Download citation
Download citation
link to html
Labuntsovite-Fe, an Fe-dominant member of the labuntsovite subgroup, was first discovered in the Khibiny alkaline massif on Mt Kukisvumchorr [Khomyakov et al. (2001). Zap. Vseross. Mineral. Oba, 130, 36–45]. However, no data are published about the crystal structure of this mineral. Labuntsovite-Fe from a peralkaline pegmatite located on Mt Nyorkpakhk, in the Khibiny alkaline complex, Kola Peninsula, Russia, has been investigated by means of electron microprobe analyses, single-crystal X-ray structure refinement, and IR and Raman spectroscopies. Monoclinic unit-cell parameters of labuntsovite-Fe are: a = 14.2584 (4), b = 13.7541 (6), c = 7.7770 (2) Å, β = 116.893 (3)°; V = 1360.22 (9) Å3; space group C2/m. The structure was refined to final R1 = 0.0467, wR2 = 0.0715 for 3202 reflections [I > 3σ(I)]. The refined crystal chemical formula is (Z = 2): Na2K2Ba0.7[(Fe0.5Ti0.1Mg0.05)(H2O)1.3]{[Ti2(Ti1.9Nb0.1)(O,OH)4]­[Si4O12]2}·4H2O. The high-pressure in situ single-crystal X-ray diffraction study of the labuntsovite-Fe has been carried out in a diamond anvil cell. The labuntsovite-type structure is stable up to 23 GPa and phase transitions are not observed. Calculations using the BM3 equation of state resulted in the bulk modulus K = 72 (2) GPa, K0 = 3.7 (2) and V0 = 1363 (2) Å3. Compressing of the heteropolyhedral zeolite-like framework leads to the deformation of main structural units. Octahedral rods show the gradual increase of distortion and the wave-like character of rods becomes more distinct. Rod deformations result in the distortion of the silicon–oxygen ring which is not equal in different directions. Structural channels are characterized by a different ellipticity–pressure relationship: the cross-section of the largest channel I and channel II demonstrates the stability of the geometrical characteristics which practically do not depend on pressure: [epsilon]channel I ≃ 0.85 (4) (cross-section is rather regular) and [epsilon]channel II ≃ 0.52 (2) within the whole pressure range. However, channel III is characterized by the increasing of ellipticity with pressure ([epsilon] = 0.40 → 0.10).

Supporting information

cif

Crystallographic Information File (CIF) https://doi.org/10.1107/S205252061700498X/bp5093sup1.cif
Contains datablocks labu_Fe_ambient, I, labu-Fe_3.15, labu-Fe_5.15, labu_Fe_7.21, labu-Fe_10.01, labu-Fe_12.59, labu-Fe_16.3, labu_Fe_20.0, labu-Fe_22.53

hkl

Structure factor file (CIF format) https://doi.org/10.1107/S205252061700498X/bp5093Isup2.hkl
Contains datablock I

hkl

Structure factor file (CIF format) https://doi.org/10.1107/S205252061700498X/bp5093labu-Fe_3.15sup3.hkl
Contains datablock I

hkl

Structure factor file (CIF format) https://doi.org/10.1107/S205252061700498X/bp5093labu-Fe_5.15sup4.hkl
Contains datablock I

hkl

Structure factor file (CIF format) https://doi.org/10.1107/S205252061700498X/bp5093labu_Fe_7.21sup5.hkl
Contains datablock I

hkl

Structure factor file (CIF format) https://doi.org/10.1107/S205252061700498X/bp5093labu-Fe_10.01sup6.hkl
Contains datablock I

hkl

Structure factor file (CIF format) https://doi.org/10.1107/S205252061700498X/bp5093labu-Fe_12.59sup7.hkl
Contains datablock I

hkl

Structure factor file (CIF format) https://doi.org/10.1107/S205252061700498X/bp5093labu-Fe_16.3sup8.hkl
Contains datablock I

hkl

Structure factor file (CIF format) https://doi.org/10.1107/S205252061700498X/bp5093labu_Fe_20.0sup9.hkl
Contains datablock I

hkl

Structure factor file (CIF format) https://doi.org/10.1107/S205252061700498X/bp5093labu-Fe_22.53sup10.hkl
Contains datablock I

pdf

Portable Document Format (PDF) file https://doi.org/10.1107/S205252061700498X/bp5093sup11.pdf
Supporting tables

CCDC references: 1541219; 1541220; 1541221; 1541222; 1541223; 1541224; 1541225; 1541226; 1541227

Computing details top

Data collection: CrysAlis PRO, Agilent Technologies, Version 1.171.34.49 (release 20-01-2011 CrysAlis171 .NET) (compiled Jan 20 2011,15:58:25) for (I). Cell refinement: CrysAlis PRO, Agilent Technologies, Version 1.171.34.49 (release 20-01-2011 CrysAlis171 .NET) (compiled Jan 20 2011,15:58:25) for (I). Data reduction: CrysAlis PRO, Agilent Technologies, Version 1.171.34.49 (release 20-01-2011 CrysAlis171 .NET) (compiled Jan 20 2011,15:58:25) for (I).

