiv | 2.6840 (14) |
Pd1—Sb2xii | 2.7888 (14) | Sb5—Pd1xxv | 2.6840 (14) |
Pd1—Sb5xii | 2.8320 (15) | Sb5—Pd1xxi | 2.8320 (15) |
Pd1—Pd1xiii | 2.895 (2) | Sb5—Pd1xi | 2.8320 (15) |
Pd1—La1viii | 3.6026 (12) | Sb5—Sb2xxvi | 3.0052 (17) |
Sb1—Pd1xvii | 2.6779 (12) | Sb5—La2xi | 3.3171 (15) |
Sb2i—La1—Sb2ii | 144.31 (5) | Sb1viii—Pd1—Sb5xii | 146.44 (5) |
Sb2i—La1—Sb4iii | 83.86 (2) | Sb2xii—Pd1—Sb5xii | 112.27 (4) |
Sb2ii—La1—Sb4iii | 86.75 (2) | Sb1xv—Pd1—Pd1xiii | 128.81 (2) |
Sb2i—La1—Sb4iv | 86.75 (2) | Sb5xvi—Pd1—Pd1xiii | 57.37 (2) |
Sb2ii—La1—Sb4iv | 83.86 (2) | Sb4x—Pd1—Pd1xiii | 128.27 (2) |
Sb4iii—La1—Sb4iv | 149.05 (5) | Sb1viii—Pd1—Pd1xiii | 128.25 (2) |
Sb2i—La1—Sb3v | 130.89 (3) | Sb2xii—Pd1—Pd1xiii | 58.74 (2) |
Sb2ii—La1—Sb3v | 79.59 (2) | Sb5xii—Pd1—Pd1xiii | 59.26 (2) |
Sb4iii—La1—Sb3v | 77.10 (2) | Sb1xv—Pd1—La2 | 123.34 (4) |
Sb4iv—La1—Sb3v | 129.48 (3) | Sb5xvi—Pd1—La2 | 121.37 (4) |
Sb2i—La1—Sb3vi | 79.59 (2) | Sb4x—Pd1—La2 | 64.32 (3) |
Sb2ii—La1—Sb3vi | 130.89 (3) | Sb1viii—Pd1—La2 | 148.84 (5) |
Sb4iii—La1—Sb3vi | 129.48 (3) | Sb2xii—Pd1—La2 | 66.96 (4) |
Sb4iv—La1—Sb3vi | 77.10 (2) | Sb5xii—Pd1—La2 | 64.12 (3) |
Sb3v—La1—Sb3vi | 78.72 (3) | Pd1xiii—Pd1—La2 | 64.483 (18) |
Sb2i—La1—Sb3i | 77.79 (2) | Sb1xv—Pd1—La1viii | 113.40 (3) |
Sb2ii—La1—Sb3i | 131.98 (3) | Sb5xvi—Pd1—La1viii | 131.24 (4) |
Sb4iii—La1—Sb3i | 74.09 (2) | Sb4x—Pd1—La1viii | 60.93 (2) |
Sb4iv—La1—Sb3i | 132.25 (3) | Sb1viii—Pd1—La1viii | 66.99 (3) |
Sb3v—La1—Sb3i | 53.60 (3) | Sb2xii—Pd1—La1viii | 60.27 (2) |
Sb3vi—La1—Sb3i | 55.886 (16) | Sb5xii—Pd1—La1viii | 143.87 (4) |
Sb2i—La1—Sb3ii | 131.98 (3) | Pd1xiii—Pd1—La1viii | 117.768 (16) |
Sb2ii—La1—Sb3ii | 77.79 (2) | La2—Pd1—La1viii | 81.91 (3) |
Sb4iii—La1—Sb3ii | 132.25 (3) | Pd1xvii—Sb1—Pd1xviii | 104.39 (6) |
Sb4iv—La1—Sb3ii | 74.09 (2) | Pd1xvii—Sb1—Pd1vii | 106.13 (3) |
Sb3v—La1—Sb3ii | 55.886 (16) | Pd1xviii—Sb1—Pd1vii | 99.82 (4) |
Sb3vi—La1—Sb3ii | 53.60 (3) | Pd1xvii—Sb1—Pd1viii | 99.82 (4) |
Sb3i—La1—Sb3ii | 83.44 (4) | Pd1xviii—Sb1—Pd1viii | 106.13 (3) |
Sb2i—La1—Sb1 | 72.16 (2) | Pd1vii—Sb1—Pd1viii | 137.09 (6) |
Sb2ii—La1—Sb1 | 72.16 (2) | Pd1xvii—Sb1—Sb1xix | 110.38 (5) |
