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Tetramethylammonium trivanadium heptaoxide crystallizes in the monoclinic space group P21/n when prepared hydrothermally. Its structure was solved from conventional X-ray powder diffraction with final R(Bragg) = 0.052, R(prof) = 0.078. Vanadium coordination polyhedra are square pyramids and a tetrahedron which form layers parallel to the bc plane. The tetramethylammonium cations are incorporated between the layers.

Supporting information

cif

Crystallographic Information File (CIF)
Contains datablocks global, tmav3o7

hkl

Structure factor file (CIF format)
Contains datablock tmav3o7

CCDC reference: 128803

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