(I) top
Crystal data top
Ba0.7Fe0.5K2.1Mg0.05Na2Nb0.1O33Si8Ti4Z = 2
Mr = 1206.8F(000) = 1167
Monoclinic, C2/mDx = 2.946 Mg m3
Hall symbol: -C 2yMo Kα radiation, λ = 0.7107 Å
a = 14.2584 (4) ÅCell parameters from 11867 reflections
b = 13.7541 (6) Åθ = 4.2–56.1°
c = 7.7770 (2) ŵ = 3.27 mm1
β = 116.893 (3)°T = 293 K
V = 1360.22 (9) Å3Anhedral grain
Data collection top
Xcalibur, Sapphire3 with high theta cut
diffractometer
3751 independent reflections
Radiation source: Enhance (Mo) X-ray Source3202 reflections with I > 3σ(I)
Graphite monochromatorRint = 0.051
Detector resolution: 16.0628 pixels mm-1θmax = 40.6°, θmin = 4.2°
ω scansh = 3333
Absorption correction: multi-scan
CrysAlisPro, Agilent Technologies, Version 1.171.34.49 (release 20-01-2011 CrysAlis171 .NET) (compiled Jan 20 2011,15:58:25) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm.
k = 3019
Tmin = 0.763, Tmax = 1l = 1818
37871 measured reflections
Refinement top
Refinement on F0 restraints
R[F2 > 2σ(F2)] = 0.04720 constraints
wR(F2) = 0.072Weighting scheme based on measured s.u.'s w = 1/(σ2(F) + 0.003025F2)
S = 1.03(Δ/σ)max = 0.047
3751 reflectionsΔρmax = 1.38 e Å3
131 parametersΔρmin = 1.17 e Å3
Fractional atomic coordinates and isotropic or equivalent isotropic displacement parameters (Å2) top
xyzUiso*/UeqOcc. (<1)
Na_a0.41379 (18)0.26252 (18)0.0121 (4)0.0275 (7)0.5
K_b0.41956 (7)00.70218 (11)0.0357 (3)
Ti_m1(1)0.250.250.50.01529 (13)0.95
Ti_m1(2)00.22729 (3)0.50.01615 (12)
Fe_m2000.50.0210 (3)0.5
Si10.31974 (3)0.11129 (3)0.25001 (5)0.00679 (12)
Si20.20825 (3)0.10994 (3)0.80309 (5)0.00632 (12)
O10.08208 (9)0.11546 (9)0.67278 (17)0.0112 (3)
O20.27382 (9)0.18333 (9)0.73861 (15)0.0097 (3)
O30.26504 (9)0.12547 (9)0.38878 (16)0.0098 (3)
O40.36441 (13)00.2714 (2)0.0105 (4)
O50.24755 (14)00.7865 (3)0.0118 (4)
O60.41951 (10)0.18040 (10)0.30303 (18)0.0123 (3)
O70.23225 (9)0.12801 (10)0.02623 (15)0.0117 (3)
Oh0.10017 (9)0.22422 (10)0.39672 (16)0.0108 (3)
Ba0.08549 (3)00.34374 (5)0.01770 (12)0.35
W10.50.1455 (4)00.130 (4)
W200.1123 (4)00.093 (4)
W_c0.08549 (3)00.34374 (5)0.01770 (12)0.65
Nb_m1(1)0.250.250.50.01529 (13)0.05
Ti_m2000.50.0210 (3)0.1
Mg_m2000.50.0210 (3)0.05
Atomic displacement parameters (Å2) top
U11U22U33U12U13U23
Na_a0.0212 (8)0.0241 (10)0.0416 (11)0.0014 (7)0.0181 (8)0.0032 (8)
K_b0.0268 (3)0.0596 (6)0.0199 (3)00.0100 (2)0
Ti_m1(1)0.0331 (2)0.00652 (17)0.01275 (14)0.00572 (13)0.01613 (14)0.00263 (10)
Ti_m1(2)0.01421 (17)0.00453 (17)0.01478 (16)00.00656 (12)0
Fe_m20.0180 (4)0.0141 (4)0.0236 (4)00.0029 (3)0
Si10.00819 (16)0.00526 (18)0.00655 (15)0.00074 (10)0.00302 (12)0.00081 (10)
Si20.00678 (16)0.00518 (18)0.00613 (15)0.00005 (10)0.00217 (12)0.00055 (10)
O10.0070 (4)0.0110 (5)0.0115 (4)0.0003 (3)0.0005 (3)0.0032 (3)
O20.0110 (4)0.0091 (5)0.0097 (3)0.0020 (3)0.0052 (3)0.0018 (3)
O30.0124 (4)0.0089 (4)0.0117 (4)0.0005 (3)0.0087 (3)0.0012 (3)
O40.0116 (5)0.0056 (6)0.0155 (6)00.0071 (5)0
O50.0141 (6)0.0053 (6)0.0174 (6)00.0084 (5)0
O60.0128 (4)0.0110 (5)0.0145 (4)0.0058 (3)0.0075 (3)0.0047 (3)
O70.0128 (4)0.0146 (5)0.0063 (3)0.0018 (3)0.0030 (3)0.0006 (3)
Oh0.0073 (4)0.0144 (5)0.0101 (4)0.0001 (3)0.0033 (3)0.0001 (3)
Ba0.01926 (16)0.01662 (18)0.01658 (15)00.00755 (12)0
W10.234 (10)0.027 (2)0.0261 (15)00.031 (3)0
W20.200 (8)0.038 (2)0.0250 (14)00.037 (3)0
W_c0.01926 (16)0.01662 (18)0.01658 (15)00.00755 (12)0
Nb_m1(1)0.0331 (2)0.00652 (17)0.01275 (14)0.00572 (13)0.01613 (14)0.00263 (10)
Ti_m20.0180 (4)0.0141 (4)0.0236 (4)00.0029 (3)0
Mg_m20.0180 (4)0.0141 (4)0.0236 (4)00.0029 (3)0
Geometric parameters (Å, º) top
Na_a—Na_ai2.549 (4)Fe_m2—O12.0674 (12)
Na_a—K_bii4.363 (3)Fe_m2—O1xii2.0674 (12)
Na_a—K_biii4.341 (2)Fe_m2—O1xiv2.0674 (12)
Na_a—Ti_m1(2)iv3.422 (3)Fe_m2—O1ix2.0674 (12)
Na_a—Si2iv3.230 (3)Fe_m2—Ba2.0742 (5)
Na_a—O2ii2.419 (2)Fe_m2—Baxii2.0742 (5)
Na_a—Bav4.196 (2)Fe_m2—W_c2.0742 (5)
Na_a—Bavi4.284 (3)Fe_m2—W_cxii2.0742 (5)
Na_a—W12.053 (5)Fe_m2—Ti_m20
Na_a—W2vii2.142 (5)Fe_m2—Mg_m20
K_b—K_biii4.6559 (15)Si1—O31.6039 (16)
K_b—K_bviii4.1361 (11)Si1—O41.6373 (8)
K_b—Si13.4939 (8)Si1—O61.6020 (14)
K_b—Si1ix3.4939 (8)Si1—O71.6352 (10)
K_b—O52.811 (3)Si2—O11.6186 (11)
K_b—Ba4.2951 (9)Si2—O21.6026 (14)
K_b—W1x2.878 (4)Si2—O51.6378 (10)
K_b—W1xi2.878 (4)Si2—O7x1.6289 (13)
Ti_m1(1)—O21.9570 (12)Si2—Ba3.5292 (5)
Ti_m1(1)—O2iv1.9570 (12)O1—Baxii2.8229 (14)
Ti_m1(1)—O31.9737 (13)O1—Ti_m22.0674 (12)
Ti_m1(1)—O3iv1.9737 (13)O1—Mg_m22.0674 (12)
Ti_m1(1)—Oh1.9449 (12)O2—Nb_m1(1)1.9570 (12)
Ti_m1(1)—Ohiv1.9449 (12)O3—Nb_m1(1)1.9737 (13)
Ti_m1(1)—Nb_m1(1)0Oh—Nb_m1(1)1.9449 (12)
Ti_m1(2)—O12.0294 (12)Ba—Baxii4.1484 (8)
Ti_m1(2)—O1xii2.0294 (12)Ba—W22.841 (3)
Ti_m1(2)—O6iv1.9197 (12)Ba—W2xv2.841 (3)
Ti_m1(2)—O6xiii1.9197 (12)Ba—W_c0
Ti_m1(2)—Oh1.9299 (15)Ba—Ti_m22.0742 (5)
Ti_m1(2)—Ohxii1.9299 (15)Ba—Mg_m22.0742 (5)
Ti_m1(2)—Ba3.7517 (5)W_c—Ti_m22.0742 (5)
Ti_m1(2)—Baxii3.7517 (5)W_c—Mg_m22.0742 (5)
Ti_m1(2)—Mg_m23.1262 (5)Ti_m2—Mg_m20
Na_ai—Na_a—K_bii72.51 (9)Na_axvii—Ba—Si2147.16 (4)
Na_ai—Na_a—K_biii73.43 (8)Na_axvii—Ba—Si2ix99.96 (4)
Na_ai—Na_a—Ti_m1(2)iv101.95 (9)Na_axvii—Ba—O1xii99.41 (4)
Na_ai—Na_a—Si2iv139.86 (11)Na_axvii—Ba—O1xiv44.57 (5)
Na_ai—Na_a—O2ii112.01 (14)Na_axvii—Ba—Baxii91.49 (5)
Na_ai—Na_a—Bav74.41 (8)Na_axvii—Ba—W287.83 (10)
Na_ai—Na_a—Bavi70.62 (9)Na_axvii—Ba—W2xv27.81 (8)
Na_ai—Na_a—W151.63 (12)Na_axvii—Ba—W_c0
Na_ai—Na_a—W2vii53.49 (12)Na_axvii—Ba—Ti_m291.49 (5)
K_bii—Na_a—K_biii56.75 (3)Na_axvii—Ba—Mg_m291.49 (5)
K_bii—Na_a—Ti_m1(2)iv124.02 (7)Na_axviii—Ba—Na_avii99.36 (6)
K_bii—Na_a—Si2iv147.55 (8)Na_axviii—Ba—Na_axiii111.57 (5)
K_bii—Na_a—O2ii49.90 (6)Na_axviii—Ba—K_b95.35 (3)
K_bii—Na_a—Bav146.35 (7)Na_axviii—Ba—Ti_m1(2)160.15 (3)
K_bii—Na_a—Bavi105.54 (7)Na_axviii—Ba—Ti_m1(2)xiv70.73 (4)
K_bii—Na_a—W133.34 (6)Na_axviii—Ba—Fe_m2123.52 (4)
K_bii—Na_a—W2vii119.10 (14)Na_axviii—Ba—Si2146.67 (3)
K_biii—Na_a—Ti_m1(2)iv68.13 (4)Na_axviii—Ba—Si2ix100.50 (3)
K_biii—Na_a—Si2iv120.28 (8)Na_axviii—Ba—O1xii130.45 (4)
K_biii—Na_a—O2ii96.80 (8)Na_axviii—Ba—O1xiv77.94 (5)
K_biii—Na_a—Bav107.50 (5)Na_axviii—Ba—Baxii123.52 (4)
K_biii—Na_a—Bavi143.52 (8)Na_axviii—Ba—W286.10 (10)
K_biii—Na_a—W134.00 (7)Na_axviii—Ba—W2xv26.23 (7)
K_biii—Na_a—W2vii119.93 (11)Na_axviii—Ba—W_c0
Ti_m1(2)iv—Na_a—Si2iv58.67 (5)Na_axviii—Ba—Ti_m2123.52 (4)
Ti_m1(2)iv—Na_a—O2ii137.14 (12)Na_axviii—Ba—Mg_m2123.52 (4)
Ti_m1(2)iv—Na_a—Bav57.95 (4)Na_avii—Ba—Na_axiii34.97 (6)
Ti_m1(2)iv—Na_a—Bavi125.48 (7)Na_avii—Ba—K_b95.35 (3)
Ti_m1(2)iv—Na_a—W199.25 (8)Na_avii—Ba—Ti_m1(2)70.73 (4)
Ti_m1(2)iv—Na_a—W2vii95.18 (8)Na_avii—Ba—Ti_m1(2)xiv160.15 (3)
Si2iv—Na_a—O2ii103.86 (9)Na_avii—Ba—Fe_m2123.52 (4)
Si2iv—Na_a—Bav65.52 (5)Na_avii—Ba—Si2100.50 (3)
Si2iv—Na_a—Bavi91.87 (6)Na_avii—Ba—Si2ix146.67 (3)
Si2iv—Na_a—W1154.21 (14)Na_avii—Ba—O1xii77.94 (5)
Si2iv—Na_a—W2vii91.05 (12)Na_avii—Ba—O1xiv130.45 (4)
O2ii—Na_a—Bav155.63 (9)Na_avii—Ba—Baxii123.52 (4)
O2ii—Na_a—Bavi91.00 (8)Na_avii—Ba—W226.23 (7)
O2ii—Na_a—W183.09 (11)Na_avii—Ba—W2xv86.10 (10)
O2ii—Na_a—W2vii125.79 (13)Na_avii—Ba—W_c0
Bav—Na_a—Bavi68.43 (4)Na_avii—Ba—Ti_m2123.52 (4)
Bav—Na_a—W1116.33 (10)Na_avii—Ba—Mg_m2123.52 (4)
Bav—Na_a—W2vii38.22 (6)Na_axiii—Ba—K_b124.50 (3)
Bavi—Na_a—W1113.06 (14)Na_axiii—Ba—Ti_m1(2)50.63 (4)
Bavi—Na_a—W2vii35.88 (5)Na_axiii—Ba—Ti_m1(2)xiv131.54 (4)
W1—Na_a—W2vii105.11 (18)Na_axiii—Ba—Fe_m291.49 (5)
Na_ax—K_b—Na_aiii34.06 (5)Na_axiii—Ba—Si299.96 (4)
Na_ax—K_b—Na_axi123.26 (5)Na_axiii—Ba—Si2ix147.16 (4)
Na_ax—K_b—Na_axvi111.72 (6)Na_axiii—Ba—O1xii44.57 (5)
Na_ax—K_b—K_biii120.75 (4)Na_axiii—Ba—O1xiv99.41 (4)
Na_ax—K_b—K_bviii61.36 (3)Na_axiii—Ba—Baxii91.49 (5)
Na_ax—K_b—Si195.31 (4)Na_axiii—Ba—W227.81 (8)
Na_ax—K_b—Si1ix144.86 (3)Na_axiii—Ba—W2xv87.83 (10)
Na_ax—K_b—O568.57 (4)Na_axiii—Ba—W_c0
Na_ax—K_b—Ba93.79 (3)Na_axiii—Ba—Ti_m291.49 (5)
Na_ax—K_b—W1x23.08 (6)Na_axiii—Ba—Mg_m291.49 (5)
Na_ax—K_b—W1xi103.36 (8)K_b—Ba—Ti_m1(2)102.544 (9)
Na_aiii—K_b—Na_axi112.56 (4)K_b—Ba—Ti_m1(2)xiv102.544 (9)
Na_aiii—K_b—Na_axvi123.26 (5)K_b—Ba—Fe_m2113.132 (18)
Na_aiii—K_b—K_biii91.31 (5)K_b—Ba—Si256.384 (15)
Na_aiii—K_b—K_bviii61.89 (4)K_b—Ba—Si2ix56.384 (15)
Na_aiii—K_b—Si191.73 (4)K_b—Ba—O1xii134.18 (2)
Na_aiii—K_b—Si1ix139.38 (5)K_b—Ba—O1xiv134.18 (2)
Na_aiii—K_b—O5102.35 (5)K_b—Ba—Baxii113.132 (17)
Na_aiii—K_b—Ba121.45 (3)K_b—Ba—W2119.25 (4)
Na_aiii—K_b—W1x23.51 (7)K_b—Ba—W2xv119.25 (4)
Na_aiii—K_b—W1xi103.88 (8)K_b—Ba—W_c0
Na_axi—K_b—Na_axvi34.06 (5)K_b—Ba—Ti_m2113.132 (18)
Na_axi—K_b—K_biii91.31 (5)K_b—Ba—Mg_m2113.132 (18)
Na_axi—K_b—K_bviii61.89 (4)Ti_m1(2)—Ba—Ti_m1(2)xiv112.872 (15)
Na_axi—K_b—Si1139.38 (5)Ti_m1(2)—Ba—Fe_m256.436 (8)
Na_axi—K_b—Si1ix91.73 (4)Ti_m1(2)—Ba—Si253.142 (8)
Na_axi—K_b—O5102.35 (5)Ti_m1(2)—Ba—Si2ix96.559 (13)
Na_axi—K_b—Ba121.45 (3)Ti_m1(2)—Ba—O1xii32.19 (2)
Na_axi—K_b—W1x103.88 (8)Ti_m1(2)—Ba—O1xiv95.23 (3)
Na_axi—K_b—W1xi23.51 (7)Ti_m1(2)—Ba—Baxii56.436 (8)
Na_axvi—K_b—K_biii120.75 (4)Ti_m1(2)—Ba—W277.75 (8)
Na_axvi—K_b—K_bviii61.36 (3)Ti_m1(2)—Ba—W2xv133.94 (7)
Na_axvi—K_b—Si1144.86 (3)Ti_m1(2)—Ba—W_c0
Na_axvi—K_b—Si1ix95.31 (4)Ti_m1(2)—Ba—Ti_m256.436 (8)
Na_axvi—K_b—O568.57 (4)Ti_m1(2)—Ba—Mg_m256.436 (8)
Na_axvi—K_b—Ba93.79 (3)Ti_m1(2)xiv—Ba—Fe_m256.436 (8)
Na_axvi—K_b—W1x103.36 (8)Ti_m1(2)xiv—Ba—Si296.559 (13)
Na_axvi—K_b—W1xi23.08 (6)Ti_m1(2)xiv—Ba—Si2ix53.142 (8)
K_biii—K_b—K_bviii124.29 (3)Ti_m1(2)xiv—Ba—O1xii95.23 (3)
K_biii—K_b—Si154.623 (18)Ti_m1(2)xiv—Ba—O1xiv32.19 (2)
K_biii—K_b—Si1ix54.623 (18)Ti_m1(2)xiv—Ba—Baxii56.436 (8)
K_biii—K_b—O5154.97 (4)Ti_m1(2)xiv—Ba—W2133.94 (7)
K_biii—K_b—Ba107.592 (19)Ti_m1(2)xiv—Ba—W2xv77.75 (8)
K_biii—K_b—W1x113.88 (4)Ti_m1(2)xiv—Ba—W_c0
K_biii—K_b—W1xi113.88 (4)Ti_m1(2)xiv—Ba—Ti_m256.436 (8)
K_bviii—K_b—Si1153.418 (10)Ti_m1(2)xiv—Ba—Mg_m256.436 (8)
K_bviii—K_b—Si1ix153.418 (10)Fe_m2—Ba—Si263.949 (13)
K_bviii—K_b—O580.74 (4)Fe_m2—Ba—Si2ix63.949 (13)
K_bviii—K_b—Ba128.12 (3)Fe_m2—Ba—O1xii46.93 (3)
K_bviii—K_b—W1x44.06 (7)Fe_m2—Ba—O1xiv46.93 (3)
K_bviii—K_b—W1xi44.06 (7)Fe_m2—Ba—Baxii0.0 (5)
Si1—K_b—Si1ix51.969 (15)Fe_m2—Ba—W2115.82 (3)
Si1—K_b—O5103.51 (4)Fe_m2—Ba—W2xv115.82 (3)
Si1—K_b—Ba61.282 (14)Fe_m2—Ba—W_c0
Si1—K_b—W1x109.76 (7)Fe_m2—Ba—Ti_m20.0 (5)
Si1—K_b—W1xi161.32 (7)Fe_m2—Ba—Mg_m20.0 (5)
Si1ix—K_b—O5103.51 (4)Si2—Ba—Si2ix50.741 (11)
Si1ix—K_b—Ba61.282 (14)Si2—Ba—O1xii80.04 (2)
Si1ix—K_b—W1x161.32 (7)Si2—Ba—O1xiv108.01 (3)
Si1ix—K_b—W1xi109.76 (7)Si2—Ba—Baxii63.949 (12)
O5—K_b—Ba47.38 (4)Si2—Ba—W2121.66 (9)
O5—K_b—W1x83.36 (3)Si2—Ba—W2xv172.20 (9)
O5—K_b—W1xi83.36 (3)Si2—Ba—W_c0
Ba—K_b—W1x116.34 (4)Si2—Ba—Ti_m263.949 (13)
Ba—K_b—W1xi116.34 (4)Si2—Ba—Mg_m263.949 (13)
W1x—K_b—W1xi88.12 (10)Si2ix—Ba—O1xii108.01 (3)
O2—Ti_m1(1)—O2iv180.0 (5)Si2ix—Ba—O1xiv80.04 (2)
O2—Ti_m1(1)—O390.13 (5)Si2ix—Ba—Baxii63.949 (12)
O2—Ti_m1(1)—O3iv89.87 (5)Si2ix—Ba—W2172.20 (9)
O2—Ti_m1(1)—Oh89.61 (5)Si2ix—Ba—W2xv121.66 (9)
O2—Ti_m1(1)—Ohiv90.39 (5)Si2ix—Ba—W_c0
O2—Ti_m1(1)—Nb_m1(1)0Si2ix—Ba—Ti_m263.949 (13)
O2iv—Ti_m1(1)—O389.87 (5)Si2ix—Ba—Mg_m263.949 (13)
O2iv—Ti_m1(1)—O3iv90.13 (5)O1xii—Ba—O1xiv68.46 (4)
O2iv—Ti_m1(1)—Oh90.39 (5)O1xii—Ba—Baxii46.93 (3)
O2iv—Ti_m1(1)—Ohiv89.61 (5)O1xii—Ba—W269.96 (5)
O2iv—Ti_m1(1)—Nb_m1(1)0O1xii—Ba—W2xv105.60 (5)
O3—Ti_m1(1)—O3iv180.0 (5)O1xii—Ba—W_c0
O3—Ti_m1(1)—Oh88.71 (5)O1xii—Ba—Ti_m246.93 (3)
O3—Ti_m1(1)—Ohiv91.29 (5)O1xii—Ba—Mg_m246.93 (3)
O3—Ti_m1(1)—Nb_m1(1)0O1xiv—Ba—Baxii46.93 (3)
O3iv—Ti_m1(1)—Oh91.29 (5)O1xiv—Ba—W2105.60 (5)
O3iv—Ti_m1(1)—Ohiv88.71 (5)O1xiv—Ba—W2xv69.96 (5)
O3iv—Ti_m1(1)—Nb_m1(1)0O1xiv—Ba—W_c0
Oh—Ti_m1(1)—Ohiv180.0 (5)O1xiv—Ba—Ti_m246.93 (3)
Oh—Ti_m1(1)—Nb_m1(1)0O1xiv—Ba—Mg_m246.93 (3)
Ohiv—Ti_m1(1)—Nb_m1(1)0Baxii—Ba—W2115.82 (3)
Na_aiv—Ti_m1(2)—Na_axiii175.31 (6)Baxii—Ba—W2xv115.82 (3)
Na_aiv—Ti_m1(2)—O159.10 (6)Baxii—Ba—W_c0
Na_aiv—Ti_m1(2)—O1xii125.14 (6)Baxii—Ba—Ti_m20.0 (5)
Na_aiv—Ti_m1(2)—O6iv45.80 (6)Baxii—Ba—Mg_m20.0 (5)
Na_aiv—Ti_m1(2)—O6xiii130.02 (6)W2—Ba—W2xv65.87 (13)
Na_aiv—Ti_m1(2)—Oh120.01 (5)W2—Ba—W_c0
Na_aiv—Ti_m1(2)—Ohxii60.11 (5)W2—Ba—Ti_m2115.82 (3)
Na_aiv—Ti_m1(2)—Ba112.76 (4)W2—Ba—Mg_m2115.82 (3)
Na_aiv—Ti_m1(2)—Baxii71.42 (4)W2xv—Ba—W_c0
Na_aiv—Ti_m1(2)—Mg_m292.35 (4)W2xv—Ba—Ti_m2115.82 (3)
Na_axiii—Ti_m1(2)—O1125.14 (6)W2xv—Ba—Mg_m2115.82 (3)
Na_axiii—Ti_m1(2)—O1xii59.10 (6)W_c—Ba—Ti_m20
Na_axiii—Ti_m1(2)—O6iv130.02 (6)W_c—Ba—Mg_m20
Na_axiii—Ti_m1(2)—O6xiii45.80 (6)Ti_m2—Ba—Mg_m20.0 (5)
Na_axiii—Ti_m1(2)—Oh60.11 (5)Na_a—W1—Na_ai76.7 (2)
Na_axiii—Ti_m1(2)—Ohxii120.01 (5)Na_a—W1—K_bii123.58 (6)
Na_axiii—Ti_m1(2)—Ba71.42 (4)Na_a—W1—K_biii122.49 (9)
Na_axiii—Ti_m1(2)—Baxii112.76 (4)Na_ai—W1—K_bii122.49 (9)
Na_axiii—Ti_m1(2)—Mg_m292.35 (4)Na_ai—W1—K_biii123.58 (6)
O1—Ti_m1(2)—O1xii81.43 (5)K_bii—W1—K_biii91.88 (15)
O1—Ti_m1(2)—O6iv90.88 (5)Na_avii—W2—Na_axiii73.0 (2)
O1—Ti_m1(2)—O6xiii170.82 (6)Na_avii—W2—Ba117.89 (7)
O1—Ti_m1(2)—Oh86.86 (6)Na_avii—W2—Baxix113.96 (9)
O1—Ti_m1(2)—Ohxii91.23 (6)Na_axiii—W2—Ba113.96 (9)
O1—Ti_m1(2)—Ba53.73 (4)Na_axiii—W2—Baxix117.89 (7)
O1—Ti_m1(2)—Baxii47.82 (4)Ba—W2—Baxix114.13 (18)
O1—Ti_m1(2)—Mg_m240.72 (3)Fe_m2—W_c—Ba0
O1xii—Ti_m1(2)—O6iv170.82 (6)Fe_m2—W_c—Ti_m20.0 (5)
O1xii—Ti_m1(2)—O6xiii90.88 (5)Fe_m2—W_c—Mg_m20.0 (5)
O1xii—Ti_m1(2)—Oh91.23 (6)Ba—W_c—Ti_m20
O1xii—Ti_m1(2)—Ohxii86.86 (6)Ba—W_c—Mg_m20
O1xii—Ti_m1(2)—Ba47.82 (4)Ti_m2—W_c—Mg_m20.0 (5)
O1xii—Ti_m1(2)—Baxii53.73 (4)Ti_m1(1)—Nb_m1(1)—O20
O1xii—Ti_m1(2)—Mg_m240.72 (3)Ti_m1(1)—Nb_m1(1)—O2iv0
O6iv—Ti_m1(2)—O6xiii97.19 (5)Ti_m1(1)—Nb_m1(1)—O30
O6iv—Ti_m1(2)—Oh93.37 (6)Ti_m1(1)—Nb_m1(1)—O3iv0
O6iv—Ti_m1(2)—Ohxii88.29 (6)Ti_m1(1)—Nb_m1(1)—Oh0
O6iv—Ti_m1(2)—Ba130.17 (4)Ti_m1(1)—Nb_m1(1)—Ohiv0
O6iv—Ti_m1(2)—Baxii117.21 (4)O2—Nb_m1(1)—O2iv180.0 (5)
O6iv—Ti_m1(2)—Mg_m2131.40 (4)O2—Nb_m1(1)—O390.13 (5)
O6xiii—Ti_m1(2)—Oh88.29 (6)O2—Nb_m1(1)—O3iv89.87 (5)
O6xiii—Ti_m1(2)—Ohxii93.37 (6)O2—Nb_m1(1)—Oh89.61 (5)
O6xiii—Ti_m1(2)—Ba117.21 (4)O2—Nb_m1(1)—Ohiv90.39 (5)
O6xiii—Ti_m1(2)—Baxii130.17 (4)O2iv—Nb_m1(1)—O389.87 (5)
O6xiii—Ti_m1(2)—Mg_m2131.40 (4)O2iv—Nb_m1(1)—O3iv90.13 (5)
Oh—Ti_m1(2)—Ohxii177.49 (6)O2iv—Nb_m1(1)—Oh90.39 (5)
Oh—Ti_m1(2)—Ba55.73 (4)O2iv—Nb_m1(1)—Ohiv89.61 (5)