Sb4iii—La1—Sb1 | 74.53 (3) | Pd1xviii—Sb1—Sb1xix | 53.54 (3) |
Sb4iv—La1—Sb1 | 74.53 (3) | Pd1vii—Sb1—Sb1xix | 138.96 (3) |
Sb3v—La1—Sb1 | 140.642 (17) | Pd1viii—Sb1—Sb1xix | 52.59 (3) |
Sb3vi—La1—Sb1 | 140.641 (17) | Pd1xvii—Sb1—Sb1xx | 53.54 (3) |
Sb3i—La1—Sb1 | 138.281 (18) | Pd1xviii—Sb1—Sb1xx | 110.38 (5) |
Sb3ii—La1—Sb1 | 138.281 (18) | Pd1vii—Sb1—Sb1xx | 52.59 (3) |
Sb2i—La1—Pd1vii | 103.78 (3) | Pd1viii—Sb1—Sb1xx | 138.96 (3) |
Sb2ii—La1—Pd1vii | 47.50 (3) | Sb1xix—Sb1—Sb1xx | 156.85 (8) |
Sb4iii—La1—Pd1vii | 108.28 (3) | Pd1xvii—Sb1—La1 | 127.81 (3) |
Sb4iv—La1—Pd1vii | 46.01 (2) | Pd1xviii—Sb1—La1 | 127.81 (3) |
Sb3v—La1—Pd1vii | 125.09 (2) | Pd1vii—Sb1—La1 | 68.55 (3) |
Sb3vi—La1—Pd1vii | 121.93 (2) | Pd1viii—Sb1—La1 | 68.55 (3) |
Sb3i—La1—Pd1vii | 177.21 (3) | Sb1xix—Sb1—La1 | 101.58 (4) |
Sb3ii—La1—Pd1vii | 93.82 (2) | Sb1xx—Sb1—La1 | 101.58 (4) |
Sb1—La1—Pd1vii | 44.463 (19) | Pd1xi—Sb2—Pd1xxi | 62.53 (5) |
Sb2i—La1—Pd1viii | 47.50 (3) | Pd1xi—Sb2—Sb5xxii | 94.40 (4) |
Sb2ii—La1—Pd1viii | 103.78 (3) | Pd1xxi—Sb2—Sb5xxii | 94.40 (4) |
Sb4iii—La1—Pd1viii | 46.01 (2) | Pd1xi—Sb2—La1ix | 133.04 (4) |
Sb4iv—La1—Pd1viii | 108.28 (3) | Pd1xxi—Sb2—La1ix | 72.24 (2) |
Sb3v—La1—Pd1viii | 121.93 (2) | Sb5xxii—Sb2—La1ix | 101.16 (3) |
Sb3vi—La1—Pd1viii | 125.09 (2) | Pd1xi—Sb2—La1x | 72.24 (2) |
Sb3i—La1—Pd1viii | 93.82 (2) | Pd1xxi—Sb2—La1x | 133.04 (4) |
Sb3ii—La1—Pd1viii | 177.21 (3) | Sb5xxii—Sb2—La1x | 101.16 (3) |
Sb1—La1—Pd1viii | 44.463 (19) | La1ix—Sb2—La1x | 144.17 (5) |
Pd1vii—La1—Pd1viii | 88.93 (4) | Pd1xi—Sb2—La2xii | 142.70 (4) |
Sb4ix—La2—Sb4x | 145.00 (5) | Pd1xxi—Sb2—La2xii | 142.70 (4) |
Sb4ix—La2—Sb2xi | 86.88 (2) | Sb5xxii—Sb2—La2xii | 63.39 (4) |
Sb4x—La2—Sb2xi | 86.88 (2) | La1ix—Sb2—La2xii | 82.70 (2) |
Sb4ix—La2—Sb5xii | 74.25 (3) | La1x—Sb2—La2xii | 82.70 (2) |
Sb4x—La2—Sb5xii | 74.25 (3) | Pd1xi—Sb2—La2xi | 64.51 (3) |
Sb2xi—La2—Sb5xii | 54.09 (3) | Pd1xxi—Sb2—La2xi | 64.51 (3) |
Sb4ix—La2—Sb3xiii | 77.78 (2) | Sb5xxii—Sb2—La2xi | 154.92 (5) |
Sb4x—La2—Sb3xiii | 134.57 (3) | La1ix—Sb2—La2xi | 85.76 (2) |
Sb2xi—La2—Sb3xiii | 80.00 (3) | La1x—Sb2—La2xi | 85.76 (2) |