Oh—Ti_m1(2)—Baxii121.77 (4)O3—Nb_m1(1)—O3iv180.0 (5)
Oh—Ti_m1(2)—Mg_m288.74 (4)O3—Nb_m1(1)—Oh88.71 (5)
Ohxii—Ti_m1(2)—Ba121.77 (4)O3—Nb_m1(1)—Ohiv91.29 (5)
Ohxii—Ti_m1(2)—Baxii55.73 (4)O3iv—Nb_m1(1)—Oh91.29 (5)
Ohxii—Ti_m1(2)—Mg_m288.74 (4)O3iv—Nb_m1(1)—Ohiv88.71 (5)
Ba—Ti_m1(2)—Baxii67.128 (12)Oh—Nb_m1(1)—Ohiv180.0 (5)
Ba—Ti_m1(2)—Mg_m233.564 (8)Fe_m2—Ti_m2—O10
Baxii—Ti_m1(2)—Mg_m233.564 (8)Fe_m2—Ti_m2—O1xii0
O1—Fe_m2—O1xii79.63 (4)Fe_m2—Ti_m2—O1xiv0
O1—Fe_m2—O1xiv180.0 (5)Fe_m2—Ti_m2—O1ix0
O1—Fe_m2—O1ix100.37 (4)Fe_m2—Ti_m2—Ba0
O1—Fe_m2—Ba94.06 (4)Fe_m2—Ti_m2—Baxii0
O1—Fe_m2—Baxii85.94 (4)Fe_m2—Ti_m2—W_c0
O1—Fe_m2—W_c94.06 (4)Fe_m2—Ti_m2—W_cxii0
O1—Fe_m2—W_cxii85.94 (4)Fe_m2—Ti_m2—Mg_m20
O1—Fe_m2—Ti_m20O1—Ti_m2—O1xii79.63 (4)
O1—Fe_m2—Mg_m20O1—Ti_m2—O1xiv180.0 (5)
O1xii—Fe_m2—O1xiv100.37 (4)O1—Ti_m2—O1ix100.37 (4)
O1xii—Fe_m2—O1ix180.0 (5)O1—Ti_m2—Ba94.06 (4)
O1xii—Fe_m2—Ba85.94 (4)O1—Ti_m2—Baxii85.94 (4)
O1xii—Fe_m2—Baxii94.06 (4)O1—Ti_m2—W_c94.06 (4)
O1xii—Fe_m2—W_c85.94 (4)O1—Ti_m2—W_cxii85.94 (4)
O1xii—Fe_m2—W_cxii94.06 (4)O1—Ti_m2—Mg_m20
O1xii—Fe_m2—Ti_m20O1xii—Ti_m2—O1xiv100.37 (4)
O1xii—Fe_m2—Mg_m20O1xii—Ti_m2—O1ix180.0 (5)
O1xiv—Fe_m2—O1ix79.63 (4)O1xii—Ti_m2—Ba85.94 (4)
O1xiv—Fe_m2—Ba85.94 (4)O1xii—Ti_m2—Baxii94.06 (4)
O1xiv—Fe_m2—Baxii94.06 (4)O1xii—Ti_m2—W_c85.94 (4)
O1xiv—Fe_m2—W_c85.94 (4)O1xii—Ti_m2—W_cxii94.06 (4)
O1xiv—Fe_m2—W_cxii94.06 (4)O1xii—Ti_m2—Mg_m20
O1xiv—Fe_m2—Ti_m20O1xiv—Ti_m2—O1ix79.63 (4)
O1xiv—Fe_m2—Mg_m20O1xiv—Ti_m2—Ba85.94 (4)
O1ix—Fe_m2—Ba94.06 (4)O1xiv—Ti_m2—Baxii94.06 (4)
O1ix—Fe_m2—Baxii85.94 (4)O1xiv—Ti_m2—W_c85.94 (4)
O1ix—Fe_m2—W_c94.06 (4)O1xiv—Ti_m2—W_cxii94.06 (4)
O1ix—Fe_m2—W_cxii85.94 (4)O1xiv—Ti_m2—Mg_m20
O1ix—Fe_m2—Ti_m20O1ix—Ti_m2—Ba94.06 (4)
O1ix—Fe_m2—Mg_m20O1ix—Ti_m2—Baxii85.94 (4)
Ba—Fe_m2—Baxii180.0 (5)O1ix—Ti_m2—W_c94.06 (4)
Ba—Fe_m2—W_c0.0 (5)O1ix—Ti_m2—W_cxii85.94 (4)
Ba—Fe_m2—W_cxii180.0 (5)O1ix—Ti_m2—Mg_m20
Ba—Fe_m2—Ti_m20Ba—Ti_m2—Baxii180.0 (5)
Ba—Fe_m2—Mg_m20Ba—Ti_m2—W_c0.0 (5)
Baxii—Fe_m2—W_c180.0 (5)Ba—Ti_m2—W_cxii180.0 (5)
Baxii—Fe_m2—W_cxii0.0 (5)Ba—Ti_m2—Mg_m20
Baxii—Fe_m2—Ti_m20Baxii—Ti_m2—W_c180.0 (5)
Baxii—Fe_m2—Mg_m20Baxii—Ti_m2—W_cxii0.0 (5)
W_c—Fe_m2—W_cxii180.0 (5)Baxii—Ti_m2—Mg_m20
W_c—Fe_m2—Ti_m20W_c—Ti_m2—W_cxii180.0 (5)
W_c—Fe_m2—Mg_m20W_c—Ti_m2—Mg_m20
W_cxii—Fe_m2—Ti_m20W_cxii—Ti_m2—Mg_m20
W_cxii—Fe_m2—Mg_m20Ti_m1(2)—Mg_m2—Ti_m1(2)xiv180.0 (5)
Ti_m2—Fe_m2—Mg_m20Ti_m1(2)—Mg_m2—Fe_m20
K_b—Si1—O358.45 (4)Ti_m1(2)—Mg_m2—O139.82 (3)
K_b—Si1—O461.66 (7)Ti_m1(2)—Mg_m2—O1xii39.82 (3)
K_b—Si1—O695.21 (5)Ti_m1(2)—Mg_m2—O1xiv140.18 (3)
K_b—Si1—O7154.18 (6)Ti_m1(2)—Mg_m2—O1ix140.18 (3)
O3—Si1—O4109.29 (9)Ti_m1(2)—Mg_m2—Ba90
O3—Si1—O6113.59 (7)Ti_m1(2)—Mg_m2—Baxii90
O3—Si1—O7109.27 (7)Ti_m1(2)—Mg_m2—W_c90
O4—Si1—O6105.62 (8)Ti_m1(2)—Mg_m2—W_cxii90
O4—Si1—O7108.31 (8)Ti_m1(2)—Mg_m2—Ti_m20
O6—Si1—O7110.59 (7)Ti_m1(2)xiv—Mg_m2—Fe_m20
Na_aiv—Si2—O165.37 (6)Ti_m1(2)xiv—Mg_m2—O1140.18 (3)
Na_aiv—Si2—O2107.76 (7)Ti_m1(2)xiv—Mg_m2—O1xii140.18 (3)
Na_aiv—Si2—O5143.97 (10)Ti_m1(2)xiv—Mg_m2—O1xiv39.82 (3)
Na_aiv—Si2—O7x48.62 (6)Ti_m1(2)xiv—Mg_m2—O1ix39.82 (3)
Na_aiv—Si2—Ba124.25 (4)Ti_m1(2)xiv—Mg_m2—Ba90
O1—Si2—O2114.52 (6)Ti_m1(2)xiv—Mg_m2—Baxii90
O1—Si2—O5108.48 (7)Ti_m1(2)xiv—Mg_m2—W_c90
O1—Si2—O7x107.36 (7)Ti_m1(2)xiv—Mg_m2—W_cxii90
O1—Si2—Ba58.96 (5)Ti_m1(2)xiv—Mg_m2—Ti_m20
O2—Si2—O5106.75 (9)Fe_m2—Mg_m2—O10
O2—Si2—O7x111.47 (7)Fe_m2—Mg_m2—O1xii0
O2—Si2—Ba92.61 (4)Fe_m2—Mg_m2—O1xiv0
O5—Si2—O7x108.07 (8)Fe_m2—Mg_m2—O1ix0
O5—Si2—Ba63.61 (6)Fe_m2—Mg_m2—Ba0
O7x—Si2—Ba155.89 (5)Fe_m2—Mg_m2—Baxii0
Ti_m1(2)—O1—Fe_m299.47 (4)Fe_m2—Mg_m2—W_c0
Ti_m1(2)—O1—Si2126.50 (8)Fe_m2—Mg_m2—W_cxii0
Ti_m1(2)—O1—Baxii99.99 (4)Fe_m2—Mg_m2—Ti_m20
Ti_m1(2)—O1—Ti_m299.47 (4)O1—Mg_m2—O1xii79.63 (4)
Ti_m1(2)—O1—Mg_m299.47 (4)O1—Mg_m2—O1xiv180.0 (5)
Fe_m2—O1—Si2120.87 (7)O1—Mg_m2—O1ix100.37 (4)
Fe_m2—O1—Baxii47.13 (3)O1—Mg_m2—Ba94.06 (4)
Fe_m2—O1—Ti_m20.0 (5)O1—Mg_m2—Baxii85.94 (4)
Fe_m2—O1—Mg_m20.0 (5)O1—Mg_m2—W_c94.06 (4)
Si2—O1—Baxii132.86 (7)O1—Mg_m2—W_cxii85.94 (4)
Si2—O1—Ti_m2120.87 (7)O1—Mg_m2—Ti_m20
Si2—O1—Mg_m2120.87 (7)O1xii—Mg_m2—O1xiv100.37 (4)
Baxii—O1—Ti_m247.13 (3)O1xii—Mg_m2—O1ix180.0 (5)
Baxii—O1—Mg_m247.13 (3)O1xii—Mg_m2—Ba85.94 (4)
Ti_m2—O1—Mg_m20.0 (5)O1xii—Mg_m2—Baxii94.06 (4)
Na_ax—O2—Ti_m1(1)110.06 (9)O1xii—Mg_m2—W_c85.94 (4)
Na_ax—O2—Si2111.99 (10)O1xii—Mg_m2—W_cxii94.06 (4)
Na_ax—O2—Nb_m1(1)110.06 (9)O1xii—Mg_m2—Ti_m20
Ti_m1(1)—O2—Si2135.74 (6)O1xiv—Mg_m2—O1ix79.63 (4)
Ti_m1(1)—O2—Nb_m1(1)0.0 (5)O1xiv—Mg_m2—Ba85.94 (4)
Si2—O2—Nb_m1(1)135.74 (6)O1xiv—Mg_m2—Baxii94.06 (4)
Ti_m1(1)—O3—Si1125.64 (8)O1xiv—Mg_m2—W_c85.94 (4)
Ti_m1(1)—O3—Nb_m1(1)0.0 (5)O1xiv—Mg_m2—W_cxii94.06 (4)
Si1—O3—Nb_m1(1)125.64 (8)O1xiv—Mg_m2—Ti_m20
Si1—O4—Si1ix138.44 (12)O1ix—Mg_m2—Ba94.06 (4)
K_b—O5—Si2112.58 (8)O1ix—Mg_m2—Baxii85.94 (4)
K_b—O5—Si2ix112.58 (8)O1ix—Mg_m2—W_c94.06 (4)
Si2—O5—Si2ix134.82 (15)O1ix—Mg_m2—W_cxii85.94 (4)
Ti_m1(2)iv—O6—Si1137.60 (10)O1ix—Mg_m2—Ti_m20
Si1—O7—Si2ii143.51 (10)Ba—Mg_m2—Baxii180.0 (5)
Ti_m1(1)—Oh—Ti_m1(2)134.87 (6)Ba—Mg_m2—W_c0.0 (5)
Ti_m1(1)—Oh—Nb_m1(1)0.0 (5)Ba—Mg_m2—W_cxii180.0 (5)
Ti_m1(2)—Oh—Nb_m1(1)134.87 (6)Ba—Mg_m2—Ti_m20
Na_axvii—Ba—Na_axviii34.97 (6)Baxii—Mg_m2—W_c180.0 (5)
Na_axvii—Ba—Na_avii111.57 (5)Baxii—Mg_m2—W_cxii0.0 (5)
Na_axvii—Ba—Na_axiii102.25 (4)Baxii—Mg_m2—Ti_m20
Na_axvii—Ba—K_b124.50 (3)W_c—Mg_m2—W_cxii180.0 (5)
Na_axvii—Ba—Ti_m1(2)131.54 (4)W_c—Mg_m2—Ti_m20
Na_axvii—Ba—Ti_m1(2)xiv50.63 (4)W_cxii—Mg_m2—Ti_m20
Na_axvii—Ba—Fe_m291.49 (5)
Symmetry codes: (i) x+1, y, z; (ii) x, y, z1; (iii) x+1, y, z+1; (iv) x+1/2, y+1/2, z+1; (v) x+1/2, y+1/2, z; (vi) x+1/2, y+1/2, z; (vii) x+1/2, y+1/2, z; (viii) x+1, y, z+2; (ix) x, y, z; (x) x, y, z+1; (xi) x+1, y, z+1; (xii) x, y, z+1; (xiii) x1/2, y+1/2, z; (xiv) x, y, z+1; (xv) x, y, z; (xvi) x, y, z+1; (xvii) x1/2, y1/2, z; (xviii) x+1/2, y1/2, z; (xix) x, y, z.
(labu-Fe_3.15) top
Crystal data top
Ba0.7Fe0.5K2.1Mg0.05Na2Nb0.1O33Si8Ti4Z = 2
Mr = 1206.8F(000) = 1167
Monoclinic, C2/mDx = 3.058 Mg m3
Hall symbol: -C 2ySynchrotron radiation, λ = 0.414 Å
a = 14.081 (13) ÅCell parameters from 3042 reflections
b = 13.5962 (10) Åθ = 1.7–18.9°
c = 7.663 (3) ŵ = 0.81 mm1
β = 116.74 (6)°T = 293 K
V = 1310.3 (15) Å3Anhedral grain
Data collection top
ESRF ID 09
diffractometer
θmax = 18.9°, θmin = 1.7°
3042 measured reflectionsh = 88
936 independent reflectionsk = 2120
760 reflections with I > 2σ(I)l = 1110
Rint = 0.072
Refinement top
Refinement on F0 restraints
R[F2 > 2σ(F2)] = 0.0746 constraints
wR(F2) = 0.134Weighting scheme based on measured s.u.'s w = 1/(σ2(F) + 0.0120999999F2)
S = 1.06(Δ/σ)max = 0.049
936 reflectionsΔρmax = 0.83 e Å3
66 parametersΔρmin = 1.03 e Å3
Fractional atomic coordinates and isotropic or equivalent isotropic displacement parameters (Å2) top
xyzUiso*/UeqOcc. (<1)
Na_a0.4156 (14)0.2641 (5)0.0131 (11)0.0253 (16)*0.5
K_b0.4244 (6)00.7085 (4)0.024 (4)
Ti_m1(1)0.250.250.50.0109 (5)*0.95
Ti_m1(2)00.22420 (12)0.50.0084 (5)*
Fe_m2000.50.0243 (11)*0.5
Si10.3213 (4)0.11100 (12)0.2553 (2)0.0053 (5)*
Si20.2094 (3)0.10955 (12)0.8066 (2)0.0051 (5)*
O10.0827 (9)0.1121 (3)0.6759 (7)0.0086 (10)*
O20.2749 (8)0.1875 (3)0.7462 (6)0.0074 (10)*
O30.2715 (9)0.1222 (3)0.4026 (6)0.0072 (10)*
O40.3735 (14)00.2759 (10)0.0098 (14)*
O50.2550 (13)00.7915 (10)0.0094 (14)*
O60.4174 (9)0.1837 (3)0.2980 (7)0.0126 (11)*
O70.2314 (9)0.1262 (3)0.0296 (7)0.0106 (11)*
Oh0.1010 (9)0.2201 (3)0.3935 (7)0.0089 (10)*
Ba0.0874 (3)00.3422 (2)0.0125 (5)*0.35
W10.50.1457 (7)00.097 (17)
W200.1134 (7)00.08 (2)
W_c0.0874 (3)00.3422 (2)0.0125 (5)*0.65
Nb_m1(1)0.250.250.50.0109 (5)*0.05
Ti_m2000.50.0243 (11)*0.1
Mg_m2000.50.0243 (11)*0.05
Atomic displacement parameters (Å2) top
U11U22U33U12U13U23
K_b0.019 (8)0.0411 (15)0.0140 (11)00.0091 (19)0
W10.19 (4)0.025 (5)0.019 (4)00.007 (8)0
W20.15 (5)0.035 (6)0.026 (5)00.020 (10)0
Geometric parameters (Å, º) top
Na_a—Na_ai2.47 (3)Si2—Si2vi2.979 (2)
Na_a—Ti_m1(2)ii3.372 (9)Si2—O11.605 (12)
Na_a—Si13.429 (15)Si2—O1vi3.414 (7)
Na_a—Si1iii3.475 (16)Si2—O21.604 (10)
Na_a—Si2iv3.349 (15)Si2—O51.647 (9)
Na_a—Si2ii3.186 (17)Si2—O6ii3.232 (8)
Na_a—O1ii2.909 (13)Si2—O7ix1.609 (7)
Na_a—O2iv2.356 (13)Si2—Oh3.204 (6)
Na_a—O3iii3.454 (12)Si2—Nb_m1(1)3.272 (3)
Na_a—O62.432 (14)Si2—Ti_m23.194 (7)
Na_a—O73.25 (2)Si2—Mg_m23.194 (7)
Na_a—O7iii2.45 (2)O1—O1xi2.655 (11)
Na_a—Ohiii3.026 (14)O1—O1vi3.048 (6)
Na_a—Ohv2.917 (13)O1—O22.711 (17)
Na_a—W12.029 (15)O1—O52.657 (18)
Na_a—W2iii2.075 (15)O1—O6ii2.784 (6)
K_b—Si13.451 (5)O1—O7ix2.580 (10)
K_b—Si1vi3.451 (5)O1—Oh2.722 (11)
K_b—O23.400 (10)O1—Ohxi2.809 (16)
K_b—O2vi3.400 (10)O1—Ba3.004 (8)
K_b—O32.890 (8)O1—Baxi2.790 (13)
K_b—O3vi2.890 (8)O1—W2ix3.183 (11)
K_b—O43.061 (10)O1—W_c3.004 (8)
K_b—O4vii2.79 (2)O1—W_cxi2.790 (13)
K_b—O52.73 (2)O1—Ti_m22.021 (5)
K_b—O6vii3.361 (11)O1—Mg_m22.021 (5)
K_b—O6viii3.361 (11)O2—O32.759 (10)
K_b—W1ix2.812 (7)O2—O3ii2.785 (6)
K_b—W1viii2.812 (7)O2—O52.605 (6)
Ti_m1(1)—Si13.129 (4)O2—O6ii3.113 (16)
Ti_m1(1)—Si1ii3.129 (4)O2—O7ix2.642 (13)
Ti_m1(1)—Si23.272 (3)O2—O7ii3.084 (8)
Ti_m1(1)—Si2ii3.272 (3)O2—Oh2.746 (11)
Ti_m1(1)—O21.952 (6)O2—Ohii2.732 (15)
Ti_m1(1)—O2ii1.952 (6)O2—W1ix2.933 (12)
Ti_m1(1)—O31.968 (6)O2—Nb_m1(1)1.952 (6)
Ti_m1(1)—O3ii1.968 (6)O3—O3vi3.322 (6)
Ti_m1(1)—O63.471 (13)O3—O42.649 (18)
Ti_m1(1)—O6ii3.471 (13)O3—O62.653 (18)
Ti_m1(1)—Oh1.922 (12)O3—O72.653 (9)
Ti_m1(1)—Ohii1.922 (12)O3—Oh2.720 (17)
Ti_m1(1)—Nb_m1(1)0O3—Ohii2.782 (9)
Ti_m1(2)—Fe_m23.0483 (17)O3—Ba2.935 (12)
Ti_m1(2)—Si1ii3.259 (5)O3—W_c2.935 (12)
Ti_m1(2)—Si1x3.259 (5)O3—Nb_m1(1)1.968 (6)
Ti_m1(2)—Si23.227 (7)O4—O5iv3.315 (10)
Ti_m1(2)—Si2xi3.227 (7)O4—O62.559 (7)
Ti_m1(2)—O12.021 (6)O4—O6vi2.559 (7)
Ti_m1(2)—O1xi2.021 (6)O4—O72.668 (12)
Ti_m1(2)—O23.496 (13)O4—O7vi2.668 (12)
Ti_m1(2)—O2xi3.496 (13)O5—O7ix2.633 (13)
Ti_m1(2)—O6ii1.923 (6)O5—O7xiii2.633 (13)
Ti_m1(2)—O6x1.923 (6)O5—Ba3.180 (9)
Ti_m1(2)—Oh1.933 (12)O5—W_c3.180 (9)
Ti_m1(2)—Ohxi1.933 (12)O5—Ti_m23.266 (17)
Ti_m1(2)—Ti_m23.0483 (17)O5—Mg_m23.266 (17)
Ti_m1(2)—Mg_m23.0483 (17)O6—O6vii2.919 (10)
Fe_m2—Si23.194 (7)O6—O72.618 (14)
Fe_m2—Si2xi3.194 (7)O6—Ohii2.814 (11)
Fe_m2—Si2xii3.194 (7)O6—Ohv2.689 (16)
Fe_m2—Si2vi3.194 (7)O6—W13.037 (11)
Fe_m2—O12.021 (5)O6—Nb_m1(1)3.471 (13)
Fe_m2—O1xi2.021 (5)O7—O7iii3.467 (8)
Fe_m2—O1xii2.021 (5)O7—O7vi3.433 (7)
Fe_m2—O1vi2.021 (5)O7—W23.167 (15)
Fe_m2—O53.266 (17)Oh—Ba3.013 (4)
Fe_m2—O5xi3.266 (17)Oh—W1iii3.253 (8)
Fe_m2—Ba2.078 (4)Oh—W23.060 (7)
Fe_m2—Baxi2.078 (4)Oh—W_c3.013 (4)
Fe_m2—W_c2.078 (4)Oh—Nb_m1(1)1.922 (12)
Fe_m2—W_cxi2.078 (4)Ba—W22.804 (6)
Fe_m2—Ti_m20Ba—W2xiv2.804 (6)
Fe_m2—Mg_m20Ba—W_c0
Si1—Si1vi3.018 (2)Ba—Ti_m22.078 (4)
Si1—Si2iv3.071 (5)Ba—Mg_m22.078 (4)
Si1—O2ii3.054 (7)W1—W2iii3.275 (14)
Si1—O31.581 (12)W2—W2xiv3.084 (14)
Si1—O41.655 (8)W2—W_c2.804 (6)
Si1—O61.586 (11)W2—W_cxv2.804 (6)
Si1—O71.633 (7)W_c—Ti_m22.078 (4)
Si1—Ohii3.326 (5)W_c—Mg_m22.078 (4)
Si1—Nb_m1(1)3.129 (4)Ti_m2—Mg_m20
Na_ai—Na_a—Ti_m1(2)ii102.5 (4)Si1vi—O4—O6168.4 (11)
Na_ai—Na_a—Si1131.6 (4)Si1vi—O4—O6vi36.9 (4)
Na_ai—Na_a—Si1iii130.8 (4)Si1vi—O4—O7111.1 (7)
Na_ai—Na_a—Si2iv128.5 (4)Si1vi—O4—O7vi35.5 (2)
Na_ai—Na_a—Si2ii140.7 (4)O3—O4—O3vi77.7 (6)
Na_ai—Na_a—O1ii114.4 (5)O3—O4—O5iv109.1 (5)
Na_ai—Na_a—O2iv113.2 (6)O3—O4—O661.2 (4)
Na_ai—Na_a—O3iii106.7 (5)O3—O4—O6vi137.9 (7)
Na_ai—Na_a—O6116.8 (6)O3—O4—O759.9 (4)
Na_ai—Na_a—O7144.7 (4)O3—O4—O7vi107.7 (7)
Na_ai—Na_a—O7iii140.7 (5)O3vi—O4—O5iv109.1 (5)
Na_ai—Na_a—Ohiii63.1 (5)O3vi—O4—O6137.9 (7)
Na_ai—Na_a—Ohv67.7 (5)O3vi—O4—O6vi61.2 (4)
Na_ai—Na_a—W152.5 (5)O3vi—O4—O7107.7 (7)
Na_ai—Na_a—W2iii53.4 (5)O3vi—O4—O7vi59.9 (4)
Ti_m1(2)ii—Na_a—Si157.3 (2)O5iv—O4—O693.4 (2)
Ti_m1(2)ii—Na_a—Si1iii113.5 (5)O5iv—O4—O6vi93.4 (2)
Ti_m1(2)ii—Na_a—Si2iv110.6 (4)O5iv—O4—O750.8 (3)
Ti_m1(2)ii—Na_a—Si2ii58.9 (2)O5iv—O4—O7vi50.8 (3)
Ti_m1(2)ii—Na_a—O1ii36.61 (15)O6—O4—O6vi154.6 (9)
Ti_m1(2)ii—Na_a—O2iv136.2 (7)O6—O4—O760.1 (3)
Ti_m1(2)ii—Na_a—O3iii137.9 (5)O6—O4—O7vi139.2 (4)
Ti_m1(2)ii—Na_a—O634.07 (18)O6vi—O4—O7139.2 (4)
Ti_m1(2)ii—Na_a—O782.8 (4)O6vi—O4—O7vi60.1 (3)
Ti_m1(2)ii—Na_a—O7iii88.6 (4)O7—O4—O7vi80.1 (4)
Ti_m1(2)ii—Na_a—Ohiii164.1 (7)K_b—O5—Fe_m2130.3 (3)
Ti_m1(2)ii—Na_a—Ohv34.9 (3)K_b—O5—Si2115.2 (6)
Ti_m1(2)ii—Na_a—W199.8 (3)K_b—O5—Si2vi115.2 (6)
Ti_m1(2)ii—Na_a—W2iii95.2 (3)K_b—O5—O1133.2 (4)
Si1—Na_a—Si1iii96.6 (5)K_b—O5—O1vi133.2 (4)
Si1—Na_a—Si2iv53.9 (2)K_b—O5—O279.1 (5)
Si1—Na_a—Si2ii70.6 (4)K_b—O5—O2vi79.1 (5)
Si1—Na_a—O1ii76.7 (4)K_b—O5—O4ix102.0 (5)
Si1—Na_a—O2iv79.8 (5)K_b—O5—O7ix123.9 (5)
Si1—Na_a—O3iii116.8 (6)K_b—O5—O7xiii123.9 (5)
Si1—Na_a—O624.6 (3)K_b—O5—Ba92.8 (3)
Si1—Na_a—O728.15 (17)K_b—O5—W_c92.8 (3)
Si1—Na_a—O7iii86.1 (6)K_b—O5—Ti_m2130.3 (3)
Si1—Na_a—Ohiii137.0 (3)K_b—O5—Mg_m2130.3 (3)
Si1—Na_a—Ohv83.9 (3)Fe_m2—O5—Si272.8 (5)
Si1—Na_a—W185.6 (3)Fe_m2—O5—Si2vi72.8 (5)
Si1—Na_a—W2iii152.0 (4)Fe_m2—O5—O138.2 (2)
Si1iii—Na_a—Si2iv68.2 (3)Fe_m2—O5—O1vi38.2 (2)
Si1iii—Na_a—Si2ii54.7 (3)Fe_m2—O5—O293.4 (4)
Si1iii—Na_a—O1ii81.6 (4)Fe_m2—O5—O2vi93.4 (4)
Si1iii—Na_a—O2iv59.6 (4)Fe_m2—O5—O4ix127.6 (7)
Si1iii—Na_a—O3iii26.4 (2)Fe_m2—O5—O7ix91.8 (5)
Si1iii—Na_a—O6111.7 (7)Fe_m2—O5—O7xiii91.8 (5)
Si1iii—Na_a—O774.6 (4)Fe_m2—O5—Ba37.58 (17)
Si1iii—Na_a—O7iii25.19 (17)Fe_m2—O5—W_c37.58 (17)
Si1iii—Na_a—Ohiii75.3 (3)Fe_m2—O5—Ti_m20.0 (5)
Si1iii—Na_a—Ohv138.1 (4)Fe_m2—O5—Mg_m20.0 (5)
Si1iii—Na_a—W1141.8 (3)Si2—O5—Si2vi129.5 (12)
Si1iii—Na_a—W2iii89.8 (3)Si2—O5—O134.7 (4)
Si2iv—Na_a—Si2ii90.7 (5)Si2—O5—O1vi102.5 (9)
Si2iv—Na_a—O1ii115.8 (7)Si2—O5—O236.2 (4)
Si2iv—Na_a—O2iv25.9 (3)Si2—O5—O2vi164.5 (10)
Si2iv—Na_a—O3iii72.9 (3)Si2—O5—O4ix86.4 (3)
Si2iv—Na_a—O678.4 (4)Si2—O5—O7ix35.6 (2)
Si2iv—Na_a—O728.18 (17)Si2—O5—O7xiii111.5 (8)
Si2iv—Na_a—O7iii79.5 (5)Si2—O5—Ba87.3 (3)
Si2iv—Na_a—Ohiii84.8 (3)Si2—O5—W_c87.3 (3)
Si2iv—Na_a—Ohv135.6 (4)Si2—O5—Ti_m272.8 (5)
Si2iv—Na_a—W183.2 (3)Si2—O5—Mg_m272.8 (5)
Si2iv—Na_a—W2iii151.0 (3)Si2vi—O5—O1102.5 (9)
Si2ii—Na_a—O1ii30.1 (3)Si2vi—O5—O1vi34.7 (4)
Si2ii—Na_a—O2iv101.6 (7)Si2vi—O5—O2164.5 (10)
Si2ii—Na_a—O3iii79.5 (4)Si2vi—O5—O2vi36.2 (4)
Si2ii—Na_a—O668.7 (5)Si2vi—O5—O4ix86.4 (3)
Si2ii—Na_a—O771.8 (4)Si2vi—O5—O7ix111.5 (8)
Si2ii—Na_a—O7iii29.7 (2)Si2vi—O5—O7xiii35.6 (2)
Si2ii—Na_a—Ohiii127.3 (4)Si2vi—O5—Ba87.3 (3)
Si2ii—Na_a—Ohv87.0 (3)Si2vi—O5—W_c87.3 (3)
Si2ii—Na_a—W1154.1 (5)Si2vi—O5—Ti_m272.8 (5)
Si2ii—Na_a—W2iii91.6 (3)Si2vi—O5—Mg_m272.8 (5)
O1ii—Na_a—O2iv131.3 (9)O1—O5—O1vi70.0 (5)
O1ii—Na_a—O3iii102.6 (4)O1—O5—O262.0 (3)
O1ii—Na_a—O662.1 (3)O1—O5—O2vi130.8 (6)
O1ii—Na_a—O790.8 (6)O1—O5—O4ix107.3 (5)
O1ii—Na_a—O7iii56.8 (4)O1—O5—O7ix58.4 (4)
O1ii—Na_a—Ohiii140.4 (3)O1—O5—O7xiii103.0 (7)
O1ii—Na_a—Ohv57.7 (3)O1—O5—Ba61.2 (3)
O1ii—Na_a—W1135.3 (4)O1—O5—W_c61.2 (3)
O1ii—Na_a—W2iii77.4 (3)O1—O5—Ti_m238.2 (2)
O2iv—Na_a—O3iii53.3 (2)O1—O5—Mg_m238.2 (2)
O2iv—Na_a—O6104.2 (6)O1vi—O5—O2130.8 (6)
O2iv—Na_a—O753.4 (4)O1vi—O5—O2vi62.0 (3)
O2iv—Na_a—O7iii79.8 (6)O1vi—O5—O4ix107.3 (5)
O2iv—Na_a—Ohiii59.5 (4)O1vi—O5—O7ix103.0 (7)
O2iv—Na_a—Ohv157.7 (3)O1vi—O5—O7xiii58.4 (4)
O2iv—Na_a—W183.6 (3)O1vi—O5—Ba61.2 (3)
O2iv—Na_a—W2iii126.1 (4)O1vi—O5—W_c61.2 (3)
O3iii—Na_a—O6136.4 (8)O1vi—O5—Ti_m238.2 (2)
O3iii—Na_a—O790.2 (4)O1vi—O5—Mg_m238.2 (2)
O3iii—Na_a—O7iii49.9 (3)O2—O5—O2vi156.3 (8)
O3iii—Na_a—Ohiii49.1 (3)O2—O5—O4ix96.84 (18)
O3iii—Na_a—Ohv149.0 (3)O2—O5—O7ix60.6 (3)
O3iii—Na_a—W1122.0 (4)O2—O5—O7xiii141.7 (5)
O3iii—Na_a—W2iii79.1 (3)O2—O5—Ba85.84 (18)
O6—Na_a—O752.5 (4)O2—O5—W_c85.84 (18)
O6—Na_a—O7iii93.4 (7)O2—O5—Ti_m293.4 (4)
O6—Na_a—Ohiii157.1 (3)O2—O5—Mg_m293.4 (4)
O6—Na_a—Ohv59.5 (3)O2vi—O5—O4ix96.84 (18)
O6—Na_a—W185.3 (3)O2vi—O5—O7ix141.7 (5)
O6—Na_a—W2iii129.0 (4)O2vi—O5—O7xiii60.6 (3)
O7—Na_a—O7iii73.4 (6)O2vi—O5—Ba85.84 (18)
O7—Na_a—Ohiii112.8 (4)O2vi—O5—W_c85.84 (18)
O7—Na_a—Ohv112.0 (4)O2vi—O5—Ti_m293.4 (4)
O7—Na_a—W192.3 (4)O2vi—O5—Mg_m293.4 (4)
O7—Na_a—W2iii161.8 (7)O4ix—O5—O7ix51.8 (3)
O7iii—Na_a—Ohiii98.6 (3)O4ix—O5—O7xiii51.8 (3)
O7iii—Na_a—Ohv114.2 (4)O4ix—O5—Ba165.2 (8)
O7iii—Na_a—W1162.6 (7)O4ix—O5—W_c165.2 (8)
O7iii—Na_a—W2iii88.4 (4)O4ix—O5—Ti_m2127.6 (7)
Ohiii—Na_a—Ohv130.1 (8)O4ix—O5—Mg_m2127.6 (7)
Ohiii—Na_a—W177.4 (5)O7ix—O5—O7xiii81.4 (4)
Ohiii—Na_a—W2iii71.0 (4)O7ix—O5—Ba119.1 (5)
Ohv—Na_a—W180.1 (5)O7ix—O5—W_c119.1 (5)
Ohv—Na_a—W2iii73.4 (4)O7ix—O5—Ti_m291.8 (5)
W1—Na_a—W2iii105.9 (9)O7ix—O5—Mg_m291.8 (5)
Si1—K_b—Si1vi51.86 (6)O7xiii—O5—Ba119.1 (5)
Si1—K_b—O276.19 (13)O7xiii—O5—W_c119.1 (5)
Si1—K_b—O2vi114.64 (18)O7xiii—O5—Ti_m291.8 (5)
Si1—K_b—O327.1 (2)O7xiii—O5—Mg_m291.8 (5)
Si1—K_b—O3vi67.18 (13)Ba—O5—W_c0.0 (5)
Si1—K_b—O428.65 (15)Ba—O5—Ti_m237.58 (17)
Si1—K_b—O4vii90.1 (2)Ba—O5—Mg_m237.58 (17)
Si1—K_b—O5102.6 (2)W_c—O5—Ti_m237.58 (17)
Si1—K_b—O6vii69.01 (15)W_c—O5—Mg_m237.58 (17)
Si1—K_b—O6viii106.9 (2)Ti_m2—O5—Mg_m20.0 (5)
Si1—K_b—W1ix109.19 (15)Na_a—O6—K_bvii93.4 (5)
Si1—K_b—W1viii160.89 (16)Na_a—O6—Ti_m1(1)123.3 (5)
Si1vi—K_b—O2114.64 (18)Na_a—O6—Ti_m1(2)ii100.8 (4)
Si1vi—K_b—O2vi76.19 (13)Na_a—O6—Si1115.6 (4)
Si1vi—K_b—O367.18 (13)Na_a—O6—Si2ii66.7 (4)
Si1vi—K_b—O3vi27.1 (2)Na_a—O6—O1ii67.4 (3)
Si1vi—K_b—O428.65 (15)Na_a—O6—O2ii89.6 (5)
Si1vi—K_b—O4vii90.1 (2)Na_a—O6—O3135.8 (6)
Si1vi—K_b—O5102.6 (2)Na_a—O6—O4118.3 (4)
Si1vi—K_b—O6vii106.9 (2)Na_a—O6—O6vii129.3 (6)
Si1vi—K_b—O6viii69.01 (15)Na_a—O6—O780.0 (4)
Si1vi—K_b—W1ix160.89 (16)Na_a—O6—Ohii125.3 (3)
Si1vi—K_b—W1viii109.19 (15)Na_a—O6—Ohv69.2 (5)
O2—K_b—O2vi97.1 (3)Na_a—O6—W141.7 (4)
O2—K_b—O351.3 (2)Na_a—O6—Nb_m1(1)123.3 (5)
O2—K_b—O3vi103.6 (3)K_bvii—O6—Ti_m1(1)141.9 (2)
O2—K_b—O4103.9 (3)K_bvii—O6—Ti_m1(2)ii109.3 (4)
O2—K_b—O4vii130.85 (19)K_bvii—O6—Si192.5 (3)
O2—K_b—O548.78 (19)K_bvii—O6—Si2ii159.7 (4)
O2—K_b—O6vii83.4 (2)K_bvii—O6—O1ii139.8 (5)
O2—K_b—O6viii176.33 (15)K_bvii—O6—O2ii165.1 (3)
O2—K_b—W1ix55.38 (17)K_bvii—O6—O3112.2 (2)
O2—K_b—W1viii119.2 (2)K_bvii—O6—O454.3 (5)
O2vi—K_b—O3103.6 (3)K_bvii—O6—O6vii78.4 (3)
O2vi—K_b—O3vi51.3 (2)K_bvii—O6—O7101.7 (3)
O2vi—K_b—O4103.9 (3)K_bvii—O6—Ohii132.1 (2)
O2vi—K_b—O4vii130.85 (19)K_bvii—O6—Ohv78.6 (4)
O2vi—K_b—O548.78 (19)K_bvii—O6—W151.8 (2)
O2vi—K_b—O6vii176.33 (15)K_bvii—O6—Nb_m1(1)141.9 (2)
O2vi—K_b—O6viii83.4 (2)Ti_m1(1)—O6—Ti_m1(2)ii76.0 (3)
O2vi—K_b—W1ix119.2 (2)Ti_m1(1)—O6—Si164.3 (4)
O2vi—K_b—W1viii55.38 (17)Ti_m1(1)—O6—Si2ii58.3 (2)
O3—K_b—O3vi70.17 (18)Ti_m1(1)—O6—O1ii71.7 (3)
O3—K_b—O452.8 (3)Ti_m1(1)—O6—O2ii33.94 (18)
O3—K_b—O4vii114.0 (3)Ti_m1(1)—O6—O334.31 (18)
O3—K_b—O577.2 (3)Ti_m1(1)—O6—O495.2 (5)
O3—K_b—O6vii79.5 (3)Ti_m1(1)—O6—O6vii84.5 (3)
O3—K_b—O6viii132.2 (2)Ti_m1(1)—O6—O777.8 (4)
O3—K_b—W1ix96.72 (18)Ti_m1(1)—O6—Ohii33.6 (3)
O3—K_b—W1viii158.0 (4)Ti_m1(1)—O6—Ohv121.0 (2)
O3vi—K_b—O452.8 (3)Ti_m1(1)—O6—W1161.1 (3)
O3vi—K_b—O4vii114.0 (3)Ti_m1(1)—O6—Nb_m1(1)0.0 (5)
O3vi—K_b—O577.2 (3)Ti_m1(2)ii—O6—Si1136.3 (6)
O3vi—K_b—O6vii132.2 (2)Ti_m1(2)ii—O6—Si2ii72.5 (2)
O3vi—K_b—O6viii79.5 (3)Ti_m1(2)ii—O6—O1ii46.54 (17)
O3vi—K_b—W1ix158.0 (4)Ti_m1(2)ii—O6—O2ii84.4 (3)
O3vi—K_b—W1viii96.72 (18)Ti_m1(2)ii—O6—O3103.4 (4)
O4—K_b—O4vii77.5 (4)Ti_m1(2)ii—O6—O4136.8 (3)
O4—K_b—O5116.7 (4)Ti_m1(2)ii—O6—O6vii40.65 (15)
O4—K_b—O6vii79.5 (3)Ti_m1(2)ii—O6—O7148.8 (6)
O4—K_b—O6viii79.5 (3)Ti_m1(2)ii—O6—Ohii43.3 (3)
O4—K_b—W1ix132.91 (19)Ti_m1(2)ii—O6—Ohv45.9 (3)
O4—K_b—W1viii132.91 (19)Ti_m1(2)ii—O6—W1114.7 (5)
O4vii—K_b—O5165.8 (2)Ti_m1(2)ii—O6—Nb_m1(1)76.0 (3)
O4vii—K_b—O6vii48.1 (2)Si1—O6—Si2ii99.6 (5)
O4vii—K_b—O6viii48.1 (2)Si1—O6—O1ii127.5 (7)
O4vii—K_b—W1ix87.2 (2)Si1—O6—O2ii73.1 (5)
O4vii—K_b—W1viii87.2 (2)Si1—O6—O333.0 (3)
O5—K_b—O6vii131.1 (2)Si1—O6—O438.8 (4)
O5—K_b—O6viii131.1 (2)Si1—O6—O6vii114.7 (4)
O5—K_b—W1ix82.71 (19)Si1—O6—O736.2 (2)
O5—K_b—W1viii82.71 (19)Si1—O6—Ohii94.1 (6)
O6vii—K_b—O6viii95.9 (3)Si1—O6—Ohv170.4 (5)
O6vii—K_b—W1ix58.13 (17)Si1—O6—W1108.6 (3)
O6vii—K_b—W1viii121.3 (2)Si1—O6—Nb_m1(1)64.3 (4)
O6viii—K_b—W1ix121.3 (2)Si2ii—O6—O1ii29.8 (2)
O6viii—K_b—W1viii58.13 (17)Si2ii—O6—O2ii29.21 (18)
W1ix—K_b—W1viii89.6 (2)Si2ii—O6—O386.2 (4)
Si1—Ti_m1(1)—Si1ii180.0 (5)Si2ii—O6—O4137.9 (6)
Si1—Ti_m1(1)—Si2106.55 (7)Si2ii—O6—O6vii110.5 (2)
Si1—Ti_m1(1)—Si2ii73.45 (7)Si2ii—O6—O779.6 (3)
Si1—Ti_m1(1)—O2110.5 (2)Si2ii—O6—Ohii63.6 (2)
Si1—Ti_m1(1)—O2ii69.5 (2)Si2ii—O6—Ohv90.0 (2)
Si1—Ti_m1(1)—O325.0 (3)Si2ii—O6—W1108.5 (2)
Si1—Ti_m1(1)—O3ii155.0 (3)Si2ii—O6—Nb_m1(1)58.3 (2)
Si1—Ti_m1(1)—O627.17 (14)O1ii—O6—O2ii54.4 (3)
Si1—Ti_m1(1)—O6ii152.83 (14)O1ii—O6—O3105.5 (5)
Si1—Ti_m1(1)—Oh101.6 (2)O1ii—O6—O4165.9 (8)
Si1—Ti_m1(1)—Ohii78.4 (2)O1ii—O6—O6vii87.1 (2)
Si1—Ti_m1(1)—Nb_m1(1)0O1ii—O6—O7108.7 (4)
Si1ii—Ti_m1(1)—Si273.45 (7)O1ii—O6—Ohii58.2 (2)
Si1ii—Ti_m1(1)—Si2ii106.55 (7)O1ii—O6—Ohv61.7 (3)
Si1ii—Ti_m1(1)—O269.5 (2)O1ii—O6—W1103.6 (4)
Si1ii—Ti_m1(1)—O2ii110.5 (2)O1ii—O6—Nb_m1(1)71.7 (3)
Si1ii—Ti_m1(1)—O3155.0 (3)O2ii—O6—O357.1 (3)
Si1ii—Ti_m1(1)—O3ii25.0 (3)O2ii—O6—O4111.7 (6)
Si1ii—Ti_m1(1)—O6152.83 (14)O2ii—O6—O6vii110.8 (3)
Si1ii—Ti_m1(1)—O6ii27.17 (14)O2ii—O6—O764.4 (3)
Si1ii—Ti_m1(1)—Oh78.4 (2)O2ii—O6—Ohii54.9 (3)
Si1ii—Ti_m1(1)—Ohii101.6 (2)O2ii—O6—Ohv116.0 (3)
Si1ii—Ti_m1(1)—Nb_m1(1)0O2ii—O6—W1128.5 (2)
Si2—Ti_m1(1)—Si2ii180.0 (5)O2ii—O6—Nb_m1(1)33.94 (18)
Si2—Ti_m1(1)—O220.8 (3)O3—O6—O461.1 (5)
Si2—Ti_m1(1)—O2ii159.2 (3)O3—O6—O6vii92.0 (4)
Si2—Ti_m1(1)—O382.2 (3)O3—O6—O760.4 (4)
Si2—Ti_m1(1)—O3ii97.8 (3)O3—O6—Ohii61.1 (3)
Si2—Ti_m1(1)—O6122.81 (11)O3—O6—Ohv148.3 (3)
Si2—Ti_m1(1)—O6ii57.19 (11)O3—O6—W1141.6 (3)
Si2—Ti_m1(1)—Oh70.80 (19)O3—O6—Nb_m1(1)34.31 (18)
Si2—Ti_m1(1)—Ohii109.20 (19)O4—O6—O6vii97.1 (3)
Si2—Ti_m1(1)—Nb_m1(1)0O4—O6—O762.0 (3)
Si2ii—Ti_m1(1)—O2159.2 (3)O4—O6—Ohii113.5 (5)
Si2ii—Ti_m1(1)—O2ii20.8 (3)O4—O6—Ohv131.8 (6)
Si2ii—Ti_m1(1)—O397.8 (3)O4—O6—W187.0 (4)
Si2ii—Ti_m1(1)—O3ii82.2 (3)O4—O6—Nb_m1(1)95.2 (5)
Si2ii—Ti_m1(1)—O657.19 (11)O6vii—O6—O7150.7 (5)
Si2ii—Ti_m1(1)—O6ii122.81 (11)O6vii—O6—Ohii55.9 (3)
Si2ii—Ti_m1(1)—Oh109.20 (19)O6vii—O6—Ohv60.1 (3)
Si2ii—Ti_m1(1)—Ohii70.80 (19)O6vii—O6—W1113.9 (5)
Si2ii—Ti_m1(1)—Nb_m1(1)0O6vii—O6—Nb_m1(1)84.5 (3)
O2—Ti_m1(1)—O2ii180.0 (5)O7—O6—Ohii111.2 (6)
O2—Ti_m1(1)—O389.5 (2)O7—O6—Ohv149.2 (4)
O2—Ti_m1(1)—O3ii90.5 (2)O7—O6—W186.8 (3)
O2—Ti_m1(1)—O6117.1 (3)O7—O6—Nb_m1(1)77.8 (4)
O2—Ti_m1(1)—O6ii62.9 (3)Ohii—O6—Ohv89.2 (3)
O2—Ti_m1(1)—Oh90.3 (4)Ohii—O6—W1157.2 (4)
O2—Ti_m1(1)—Ohii89.7 (4)Ohii—O6—Nb_m1(1)33.6 (3)
O2—Ti_m1(1)—Nb_m1(1)0Ohv—O6—W168.9 (4)
O2ii—Ti_m1(1)—O390.5 (2)Ohv—O6—Nb_m1(1)121.0 (2)
O2ii—Ti_m1(1)—O3ii89.5 (2)W1—O6—Nb_m1(1)161.1 (3)
O2ii—Ti_m1(1)—O662.9 (3)Na_a—O7—Na_aiii106.6 (4)
O2ii—Ti_m1(1)—O6ii117.1 (3)Na_a—O7—Si182.1 (5)
O2ii—Ti_m1(1)—Oh89.7 (4)Na_a—O7—Si2iv79.4 (5)
O2ii—Ti_m1(1)—Ohii90.3 (4)Na_a—O7—O1iv106.7 (4)
O2ii—Ti_m1(1)—Nb_m1(1)0Na_a—O7—O2iv45.7 (3)
O3—Ti_m1(1)—O3ii180.0 (5)Na_a—O7—O2ii76.8 (3)
O3—Ti_m1(1)—O649.5 (4)Na_a—O7—O3105.5 (4)
O3—Ti_m1(1)—O6ii130.5 (4)Na_a—O7—O492.3 (5)
O3—Ti_m1(1)—Oh88.7 (4)Na_a—O7—O5iv89.8 (5)
O3—Ti_m1(1)—Ohii91.3 (4)Na_a—O7—O647.5 (3)
O3—Ti_m1(1)—Nb_m1(1)0Na_a—O7—O7iii42.7 (3)
O3ii—Ti_m1(1)—O6130.5 (4)Na_a—O7—O7vi125.2 (5)
O3ii—Ti_m1(1)—O6ii49.5 (4)Na_a—O7—W2147.4 (4)
O3ii—Ti_m1(1)—Oh91.3 (4)Na_aiii—O7—Si1115.1 (5)
O3ii—Ti_m1(1)—Ohii88.7 (4)Na_aiii—O7—Si2iv101.3 (4)
O3ii—Ti_m1(1)—Nb_m1(1)0Na_aiii—O7—O1iv70.6 (4)
O6—Ti_m1(1)—O6ii180.0 (5)Na_aiii—O7—O2iv101.1 (4)
O6—Ti_m1(1)—Oh125.9 (3)Na_aiii—O7—O2ii48.7 (3)
O6—Ti_m1(1)—Ohii54.1 (3)Na_aiii—O7—O385.1 (4)
O6—Ti_m1(1)—Nb_m1(1)0Na_aiii—O7—O4143.7 (6)
O6ii—Ti_m1(1)—Oh54.1 (3)Na_aiii—O7—O5iv131.8 (4)
O6ii—Ti_m1(1)—Ohii125.9 (3)Na_aiii—O7—O6114.2 (3)
O6ii—Ti_m1(1)—Nb_m1(1)0Na_aiii—O7—O7iii63.9 (4)
Oh—Ti_m1(1)—Ohii180.0 (5)Na_aiii—O7—O7vi127.5 (6)
Oh—Ti_m1(1)—Nb_m1(1)0Na_aiii—O7—W240.9 (4)
Ohii—Ti_m1(1)—Nb_m1(1)0Si1—O7—Si2iv142.5 (9)
Na_aii—Ti_m1(2)—Na_ax174.58 (17)Si1—O7—O1iv168.2 (3)
Na_aii—Ti_m1(2)—Fe_m292.71 (12)Si1—O7—O2iv123.7 (7)
Na_aii—Ti_m1(2)—Si1ii62.3 (2)Si1—O7—O2ii73.6 (2)
Na_aii—Ti_m1(2)—Si1x113.6 (2)Si1—O7—O333.7 (4)
Na_aii—Ti_m1(2)—Si257.7 (3)Si1—O7—O436.1 (2)
Na_aii—Ti_m1(2)—Si2xi125.5 (3)Si1—O7—O5iv111.8 (5)
Na_aii—Ti_m1(2)—O159.1 (3)Si1—O7—O635.0 (3)
Na_aii—Ti_m1(2)—O1xi125.7 (3)Si1—O7—O7iii99.8 (3)
Na_aii—Ti_m1(2)—O269.9 (4)Si1—O7—O7vi82.7 (2)
Na_aii—Ti_m1(2)—O2xi110.9 (4)Si1—O7—W2110.6 (5)
Na_aii—Ti_m1(2)—O6ii45.1 (3)Si2iv—O7—O1iv36.6 (4)
Na_aii—Ti_m1(2)—O6x130.1 (3)Si2iv—O7—O2iv34.6 (3)
Na_aii—Ti_m1(2)—Oh120.6 (4)Si2iv—O7—O2ii131.9 (3)
Na_aii—Ti_m1(2)—Ohxi59.6 (4)Si2iv—O7—O3170.6 (3)
Na_aii—Ti_m1(2)—Ti_m292.71 (12)Si2iv—O7—O4112.6 (5)
Na_aii—Ti_m1(2)—Mg_m292.71 (12)Si2iv—O7—O5iv36.5 (2)
Na_ax—Ti_m1(2)—Fe_m292.71 (12)Si2iv—O7—O6121.5 (7)
Na_ax—Ti_m1(2)—Si1ii113.6 (2)Si2iv—O7—O7iii88.1 (3)
Na_ax—Ti_m1(2)—Si1x62.3 (2)Si2iv—O7—O7vi81.9 (2)
Na_ax—Ti_m1(2)—Si2125.5 (3)Si2iv—O7—W2102.5 (5)
Na_ax—Ti_m1(2)—Si2xi57.7 (3)O1iv—O7—O2iv62.5 (4)
Na_ax—Ti_m1(2)—O1125.7 (3)O1iv—O7—O2ii115.7 (4)
Na_ax—Ti_m1(2)—O1xi59.1 (3)O1iv—O7—O3144.0 (7)
Na_ax—Ti_m1(2)—O2110.9 (4)O1iv—O7—O4133.7 (3)
Na_ax—Ti_m1(2)—O2xi69.9 (4)O1iv—O7—O5iv61.3 (4)
Na_ax—Ti_m1(2)—O6ii130.1 (3)O1iv—O7—O6154.1 (5)
Na_ax—Ti_m1(2)—O6x45.1 (3)O1iv—O7—O7iii91.95 (19)
Na_ax—Ti_m1(2)—Oh59.6 (4)O1iv—O7—O7vi85.73 (19)
Na_ax—Ti_m1(2)—Ohxi120.6 (4)O1iv—O7—W266.3 (4)
Na_ax—Ti_m1(2)—Ti_m292.71 (12)O2iv—O7—O2ii105.9 (3)
Na_ax—Ti_m1(2)—Mg_m292.71 (12)O2iv—O7—O3151.2 (5)
Fe_m2—Ti_m1(2)—Si1ii133.43 (6)O2iv—O7—O4114.0 (6)
Fe_m2—Ti_m1(2)—Si1x133.43 (6)O2iv—O7—O5iv59.2 (3)
Fe_m2—Ti_m1(2)—Si261.11 (5)O2iv—O7—O691.8 (5)
Fe_m2—Ti_m1(2)—Si2xi61.11 (5)O2iv—O7—O7iii58.8 (2)
Fe_m2—Ti_m1(2)—O141.05 (16)O2iv—O7—O7vi108.4 (3)
Fe_m2—Ti_m1(2)—O1xi41.05 (16)O2iv—O7—W2124.8 (3)
Fe_m2—Ti_m1(2)—O281.79 (8)O2ii—O7—O357.49 (18)
Fe_m2—Ti_m1(2)—O2xi81.79 (8)O2ii—O7—O4109.6 (2)
Fe_m2—Ti_m1(2)—O6ii130.65 (16)O2ii—O7—O5iv165.0 (5)
Fe_m2—Ti_m1(2)—O6x130.65 (16)O2ii—O7—O665.6 (3)
Fe_m2—Ti_m1(2)—Oh88.35 (14)O2ii—O7—O7iii47.1 (2)
Fe_m2—Ti_m1(2)—Ohxi88.35 (14)O2ii—O7—O7vi145.2 (3)
Fe_m2—Ti_m1(2)—Ti_m20.0 (5)O2ii—O7—W278.4 (4)
Fe_m2—Ti_m1(2)—Mg_m20.0 (5)O3—O7—O459.7 (4)
Si1ii—Ti_m1(2)—Si1x93.14 (11)O3—O7—O5iv134.5 (3)
Si1ii—Ti_m1(2)—Si272.37 (9)O3—O7—O660.4 (4)
Si1ii—Ti_m1(2)—Si2xi165.27 (7)O3—O7—O7iii100.9 (2)
Si1ii—Ti_m1(2)—O194.0 (2)O3—O7—O7vi88.8 (2)
Si1ii—Ti_m1(2)—O1xi165.1 (4)O3—O7—W277.9 (4)
Si1ii—Ti_m1(2)—O253.62 (11)O4—O7—O5iv77.4 (3)
Si1ii—Ti_m1(2)—O2xi142.14 (12)O4—O7—O657.9 (3)
Si1ii—Ti_m1(2)—O6ii19.6 (4)O4—O7—O7iii127.4 (4)
Si1ii—Ti_m1(2)—O6x92.6 (2)O4—O7—O7vi49.9 (2)
Si1ii—Ti_m1(2)—Oh74.84 (18)O4—O7—W2115.8 (5)
Si1ii—Ti_m1(2)—Ohxi107.53 (18)O5iv—O7—O6110.2 (6)
Si1ii—Ti_m1(2)—Ti_m2133.43 (6)O5iv—O7—O7iii117.9 (4)
Si1ii—Ti_m1(2)—Mg_m2133.43 (6)O5iv—O7—O7vi49.3 (3)
Si1x—Ti_m1(2)—Si2165.27 (7)O5iv—O7—W2111.2 (5)
Si1x—Ti_m1(2)—Si2xi72.37 (9)O6—O7—O7iii69.9 (2)
Si1x—Ti_m1(2)—O1165.1 (4)O6—O7—O7vi107.3 (3)
Si1x—Ti_m1(2)—O1xi94.0 (2)O6—O7—W2134.9 (4)
Si1x—Ti_m1(2)—O2142.14 (12)O7iii—O7—O7vi166.1 (5)
Si1x—Ti_m1(2)—O2xi53.62 (11)O7iii—O7—W2104.8 (4)
Si1x—Ti_m1(2)—O6ii92.6 (2)O7vi—O7—W286.8 (4)
Si1x—Ti_m1(2)—O6x19.6 (4)Na_aiii—Oh—Na_ax49.1 (5)
Si1x—Ti_m1(2)—Oh107.53 (18)Na_aiii—Oh—Ti_m1(1)89.2 (5)
Si1x—Ti_m1(2)—Ohxi74.84 (18)Na_aiii—Oh—Ti_m1(2)134.6 (5)
Si1x—Ti_m1(2)—Ti_m2133.43 (6)Na_aiii—Oh—Si1ii129.0 (3)
Si1x—Ti_m1(2)—Mg_m2133.43 (6)Na_aiii—Oh—Si2146.4 (4)
Si2—Ti_m1(2)—Si2xi122.22 (9)Na_aiii—Oh—O1150.0 (2)
Si2—Ti_m1(2)—O124.0 (3)Na_aiii—Oh—O1xi101.8 (4)
Si2—Ti_m1(2)—O1xi100.7 (2)Na_aiii—Oh—O2130.3 (6)
Si2—Ti_m1(2)—O227.23 (13)Na_aiii—Oh—O2ii48.0 (3)
Si2—Ti_m1(2)—O2xi138.69 (12)Na_aiii—Oh—O373.7 (4)
Si2—Ti_m1(2)—O6ii72.8 (2)Na_aiii—Oh—O3ii104.8 (4)
Si2—Ti_m1(2)—O6x157.6 (4)Na_aiii—Oh—O6ii147.0 (3)
Si2—Ti_m1(2)—Oh71.86 (19)Na_aiii—Oh—O6x93.8 (4)
Si2—Ti_m1(2)—Ohxi106.5 (2)Na_aiii—Oh—Ba88.0 (2)
Si2—Ti_m1(2)—Ti_m261.11 (5)Na_aiii—Oh—W1iii37.5 (3)
Si2—Ti_m1(2)—Mg_m261.11 (5)Na_aiii—Oh—W239.9 (3)
Si2xi—Ti_m1(2)—O1100.7 (2)Na_aiii—Oh—W_c88.0 (2)
Si2xi—Ti_m1(2)—O1xi24.0 (3)Na_aiii—Oh—Nb_m1(1)89.2 (5)
Si2xi—Ti_m1(2)—O2138.69 (12)Na_ax—Oh—Ti_m1(1)136.4 (5)
Si2xi—Ti_m1(2)—O2xi27.23 (13)Na_ax—Oh—Ti_m1(2)85.6 (5)
Si2xi—Ti_m1(2)—O6ii157.6 (4)Na_ax—Oh—Si1ii125.3 (3)
Si2xi—Ti_m1(2)—O6x72.8 (2)Na_ax—Oh—Si2146.8 (4)
Si2xi—Ti_m1(2)—Oh106.5 (2)Na_ax—Oh—O1118.2 (5)
Si2xi—Ti_m1(2)—Ohxi71.86 (19)Na_ax—Oh—O1xi61.0 (4)
Si2xi—Ti_m1(2)—Ti_m261.11 (5)Na_ax—Oh—O2174.9 (2)
Si2xi—Ti_m1(2)—Mg_m261.11 (5)Na_ax—Oh—O2ii91.0 (4)
O1—Ti_m1(2)—O1xi82.1 (2)Na_ax—Oh—O3116.4 (4)