Sb5xii—La2—Sb3xiii | 126.53 (4) | La2xii—Sb2—La2xi | 141.69 (5) |
Sb4ix—La2—Sb3 | 134.57 (3) | Sb3xxiii—Sb3—Sb3xii | 86.95 (3) |
Sb4x—La2—Sb3 | 77.78 (2) | Sb3xxiii—Sb3—Sb3xi | 92.98 (3) |
Sb2xi—La2—Sb3 | 80.00 (3) | Sb3xii—Sb3—Sb3xi | 177.13 (6) |
Sb5xii—La2—Sb3 | 126.53 (4) | Sb3xxiii—Sb3—Sb3xiii | 176.64 (3) |
Sb3xiii—La2—Sb3 | 57.23 (3) | Sb3xii—Sb3—Sb3xiii | 90.0 |
Sb4ix—La2—Sb3xii | 130.31 (3) | Sb3xi—Sb3—Sb3xiii | 89.999 (1) |
Sb4x—La2—Sb3xii | 74.75 (2) | Sb3xxiii—Sb3—La2 | 115.77 (4) |
Sb2xi—La2—Sb3xii | 135.20 (3) | Sb3xii—Sb3—La2 | 61.95 (3) |
Sb5xii—La2—Sb3xii | 146.74 (3) | Sb3xi—Sb3—La2 | 115.63 (4) |
Sb3xiii—La2—Sb3xii | 84.57 (3) | Sb3xiii—Sb3—La2 | 61.386 (16) |
Sb3—La2—Sb3xii | 56.525 (17) | Sb3xxiii—Sb3—La2xi | 121.40 (4) |
Sb4ix—La2—Sb3xiv | 74.75 (2) | Sb3xii—Sb3—La2xi | 120.87 (4) |
Sb4x—La2—Sb3xiv | 130.31 (3) | Sb3xi—Sb3—La2xi | 61.52 (3) |
Sb2xi—La2—Sb3xiv | 135.20 (3) | Sb3xiii—Sb3—La2xi | 61.510 (16) |
Sb5xii—La2—Sb3xiv | 146.74 (3) | La2—Sb3—La2xi | 122.81 (3) |
Sb3xiii—La2—Sb3xiv | 56.526 (17) | Sb3xxiii—Sb3—La1vi | 63.45 (3) |
Sb3—La2—Sb3xiv | 84.57 (3) | Sb3xii—Sb3—La1vi | 115.23 (3) |
Sb3xii—La2—Sb3xiv | 56.98 (3) | Sb3xi—Sb3—La1vi | 62.29 (2) |
Sb4ix—La2—Pd1 | 98.90 (3) | Sb3xiii—Sb3—La1vi | 116.814 (15) |
Sb4x—La2—Pd1 | 48.17 (3) | La2—Sb3—La1vi | 80.52 (3) |
Sb2xi—La2—Pd1 | 98.03 (4) | La2xi—Sb3—La1vi | 123.78 (3) |
Sb5xii—La2—Pd1 | 50.19 (3) | Sb3xxiii—Sb3—La1x | 62.95 (3) |
Sb3xiii—La2—Pd1 | 176.18 (3) | Sb3xii—Sb3—La1x | 61.82 (2) |
Sb3—La2—Pd1 | 125.82 (2) | Sb3xi—Sb3—La1x | 120.64 (3) |
Sb3xii—La2—Pd1 | 99.08 (3) | Sb3xiii—Sb3—La1x | 116.688 (15) |
Sb3xiv—La2—Pd1 | 124.67 (4) | La2—Sb3—La1x | 123.73 (3) |
Sb4ix—La2—Pd1xiii | 48.17 (3) | La2xi—Sb3—La1x | 85.14 (3) |
Sb4x—La2—Pd1xiii | 98.90 (3) | La1vi—Sb3—La1x | 126.40 (3) |
Sb2xi—La2—Pd1xiii | 98.03 (4) | Pd1i—Sb4—Pd1ii | 102.67 (6) |
Sb5xii—La2—Pd1xiii | 50.19 (3) | Pd1i—Sb4—La2i | 67.51 (3) |
Sb3xiii—La2—Pd1xiii | 125.82 (2) | Pd1ii—Sb4—La2i | 138.90 (3) |
Sb3—La2—Pd1xiii | 176.18 (3) | Pd1i—Sb4—La2ii | 138.90 (3) |
Sb3xii—La2—Pd1xiii | 124.67 (4) | Pd1ii—Sb4—La2ii | 67.51 (3) |