O1—Ti_m1(2)—O250.7 (4)Na_ax—Oh—O3ii124.4 (2)
O1—Ti_m1(2)—O2xi114.7 (3)Na_ax—Oh—O6ii115.2 (5)
O1—Ti_m1(2)—O6ii89.8 (2)Na_ax—Oh—O6x51.2 (4)
O1—Ti_m1(2)—O6x170.6 (2)Na_ax—Oh—Ba88.1 (2)
O1—Ti_m1(2)—Oh87.0 (4)Na_ax—Oh—W1iii37.9 (3)
O1—Ti_m1(2)—Ohxi90.5 (4)Na_ax—Oh—W240.5 (3)
O1—Ti_m1(2)—Ti_m241.05 (16)Na_ax—Oh—W_c88.1 (2)
O1—Ti_m1(2)—Mg_m241.05 (16)Na_ax—Oh—Nb_m1(1)136.4 (5)
O1xi—Ti_m1(2)—O2114.7 (3)Ti_m1(1)—Oh—Ti_m1(2)133.2 (3)
O1xi—Ti_m1(2)—O2xi50.7 (4)Ti_m1(1)—Oh—Si1ii67.15 (16)
O1xi—Ti_m1(2)—O6ii170.6 (2)Ti_m1(1)—Oh—Si274.7 (2)
O1xi—Ti_m1(2)—O6x89.8 (2)Ti_m1(1)—Oh—O1104.6 (3)
O1xi—Ti_m1(2)—Oh90.5 (4)Ti_m1(1)—Oh—O1xi158.0 (3)
O1xi—Ti_m1(2)—Ohxi87.0 (4)Ti_m1(1)—Oh—O245.3 (3)
O1xi—Ti_m1(2)—Ti_m241.05 (16)Ti_m1(1)—Oh—O2ii45.6 (3)
O1xi—Ti_m1(2)—Mg_m241.05 (16)Ti_m1(1)—Oh—O346.4 (3)
O2—Ti_m1(2)—O2xi163.58 (12)Ti_m1(1)—Oh—O3ii45.0 (3)
O2—Ti_m1(2)—O6ii62.4 (4)Ti_m1(1)—Oh—O6ii92.3 (3)
O2—Ti_m1(2)—O6x130.5 (4)Ti_m1(1)—Oh—O6x138.2 (3)
O2—Ti_m1(2)—Oh51.5 (2)Ti_m1(1)—Oh—Ba105.0 (3)
O2—Ti_m1(2)—Ohxi127.9 (2)Ti_m1(1)—Oh—W1iii102.3 (3)
O2—Ti_m1(2)—Ti_m281.79 (8)Ti_m1(1)—Oh—W2116.9 (4)
O2—Ti_m1(2)—Mg_m281.79 (8)Ti_m1(1)—Oh—W_c105.0 (3)
O2xi—Ti_m1(2)—O6ii130.5 (4)Ti_m1(1)—Oh—Nb_m1(1)0.0 (5)
O2xi—Ti_m1(2)—O6x62.4 (4)Ti_m1(2)—Oh—Si1ii71.0 (2)
O2xi—Ti_m1(2)—Oh127.9 (2)Ti_m1(2)—Oh—Si273.2 (2)
O2xi—Ti_m1(2)—Ohxi51.5 (2)Ti_m1(2)—Oh—O147.9 (3)
O2xi—Ti_m1(2)—Ti_m281.79 (8)Ti_m1(2)—Oh—O1xi46.0 (3)
O2xi—Ti_m1(2)—Mg_m281.79 (8)Ti_m1(2)—Oh—O295.1 (3)
O6ii—Ti_m1(2)—O6x98.7 (2)Ti_m1(2)—Oh—O2ii151.0 (3)
O6ii—Ti_m1(2)—Oh93.7 (4)Ti_m1(2)—Oh—O3144.3 (3)
O6ii—Ti_m1(2)—Ohxi88.4 (4)Ti_m1(2)—Oh—O3ii98.7 (3)
O6ii—Ti_m1(2)—Ti_m2130.65 (16)Ti_m1(2)—Oh—O6ii43.0 (3)
O6ii—Ti_m1(2)—Mg_m2130.65 (16)Ti_m1(2)—Oh—O6x45.6 (3)
O6x—Ti_m1(2)—Oh88.4 (4)Ti_m1(2)—Oh—Ba93.9 (3)
O6x—Ti_m1(2)—Ohxi93.7 (4)Ti_m1(2)—Oh—W1iii106.1 (3)
O6x—Ti_m1(2)—Ti_m2130.65 (16)Ti_m1(2)—Oh—W2109.0 (4)
O6x—Ti_m1(2)—Mg_m2130.65 (16)Ti_m1(2)—Oh—W_c93.9 (3)
Oh—Ti_m1(2)—Ohxi176.7 (2)Ti_m1(2)—Oh—Nb_m1(1)133.2 (3)
Oh—Ti_m1(2)—Ti_m288.35 (14)Si1ii—Oh—Si271.78 (11)
Oh—Ti_m1(2)—Mg_m288.35 (14)Si1ii—Oh—O180.99 (19)
Ohxi—Ti_m1(2)—Ti_m288.35 (14)Si1ii—Oh—O1xi117.0 (4)
Ohxi—Ti_m1(2)—Mg_m288.35 (14)Si1ii—Oh—O259.48 (16)
Ti_m2—Ti_m1(2)—Mg_m20.0 (5)Si1ii—Oh—O2ii87.9 (2)
Ti_m1(2)—Fe_m2—Ti_m1(2)xii180.0 (5)Si1ii—Oh—O3110.6 (3)
Ti_m1(2)—Fe_m2—Si262.20 (5)Si1ii—Oh—O3ii28.2 (3)
Ti_m1(2)—Fe_m2—Si2xi62.20 (5)Si1ii—Oh—O6ii28.4 (2)
Ti_m1(2)—Fe_m2—Si2xii117.80 (5)Si1ii—Oh—O6x79.1 (2)
Ti_m1(2)—Fe_m2—Si2vi117.80 (5)Si1ii—Oh—Ba140.34 (17)
Ti_m1(2)—Fe_m2—O141.05 (16)Si1ii—Oh—W1iii102.15 (19)
Ti_m1(2)—Fe_m2—O1xi41.05 (16)Si1ii—Oh—W2164.3 (2)
Ti_m1(2)—Fe_m2—O1xii138.95 (16)Si1ii—Oh—W_c140.34 (17)
Ti_m1(2)—Fe_m2—O1vi138.95 (16)Si1ii—Oh—Nb_m1(1)67.15 (16)
Ti_m1(2)—Fe_m2—O590Si2—Oh—O130.1 (3)
Ti_m1(2)—Fe_m2—O5xi90Si2—Oh—O1xi86.0 (2)
Ti_m1(2)—Fe_m2—Ba90Si2—Oh—O230.0 (2)
Ti_m1(2)—Fe_m2—Baxi90Si2—Oh—O2ii119.9 (4)
Ti_m1(2)—Fe_m2—W_c90Si2—Oh—O373.9 (2)
Ti_m1(2)—Fe_m2—W_cxi90Si2—Oh—O3ii84.63 (17)
Ti_m1(2)—Fe_m2—Ti_m20Si2—Oh—O6ii64.59 (17)
Ti_m1(2)—Fe_m2—Mg_m20Si2—Oh—O6x118.0 (4)
Ti_m1(2)xii—Fe_m2—Si2117.80 (5)Si2—Oh—Ba68.72 (10)
Ti_m1(2)xii—Fe_m2—Si2xi117.80 (5)Si2—Oh—W1iii173.9 (2)
Ti_m1(2)xii—Fe_m2—Si2xii62.20 (5)Si2—Oh—W2123.7 (2)
Ti_m1(2)xii—Fe_m2—Si2vi62.20 (5)Si2—Oh—W_c68.72 (10)
Ti_m1(2)xii—Fe_m2—O1138.95 (16)Si2—Oh—Nb_m1(1)74.7 (2)
Ti_m1(2)xii—Fe_m2—O1xi138.95 (16)O1—Oh—O1xi57.3 (3)
Ti_m1(2)xii—Fe_m2—O1xii41.05 (16)O1—Oh—O259.4 (3)
Ti_m1(2)xii—Fe_m2—O1vi41.05 (16)O1—Oh—O2ii150.0 (5)
Ti_m1(2)xii—Fe_m2—O590O1—Oh—O396.5 (3)
Ti_m1(2)xii—Fe_m2—O5xi90O1—Oh—O3ii103.7 (2)
Ti_m1(2)xii—Fe_m2—Ba90O1—Oh—O6ii60.4 (2)
Ti_m1(2)xii—Fe_m2—Baxi90O1—Oh—O6x93.2 (5)
Ti_m1(2)xii—Fe_m2—W_c90O1—Oh—Ba62.93 (17)
Ti_m1(2)xii—Fe_m2—W_cxi90O1—Oh—W1iii151.8 (5)
Ti_m1(2)xii—Fe_m2—Ti_m20O1—Oh—W2111.1 (3)
Ti_m1(2)xii—Fe_m2—Mg_m20O1—Oh—W_c62.93 (17)
Si2—Fe_m2—Si2xi124.40 (8)O1—Oh—Nb_m1(1)104.6 (3)
Si2—Fe_m2—Si2xii180.0 (5)O1xi—Oh—O2116.1 (3)
Si2—Fe_m2—Si2vi55.60 (8)O1xi—Oh—O2ii149.7 (2)
Si2—Fe_m2—O124.9 (3)O1xi—Oh—O3118.4 (3)
Si2—Fe_m2—O1xi101.7 (2)O1xi—Oh—O3ii144.7 (5)
Si2—Fe_m2—O1xii155.1 (3)O1xi—Oh—O6ii88.7 (4)
Si2—Fe_m2—O1vi78.3 (2)O1xi—Oh—O6x60.8 (3)
Si2—Fe_m2—O529.51 (10)O1xi—Oh—Ba57.1 (2)
Si2—Fe_m2—O5xi150.49 (10)O1xi—Oh—W1iii97.8 (3)
Si2—Fe_m2—Ba80.55 (12)O1xi—Oh—W265.5 (2)
Si2—Fe_m2—Baxi99.45 (12)O1xi—Oh—W_c57.1 (2)
Si2—Fe_m2—W_c80.55 (12)O1xi—Oh—Nb_m1(1)158.0 (3)
Si2—Fe_m2—W_cxi99.45 (12)O2—Oh—O2ii90.9 (4)
Si2—Fe_m2—Ti_m20O2—Oh—O360.6 (3)
Si2—Fe_m2—Mg_m20O2—Oh—O3ii60.5 (2)
Si2xi—Fe_m2—Si2xii55.60 (8)O2—Oh—O6ii68.1 (3)
Si2xi—Fe_m2—Si2vi180.0 (5)O2—Oh—O6x132.0 (4)
Si2xi—Fe_m2—O1101.7 (2)O2—Oh—Ba86.80 (17)
Si2xi—Fe_m2—O1xi24.9 (3)O2—Oh—W1iii145.8 (4)
Si2xi—Fe_m2—O1xii78.3 (2)O2—Oh—W2135.0 (3)
Si2xi—Fe_m2—O1vi155.1 (3)O2—Oh—W_c86.80 (17)
Si2xi—Fe_m2—O5150.49 (10)O2—Oh—Nb_m1(1)45.3 (3)
Si2xi—Fe_m2—O5xi29.51 (10)O2ii—Oh—O361.4 (3)
Si2xi—Fe_m2—Ba99.45 (12)O2ii—Oh—O3ii60.0 (3)
Si2xi—Fe_m2—Baxi80.55 (12)O2ii—Oh—O6ii115.6 (3)
Si2xi—Fe_m2—W_c99.45 (12)O2ii—Oh—O6x112.1 (3)
Si2xi—Fe_m2—W_cxi80.55 (12)O2ii—Oh—Ba114.8 (4)
Si2xi—Fe_m2—Ti_m20O2ii—Oh—W1iii57.9 (2)
Si2xi—Fe_m2—Mg_m20O2ii—Oh—W285.8 (3)
Si2xii—Fe_m2—Si2vi124.40 (8)O2ii—Oh—W_c114.8 (4)
Si2xii—Fe_m2—O1155.1 (3)O2ii—Oh—Nb_m1(1)45.6 (3)
Si2xii—Fe_m2—O1xi78.3 (2)O3—Oh—O3ii91.4 (4)
Si2xii—Fe_m2—O1xii24.9 (3)O3—Oh—O6ii128.3 (3)
Si2xii—Fe_m2—O1vi101.7 (2)O3—Oh—O6x167.2 (3)
Si2xii—Fe_m2—O5150.49 (10)O3—Oh—Ba61.3 (2)
Si2xii—Fe_m2—O5xi29.51 (10)O3—Oh—W1iii108.1 (3)
Si2xii—Fe_m2—Ba99.45 (12)O3—Oh—W278.8 (2)
Si2xii—Fe_m2—Baxi80.55 (12)O3—Oh—W_c61.3 (2)
Si2xii—Fe_m2—W_c99.45 (12)O3—Oh—Nb_m1(1)46.4 (3)
Si2xii—Fe_m2—W_cxi80.55 (12)O3ii—Oh—O6ii56.6 (3)
Si2xii—Fe_m2—Ti_m20O3ii—Oh—O6x94.4 (3)
Si2xii—Fe_m2—Mg_m20O3ii—Oh—Ba145.7 (4)
Si2vi—Fe_m2—O178.3 (2)O3ii—Oh—W1iii89.5 (2)
Si2vi—Fe_m2—O1xi155.1 (3)O3ii—Oh—W2144.6 (4)
Si2vi—Fe_m2—O1xii101.7 (2)O3ii—Oh—W_c145.7 (4)
Si2vi—Fe_m2—O1vi24.9 (3)O3ii—Oh—Nb_m1(1)45.0 (3)
Si2vi—Fe_m2—O529.51 (10)O6ii—Oh—O6x64.0 (3)
Si2vi—Fe_m2—O5xi150.49 (10)O6ii—Oh—Ba123.2 (3)
Si2vi—Fe_m2—Ba80.55 (12)O6ii—Oh—W1iii110.5 (3)
Si2vi—Fe_m2—Baxi99.45 (12)O6ii—Oh—W2150.6 (5)
Si2vi—Fe_m2—W_c80.55 (12)O6ii—Oh—W_c123.2 (3)
Si2vi—Fe_m2—W_cxi99.45 (12)O6ii—Oh—Nb_m1(1)92.3 (3)
Si2vi—Fe_m2—Ti_m20O6x—Oh—Ba116.8 (4)
Si2vi—Fe_m2—Mg_m20O6x—Oh—W1iii60.6 (2)
O1—Fe_m2—O1xi82.1 (2)O6x—Oh—W289.9 (3)
O1—Fe_m2—O1xii180.0 (5)O6x—Oh—W_c116.8 (4)
O1—Fe_m2—O1vi97.9 (2)O6x—Oh—Nb_m1(1)138.2 (3)
O1—Fe_m2—O554.4 (3)Ba—Oh—W1iii117.4 (2)
O1—Fe_m2—O5xi125.6 (3)Ba—Oh—W254.99 (18)
O1—Fe_m2—Ba94.2 (4)Ba—Oh—W_c0.0 (5)
O1—Fe_m2—Baxi85.8 (4)Ba—Oh—Nb_m1(1)105.0 (3)
O1—Fe_m2—W_c94.2 (4)W1iii—Oh—W262.4 (2)
O1—Fe_m2—W_cxi85.8 (4)W1iii—Oh—W_c117.4 (2)
O1—Fe_m2—Ti_m20W1iii—Oh—Nb_m1(1)102.3 (3)
O1—Fe_m2—Mg_m20W2—Oh—W_c54.99 (18)
O1xi—Fe_m2—O1xii97.9 (2)W2—Oh—Nb_m1(1)116.9 (4)
O1xi—Fe_m2—O1vi180.0 (5)W_c—Oh—Nb_m1(1)105.0 (3)
O1xi—Fe_m2—O5125.6 (3)Fe_m2—Ba—O142.1 (2)
O1xi—Fe_m2—O5xi54.4 (3)Fe_m2—Ba—O1xi46.26 (17)
O1xi—Fe_m2—Ba85.8 (4)Fe_m2—Ba—O1xii46.26 (17)
O1xi—Fe_m2—Baxi94.2 (4)Fe_m2—Ba—O1vi42.1 (2)
O1xi—Fe_m2—W_c85.8 (4)Fe_m2—Ba—O3128.37 (16)
O1xi—Fe_m2—W_cxi94.2 (4)Fe_m2—Ba—O3vi128.37 (16)
O1xi—Fe_m2—Ti_m20Fe_m2—Ba—O573.4 (4)
O1xi—Fe_m2—Mg_m20Fe_m2—Ba—Oh86.8 (2)
O1xii—Fe_m2—O1vi82.1 (2)Fe_m2—Ba—Ohvi86.8 (2)
O1xii—Fe_m2—O5125.6 (3)Fe_m2—Ba—W2114.75 (16)
O1xii—Fe_m2—O5xi54.4 (3)Fe_m2—Ba—W2xiv114.75 (16)
O1xii—Fe_m2—Ba85.8 (4)Fe_m2—Ba—W_c0
O1xii—Fe_m2—Baxi94.2 (4)Fe_m2—Ba—Ti_m20.0 (5)
O1xii—Fe_m2—W_c85.8 (4)Fe_m2—Ba—Mg_m20.0 (5)
O1xii—Fe_m2—W_cxi94.2 (4)O1—Ba—O1xi54.4 (2)
O1xii—Fe_m2—Ti_m20O1—Ba—O1xii88.4 (3)
O1xii—Fe_m2—Mg_m20O1—Ba—O1vi60.99 (15)
O1vi—Fe_m2—O554.4 (3)O1—Ba—O386.3 (3)
O1vi—Fe_m2—O5xi125.6 (3)O1—Ba—O3vi120.6 (2)
O1vi—Fe_m2—Ba94.2 (4)O1—Ba—O550.8 (3)
O1vi—Fe_m2—Baxi85.8 (4)O1—Ba—Oh53.78 (19)
O1vi—Fe_m2—W_c94.2 (4)O1—Ba—Ohvi114.65 (19)
O1vi—Fe_m2—W_cxi85.8 (4)O1—Ba—W2110.41 (18)
O1vi—Fe_m2—Ti_m20O1—Ba—W2xiv155.1 (3)
O1vi—Fe_m2—Mg_m20O1—Ba—W_c0
O5—Fe_m2—O5xi180.0 (5)O1—Ba—Ti_m242.1 (2)
O5—Fe_m2—Ba69.0 (3)O1—Ba—Mg_m242.1 (2)
O5—Fe_m2—Baxi111.0 (3)O1xi—Ba—O1xii66.2 (3)
O5—Fe_m2—W_c69.0 (3)O1xi—Ba—O1vi88.4 (3)
O5—Fe_m2—W_cxi111.0 (3)O1xi—Ba—O3112.1 (2)
O5—Fe_m2—Ti_m20O1xi—Ba—O3vi174.20 (18)
O5—Fe_m2—Mg_m20O1xi—Ba—O5104.8 (3)
O5xi—Fe_m2—Ba111.0 (3)O1xi—Ba—Oh57.8 (3)
O5xi—Fe_m2—Baxi69.0 (3)O1xi—Ba—Ohvi123.5 (3)
O5xi—Fe_m2—W_c111.0 (3)O1xi—Ba—W269.35 (17)
O5xi—Fe_m2—W_cxi69.0 (3)O1xi—Ba—W2xiv104.36 (18)
O5xi—Fe_m2—Ti_m20O1xi—Ba—W_c0
O5xi—Fe_m2—Mg_m20O1xi—Ba—Ti_m246.26 (17)
Ba—Fe_m2—Baxi180.0 (5)O1xi—Ba—Mg_m246.26 (17)
Ba—Fe_m2—W_c0.0 (5)O1xii—Ba—O1vi54.4 (2)
Ba—Fe_m2—W_cxi180.0 (5)O1xii—Ba—O3174.20 (18)
Ba—Fe_m2—Ti_m20O1xii—Ba—O3vi112.1 (2)
Ba—Fe_m2—Mg_m20O1xii—Ba—O5104.8 (3)
Baxi—Fe_m2—W_c180.0 (5)O1xii—Ba—Oh123.5 (3)
Baxi—Fe_m2—W_cxi0.0 (5)O1xii—Ba—Ohvi57.8 (3)
Baxi—Fe_m2—Ti_m20O1xii—Ba—W2104.36 (18)
Baxi—Fe_m2—Mg_m20O1xii—Ba—W2xiv69.35 (17)
W_c—Fe_m2—W_cxi180.0 (5)O1xii—Ba—W_c0
W_c—Fe_m2—Ti_m20O1xii—Ba—Ti_m246.26 (17)
W_c—Fe_m2—Mg_m20O1xii—Ba—Mg_m246.26 (17)
W_cxi—Fe_m2—Ti_m20O1vi—Ba—O3120.6 (2)
W_cxi—Fe_m2—Mg_m20O1vi—Ba—O3vi86.3 (3)
Ti_m2—Fe_m2—Mg_m20O1vi—Ba—O550.8 (3)
Na_a—Si1—Na_aiii83.4 (4)O1vi—Ba—Oh114.65 (19)
Na_a—Si1—K_b136.1 (3)O1vi—Ba—Ohvi53.78 (19)
Na_a—Si1—Ti_m1(1)105.35 (19)O1vi—Ba—W2155.1 (3)
Na_a—Si1—Ti_m1(2)ii60.49 (15)O1vi—Ba—W2xiv110.41 (18)
Na_a—Si1—Si1vi127.4 (2)O1vi—Ba—W_c0
Na_a—Si1—Si2iv61.74 (18)O1vi—Ba—Ti_m242.1 (2)
Na_a—Si1—O2ii74.5 (3)O1vi—Ba—Mg_m242.1 (2)
Na_a—Si1—O3137.1 (3)O3—Ba—O3vi68.9 (2)
Na_a—Si1—O4110.0 (7)O3—Ba—O569.9 (3)
Na_a—Si1—O639.8 (3)O3—Ba—Oh54.4 (3)
Na_a—Si1—O769.8 (4)O3—Ba—Ohvi122.8 (3)
Na_a—Si1—Ohii87.3 (2)O3—Ba—W279.70 (16)
Na_a—Si1—Nb_m1(1)105.35 (19)O3—Ba—W2xiv116.3 (2)
Na_aiii—Si1—K_b131.8 (3)O3—Ba—W_c0
Na_aiii—Si1—Ti_m1(1)65.04 (19)O3—Ba—Ti_m2128.37 (16)
Na_aiii—Si1—Ti_m1(2)ii106.96 (17)O3—Ba—Mg_m2128.37 (16)
Na_aiii—Si1—Si1vi119.3 (2)O3vi—Ba—O569.9 (3)
Na_aiii—Si1—Si2iv57.9 (2)O3vi—Ba—Oh122.8 (3)
Na_aiii—Si1—O2ii41.68 (18)O3vi—Ba—Ohvi54.4 (3)
Na_aiii—Si1—O376.1 (4)O3vi—Ba—W2116.3 (2)
Na_aiii—Si1—O4140.3 (5)O3vi—Ba—W2xiv79.70 (16)
Na_aiii—Si1—O6108.7 (4)O3vi—Ba—W_c0
Na_aiii—Si1—O739.7 (4)O3vi—Ba—Ti_m2128.37 (16)
Na_aiii—Si1—Ohii91.2 (2)O3vi—Ba—Mg_m2128.37 (16)
Na_aiii—Si1—Nb_m1(1)65.04 (19)O5—Ba—Oh83.45 (10)
K_b—Si1—Ti_m1(1)76.36 (11)O5—Ba—Ohvi83.45 (10)
K_b—Si1—Ti_m1(2)ii81.68 (10)O5—Ba—W2144.3 (2)
K_b—Si1—Si1vi64.07 (5)O5—Ba—W2xiv144.3 (2)
K_b—Si1—Si2iv153.58 (7)O5—Ba—W_c0
K_b—Si1—O2ii112.41 (15)O5—Ba—Ti_m273.4 (4)
K_b—Si1—O356.3 (3)O5—Ba—Mg_m273.4 (4)
K_b—Si1—O462.5 (3)Oh—Ba—Ohvi166.59 (14)
K_b—Si1—O697.5 (2)Oh—Ba—W263.35 (19)
K_b—Si1—O7153.6 (4)Oh—Ba—W2xiv130.1 (2)
K_b—Si1—Ohii69.60 (9)Oh—Ba—W_c0
K_b—Si1—Nb_m1(1)76.36 (11)Oh—Ba—Ti_m286.8 (2)
Ti_m1(1)—Si1—Ti_m1(2)ii67.22 (6)Oh—Ba—Mg_m286.8 (2)
Ti_m1(1)—Si1—Si1vi127.16 (15)Ohvi—Ba—W2130.1 (2)
Ti_m1(1)—Si1—Si2iv122.24 (14)Ohvi—Ba—W2xiv63.35 (19)
Ti_m1(1)—Si1—O2ii36.78 (13)Ohvi—Ba—W_c0
Ti_m1(1)—Si1—O331.72 (16)Ohvi—Ba—Ti_m286.8 (2)
Ti_m1(1)—Si1—O4137.9 (4)Ohvi—Ba—Mg_m286.8 (2)
Ti_m1(1)—Si1—O688.5 (4)W2—Ba—W2xiv66.7 (2)
Ti_m1(1)—Si1—O7104.7 (4)W2—Ba—W_c0
Ti_m1(1)—Si1—Ohii34.5 (2)W2—Ba—Ti_m2114.75 (16)
Ti_m1(1)—Si1—Nb_m1(1)0.0 (5)W2—Ba—Mg_m2114.75 (16)
Ti_m1(2)ii—Si1—Si1vi133.43 (14)W2xiv—Ba—W_c0
Ti_m1(2)ii—Si1—Si2iv121.54 (13)W2xiv—Ba—Ti_m2114.75 (16)
Ti_m1(2)ii—Si1—O2ii67.16 (18)W2xiv—Ba—Mg_m2114.75 (16)
Ti_m1(2)ii—Si1—O389.9 (3)W_c—Ba—Ti_m20
Ti_m1(2)ii—Si1—O4112.2 (5)W_c—Ba—Mg_m20
Ti_m1(2)ii—Si1—O624.1 (3)Ti_m2—Ba—Mg_m20.0 (5)
Ti_m1(2)ii—Si1—O7123.5 (3)Na_a—W1—Na_ai75.1 (7)
Ti_m1(2)ii—Si1—Ohii34.1 (2)Na_a—W1—K_biv125.3 (3)
Ti_m1(2)ii—Si1—Nb_m1(1)67.22 (6)Na_a—W1—K_bvii122.7 (3)
Si1vi—Si1—Si2iv89.63 (6)Na_a—W1—O2iv52.9 (3)
Si1vi—Si1—O2ii153.8 (3)Na_a—W1—O2vii107.2 (5)
Si1vi—Si1—O395.5 (2)Na_a—W1—O652.9 (4)
Si1vi—Si1—O424.2 (6)Na_a—W1—O6i109.5 (5)
Si1vi—Si1—O6128.5 (4)Na_a—W1—Ohiii65.2 (4)
Si1vi—Si1—O797.29 (19)Na_a—W1—Ohv62.0 (3)
Si1vi—Si1—Ohii133.66 (10)Na_a—W1—W2iii37.5 (5)
Si1vi—Si1—Nb_m1(1)127.16 (15)Na_ai—W1—K_biv122.7 (3)
Si2iv—Si1—O2ii89.90 (12)Na_ai—W1—K_bvii125.3 (3)
Si2iv—Si1—O3129.1 (4)Na_ai—W1—O2iv107.2 (5)
Si2iv—Si1—O494.8 (3)Na_ai—W1—O2vii52.9 (3)
Si2iv—Si1—O6101.3 (3)Na_ai—W1—O6109.5 (5)
Si2iv—Si1—O718.6 (4)Na_ai—W1—O6i52.9 (4)
Si2iv—Si1—Ohii136.61 (10)Na_ai—W1—Ohiii62.0 (3)
Si2iv—Si1—Nb_m1(1)122.24 (14)Na_ai—W1—Ohv65.2 (4)
O2ii—Si1—O365.1 (3)Na_ai—W1—W2iii37.5 (5)
O2ii—Si1—O4174.7 (4)K_biv—W1—K_bvii90.4 (3)
O2ii—Si1—O677.2 (4)K_biv—W1—O2iv72.54 (19)
O2ii—Si1—O775.6 (3)K_biv—W1—O2vii124.9 (3)
O2ii—Si1—Ohii50.77 (17)K_biv—W1—O6125.5 (3)
O2ii—Si1—Nb_m1(1)36.78 (13)K_biv—W1—O6i70.03 (19)
O3—Si1—O4109.9 (5)K_biv—W1—Ohiii78.90 (9)
O3—Si1—O6113.8 (4)K_biv—W1—Ohv169.3 (3)
O3—Si1—O7111.2 (6)K_biv—W1—W2iii134.80 (14)
O3—Si1—Ohii56.4 (3)K_bvii—W1—O2iv124.9 (3)
O3—Si1—Nb_m1(1)31.72 (16)K_bvii—W1—O2vii72.54 (19)
O4—Si1—O6104.3 (7)K_bvii—W1—O670.03 (19)
O4—Si1—O7108.4 (3)K_bvii—W1—O6i125.5 (3)
O4—Si1—Ohii125.6 (3)K_bvii—W1—Ohiii169.3 (3)
O4—Si1—Nb_m1(1)137.9 (4)K_bvii—W1—Ohv78.90 (9)
O6—Si1—O7108.8 (4)K_bvii—W1—W2iii134.80 (14)
O6—Si1—Ohii57.6 (4)O2iv—W1—O2vii157.7 (4)
O6—Si1—Nb_m1(1)88.5 (4)O2iv—W1—O678.5 (2)
O7—Si1—Ohii125.8 (3)O2iv—W1—O6i97.7 (3)
O7—Si1—Nb_m1(1)104.7 (4)O2iv—W1—Ohiii52.1 (3)
Ohii—Si1—Nb_m1(1)34.5 (2)O2iv—W1—Ohv113.4 (3)
Na_aix—Si2—Na_aii89.3 (4)O2iv—W1—W2iii78.8 (2)
Na_aix—Si2—Ti_m1(1)65.08 (18)O2vii—W1—O697.7 (3)
Na_aix—Si2—Ti_m1(2)110.80 (18)O2vii—W1—O6i78.5 (2)
Na_aix—Si2—Fe_m2163.23 (16)O2vii—W1—Ohiii113.4 (3)
Na_aix—Si2—Si1ix64.4 (2)O2vii—W1—Ohv52.1 (3)
Na_aix—Si2—Si2vi128.8 (3)O2vii—W1—W2iii78.8 (2)
Na_aix—Si2—O1139.9 (3)O6—W1—O6i160.5 (4)
Na_aix—Si2—O1vi156.9 (3)O6—W1—Ohiii116.5 (3)
Na_aix—Si2—O239.9 (2)O6—W1—Ohv50.5 (3)
Na_aix—Si2—O5108.5 (6)O6—W1—W2iii80.2 (2)
Na_aix—Si2—O6ii80.6 (3)O6i—W1—Ohiii50.5 (3)
Na_aix—Si2—O7ix72.4 (5)O6i—W1—Ohv116.5 (3)
Na_aix—Si2—Oh95.7 (2)O6i—W1—W2iii80.2 (2)
Na_aix—Si2—Nb_m1(1)65.08 (18)Ohiii—W1—Ohv111.8 (3)
Na_aix—Si2—Ti_m2163.23 (16)Ohiii—W1—W2iii55.90 (16)
Na_aix—Si2—Mg_m2163.23 (16)Ohv—W1—W2iii55.90 (16)
Na_aii—Si2—Ti_m1(1)107.81 (18)Na_aiii—W2—Na_ax73.2 (7)
Na_aii—Si2—Ti_m1(2)63.45 (17)Na_aiii—W2—O1iv63.1 (4)
Na_aii—Si2—Fe_m293.6 (3)Na_aiii—W2—O1xi117.4 (5)
Na_aii—Si2—Si1ix67.4 (2)Na_aiii—W2—O750.7 (5)
Na_aii—Si2—Si2vi122.6 (3)Na_aiii—W2—O7xv123.0 (6)
Na_aii—Si2—O165.4 (4)Na_aiii—W2—Oh69.2 (4)
Na_aii—Si2—O1vi106.6 (3)Na_aiii—W2—Ohxv66.0 (3)
Na_aii—Si2—O2105.7 (4)Na_aiii—W2—Ba117.8 (3)
Na_aii—Si2—O5145.8 (6)Na_aiii—W2—Baxv114.6 (3)
Na_aii—Si2—O6ii44.5 (2)Na_aiii—W2—W1iii36.6 (5)
Na_aii—Si2—O7ix49.0 (4)Na_aiii—W2—W2xiv143.4 (5)
Na_aii—Si2—Oh93.7 (2)Na_aiii—W2—W_c117.8 (3)
Na_aii—Si2—Nb_m1(1)107.81 (18)Na_aiii—W2—W_cxv114.6 (3)
Na_aii—Si2—Ti_m293.6 (3)Na_ax—W2—O1iv117.4 (5)
Na_aii—Si2—Mg_m293.6 (3)Na_ax—W2—O1xi63.1 (4)
Ti_m1(1)—Si2—Ti_m1(2)65.96 (7)Na_ax—W2—O7123.0 (6)
Ti_m1(1)—Si2—Fe_m298.37 (7)Na_ax—W2—O7xv50.7 (5)
Ti_m1(1)—Si2—Si1ix129.27 (13)Na_ax—W2—Oh66.0 (3)
Ti_m1(1)—Si2—Si2vi125.71 (13)Na_ax—W2—Ohxv69.2 (4)
Ti_m1(1)—Si2—O192.5 (3)Na_ax—W2—Ba114.6 (3)
Ti_m1(1)—Si2—O1vi122.78 (13)Na_ax—W2—Baxv117.8 (3)
Ti_m1(1)—Si2—O225.57 (19)Na_ax—W2—W1iii36.6 (5)
Ti_m1(1)—Si2—O5106.1 (5)Na_ax—W2—W2xiv143.4 (5)
Ti_m1(1)—Si2—O6ii64.5 (2)Na_ax—W2—W_c114.6 (3)
Ti_m1(1)—Si2—O7ix131.9 (3)Na_ax—W2—W_cxv117.8 (3)
Ti_m1(1)—Si2—Oh34.5 (2)O1iv—W2—O1xi179.4 (4)
Ti_m1(1)—Si2—Nb_m1(1)0.0 (5)O1iv—W2—O747.9 (2)
Ti_m1(1)—Si2—Ti_m298.37 (7)O1iv—W2—O7xv132.1 (2)
Ti_m1(1)—Si2—Mg_m298.37 (7)O1iv—W2—Oh126.9 (3)
Ti_m1(2)—Si2—Fe_m256.69 (9)O1iv—W2—Ohxv53.5 (3)
Ti_m1(2)—Si2—Si1ix130.75 (16)O1iv—W2—Ba124.5 (3)
Ti_m1(2)—Si2—Si2vi118.89 (12)O1iv—W2—Baxv55.11 (17)
Ti_m1(2)—Si2—O130.8 (2)O1iv—W2—W1iii90.32 (19)
Ti_m1(2)—Si2—O1vi91.56 (18)O1iv—W2—W2xiv89.68 (19)
Ti_m1(2)—Si2—O285.8 (3)O1iv—W2—W_c124.5 (3)
Ti_m1(2)—Si2—O5130.0 (3)O1iv—W2—W_cxv55.11 (17)
Ti_m1(2)—Si2—O6ii34.65 (12)O1xi—W2—O7132.1 (2)
Ti_m1(2)—Si2—O7ix112.4 (4)O1xi—W2—O7xv47.9 (2)
Ti_m1(2)—Si2—Oh35.0 (2)O1xi—W2—Oh53.5 (3)
Ti_m1(2)—Si2—Nb_m1(1)65.96 (7)O1xi—W2—Ohxv126.9 (3)
Ti_m1(2)—Si2—Ti_m256.69 (9)O1xi—W2—Ba55.11 (17)
Ti_m1(2)—Si2—Mg_m256.69 (9)O1xi—W2—Baxv124.5 (3)
Fe_m2—Si2—Si1ix131.73 (16)O1xi—W2—W1iii90.32 (19)
Fe_m2—Si2—Si2vi62.20 (8)O1xi—W2—W2xiv89.68 (19)
Fe_m2—Si2—O132.05 (19)O1xi—W2—W_c55.11 (17)
Fe_m2—Si2—O1vi35.42 (12)O1xi—W2—W_cxv124.5 (3)
Fe_m2—Si2—O2123.79 (19)O7—W2—O7xv173.7 (4)
Fe_m2—Si2—O577.7 (5)O7—W2—Oh84.1 (3)
Fe_m2—Si2—O6ii89.96 (18)O7—W2—Ohxv92.9 (3)
Fe_m2—Si2—O7ix121.3 (5)O7—W2—Ba87.64 (17)
Fe_m2—Si2—Oh67.67 (17)O7—W2—Baxv95.84 (18)
Fe_m2—Si2—Nb_m1(1)98.37 (7)O7—W2—W1iii86.8 (2)
Fe_m2—Si2—Ti_m20.0 (5)O7—W2—W2xiv93.2 (2)
Fe_m2—Si2—Mg_m20.0 (5)O7—W2—W_c87.64 (17)
Si1ix—Si2—Si2vi90.37 (6)O7—W2—W_cxv95.84 (18)
Si1ix—Si2—O1124.4 (4)O7xv—W2—Oh92.9 (3)
Si1ix—Si2—O1vi105.74 (12)O7xv—W2—Ohxv84.1 (3)
Si1ix—Si2—O2104.3 (2)O7xv—W2—Ba95.84 (18)
Si1ix—Si2—O593.7 (2)O7xv—W2—Baxv87.64 (17)
Si1ix—Si2—O6ii102.72 (13)O7xv—W2—W1iii86.8 (2)
Si1ix—Si2—O7ix18.9 (4)O7xv—W2—W2xiv93.2 (2)
Si1ix—Si2—Oh151.61 (10)O7xv—W2—W_c95.84 (18)
Si1ix—Si2—Nb_m1(1)129.27 (13)O7xv—W2—W_cxv87.64 (17)
Si1ix—Si2—Ti_m2131.73 (16)Oh—W2—Ohxv123.4 (3)
Si1ix—Si2—Mg_m2131.73 (16)Oh—W2—Ba61.66 (9)
Si2vi—Si2—O191.24 (19)Oh—W2—Baxv174.9 (3)
Si2vi—Si2—O1vi28.04 (19)Oh—W2—W1iii61.70 (18)
Si2vi—Si2—O2131.3 (4)Oh—W2—W2xiv118.30 (18)
Si2vi—Si2—O525.2 (6)Oh—W2—W_c61.66 (9)
Si2vi—Si2—O6ii150.4 (3)Oh—W2—W_cxv174.9 (3)
Si2vi—Si2—O7ix98.11 (19)Ohxv—W2—Ba174.9 (3)
Si2vi—Si2—Oh117.98 (10)Ohxv—W2—Baxv61.66 (9)
Si2vi—Si2—Nb_m1(1)125.71 (13)Ohxv—W2—W1iii61.70 (18)
Si2vi—Si2—Ti_m262.20 (8)Ohxv—W2—W2xiv118.30 (18)
Si2vi—Si2—Mg_m262.20 (8)Ohxv—W2—W_c174.9 (3)
O1—Si2—O1vi63.2 (2)Ohxv—W2—W_cxv61.66 (9)
O1—Si2—O2115.3 (4)Ba—W2—Baxv113.3 (3)
O1—Si2—O5109.5 (5)Ba—W2—W1iii123.35 (17)
O1—Si2—O6ii59.5 (2)Ba—W2—W2xiv56.65 (17)
O1—Si2—O7ix106.8 (6)Ba—W2—W_c0.0 (5)
O1—Si2—Oh58.1 (4)Ba—W2—W_cxv113.3 (3)
O1—Si2—Nb_m1(1)92.5 (3)Baxv—W2—W1iii123.35 (17)
O1—Si2—Ti_m232.05 (19)Baxv—W2—W2xiv56.65 (17)
O1—Si2—Mg_m232.05 (19)Baxv—W2—W_c113.3 (3)
O1vi—Si2—O2142.3 (3)Baxv—W2—W_cxv0.0 (5)
O1vi—Si2—O549.4 (6)W1iii—W2—W2xiv180.0 (5)
O1vi—Si2—O6ii122.5 (3)W1iii—W2—W_c123.35 (17)
O1vi—Si2—O7ix105.2 (3)W1iii—W2—W_cxv123.35 (17)
O1vi—Si2—Oh99.82 (15)W2xiv—W2—W_c56.65 (17)
O1vi—Si2—Nb_m1(1)122.78 (13)W2xiv—W2—W_cxv56.65 (17)
O1vi—Si2—Ti_m235.42 (12)W_c—W2—W_cxv113.3 (3)
O1vi—Si2—Mg_m235.42 (12)Fe_m2—W_c—O142.1 (2)
O2—Si2—O5106.5 (7)Fe_m2—W_c—O1xi46.26 (17)
O2—Si2—O6ii71.3 (4)Fe_m2—W_c—O1xii46.26 (17)
O2—Si2—O7ix110.6 (4)Fe_m2—W_c—O1vi42.1 (2)
O2—Si2—Oh59.0 (3)Fe_m2—W_c—O3128.37 (16)
O2—Si2—Nb_m1(1)25.57 (19)Fe_m2—W_c—O3vi128.37 (16)
O2—Si2—Ti_m2123.79 (19)Fe_m2—W_c—O573.4 (4)
O2—Si2—Mg_m2123.79 (19)Fe_m2—W_c—Oh86.8 (2)
O5—Si2—O6ii163.5 (3)Fe_m2—W_c—Ohvi86.8 (2)
O5—Si2—O7ix107.9 (4)Fe_m2—W_c—Ba0
O5—Si2—Oh112.5 (3)Fe_m2—W_c—W2114.75 (16)
O5—Si2—Nb_m1(1)106.1 (5)Fe_m2—W_c—W2xiv114.75 (16)
O5—Si2—Ti_m277.7 (5)Fe_m2—W_c—Ti_m20.0 (5)
O5—Si2—Mg_m277.7 (5)Fe_m2—W_c—Mg_m20.0 (5)
O6ii—Si2—O7ix87.8 (3)O1—W_c—O1xi54.4 (2)
O6ii—Si2—Oh51.85 (19)O1—W_c—O1xii88.4 (3)
O6ii—Si2—Nb_m1(1)64.5 (2)O1—W_c—O1vi60.99 (15)
O6ii—Si2—Ti_m289.96 (18)O1—W_c—O386.3 (3)
O6ii—Si2—Mg_m289.96 (18)O1—W_c—O3vi120.6 (2)
O7ix—Si2—Oh139.6 (3)O1—W_c—O550.8 (3)
O7ix—Si2—Nb_m1(1)131.9 (3)O1—W_c—Oh53.78 (19)
O7ix—Si2—Ti_m2121.3 (5)O1—W_c—Ohvi114.65 (19)
O7ix—Si2—Mg_m2121.3 (5)O1—W_c—Ba0
Oh—Si2—Nb_m1(1)34.5 (2)O1—W_c—W2110.41 (18)
Oh—Si2—Ti_m267.67 (17)O1—W_c—W2xiv155.1 (3)
Oh—Si2—Mg_m267.67 (17)O1—W_c—Ti_m242.1 (2)
Nb_m1(1)—Si2—Ti_m298.37 (7)O1—W_c—Mg_m242.1 (2)
Nb_m1(1)—Si2—Mg_m298.37 (7)O1xi—W_c—O1xii66.2 (3)
Ti_m2—Si2—Mg_m20.0 (5)O1xi—W_c—O1vi88.4 (3)
Na_aii—O1—Ti_m1(2)84.2 (3)O1xi—W_c—O3112.1 (2)
Na_aii—O1—Fe_m2140.6 (7)O1xi—W_c—O3vi174.20 (18)
Na_aii—O1—Si284.5 (4)O1xi—W_c—O5104.8 (3)
Na_aii—O1—Si2vi117.4 (2)O1xi—W_c—Oh57.8 (3)
Na_aii—O1—O1xi120.8 (5)O1xi—W_c—Ohvi123.5 (3)
Na_aii—O1—O1vi125.4 (3)O1xi—W_c—Ba0
Na_aii—O1—O288.8 (4)O1xi—W_c—W269.35 (17)
Na_aii—O1—O5112.9 (4)O1xi—W_c—W2xiv104.36 (18)
Na_aii—O1—O6ii50.5 (3)O1xi—W_c—Ti_m246.26 (17)
Na_aii—O1—O7ix52.6 (4)O1xi—W_c—Mg_m246.26 (17)
Na_aii—O1—Oh111.7 (3)O1xii—W_c—O1vi54.4 (2)
Na_aii—O1—Ohxi61.3 (4)O1xii—W_c—O3174.20 (18)
Na_aii—O1—Ba174.9 (4)O1xii—W_c—O3vi112.1 (2)
Na_aii—O1—Baxi92.7 (5)O1xii—W_c—O5104.8 (3)
Na_aii—O1—W2ix39.5 (4)O1xii—W_c—Oh123.5 (3)
Na_aii—O1—W_c174.9 (4)O1xii—W_c—Ohvi57.8 (3)
Na_aii—O1—W_cxi92.7 (5)O1xii—W_c—Ba0
Na_aii—O1—Ti_m2140.6 (7)O1xii—W_c—W2104.36 (18)
Na_aii—O1—Mg_m2140.6 (7)O1xii—W_c—W2xiv69.35 (17)
Ti_m1(2)—O1—Fe_m297.9 (3)O1xii—W_c—Ti_m246.26 (17)
Ti_m1(2)—O1—Si2125.3 (5)O1xii—W_c—Mg_m246.26 (17)
Ti_m1(2)—O1—Si2vi158.4 (3)O1vi—W_c—O3120.6 (2)
Ti_m1(2)—O1—O1xi48.95 (17)O1vi—W_c—O3vi86.3 (3)
Ti_m1(2)—O1—O1vi138.9 (3)O1vi—W_c—O550.8 (3)
Ti_m1(2)—O1—O294.1 (3)O1vi—W_c—Oh114.65 (19)
Ti_m1(2)—O1—O5145.2 (6)O1vi—W_c—Ohvi53.78 (19)
Ti_m1(2)—O1—O6ii43.69 (15)O1vi—W_c—Ba0
Ti_m1(2)—O1—O7ix126.6 (2)O1vi—W_c—W2155.1 (3)
Ti_m1(2)—O1—Oh45.2 (3)O1vi—W_c—W2xiv110.41 (18)
Ti_m1(2)—O1—Ohxi43.5 (3)O1vi—W_c—Ti_m242.1 (2)
Ti_m1(2)—O1—Ba92.4 (2)O1vi—W_c—Mg_m242.1 (2)
Ti_m1(2)—O1—Baxi98.9 (5)O3—W_c—O3vi68.9 (2)
Ti_m1(2)—O1—W2ix102.3 (4)O3—W_c—O569.9 (3)
Ti_m1(2)—O1—W_c92.4 (2)O3—W_c—Oh54.4 (3)
Ti_m1(2)—O1—W_cxi98.9 (5)O3—W_c—Ohvi122.8 (3)
Ti_m1(2)—O1—Ti_m297.9 (3)O3—W_c—Ba0
Ti_m1(2)—O1—Mg_m297.9 (3)O3—W_c—W279.70 (16)
Fe_m2—O1—Si2123.0 (5)O3—W_c—W2xiv116.3 (2)
Fe_m2—O1—Si2vi66.31 (16)O3—W_c—Ti_m2128.37 (16)
Fe_m2—O1—O1xi48.95 (16)O3—W_c—Mg_m2128.37 (16)
Fe_m2—O1—O1vi41.05 (15)O3vi—W_c—O569.9 (3)
Fe_m2—O1—O2129.9 (5)O3vi—W_c—Oh122.8 (3)
Fe_m2—O1—O587.5 (3)O3vi—W_c—Ohvi54.4 (3)
Fe_m2—O1—O6ii141.4 (3)O3vi—W_c—Ba0
Fe_m2—O1—O7ix135.1 (2)O3vi—W_c—W2116.3 (2)
Fe_m2—O1—Oh96.2 (2)O3vi—W_c—W2xiv79.70 (16)
Fe_m2—O1—Ohxi93.6 (4)O3vi—W_c—Ti_m2128.37 (16)
Fe_m2—O1—Ba43.62 (17)O3vi—W_c—Mg_m2128.37 (16)
Fe_m2—O1—Baxi48.0 (2)O5—W_c—Oh83.45 (10)
Fe_m2—O1—W2ix102.8 (5)O5—W_c—Ohvi83.45 (10)
Fe_m2—O1—W_c43.62 (17)O5—W_c—Ba0
Fe_m2—O1—W_cxi48.0 (2)O5—W_c—W2144.3 (2)
Fe_m2—O1—Ti_m20.0 (5)O5—W_c—W2xiv144.3 (2)
Fe_m2—O1—Mg_m20.0 (5)O5—W_c—Ti_m273.4 (4)
Si2—O1—Si2vi60.7 (2)O5—W_c—Mg_m273.4 (4)
Si2—O1—O1xi148.7 (7)Oh—W_c—Ohvi166.59 (14)
Si2—O1—O1vi88.8 (3)Oh—W_c—Ba0
Si2—O1—O232.3 (3)Oh—W_c—W263.35 (19)
Si2—O1—O535.7 (3)Oh—W_c—W2xiv130.1 (2)
Si2—O1—O6ii90.8 (3)Oh—W_c—Ti_m286.8 (2)
Si2—O1—O7ix36.7 (3)Oh—W_c—Mg_m286.8 (2)
Si2—O1—Oh91.8 (6)Ohvi—W_c—Ba0
Si2—O1—Ohxi143.1 (3)Ohvi—W_c—W2130.1 (2)
Si2—O1—Ba94.4 (5)Ohvi—W_c—W2xiv63.35 (19)
Si2—O1—Baxi135.0 (3)Ohvi—W_c—Ti_m286.8 (2)
Si2—O1—W2ix102.0 (3)Ohvi—W_c—Mg_m286.8 (2)
Si2—O1—W_c94.4 (5)Ba—W_c—W20
Si2—O1—W_cxi135.0 (3)Ba—W_c—W2xiv0
Si2—O1—Ti_m2123.0 (5)Ba—W_c—Ti_m20
Si2—O1—Mg_m2123.0 (5)Ba—W_c—Mg_m20
Si2vi—O1—O1xi113.69 (18)W2—W_c—W2xiv66.7 (2)
Si2vi—O1—O1vi28.0 (2)W2—W_c—Ti_m2114.75 (16)
Si2vi—O1—O286.1 (3)W2—W_c—Mg_m2114.75 (16)
Si2vi—O1—O528.1 (3)W2xiv—W_c—Ti_m2114.75 (16)
Si2vi—O1—O6ii151.2 (4)W2xiv—W_c—Mg_m2114.75 (16)
Si2vi—O1—O7ix71.8 (2)Ti_m2—W_c—Mg_m20.0 (5)
Si2vi—O1—Oh119.1 (4)Ti_m1(1)—Nb_m1(1)—Si10
Si2vi—O1—Ohxi146.3 (4)Ti_m1(1)—Nb_m1(1)—Si1ii0
Si2vi—O1—Ba66.00 (16)Ti_m1(1)—Nb_m1(1)—Si20
Si2vi—O1—Baxi81.71 (16)Ti_m1(1)—Nb_m1(1)—Si2ii0
Si2vi—O1—W2ix95.9 (2)Ti_m1(1)—Nb_m1(1)—O20
Si2vi—O1—W_c66.00 (16)Ti_m1(1)—Nb_m1(1)—O2ii0
Si2vi—O1—W_cxi81.71 (16)Ti_m1(1)—Nb_m1(1)—O30
Si2vi—O1—Ti_m266.31 (16)Ti_m1(1)—Nb_m1(1)—O3ii0
Si2vi—O1—Mg_m266.31 (16)Ti_m1(1)—Nb_m1(1)—O60
O1xi—O1—O1vi90.0 (2)Ti_m1(1)—Nb_m1(1)—O6ii0
O1xi—O1—O2122.9 (4)Ti_m1(1)—Nb_m1(1)—Oh0
O1xi—O1—O5126.2 (4)Ti_m1(1)—Nb_m1(1)—Ohii0
O1xi—O1—O6ii92.5 (2)Si1—Nb_m1(1)—Si1ii180.0 (5)
O1xi—O1—O7ix173.4 (5)Si1—Nb_m1(1)—Si2106.55 (7)
O1xi—O1—Oh63.0 (3)Si1—Nb_m1(1)—Si2ii73.45 (7)
O1xi—O1—Ohxi59.7 (3)Si1—Nb_m1(1)—O2110.5 (2)
O1xi—O1—Ba58.7 (3)Si1—Nb_m1(1)—O2ii69.5 (2)
O1xi—O1—Baxi66.9 (3)Si1—Nb_m1(1)—O325.0 (3)
O1xi—O1—W2ix109.3 (5)Si1—Nb_m1(1)—O3ii155.0 (3)
O1xi—O1—W_c58.7 (3)Si1—Nb_m1(1)—O627.17 (14)
O1xi—O1—W_cxi66.9 (3)Si1—Nb_m1(1)—O6ii152.83 (14)
O1xi—O1—Ti_m248.95 (16)Si1—Nb_m1(1)—Oh101.6 (2)
O1xi—O1—Mg_m248.95 (16)Si1—Nb_m1(1)—Ohii78.4 (2)
O1vi—O1—O2112.2 (5)Si1ii—Nb_m1(1)—Si273.45 (7)
O1vi—O1—O555.0 (3)Si1ii—Nb_m1(1)—Si2ii106.55 (7)
O1vi—O1—O6ii175.9 (4)Si1ii—Nb_m1(1)—O269.5 (2)
O1vi—O1—O7ix94.3 (2)Si1ii—Nb_m1(1)—O2ii110.5 (2)
O1vi—O1—Oh122.7 (3)Si1ii—Nb_m1(1)—O3155.0 (3)
O1vi—O1—Ohxi121.5 (5)Si1ii—Nb_m1(1)—O3ii25.0 (3)
O1vi—O1—Ba59.51 (18)Si1ii—Nb_m1(1)—O6152.83 (14)
O1vi—O1—Baxi56.9 (3)Si1ii—Nb_m1(1)—O6ii27.17 (14)
O1vi—O1—W2ix90.3 (3)Si1ii—Nb_m1(1)—Oh78.4 (2)
O1vi—O1—W_c59.51 (18)Si1ii—Nb_m1(1)—Ohii101.6 (2)
O1vi—O1—W_cxi56.9 (3)Si2—Nb_m1(1)—Si2ii180.0 (5)
O1vi—O1—Ti_m241.05 (15)Si2—Nb_m1(1)—O220.8 (3)
O1vi—O1—Mg_m241.05 (15)Si2—Nb_m1(1)—O2ii159.2 (3)
O2—O1—O558.0 (4)Si2—Nb_m1(1)—O382.2 (3)
O2—O1—O6ii69.0 (3)Si2—Nb_m1(1)—O3ii97.8 (3)
O2—O1—O7ix59.9 (4)Si2—Nb_m1(1)—O6122.81 (11)
O2—O1—Oh60.7 (3)Si2—Nb_m1(1)—O6ii57.19 (11)
O2—O1—Ohxi126.3 (3)Si2—Nb_m1(1)—Oh70.80 (19)
O2—O1—Ba87.6 (4)Si2—Nb_m1(1)—Ohii109.20 (19)
O2—O1—Baxi167.0 (3)Si2ii—Nb_m1(1)—O2159.2 (3)
O2—O1—W2ix121.7 (2)Si2ii—Nb_m1(1)—O2ii20.8 (3)
O2—O1—W_c87.6 (4)Si2ii—Nb_m1(1)—O397.8 (3)
O2—O1—W_cxi167.0 (3)Si2ii—Nb_m1(1)—O3ii82.2 (3)
O2—O1—Ti_m2129.9 (5)Si2ii—Nb_m1(1)—O657.19 (11)
O2—O1—Mg_m2129.9 (5)Si2ii—Nb_m1(1)—O6ii122.81 (11)
O5—O1—O6ii125.3 (5)Si2ii—Nb_m1(1)—Oh109.20 (19)
O5—O1—O7ix60.3 (3)Si2ii—Nb_m1(1)—Ohii70.80 (19)
O5—O1—Oh100.1 (6)O2—Nb_m1(1)—O2ii180.0 (5)
O5—O1—Ohxi171.0 (4)O2—Nb_m1(1)—O389.5 (2)
O5—O1—Ba68.1 (3)O2—Nb_m1(1)—O3ii90.5 (2)
O5—O1—Baxi109.7 (3)O2—Nb_m1(1)—O6117.1 (3)
O5—O1—W2ix110.0 (3)O2—Nb_m1(1)—O6ii62.9 (3)
O5—O1—W_c68.1 (3)O2—Nb_m1(1)—Oh90.3 (4)
O5—O1—W_cxi109.7 (3)O2—Nb_m1(1)—Ohii89.7 (4)
O5—O1—Ti_m287.5 (3)O2ii—Nb_m1(1)—O390.5 (2)
O5—O1—Mg_m287.5 (3)O2ii—Nb_m1(1)—O3ii89.5 (2)
O6ii—O1—O7ix82.9 (2)O2ii—Nb_m1(1)—O662.9 (3)
O6ii—O1—Oh61.5 (2)O2ii—Nb_m1(1)—O6ii117.1 (3)
O6ii—O1—Ohxi57.5 (3)O2ii—Nb_m1(1)—Oh89.7 (4)
O6ii—O1—Ba124.6 (3)O2ii—Nb_m1(1)—Ohii90.3 (4)
O6ii—O1—Baxi121.4 (5)O3—Nb_m1(1)—O3ii180.0 (5)
O6ii—O1—W2ix85.8 (4)O3—Nb_m1(1)—O649.5 (4)
O6ii—O1—W_c124.6 (3)O3—Nb_m1(1)—O6ii130.5 (4)
O6ii—O1—W_cxi121.4 (5)O3—Nb_m1(1)—Oh88.7 (4)
O6ii—O1—Ti_m2141.4 (3)O3—Nb_m1(1)—Ohii91.3 (4)
O6ii—O1—Mg_m2141.4 (3)O3ii—Nb_m1(1)—O6130.5 (4)
O7ix—O1—Oh118.2 (5)O3ii—Nb_m1(1)—O6ii49.5 (4)
O7ix—O1—Ohxi113.7 (4)O3ii—Nb_m1(1)—Oh91.3 (4)
O7ix—O1—Ba127.9 (5)O3ii—Nb_m1(1)—Ohii88.7 (4)
O7ix—O1—Baxi111.4 (4)O6—Nb_m1(1)—O6ii180.0 (5)
O7ix—O1—W2ix65.7 (3)O6—Nb_m1(1)—Oh125.9 (3)
O7ix—O1—W_c127.9 (5)O6—Nb_m1(1)—Ohii54.1 (3)
O7ix—O1—W_cxi111.4 (4)O6ii—Nb_m1(1)—Oh54.1 (3)
O7ix—O1—Ti_m2135.1 (2)O6ii—Nb_m1(1)—Ohii125.9 (3)
O7ix—O1—Mg_m2135.1 (2)Oh—Nb_m1(1)—Ohii180.0 (5)
Oh—O1—Ohxi88.6 (3)Ti_m1(2)—Ti_m2—Ti_m1(2)xii180.0 (5)
Oh—O1—Ba63.3 (2)Ti_m1(2)—Ti_m2—Fe_m20
Oh—O1—Baxi129.9 (3)Ti_m1(2)—Ti_m2—Si262.20 (5)
Oh—O1—W2ix144.7 (4)Ti_m1(2)—Ti_m2—Si2xi62.20 (5)
Oh—O1—W_c63.3 (2)Ti_m1(2)—Ti_m2—Si2xii117.80 (5)
Oh—O1—W_cxi129.9 (3)Ti_m1(2)—Ti_m2—Si2vi117.80 (5)
Oh—O1—Ti_m296.2 (2)Ti_m1(2)—Ti_m2—O141.05 (16)
Oh—O1—Mg_m296.2 (2)Ti_m1(2)—Ti_m2—O1xi41.05 (16)
Ohxi—O1—Ba118.4 (2)Ti_m1(2)—Ti_m2—O1xii138.95 (16)
Ohxi—O1—Baxi65.1 (3)Ti_m1(2)—Ti_m2—O1vi138.95 (16)
Ohxi—O1—W2ix61.0 (3)Ti_m1(2)—Ti_m2—O590
Ohxi—O1—W_c118.4 (2)Ti_m1(2)—Ti_m2—O5xi90
Ohxi—O1—W_cxi65.1 (3)Ti_m1(2)—Ti_m2—Ba90
Ohxi—O1—Ti_m293.6 (4)Ti_m1(2)—Ti_m2—Baxi90
Ohxi—O1—Mg_m293.6 (4)Ti_m1(2)—Ti_m2—W_c90
Ba—O1—Baxi91.59 (17)Ti_m1(2)—Ti_m2—W_cxi90
Ba—O1—W2ix145.4 (3)Ti_m1(2)—Ti_m2—Mg_m20
Ba—O1—W_c0.0 (5)Ti_m1(2)xii—Ti_m2—Fe_m20
Ba—O1—W_cxi91.59 (17)Ti_m1(2)xii—Ti_m2—Si2117.80 (5)
Ba—O1—Ti_m243.62 (17)Ti_m1(2)xii—Ti_m2—Si2xi117.80 (5)
Ba—O1—Mg_m243.62 (17)Ti_m1(2)xii—Ti_m2—Si2xii62.20 (5)
Baxi—O1—W2ix55.5 (3)Ti_m1(2)xii—Ti_m2—Si2vi62.20 (5)
Baxi—O1—W_c91.59 (17)Ti_m1(2)xii—Ti_m2—O1138.95 (16)
Baxi—O1—W_cxi0.0 (5)Ti_m1(2)xii—Ti_m2—O1xi138.95 (16)
Baxi—O1—Ti_m248.0 (2)Ti_m1(2)xii—Ti_m2—O1xii41.05 (16)
Baxi—O1—Mg_m248.0 (2)Ti_m1(2)xii—Ti_m2—O1vi41.05 (16)
W2ix—O1—W_c145.4 (3)Ti_m1(2)xii—Ti_m2—O590
W2ix—O1—W_cxi55.5 (3)Ti_m1(2)xii—Ti_m2—O5xi90
W2ix—O1—Ti_m2102.8 (5)Ti_m1(2)xii—Ti_m2—Ba90
W2ix—O1—Mg_m2102.8 (5)Ti_m1(2)xii—Ti_m2—Baxi90
W_c—O1—W_cxi91.59 (17)Ti_m1(2)xii—Ti_m2—W_c90
W_c—O1—Ti_m243.62 (17)Ti_m1(2)xii—Ti_m2—W_cxi90
W_c—O1—Mg_m243.62 (17)Ti_m1(2)xii—Ti_m2—Mg_m20
W_cxi—O1—Ti_m248.0 (2)Fe_m2—Ti_m2—Si20
W_cxi—O1—Mg_m248.0 (2)Fe_m2—Ti_m2—Si2xi0
Ti_m2—O1—Mg_m20.0 (5)Fe_m2—Ti_m2—Si2xii0
Na_aix—O2—K_b95.4 (5)Fe_m2—Ti_m2—Si2vi0
Na_aix—O2—Ti_m1(1)111.2 (5)Fe_m2—Ti_m2—O10