Sb3xiv—La2—Pd1xiii | 99.08 (3) | La2i—Sb4—La2ii | 145.46 (5) |
Pd1—La2—Pd1xiii | 51.03 (4) | Pd1i—Sb4—La1iii | 128.67 (3) |
Sb4ix—La2—Sb2xii | 81.92 (2) | Pd1ii—Sb4—La1iii | 73.05 (3) |
Sb4x—La2—Sb2xii | 81.92 (2) | La2i—Sb4—La1iii | 82.81 (2) |
Sb2xi—La2—Sb2xii | 141.69 (5) | La2ii—Sb4—La1iii | 88.10 (2) |
Sb5xii—La2—Sb2xii | 87.60 (4) | Pd1i—Sb4—La1iv | 73.05 (3) |
Sb3xiii—La2—Sb2xii | 132.04 (3) | Pd1ii—Sb4—La1iv | 128.67 (3) |
Sb3—La2—Sb2xii | 132.04 (3) | La2i—Sb4—La1iv | 88.10 (2) |
Sb3xii—La2—Sb2xii | 76.39 (3) | La2ii—Sb4—La1iv | 82.81 (2) |
Sb3xiv—La2—Sb2xii | 76.39 (3) | La1iii—Sb4—La1iv | 149.05 (5) |
Pd1—La2—Sb2xii | 48.53 (3) | Pd1xxiv—Sb5—Pd1xxv | 65.27 (5) |
Pd1xiii—La2—Sb2xii | 48.53 (3) | Pd1xxiv—Sb5—Pd1xxi | 131.91 (5) |
Sb1xv—Pd1—Sb5xvi | 89.82 (4) | Pd1xxv—Sb5—Pd1xxi | 96.71 (4) |
Sb1xv—Pd1—Sb4x | 76.47 (4) | Pd1xxiv—Sb5—Pd1xi | 96.71 (4) |
Sb5xvi—Pd1—Sb4x | 165.30 (5) | Pd1xxv—Sb5—Pd1xi | 131.91 (5) |
Sb1xv—Pd1—Sb1viii | 73.87 (3) | Pd1xxi—Sb5—Pd1xi | 61.47 (5) |
Sb5xvi—Pd1—Sb1viii | 80.78 (4) | Pd1xxiv—Sb5—Sb2xxvi | 109.44 (5) |
Sb4x—Pd1—Sb1viii | 100.11 (4) | Pd1xxv—Sb5—Sb2xxvi | 109.44 (5) |
Sb1xv—Pd1—Sb2xii | 168.35 (5) | Pd1xxi—Sb5—Sb2xxvi | 118.65 (4) |
Sb5xvi—Pd1—Sb2xii | 88.38 (4) | Pd1xi—Sb5—Sb2xxvi | 118.65 (4) |
Sb4x—Pd1—Sb2xii | 106.12 (4) | Pd1xxiv—Sb5—La2xi | 147.13 (3) |
Sb1viii—Pd1—Sb2xii | 94.49 (4) | Pd1xxv—Sb5—La2xi | 147.13 (3) |
Sb1xv—Pd1—Sb5xii | 78.72 (3) | Pd1xxi—Sb5—La2xi | 65.69 (3) |
Sb5xvi—Pd1—Sb5xii | 80.15 (3) | Pd1xi—Sb5—La2xi | 65.69 (3) |
Sb4x—Pd1—Sb5xii | 91.79 (4) | Sb2xxvi—Sb5—La2xi | 62.52 (4) |
Symmetry codes: (i) x, −y+1/2, −z+1; (ii) x, y, z−1; (iii) −x+1, −y, −z; (iv) −x+1, −y+1, −z; (v) −x+1, y−1/2, z−1; (vi) −x+1, −y+1, −z+1; (vii) −x+1, y+1/2, z−1; (viii) −x+1, −y, −z+1; (ix) x, y, −z+1/2; (x) x, y, z+1; (xi) −x+1, y+1/2, z; (xii) −x+1, y−1/2, z; (xiii) x, y, −z+3/2; (xiv) −x+1, y−1/2, −z+3/2; (xv) x−1, y, z+1; (xvi) x−1, y−1, z; (xvii) x+1, −y+1/2, −z+1; (xviii) x+1, y, z−1; (xix) −x+2, −y, −z; (xx) −x+2, −y+1, −z; (xxi) −x+1, y+1/2, −z+3/2; (xxii) x, y−1, z; (xxiii) −x+1, −y+1, −z+2; (xxiv) x+1, y+1, z; (xxv) x+1, y+1, −z+3/2; (xxvi) x, y+1, z. |