Na_aix—O2—Ti_m1(2)134.4 (5)Fe_m2—Ti_m2—O1xi0
Na_aix—O2—Si1ii78.8 (3)Fe_m2—Ti_m2—O1xii0
Na_aix—O2—Si2114.2 (4)Fe_m2—Ti_m2—O1vi0
Na_aix—O2—O1135.6 (6)Fe_m2—Ti_m2—O50
Na_aix—O2—O3128.1 (7)Fe_m2—Ti_m2—O5xi0
Na_aix—O2—O3ii84.0 (3)Fe_m2—Ti_m2—Ba0
Na_aix—O2—O5114.6 (3)Fe_m2—Ti_m2—Baxi0
Na_aix—O2—O6ii101.3 (5)Fe_m2—Ti_m2—W_c0
Na_aix—O2—O7ix80.9 (4)Fe_m2—Ti_m2—W_cxi0
Na_aix—O2—O7ii51.5 (4)Fe_m2—Ti_m2—Mg_m20
Na_aix—O2—Oh144.3 (3)Si2—Ti_m2—Si2xi124.40 (8)
Na_aix—O2—Ohii72.6 (5)Si2—Ti_m2—Si2xii180.0 (5)
Na_aix—O2—W1ix43.4 (4)Si2—Ti_m2—Si2vi55.60 (8)
Na_aix—O2—Nb_m1(1)111.2 (5)Si2—Ti_m2—O124.9 (3)
K_b—O2—Ti_m1(1)95.3 (3)Si2—Ti_m2—O1xi101.7 (2)
K_b—O2—Ti_m1(2)129.71 (17)Si2—Ti_m2—O1xii155.1 (3)
K_b—O2—Si1ii164.3 (4)Si2—Ti_m2—O1vi78.3 (2)
K_b—O2—Si289.3 (3)Si2—Ti_m2—O529.51 (10)
K_b—O2—O1107.5 (2)Si2—Ti_m2—O5xi150.49 (10)
K_b—O2—O354.8 (2)Si2—Ti_m2—Ba80.55 (12)
K_b—O2—O3ii134.6 (4)Si2—Ti_m2—Baxi99.45 (12)
K_b—O2—O552.1 (4)Si2—Ti_m2—W_c80.55 (12)
K_b—O2—O6ii162.6 (3)Si2—Ti_m2—W_cxi99.45 (12)
K_b—O2—O7ix102.4 (2)Si2—Ti_m2—Mg_m20
K_b—O2—O7ii146.8 (3)Si2xi—Ti_m2—Si2xii55.60 (8)
K_b—O2—Oh110.5 (2)Si2xi—Ti_m2—Si2vi180.0 (5)
K_b—O2—Ohii77.4 (3)Si2xi—Ti_m2—O1101.7 (2)
K_b—O2—W1ix52.1 (2)Si2xi—Ti_m2—O1xi24.9 (3)
K_b—O2—Nb_m1(1)95.3 (3)Si2xi—Ti_m2—O1xii78.3 (2)
Ti_m1(1)—O2—Ti_m1(2)75.1 (3)Si2xi—Ti_m2—O1vi155.1 (3)
Ti_m1(1)—O2—Si1ii73.69 (16)Si2xi—Ti_m2—O5150.49 (10)
Ti_m1(1)—O2—Si2133.7 (4)Si2xi—Ti_m2—O5xi29.51 (10)
Ti_m1(1)—O2—O1104.1 (3)Si2xi—Ti_m2—Ba99.45 (12)
Ti_m1(1)—O2—O345.50 (17)Si2xi—Ti_m2—Baxi80.55 (12)
Ti_m1(1)—O2—O3ii44.98 (17)Si2xi—Ti_m2—W_c99.45 (12)
Ti_m1(1)—O2—O5124.9 (3)Si2xi—Ti_m2—W_cxi80.55 (12)
Ti_m1(1)—O2—O6ii83.1 (3)Si2xi—Ti_m2—Mg_m20
Ti_m1(1)—O2—O7ix157.6 (6)Si2xii—Ti_m2—Si2vi124.40 (8)
Ti_m1(1)—O2—O7ii98.24 (19)Si2xii—Ti_m2—O1155.1 (3)
Ti_m1(1)—O2—Oh44.4 (3)Si2xii—Ti_m2—O1xi78.3 (2)
Ti_m1(1)—O2—Ohii44.7 (3)Si2xii—Ti_m2—O1xii24.9 (3)
Ti_m1(1)—O2—W1ix113.3 (5)Si2xii—Ti_m2—O1vi101.7 (2)
Ti_m1(1)—O2—Nb_m1(1)0.0 (5)Si2xii—Ti_m2—O5150.49 (10)
Ti_m1(2)—O2—Si1ii59.22 (19)Si2xii—Ti_m2—O5xi29.51 (10)
Ti_m1(2)—O2—Si267.0 (4)Si2xii—Ti_m2—Ba99.45 (12)
Ti_m1(2)—O2—O135.21 (17)Si2xii—Ti_m2—Baxi80.55 (12)
Ti_m1(2)—O2—O389.5 (3)Si2xii—Ti_m2—W_c99.45 (12)
Ti_m1(2)—O2—O3ii69.3 (3)Si2xii—Ti_m2—W_cxi80.55 (12)
Ti_m1(2)—O2—O593.0 (5)Si2xii—Ti_m2—Mg_m20
Ti_m1(2)—O2—O6ii33.20 (16)Si2vi—Ti_m2—O178.3 (2)
Ti_m1(2)—O2—O7ix83.0 (4)Si2vi—Ti_m2—O1xi155.1 (3)
Ti_m1(2)—O2—O7ii83.2 (3)Si2vi—Ti_m2—O1xii101.7 (2)
Ti_m1(2)—O2—Oh33.4 (3)Si2vi—Ti_m2—O1vi24.9 (3)
Ti_m1(2)—O2—Ohii118.1 (2)Si2vi—Ti_m2—O529.51 (10)
Ti_m1(2)—O2—W1ix171.6 (3)Si2vi—Ti_m2—O5xi150.49 (10)
Ti_m1(2)—O2—Nb_m1(1)75.1 (3)Si2vi—Ti_m2—Ba80.55 (12)
Si1ii—O2—Si2106.4 (5)Si2vi—Ti_m2—Baxi99.45 (12)
Si1ii—O2—O186.4 (3)Si2vi—Ti_m2—W_c80.55 (12)
Si1ii—O2—O3117.90 (19)Si2vi—Ti_m2—W_cxi99.45 (12)
Si1ii—O2—O3ii31.0 (2)Si2vi—Ti_m2—Mg_m20
Si1ii—O2—O5143.5 (6)O1—Ti_m2—O1xi82.1 (2)
Si1ii—O2—O6ii29.78 (19)O1—Ti_m2—O1xii180.0 (5)
Si1ii—O2—O7ix91.1 (3)O1—Ti_m2—O1vi97.9 (2)
Si1ii—O2—O7ii30.86 (14)O1—Ti_m2—O554.4 (3)
Si1ii—O2—Oh69.7 (2)O1—Ti_m2—O5xi125.6 (3)
Si1ii—O2—Ohii87.0 (2)O1—Ti_m2—Ba94.2 (4)
Si1ii—O2—W1ix121.4 (3)O1—Ti_m2—Baxi85.8 (4)
Si1ii—O2—Nb_m1(1)73.69 (16)O1—Ti_m2—W_c94.2 (4)
Si2—O2—O132.4 (3)O1—Ti_m2—W_cxi85.8 (4)
Si2—O2—O3107.3 (3)O1—Ti_m2—Mg_m20
Si2—O2—O3ii132.3 (6)O1xi—Ti_m2—O1xii97.9 (2)
Si2—O2—O537.3 (4)O1xi—Ti_m2—O1vi180.0 (5)
Si2—O2—O6ii79.5 (5)O1xi—Ti_m2—O5125.6 (3)
Si2—O2—O7ix34.7 (2)O1xi—Ti_m2—O5xi54.4 (3)
Si2—O2—O7ii102.5 (5)O1xi—Ti_m2—Ba85.8 (4)
Si2—O2—Oh91.0 (4)O1xi—Ti_m2—Baxi94.2 (4)
Si2—O2—Ohii165.8 (4)O1xi—Ti_m2—W_c85.8 (4)
Si2—O2—W1ix105.7 (3)O1xi—Ti_m2—W_cxi94.2 (4)
Si2—O2—Nb_m1(1)133.7 (4)O1xi—Ti_m2—Mg_m20
O1—O2—O395.8 (3)O1xii—Ti_m2—O1vi82.1 (2)
O1—O2—O3ii103.9 (4)O1xii—Ti_m2—O5125.6 (3)
O1—O2—O559.9 (5)O1xii—Ti_m2—O5xi54.4 (3)
O1—O2—O6ii56.6 (3)O1xii—Ti_m2—Ba85.8 (4)
O1—O2—O7ix57.6 (3)O1xii—Ti_m2—Baxi94.2 (4)
O1—O2—O7ii98.3 (4)O1xii—Ti_m2—W_c85.8 (4)
O1—O2—Oh59.8 (3)O1xii—Ti_m2—W_cxi94.2 (4)
O1—O2—Ohii148.6 (2)O1xii—Ti_m2—Mg_m20
O1—O2—W1ix138.0 (3)O1vi—Ti_m2—O554.4 (3)
O1—O2—Nb_m1(1)104.1 (3)O1vi—Ti_m2—O5xi125.6 (3)
O3—O2—O3ii90.5 (2)O1vi—Ti_m2—Ba94.2 (4)
O3—O2—O581.7 (3)O1vi—Ti_m2—Baxi85.8 (4)
O3—O2—O6ii115.9 (3)O1vi—Ti_m2—W_c94.2 (4)
O3—O2—O7ix140.6 (3)O1vi—Ti_m2—W_cxi85.8 (4)
O3—O2—O7ii143.5 (2)O1vi—Ti_m2—Mg_m20
O3—O2—Oh59.2 (3)O5—Ti_m2—O5xi180.0 (5)
O3—O2—Ohii60.9 (3)O5—Ti_m2—Ba69.0 (3)
O3—O2—W1ix96.9 (4)O5—Ti_m2—Baxi111.0 (3)
O3—O2—Nb_m1(1)45.50 (17)O5—Ti_m2—W_c69.0 (3)
O3ii—O2—O5160.8 (5)O5—Ti_m2—W_cxi111.0 (3)
O3ii—O2—O6ii53.1 (3)O5—Ti_m2—Mg_m20
O3ii—O2—O7ix122.1 (4)O5xi—Ti_m2—Ba111.0 (3)
O3ii—O2—O7ii53.46 (18)O5xi—Ti_m2—Baxi69.0 (3)
O3ii—O2—Oh60.4 (2)O5xi—Ti_m2—W_c111.0 (3)
O3ii—O2—Ohii59.1 (3)O5xi—Ti_m2—W_cxi69.0 (3)
O3ii—O2—W1ix115.8 (4)O5xi—Ti_m2—Mg_m20
O3ii—O2—Nb_m1(1)44.98 (17)Ba—Ti_m2—Baxi180.0 (5)
O5—O2—O6ii115.1 (6)Ba—Ti_m2—W_c0.0 (5)
O5—O2—O7ix60.2 (3)Ba—Ti_m2—W_cxi180.0 (5)
O5—O2—O7ii134.2 (4)Ba—Ti_m2—Mg_m20
O5—O2—Oh100.8 (3)Baxi—Ti_m2—W_c180.0 (5)
O5—O2—Ohii128.9 (6)Baxi—Ti_m2—W_cxi0.0 (5)
O5—O2—W1ix82.6 (4)Baxi—Ti_m2—Mg_m20
O5—O2—Nb_m1(1)124.9 (3)W_c—Ti_m2—W_cxi180.0 (5)
O6ii—O2—O7ix75.8 (4)W_c—Ti_m2—Mg_m20
O6ii—O2—O7ii50.0 (3)W_cxi—Ti_m2—Mg_m20
O6ii—O2—Oh57.0 (3)Ti_m1(2)—Mg_m2—Ti_m1(2)xii180.0 (5)
O6ii—O2—Ohii112.1 (3)Ti_m1(2)—Mg_m2—Fe_m20
O6ii—O2—W1ix144.0 (2)Ti_m1(2)—Mg_m2—Si262.20 (5)
O6ii—O2—Nb_m1(1)83.1 (3)Ti_m1(2)—Mg_m2—Si2xi62.20 (5)
O7ix—O2—O7ii74.1 (3)Ti_m1(2)—Mg_m2—Si2xii117.80 (5)
O7ix—O2—Oh115.2 (5)Ti_m1(2)—Mg_m2—Si2vi117.80 (5)
O7ix—O2—Ohii153.2 (3)Ti_m1(2)—Mg_m2—O141.05 (16)
O7ix—O2—W1ix88.6 (3)Ti_m1(2)—Mg_m2—O1xi41.05 (16)
O7ix—O2—Nb_m1(1)157.6 (6)Ti_m1(2)—Mg_m2—O1xii138.95 (16)
O7ii—O2—Oh100.3 (3)Ti_m1(2)—Mg_m2—O1vi138.95 (16)
O7ii—O2—Ohii91.4 (3)Ti_m1(2)—Mg_m2—O590
O7ii—O2—W1ix94.7 (3)Ti_m1(2)—Mg_m2—O5xi90
O7ii—O2—Nb_m1(1)98.24 (19)Ti_m1(2)—Mg_m2—Ba90
Oh—O2—Ohii89.1 (3)Ti_m1(2)—Mg_m2—Baxi90
Oh—O2—W1ix154.5 (5)Ti_m1(2)—Mg_m2—W_c90
Oh—O2—Nb_m1(1)44.4 (3)Ti_m1(2)—Mg_m2—W_cxi90
Ohii—O2—W1ix70.0 (3)Ti_m1(2)—Mg_m2—Ti_m20
Ohii—O2—Nb_m1(1)44.7 (3)Ti_m1(2)xii—Mg_m2—Fe_m20
W1ix—O2—Nb_m1(1)113.3 (5)Ti_m1(2)xii—Mg_m2—Si2117.80 (5)
Na_aiii—O3—K_b170.6 (2)Ti_m1(2)xii—Mg_m2—Si2xi117.80 (5)
Na_aiii—O3—Ti_m1(1)76.7 (2)Ti_m1(2)xii—Mg_m2—Si2xii62.20 (5)
Na_aiii—O3—Si177.5 (4)Ti_m1(2)xii—Mg_m2—Si2vi62.20 (5)
Na_aiii—O3—O2114.5 (4)Ti_m1(2)xii—Mg_m2—O1138.95 (16)
Na_aiii—O3—O2ii42.7 (2)Ti_m1(2)xii—Mg_m2—O1xi138.95 (16)
Na_aiii—O3—O3vi116.6 (2)Ti_m1(2)xii—Mg_m2—O1xii41.05 (16)
Na_aiii—O3—O4104.9 (3)Ti_m1(2)xii—Mg_m2—O1vi41.05 (16)
Na_aiii—O3—O687.3 (4)Ti_m1(2)xii—Mg_m2—O590
Na_aiii—O3—O745.0 (4)Ti_m1(2)xii—Mg_m2—O5xi90
Na_aiii—O3—Oh57.2 (3)Ti_m1(2)xii—Mg_m2—Ba90
Na_aiii—O3—Ohii101.8 (2)Ti_m1(2)xii—Mg_m2—Baxi90
Na_aiii—O3—Ba81.6 (4)Ti_m1(2)xii—Mg_m2—W_c90
Na_aiii—O3—W_c81.6 (4)Ti_m1(2)xii—Mg_m2—W_cxi90
Na_aiii—O3—Nb_m1(1)76.7 (2)Ti_m1(2)xii—Mg_m2—Ti_m20
K_b—O3—Ti_m1(1)112.67 (19)Fe_m2—Mg_m2—Si20
K_b—O3—Si196.7 (5)Fe_m2—Mg_m2—Si2xi0
K_b—O3—O274.0 (2)Fe_m2—Mg_m2—Si2xii0
K_b—O3—O2ii144.9 (3)Fe_m2—Mg_m2—Si2vi0
K_b—O3—O3vi54.92 (15)Fe_m2—Mg_m2—O10
K_b—O3—O466.9 (3)Fe_m2—Mg_m2—O1xi0
K_b—O3—O691.8 (4)Fe_m2—Mg_m2—O1xii0
K_b—O3—O7127.3 (4)Fe_m2—Mg_m2—O1vi0
K_b—O3—Oh129.0 (4)Fe_m2—Mg_m2—O50
K_b—O3—Ohii86.0 (2)Fe_m2—Mg_m2—O5xi0
K_b—O3—Ba94.9 (2)Fe_m2—Mg_m2—Ba0
K_b—O3—W_c94.9 (2)Fe_m2—Mg_m2—Baxi0
K_b—O3—Nb_m1(1)112.67 (19)Fe_m2—Mg_m2—W_c0
Ti_m1(1)—O3—Si1123.3 (4)Fe_m2—Mg_m2—W_cxi0
Ti_m1(1)—O3—O245.02 (17)Fe_m2—Mg_m2—Ti_m20
Ti_m1(1)—O3—O2ii44.50 (17)Si2—Mg_m2—Si2xi124.40 (8)
Ti_m1(1)—O3—O3vi152.0 (5)Si2—Mg_m2—Si2xii180.0 (5)
Ti_m1(1)—O3—O4153.4 (6)Si2—Mg_m2—Si2vi55.60 (8)
Ti_m1(1)—O3—O696.2 (3)Si2—Mg_m2—O124.9 (3)
Ti_m1(1)—O3—O7113.3 (2)Si2—Mg_m2—O1xi101.7 (2)
Ti_m1(1)—O3—Oh44.9 (3)Si2—Mg_m2—O1xii155.1 (3)
Ti_m1(1)—O3—Ohii43.7 (3)Si2—Mg_m2—O1vi78.3 (2)
Ti_m1(1)—O3—Ba106.5 (5)Si2—Mg_m2—O529.51 (10)
Ti_m1(1)—O3—W_c106.5 (5)Si2—Mg_m2—O5xi150.49 (10)
Ti_m1(1)—O3—Nb_m1(1)0.0 (5)Si2—Mg_m2—Ba80.55 (12)
Si1—O3—O2152.8 (6)Si2—Mg_m2—Baxi99.45 (12)
Si1—O3—O2ii84.0 (3)Si2—Mg_m2—W_c80.55 (12)
Si1—O3—O3vi84.5 (3)Si2—Mg_m2—W_cxi99.45 (12)
Si1—O3—O436.0 (3)Si2—Mg_m2—Ti_m20
Si1—O3—O633.1 (3)Si2xi—Mg_m2—Si2xii55.60 (8)
Si1—O3—O735.0 (3)Si2xi—Mg_m2—Si2vi180.0 (5)
Si1—O3—Oh134.3 (3)Si2xi—Mg_m2—O1101.7 (2)
Si1—O3—Ohii95.4 (5)Si2xi—Mg_m2—O1xi24.9 (3)
Si1—O3—Ba118.5 (3)Si2xi—Mg_m2—O1xii78.3 (2)
Si1—O3—W_c118.5 (3)Si2xi—Mg_m2—O1vi155.1 (3)
Si1—O3—Nb_m1(1)123.3 (4)Si2xi—Mg_m2—O5150.49 (10)
O2—O3—O2ii89.5 (2)Si2xi—Mg_m2—O5xi29.51 (10)
O2—O3—O3vi108.8 (3)Si2xi—Mg_m2—Ba99.45 (12)
O2—O3—O4140.5 (3)Si2xi—Mg_m2—Baxi80.55 (12)
O2—O3—O6120.2 (3)Si2xi—Mg_m2—W_c99.45 (12)
O2—O3—O7157.7 (3)Si2xi—Mg_m2—W_cxi80.55 (12)
O2—O3—Oh60.2 (3)Si2xi—Mg_m2—Ti_m20
O2—O3—Ohii59.1 (3)Si2xii—Mg_m2—Si2vi124.40 (8)
O2—O3—Ba88.1 (4)Si2xii—Mg_m2—O1155.1 (3)
O2—O3—W_c88.1 (4)Si2xii—Mg_m2—O1xi78.3 (2)
O2—O3—Nb_m1(1)45.02 (17)Si2xii—Mg_m2—O1xii24.9 (3)
O2ii—O3—O3vi158.3 (2)Si2xii—Mg_m2—O1vi101.7 (2)
O2ii—O3—O4119.9 (4)Si2xii—Mg_m2—O5150.49 (10)
O2ii—O3—O669.8 (3)Si2xii—Mg_m2—O5xi29.51 (10)
O2ii—O3—O769.1 (2)Si2xii—Mg_m2—Ba99.45 (12)
O2ii—O3—Oh59.5 (3)Si2xii—Mg_m2—Baxi80.55 (12)
O2ii—O3—Ohii59.1 (2)Si2xii—Mg_m2—W_c99.45 (12)
O2ii—O3—Ba115.7 (4)Si2xii—Mg_m2—W_cxi80.55 (12)
O2ii—O3—W_c115.7 (4)Si2xii—Mg_m2—Ti_m20
O2ii—O3—Nb_m1(1)44.50 (17)Si2vi—Mg_m2—O178.3 (2)
O3vi—O3—O451.2 (3)Si2vi—Mg_m2—O1xi155.1 (3)
O3vi—O3—O6108.4 (4)Si2vi—Mg_m2—O1xii101.7 (2)
O3vi—O3—O791.2 (2)Si2vi—Mg_m2—O1vi24.9 (3)
O3vi—O3—Oh119.3 (5)Si2vi—Mg_m2—O529.51 (10)
O3vi—O3—Ohii140.4 (3)Si2vi—Mg_m2—O5xi150.49 (10)
O3vi—O3—Ba55.5 (2)Si2vi—Mg_m2—Ba80.55 (12)
O3vi—O3—W_c55.5 (2)Si2vi—Mg_m2—Baxi99.45 (12)
O3vi—O3—Nb_m1(1)152.0 (5)Si2vi—Mg_m2—W_c80.55 (12)
O4—O3—O657.7 (4)Si2vi—Mg_m2—W_cxi99.45 (12)
O4—O3—O760.4 (3)Si2vi—Mg_m2—Ti_m20
O4—O3—Oh156.3 (4)O1—Mg_m2—O1xi82.1 (2)
O4—O3—Ohii111.7 (6)O1—Mg_m2—O1xii180.0 (5)
O4—O3—Ba100.0 (3)O1—Mg_m2—O1vi97.9 (2)
O4—O3—W_c100.0 (3)O1—Mg_m2—O554.4 (3)
O4—O3—Nb_m1(1)153.4 (6)O1—Mg_m2—O5xi125.6 (3)
O6—O3—O759.1 (4)O1—Mg_m2—Ba94.2 (4)
O6—O3—Oh129.2 (3)O1—Mg_m2—Baxi85.8 (4)
O6—O3—Ohii62.3 (3)O1—Mg_m2—W_c94.2 (4)
O6—O3—Ba151.6 (2)O1—Mg_m2—W_cxi85.8 (4)
O6—O3—W_c151.6 (2)O1—Mg_m2—Ti_m20
O6—O3—Nb_m1(1)96.2 (3)O1xi—Mg_m2—O1xii97.9 (2)
O7—O3—Oh101.8 (4)O1xi—Mg_m2—O1vi180.0 (5)
O7—O3—Ohii111.1 (4)O1xi—Mg_m2—O5125.6 (3)
O7—O3—Ba95.6 (3)O1xi—Mg_m2—O5xi54.4 (3)
O7—O3—W_c95.6 (3)O1xi—Mg_m2—Ba85.8 (4)
O7—O3—Nb_m1(1)113.3 (2)O1xi—Mg_m2—Baxi94.2 (4)
Oh—O3—Ohii88.6 (3)O1xi—Mg_m2—W_c85.8 (4)
Oh—O3—Ba64.3 (3)O1xi—Mg_m2—W_cxi94.2 (4)
Oh—O3—W_c64.3 (3)O1xi—Mg_m2—Ti_m20
Oh—O3—Nb_m1(1)44.9 (3)O1xii—Mg_m2—O1vi82.1 (2)
Ohii—O3—Ba145.7 (5)O1xii—Mg_m2—O5125.6 (3)
Ohii—O3—W_c145.7 (5)O1xii—Mg_m2—O5xi54.4 (3)
Ohii—O3—Nb_m1(1)43.7 (3)O1xii—Mg_m2—Ba85.8 (4)
Ba—O3—W_c0.0 (5)O1xii—Mg_m2—Baxi94.2 (4)
Ba—O3—Nb_m1(1)106.5 (5)O1xii—Mg_m2—W_c85.8 (4)
W_c—O3—Nb_m1(1)106.5 (5)O1xii—Mg_m2—W_cxi94.2 (4)
K_b—O4—K_bvii102.5 (4)O1xii—Mg_m2—Ti_m20
K_b—O4—Si188.9 (4)O1vi—Mg_m2—O554.4 (3)
K_b—O4—Si1vi88.9 (4)O1vi—Mg_m2—O5xi125.6 (3)
K_b—O4—O360.3 (3)O1vi—Mg_m2—Ba94.2 (4)
K_b—O4—O3vi60.3 (3)O1vi—Mg_m2—Baxi85.8 (4)
K_b—O4—O5iv165.4 (8)O1vi—Mg_m2—W_c94.2 (4)
K_b—O4—O689.8 (2)O1vi—Mg_m2—W_cxi85.8 (4)
K_b—O4—O6vi89.8 (2)O1vi—Mg_m2—Ti_m20
K_b—O4—O7120.1 (5)O5—Mg_m2—O5xi180.0 (5)
K_b—O4—O7vi120.1 (5)O5—Mg_m2—Ba69.0 (3)
K_bvii—O4—Si1113.8 (6)O5—Mg_m2—Baxi111.0 (3)
K_bvii—O4—Si1vi113.8 (6)O5—Mg_m2—W_c69.0 (3)
K_bvii—O4—O3133.9 (4)O5—Mg_m2—W_cxi111.0 (3)
K_bvii—O4—O3vi133.9 (4)O5—Mg_m2—Ti_m20
K_bvii—O4—O5iv92.2 (5)O5xi—Mg_m2—Ba111.0 (3)
K_bvii—O4—O677.7 (5)O5xi—Mg_m2—Baxi69.0 (3)
K_bvii—O4—O6vi77.7 (5)O5xi—Mg_m2—W_c111.0 (3)
K_bvii—O4—O7117.1 (5)O5xi—Mg_m2—W_cxi69.0 (3)
K_bvii—O4—O7vi117.1 (5)O5xi—Mg_m2—Ti_m20
Si1—O4—Si1vi131.6 (12)Ba—Mg_m2—Baxi180.0 (5)
Si1—O4—O334.1 (4)Ba—Mg_m2—W_c0.0 (5)
Si1—O4—O3vi108.4 (9)Ba—Mg_m2—W_cxi180.0 (5)
Si1—O4—O5iv85.1 (3)Ba—Mg_m2—Ti_m20
Si1—O4—O636.9 (4)Baxi—Mg_m2—W_c180.0 (5)
Si1—O4—O6vi168.4 (11)Baxi—Mg_m2—W_cxi0.0 (5)
Si1—O4—O735.5 (2)Baxi—Mg_m2—Ti_m20
Si1—O4—O7vi111.1 (7)W_c—Mg_m2—W_cxi180.0 (5)
Si1vi—O4—O3108.4 (9)W_c—Mg_m2—Ti_m20
Si1vi—O4—O3vi34.1 (4)W_cxi—Mg_m2—Ti_m20
Si1vi—O4—O5iv85.1 (3)
Symmetry codes: (i) x+1, y, z; (ii) x+1/2, y+1/2, z+1; (iii) x+1/2, y+1/2, z; (iv) x, y, z1; (v) x+1/2, y+1/2, z; (vi) x, y, z; (vii) x+1, y, z+1; (viii) x+1, y, z+1; (ix) x, y, z+1; (x) x1/2, y+1/2, z; (xi) x, y, z+1; (xii) x, y, z+1; (xiii) x, y, z+1; (xiv) x, y, z; (xv) x, y, z.
(labu-Fe_5.15) top
Crystal data top
Ba0.7Fe0.5K2.1Mg0.05Na2Nb0.1O33Si8Ti4Z = 2
Mr = 1206.8F(000) = 1167
Monoclinic, C2/mDx = 3.137 Mg m3
Hall symbol: -C 2ySynchrotron radiation, λ = 0.414 Å
a = 13.958 (7) ÅCell parameters from 3342 reflections
b = 13.4952 (8) Åθ = 1.8–19.1°
c = 7.5836 (11) ŵ = 0.83 mm1
β = 116.62 (4)°T = 293 K
V = 1277.1 (8) Å3Anhedral grain
Data collection top
ESRF ID 09
diffractometer
θmax = 19.1°, θmin = 1.8°
3342 measured reflectionsh = 78
980 independent reflectionsk = 2120
672 reflections with I > 2σ(I)l = 1110
Rint = 0.065
Refinement top
Refinement on F0 restraints
R[F2 > 2σ(F2)] = 0.08211 constraints
wR(F2) = 0.147Weighting scheme based on measured s.u.'s w = 1/(σ2(F) + 0.0100000007F2)
S = 1.17(Δ/σ)max = 0.045
980 reflectionsΔρmax = 0.88 e Å3
89 parametersΔρmin = 1.13 e Å3
Fractional atomic coordinates and isotropic or equivalent isotropic displacement parameters (Å2) top
xyzUiso*/UeqOcc. (<1)
Na_a0.4181 (18)0.2648 (6)0.0154 (14)0.031 (11)0.5
K_b0.4260 (7)00.7119 (5)0.032 (4)
Ti_m1(1)0.250.250.50.028 (3)0.95
Ti_m1(2)00.22270 (15)0.50.025 (3)
Fe_m2000.50.0300 (13)*0.5
Si10.3235 (5)0.11099 (15)0.2585 (3)0.021 (3)
Si20.2104 (5)0.10971 (15)0.8086 (3)0.024 (3)
O10.0837 (12)0.1107 (4)0.6763 (8)0.0144 (13)*
O20.2743 (11)0.1901 (4)0.7496 (8)0.0111 (12)*
O30.2730 (12)0.1204 (4)0.4090 (8)0.0132 (12)*
O40.3757 (16)00.2758 (12)0.0136 (17)*
O50.2565 (15)00.7933 (11)0.0120 (17)*
O60.4179 (12)0.1844 (5)0.2979 (9)0.0220 (15)*
O70.2285 (12)0.1245 (4)0.0338 (9)0.0167 (14)*
Oh0.1019 (12)0.2185 (4)0.3909 (8)0.0121 (12)*
Ba0.0893 (4)00.3418 (3)0.0185 (5)*0.35
W10.50.1469 (7)00.049 (15)
W200.1103 (7)00.11 (2)
W_c0.0893 (4)00.3418 (3)0.0185 (5)*0.65
Nb_m1(1)0.250.250.50.028 (3)0.05
Ti_m2000.50.0300 (13)*0.1
Mg_m2000.50.0300 (13)*0.05
Atomic displacement parameters (Å2) top
U11U22U33U12U13U23
Na_a0.03 (2)0.028 (4)0.035 (4)0.005 (6)0.013 (7)0.003 (3)
K_b0.029 (10)0.0424 (18)0.0193 (14)00.006 (2)0
Ti_m1(1)0.050 (7)0.0121 (9)0.0154 (9)0.0069 (13)0.0095 (16)0.0030 (6)
Ti_m1(2)0.026 (7)0.0109 (9)0.0175 (10)00.0089 (16)0
Si10.031 (7)0.0100 (9)0.0110 (10)0.0004 (13)0.0010 (16)0.0006 (6)
Si20.040 (7)0.0104 (9)0.0089 (10)0.0038 (13)0.0002 (16)0.0005 (6)
W10.08 (3)0.023 (5)0.025 (5)00.009 (8)0
W20.22 (5)0.021 (5)0.020 (5)00.003 (10)0
Nb_m1(1)0.050 (7)0.0121 (9)0.0154 (9)0.0069 (13)0.0095 (16)0.0030 (6)
Geometric parameters (Å, º) top
Na_a—Na_ai2.40 (4)Si2—O11.595 (15)
Na_a—Ti_m1(2)ii3.328 (11)Si2—O1vi3.376 (8)
Na_a—Si13.410 (19)Si2—O21.591 (12)
Na_a—Si1iii3.496 (19)Si2—O51.639 (10)
Na_a—Si2iv3.342 (18)Si2—O6ii3.206 (10)
Na_a—Si2ii3.16 (2)Si2—O7ix1.622 (9)
Na_a—O1ii2.888 (16)Si2—Oh3.191 (6)
Na_a—O2iv2.341 (15)Si2—Ba3.496 (3)
Na_a—O3iii3.491 (14)Si2—W_c3.496 (3)
Na_a—O62.402 (17)Si2—Nb_m1(1)3.244 (4)
Na_a—O73.31 (3)Si2—Ti_m23.183 (5)
Na_a—O7iii2.42 (2)Si2—Mg_m23.183 (5)
Na_a—Ohiii2.976 (16)O1—O1xi2.647 (12)
Na_a—Ohv2.863 (15)O1—O1vi2.989 (7)
Na_a—W11.992 (18)O1—O22.69 (2)
Na_a—W2iii2.070 (18)O1—O52.63 (2)
K_b—Si13.421 (4)O1—O6ii2.772 (8)
K_b—Si1vi3.421 (4)O1—O7ix2.561 (10)
K_b—O23.419 (12)O1—Oh2.712 (13)
K_b—O2vi3.419 (12)O1—Ohxi2.81 (2)
K_b—O32.842 (9)O1—Ba2.975 (9)
K_b—O3vi2.842 (9)O1—Baxi2.790 (15)
K_b—O43.057 (11)O1—W2ix3.156 (13)
K_b—O4vii2.73 (3)O1—W_c2.975 (9)
K_b—O52.70 (2)O1—W_cxi2.790 (15)
K_b—O6vii3.330 (14)O1—Ti_m21.996 (7)
K_b—O6viii3.330 (14)O1—Mg_m21.996 (7)
K_b—W1ix2.784 (8)O2—O32.741 (13)
K_b—W1viii2.784 (8)O2—O3ii2.777 (7)
Ti_m1(1)—Si13.100 (5)O2—O52.613 (7)
Ti_m1(1)—Si1ii3.100 (5)O2—O6ii3.055 (19)
Ti_m1(1)—Si23.244 (4)O2—O7ix2.660 (16)
Ti_m1(1)—Si2ii3.244 (4)O2—O7ii3.004 (10)
Ti_m1(1)—O21.943 (7)O2—Oh2.733 (11)
Ti_m1(1)—O2ii1.943 (7)O2—Ohii2.700 (19)
Ti_m1(1)—O31.959 (7)O2—W1ix2.917 (13)
Ti_m1(1)—O3ii1.959 (7)O2—Nb_m1(1)1.943 (7)
Ti_m1(1)—O63.441 (16)O3—O3vi3.249 (7)
Ti_m1(1)—O6ii3.441 (16)O3—O42.65 (2)
Ti_m1(1)—Oh1.899 (15)O3—O53.433 (15)
Ti_m1(1)—Ohii1.899 (15)O3—O62.66 (2)
Ti_m1(1)—Nb_m1(1)0O3—O72.627 (11)
Ti_m1(2)—Fe_m23.005 (2)O3—Oh2.68 (2)
Ti_m1(2)—Si1ii3.227 (5)O3—Ohii2.775 (11)
Ti_m1(2)—Si1x3.227 (5)O3—Ba2.882 (14)
Ti_m1(2)—Si23.204 (5)O3—W_c2.882 (14)
Ti_m1(2)—Si2xi3.204 (5)O3—Nb_m1(1)1.959 (7)
Ti_m1(2)—O12.009 (7)O4—O5iv3.271 (11)
Ti_m1(2)—O1xi2.009 (7)O4—O62.546 (9)
Ti_m1(2)—O23.456 (14)O4—O6vi2.546 (9)
Ti_m1(2)—O2xi3.456 (14)O4—O72.652 (14)
Ti_m1(2)—O6ii1.913 (7)O4—O7vi2.652 (14)
Ti_m1(2)—O6x1.913 (7)O5—O7ix2.634 (15)
Ti_m1(2)—Oh1.940 (16)O5—O7xiii2.634 (15)
Ti_m1(2)—Ohxi1.940 (16)O5—Ba3.164 (9)
Ti_m1(2)—Ti_m23.005 (2)O5—W_c3.164 (9)
Ti_m1(2)—Mg_m23.005 (2)O5—Ti_m23.261 (18)
Fe_m2—Si23.183 (5)O5—Mg_m23.261 (18)
Fe_m2—Si2xi3.183 (5)O6—O6vii2.890 (11)
Fe_m2—Si2xii3.183 (5)O6—O72.629 (17)
Fe_m2—Si2vi3.183 (5)O6—Ohii2.819 (14)
Fe_m2—O11.996 (7)O6—Ohv2.68 (2)
Fe_m2—O1xi1.996 (7)O6—W12.999 (14)
Fe_m2—O1xii1.996 (7)O6—Nb_m1(1)3.441 (16)
Fe_m2—O1vi1.996 (7)O7—O7vi3.359 (8)
Fe_m2—O53.261 (18)O7—W23.089 (17)
Fe_m2—O5xi3.261 (18)Oh—Ba2.967 (5)
Fe_m2—Ba2.081 (5)Oh—W1iii3.214 (8)
Fe_m2—Baxi2.081 (5)Oh—W23.028 (7)
Fe_m2—W_c2.081 (5)Oh—W_c2.967 (5)
Fe_m2—W_cxi2.081 (5)Oh—Nb_m1(1)1.899 (15)
Fe_m2—Ti_m20Ba—W22.755 (6)
Fe_m2—Mg_m20Ba—W2xiv2.755 (6)
Si1—Si1vi2.996 (3)Ba—W_c0
Si1—Si2iv3.051 (4)Ba—Ti_m22.081 (5)
Si1—O2ii3.000 (9)Ba—Mg_m22.081 (5)
Si1—O31.593 (15)W1—W2iii3.277 (14)
Si1—O41.645 (10)W2—W2xiv2.976 (14)
Si1—O61.566 (15)W2—W_c2.755 (6)
Si1—O71.635 (8)W2—W_cxv2.755 (6)
Si1—Ohii3.312 (6)W_c—Ti_m22.081 (5)
Si1—Nb_m1(1)3.100 (5)W_c—Mg_m22.081 (5)
Si2—Si2vi2.961 (3)Ti_m2—Mg_m20
Na_ai—Na_a—Ti_m1(2)ii103.7 (5)O5iv—O4—O693.5 (3)
Na_ai—Na_a—Si1132.0 (5)O5iv—O4—O6vi93.5 (3)
Na_ai—Na_a—Si1iii130.5 (5)O5iv—O4—O751.5 (3)
Na_ai—Na_a—Si2iv128.2 (5)O5iv—O4—O7vi51.5 (3)
Na_ai—Na_a—Si2ii141.8 (5)O6—O4—O6vi155.7 (11)
Na_ai—Na_a—O1ii115.7 (7)O6—O4—O760.7 (3)
Na_ai—Na_a—O2iv113.7 (8)O6—O4—O7vi138.5 (5)
Na_ai—Na_a—O3iii106.1 (6)O6vi—O4—O7138.5 (5)
Na_ai—Na_a—O6117.9 (8)O6vi—O4—O7vi60.7 (3)
Na_ai—Na_a—O7145.0 (5)O7—O4—O7vi78.6 (5)
Na_ai—Na_a—O7iii139.5 (6)K_b—O5—Fe_m2130.6 (3)
Na_ai—Na_a—Ohiii63.3 (6)K_b—O5—Si2115.4 (7)
Na_ai—Na_a—Ohv68.2 (6)K_b—O5—Si2vi115.4 (7)
Na_ai—Na_a—W153.0 (6)K_b—O5—O1133.5 (4)
Na_ai—Na_a—W2iii54.6 (6)K_b—O5—O1vi133.5 (4)
Ti_m1(2)ii—Na_a—Si157.2 (3)K_b—O5—O280.1 (6)
Ti_m1(2)ii—Na_a—Si1iii113.2 (6)K_b—O5—O2vi80.1 (6)
Ti_m1(2)ii—Na_a—Si2iv110.3 (6)K_b—O5—O353.6 (4)
Ti_m1(2)ii—Na_a—Si2ii59.1 (3)K_b—O5—O3vi53.6 (4)
Ti_m1(2)ii—Na_a—O1ii36.85 (19)K_b—O5—O4ix101.4 (6)
Ti_m1(2)ii—Na_a—O2iv135.3 (9)K_b—O5—O7ix125.1 (6)
Ti_m1(2)ii—Na_a—O3iii137.6 (6)K_b—O5—O7xiii125.1 (6)
Ti_m1(2)ii—Na_a—O634.4 (2)K_b—O5—Ba92.8 (4)
Ti_m1(2)ii—Na_a—O782.4 (4)K_b—O5—W_c92.8 (4)
Ti_m1(2)ii—Na_a—O7iii89.3 (5)K_b—O5—Ti_m2130.6 (3)
Ti_m1(2)ii—Na_a—Ohiii165.0 (8)K_b—O5—Mg_m2130.6 (3)
Ti_m1(2)ii—Na_a—Ohv35.5 (3)Fe_m2—O5—Si272.7 (6)
Ti_m1(2)ii—Na_a—W1100.6 (4)Fe_m2—O5—Si2vi72.7 (6)
Ti_m1(2)ii—Na_a—W2iii95.5 (3)Fe_m2—O5—O137.7 (3)
Si1—Na_a—Si1iii96.3 (6)Fe_m2—O5—O1vi37.7 (3)
Si1—Na_a—Si2iv53.7 (3)Fe_m2—O5—O292.9 (4)
Si1—Na_a—Si2ii70.6 (5)Fe_m2—O5—O2vi92.9 (4)
Si1—Na_a—O1ii76.7 (5)Fe_m2—O5—O383.8 (3)
Si1—Na_a—O2iv79.3 (6)Fe_m2—O5—O3vi83.8 (3)
Si1—Na_a—O3iii116.6 (7)Fe_m2—O5—O4ix128.0 (8)
Si1—Na_a—O624.2 (4)Fe_m2—O5—O7ix90.8 (6)
Si1—Na_a—O728.1 (2)Fe_m2—O5—O7xiii90.8 (6)
Si1—Na_a—O7iii87.4 (7)Fe_m2—O5—Ba37.76 (19)
Si1—Na_a—Ohiii136.6 (4)Fe_m2—O5—W_c37.76 (19)
Si1—Na_a—Ohv84.4 (4)Fe_m2—O5—Ti_m20.0 (5)
Si1—Na_a—W185.3 (4)Fe_m2—O5—Mg_m20.0 (5)
Si1—Na_a—W2iii152.1 (5)Si2—O5—Si2vi129.2 (14)
Si1iii—Na_a—Si2iv67.6 (4)Si2—O5—O135.0 (4)
Si1iii—Na_a—Si2ii54.2 (3)Si2—O5—O1vi101.9 (10)
Si1iii—Na_a—O1ii81.1 (5)Si2—O5—O235.4 (4)
Si1iii—Na_a—O2iv57.9 (4)Si2—O5—O2vi163.4 (12)
Si1iii—Na_a—O3iii26.4 (3)Si2—O5—O379.1 (4)
Si1iii—Na_a—O6111.1 (9)Si2—O5—O3vi131.7 (4)
Si1iii—Na_a—O773.9 (5)Si2—O5—O4ix86.6 (4)
Si1iii—Na_a—O7iii24.5 (2)Si2—O5—O7ix35.9 (3)
Si1iii—Na_a—Ohiii74.4 (4)Si2—O5—O7xiii110.0 (9)
Si1iii—Na_a—Ohv138.5 (5)Si2—O5—Ba87.4 (4)
Si1iii—Na_a—W1140.7 (4)Si2—O5—W_c87.4 (4)
Si1iii—Na_a—W2iii89.2 (4)Si2—O5—Ti_m272.7 (6)
Si2iv—Na_a—Si2ii89.8 (6)Si2—O5—Mg_m272.7 (6)
Si2iv—Na_a—O1ii115.1 (8)Si2vi—O5—O1101.9 (10)
Si2iv—Na_a—O2iv25.5 (3)Si2vi—O5—O1vi35.0 (4)
Si2iv—Na_a—O3iii72.6 (4)Si2vi—O5—O2163.4 (12)
Si2iv—Na_a—O677.8 (6)Si2vi—O5—O2vi35.4 (4)
Si2iv—Na_a—O728.2 (2)Si2vi—O5—O3131.7 (4)
Si2iv—Na_a—O7iii79.6 (6)Si2vi—O5—O3vi79.1 (4)
Si2iv—Na_a—Ohiii84.4 (3)Si2vi—O5—O4ix86.6 (4)
Si2iv—Na_a—Ohv135.9 (5)Si2vi—O5—O7ix110.0 (9)
Si2iv—Na_a—W182.7 (4)Si2vi—O5—O7xiii35.9 (3)
Si2iv—Na_a—W2iii150.3 (4)Si2vi—O5—Ba87.4 (4)
Si2ii—Na_a—O1ii30.1 (3)Si2vi—O5—W_c87.4 (4)
Si2ii—Na_a—O2iv99.5 (8)Si2vi—O5—Ti_m272.7 (6)
Si2ii—Na_a—O3iii78.9 (4)Si2vi—O5—Mg_m272.7 (6)
Si2ii—Na_a—O668.8 (6)O1—O5—O1vi69.2 (6)
Si2ii—Na_a—O770.9 (5)O1—O5—O261.6 (4)
Si2ii—Na_a—O7iii30.2 (3)O1—O5—O2vi129.8 (7)
Si2ii—Na_a—Ohiii126.0 (5)O1—O5—O381.1 (4)
Si2ii—Na_a—Ohv87.9 (4)O1—O5—O3vi112.5 (3)
Si2ii—Na_a—W1154.2 (6)O1—O5—O4ix107.9 (6)
Si2ii—Na_a—W2iii91.1 (4)O1—O5—O7ix58.2 (4)
O1ii—Na_a—O2iv129.2 (11)O1—O5—O7xiii101.4 (8)
O1ii—Na_a—O3iii102.0 (5)O1—O5—Ba61.0 (3)
O1ii—Na_a—O662.4 (4)O1—O5—W_c61.0 (3)
O1ii—Na_a—O790.1 (7)O1—O5—Ti_m237.7 (3)
O1ii—Na_a—O7iii56.8 (4)O1—O5—Mg_m237.7 (3)
O1ii—Na_a—Ohiii139.8 (4)O1vi—O5—O2129.8 (7)
O1ii—Na_a—Ohv58.5 (4)O1vi—O5—O2vi61.6 (4)
O1ii—Na_a—W1136.5 (5)O1vi—O5—O3112.5 (3)
O1ii—Na_a—W2iii77.1 (4)O1vi—O5—O3vi81.1 (4)
O2iv—Na_a—O3iii52.5 (3)O1vi—O5—O4ix107.9 (6)
O2iv—Na_a—O6103.3 (8)O1vi—O5—O7ix101.4 (8)
O2iv—Na_a—O752.9 (5)O1vi—O5—O7xiii58.2 (4)
O2iv—Na_a—O7iii78.1 (7)O1vi—O5—Ba61.0 (3)
O2iv—Na_a—Ohiii59.6 (4)O1vi—O5—W_c61.0 (3)
O2iv—Na_a—Ohv158.6 (4)O1vi—O5—Ti_m237.7 (3)
O2iv—Na_a—W184.2 (4)O1vi—O5—Mg_m237.7 (3)
O2iv—Na_a—W2iii125.7 (5)O2—O5—O2vi158.1 (9)
O3iii—Na_a—O6135.8 (10)O2—O5—O351.8 (3)
O3iii—Na_a—O789.9 (5)O2—O5—O3vi108.1 (5)
O3iii—Na_a—O7iii48.8 (3)O2—O5—O4ix96.5 (2)
O3iii—Na_a—Ohiii48.2 (4)O2—O5—O7ix60.9 (3)
O3iii—Na_a—Ohv148.9 (4)O2—O5—O7xiii140.0 (6)
O3iii—Na_a—W1121.5 (5)O2—O5—Ba85.9 (2)
O3iii—Na_a—W2iii78.4 (3)O2—O5—W_c85.9 (2)
O6—Na_a—O751.9 (5)O2—O5—Ti_m292.9 (4)
O6—Na_a—O7iii94.4 (9)O2—O5—Mg_m292.9 (4)
O6—Na_a—Ohiii157.1 (4)O2vi—O5—O3108.1 (5)
O6—Na_a—Ohv60.5 (5)O2vi—O5—O3vi51.8 (3)
O6—Na_a—W185.5 (4)O2vi—O5—O4ix96.5 (2)
O6—Na_a—W2iii129.7 (5)O2vi—O5—O7ix140.0 (6)
O7—Na_a—O7iii73.9 (7)O2vi—O5—O7xiii60.9 (3)
O7—Na_a—Ohiii112.4 (5)O2vi—O5—Ba85.9 (2)
O7—Na_a—Ohv112.4 (5)O2vi—O5—W_c85.9 (2)
O7—Na_a—W192.1 (5)O2vi—O5—Ti_m292.9 (4)
O7—Na_a—W2iii160.3 (9)O2vi—O5—Mg_m292.9 (4)
O7iii—Na_a—Ohiii96.5 (4)O3—O5—O3vi56.5 (3)
O7iii—Na_a—Ohv115.0 (5)O3—O5—O4ix139.1 (6)
O7iii—Na_a—W1161.8 (8)O3—O5—O7ix111.9 (2)
O7iii—Na_a—W2iii86.5 (5)O3—O5—O7xiii167.6 (2)
Ohiii—Na_a—Ohv130.6 (10)O3—O5—Ba51.6 (2)
Ohiii—Na_a—W177.9 (6)O3—O5—W_c51.6 (2)
Ohiii—Na_a—W2iii71.2 (5)O3—O5—Ti_m283.8 (3)
Ohv—Na_a—W180.8 (6)O3—O5—Mg_m283.8 (3)
Ohv—Na_a—W2iii73.8 (5)O3vi—O5—O4ix139.1 (6)
W1—Na_a—W2iii107.5 (12)O3vi—O5—O7ix167.6 (2)
Si1—K_b—Si1vi51.93 (7)O3vi—O5—O7xiii111.9 (2)
Si1—K_b—O276.10 (16)O3vi—O5—Ba51.6 (2)
Si1—K_b—O2vi114.6 (2)O3vi—O5—W_c51.6 (2)
Si1—K_b—O327.5 (3)O3vi—O5—Ti_m283.8 (3)
Si1—K_b—O3vi67.28 (16)O3vi—O5—Mg_m283.8 (3)
Si1—K_b—O428.72 (18)O4ix—O5—O7ix52.0 (3)
Si1—K_b—O4vii89.7 (3)O4ix—O5—O7xiii52.0 (3)
Si1—K_b—O5102.4 (3)O4ix—O5—Ba165.8 (9)
Si1—K_b—O6vii68.51 (17)O4ix—O5—W_c165.8 (9)
Si1—K_b—O6viii106.7 (2)O4ix—O5—Ti_m2128.0 (8)
Si1—K_b—W1ix108.54 (15)O4ix—O5—Mg_m2128.0 (8)
Si1—K_b—W1viii160.34 (17)O7ix—O5—O7xiii79.2 (5)
Si1vi—K_b—O2114.6 (2)O7ix—O5—Ba118.9 (6)
Si1vi—K_b—O2vi76.10 (16)O7ix—O5—W_c118.9 (6)
Si1vi—K_b—O367.28 (16)O7ix—O5—Ti_m290.8 (6)
Si1vi—K_b—O3vi27.5 (3)O7ix—O5—Mg_m290.8 (6)
Si1vi—K_b—O428.72 (18)O7xiii—O5—Ba118.9 (6)
Si1vi—K_b—O4vii89.7 (3)O7xiii—O5—W_c118.9 (6)
Si1vi—K_b—O5102.4 (3)O7xiii—O5—Ti_m290.8 (6)
Si1vi—K_b—O6vii106.7 (2)O7xiii—O5—Mg_m290.8 (6)
Si1vi—K_b—O6viii68.51 (17)Ba—O5—W_c0.0 (5)
Si1vi—K_b—W1ix160.34 (17)Ba—O5—Ti_m237.76 (19)
Si1vi—K_b—W1viii108.54 (15)Ba—O5—Mg_m237.76 (19)
O2—K_b—O2vi97.2 (4)W_c—O5—Ti_m237.76 (19)
O2—K_b—O350.9 (3)W_c—O5—Mg_m237.76 (19)
O2—K_b—O3vi103.1 (4)Ti_m2—O5—Mg_m20.0 (5)
O2—K_b—O4103.9 (3)Na_a—O6—K_bvii93.2 (6)
O2—K_b—O4vii130.9 (2)Na_a—O6—Ti_m1(1)123.7 (6)
O2—K_b—O548.8 (2)Na_a—O6—Ti_m1(2)ii100.3 (5)
O2—K_b—O6vii82.9 (3)Na_a—O6—Si1116.9 (5)
O2—K_b—O6viii176.82 (18)Na_a—O6—Si2ii66.9 (5)
O2—K_b—W1ix54.95 (18)Na_a—O6—O1ii67.4 (4)
O2—K_b—W1viii119.6 (3)Na_a—O6—O2ii89.8 (6)
O2vi—K_b—O3103.1 (4)Na_a—O6—O3137.2 (8)
O2vi—K_b—O3vi50.9 (3)Na_a—O6—O4118.4 (5)
O2vi—K_b—O4103.9 (3)Na_a—O6—O6vii128.9 (8)
O2vi—K_b—O4vii130.9 (2)Na_a—O6—O782.1 (5)
O2vi—K_b—O548.8 (2)Na_a—O6—Ohii125.2 (4)
O2vi—K_b—O6vii176.82 (18)Na_a—O6—Ohv68.3 (6)
O2vi—K_b—O6viii82.9 (3)Na_a—O6—W141.5 (5)
O2vi—K_b—W1ix119.6 (3)Na_a—O6—Nb_m1(1)123.7 (6)
O2vi—K_b—W1viii54.95 (18)K_bvii—O6—Ti_m1(1)141.7 (3)
O3—K_b—O3vi69.7 (2)K_bvii—O6—Ti_m1(2)ii110.1 (6)
O3—K_b—O453.2 (4)K_bvii—O6—Si191.5 (4)
O3—K_b—O4vii114.3 (4)K_bvii—O6—Si2ii159.9 (5)
O3—K_b—O576.5 (4)K_bvii—O6—O1ii140.6 (7)
O3—K_b—O6vii79.5 (3)K_bvii—O6—O2ii163.8 (4)
O3—K_b—O6viii132.2 (3)K_bvii—O6—O3111.2 (3)
O3—K_b—W1ix96.15 (19)K_bvii—O6—O453.3 (6)
O3—K_b—W1viii157.1 (5)K_bvii—O6—O6vii78.9 (4)
O3vi—K_b—O453.2 (4)K_bvii—O6—O7101.4 (3)
O3vi—K_b—O4vii114.3 (4)K_bvii—O6—Ohii132.6 (3)
O3vi—K_b—O576.5 (4)K_bvii—O6—Ohv79.2 (5)
O3vi—K_b—O6vii132.2 (3)K_bvii—O6—W151.9 (3)
O3vi—K_b—O6viii79.5 (3)K_bvii—O6—Nb_m1(1)141.7 (3)
O3vi—K_b—W1ix157.1 (5)Ti_m1(1)—O6—Ti_m1(2)ii76.0 (4)
O3vi—K_b—W1viii96.15 (19)Ti_m1(1)—O6—Si164.2 (6)
O4—K_b—O4vii77.0 (5)Ti_m1(1)—O6—Si2ii58.3 (3)
O4—K_b—O5116.6 (5)Ti_m1(1)—O6—O1ii71.6 (4)
O4—K_b—O6vii79.1 (3)Ti_m1(1)—O6—O2ii34.2 (2)
O4—K_b—O6viii79.1 (3)Ti_m1(1)—O6—O334.5 (2)
O4—K_b—W1ix132.3 (2)Ti_m1(1)—O6—O495.6 (7)
O4—K_b—W1viii132.3 (2)Ti_m1(1)—O6—O6vii84.4 (4)
O4vii—K_b—O5166.4 (3)Ti_m1(1)—O6—O776.4 (5)
O4vii—K_b—O6vii48.5 (3)Ti_m1(1)—O6—Ohii33.5 (3)
O4vii—K_b—O6viii48.5 (3)Ti_m1(1)—O6—Ohv121.4 (3)
O4vii—K_b—W1ix87.7 (2)Ti_m1(1)—O6—W1161.0 (3)
O4vii—K_b—W1viii87.7 (2)Ti_m1(1)—O6—Nb_m1(1)0.0 (5)
O5—K_b—O6vii130.9 (3)Ti_m1(2)ii—O6—Si1135.9 (8)
O5—K_b—O6viii130.9 (3)Ti_m1(2)ii—O6—Si2ii72.6 (3)
O5—K_b—W1ix82.8 (2)Ti_m1(2)ii—O6—O1ii46.4 (2)
O5—K_b—W1viii82.8 (2)Ti_m1(2)ii—O6—O2ii84.9 (4)
O6vii—K_b—O6viii96.7 (4)Ti_m1(2)ii—O6—O3103.1 (5)
O6vii—K_b—W1ix57.9 (2)Ti_m1(2)ii—O6—O4137.0 (4)
O6vii—K_b—W1viii122.2 (3)Ti_m1(2)ii—O6—O6vii40.9 (2)
O6viii—K_b—W1ix122.2 (3)Ti_m1(2)ii—O6—O7148.1 (8)
O6viii—K_b—W1viii57.9 (2)Ti_m1(2)ii—O6—Ohii43.4 (4)
W1ix—K_b—W1viii90.8 (2)Ti_m1(2)ii—O6—Ohv46.3 (4)
Si1—Ti_m1(1)—Si1ii180.0 (5)Ti_m1(2)ii—O6—W1114.8 (7)
Si1—Ti_m1(1)—Si2106.35 (9)Ti_m1(2)ii—O6—Nb_m1(1)76.0 (4)
Si1—Ti_m1(1)—Si2ii73.65 (9)Si1—O6—Si2ii100.0 (7)
Si1—Ti_m1(1)—O2111.3 (3)Si1—O6—O1ii127.7 (9)
Si1—Ti_m1(1)—O2ii68.7 (3)Si1—O6—O2ii73.1 (6)
Si1—Ti_m1(1)—O326.1 (4)Si1—O6—O333.0 (4)
Si1—Ti_m1(1)—O3ii153.9 (4)Si1—O6—O438.6 (5)
Si1—Ti_m1(1)—O627.07 (18)Si1—O6—O6vii113.7 (5)
Si1—Ti_m1(1)—O6ii152.93 (18)Si1—O6—O735.6 (3)
Si1—Ti_m1(1)—Oh101.0 (3)Si1—O6—Ohii93.7 (7)
Si1—Ti_m1(1)—Ohii79.0 (3)Si1—O6—Ohv169.7 (6)
Si1—Ti_m1(1)—Nb_m1(1)0Si1—O6—W1108.8 (4)
Si1ii—Ti_m1(1)—Si273.65 (9)Si1—O6—Nb_m1(1)64.2 (6)
Si1ii—Ti_m1(1)—Si2ii106.35 (9)Si2ii—O6—O1ii29.8 (3)
Si1ii—Ti_m1(1)—O268.7 (3)Si2ii—O6—O2ii29.3 (2)
Si1ii—Ti_m1(1)—O2ii111.3 (3)Si2ii—O6—O386.8 (5)
Si1ii—Ti_m1(1)—O3153.9 (4)Si2ii—O6—O4138.1 (7)
Si1ii—Ti_m1(1)—O3ii26.1 (4)Si2ii—O6—O6vii110.8 (3)
Si1ii—Ti_m1(1)—O6152.93 (18)Si2ii—O6—O779.5 (4)
Si1ii—Ti_m1(1)—O6ii27.07 (18)Si2ii—O6—Ohii63.6 (3)
Si1ii—Ti_m1(1)—Oh79.0 (3)Si2ii—O6—Ohv90.2 (3)
Si1ii—Ti_m1(1)—Ohii101.0 (3)Si2ii—O6—W1108.4 (3)
Si1ii—Ti_m1(1)—Nb_m1(1)0Si2ii—O6—Nb_m1(1)58.3 (3)
Si2—Ti_m1(1)—Si2ii180.0 (5)O1ii—O6—O2ii54.6 (4)
Si2—Ti_m1(1)—O221.0 (3)O1ii—O6—O3105.7 (6)
Si2—Ti_m1(1)—O2ii159.0 (3)O1ii—O6—O4166.1 (10)
Si2—Ti_m1(1)—O380.8 (3)O1ii—O6—O6vii87.3 (3)
Si2—Ti_m1(1)—O3ii99.2 (3)O1ii—O6—O7108.9 (5)
Si2—Ti_m1(1)—O6122.78 (14)O1ii—O6—Ohii58.0 (3)
Si2—Ti_m1(1)—O6ii57.22 (14)O1ii—O6—Ohv62.0 (4)
Si2—Ti_m1(1)—Oh71.3 (2)O1ii—O6—W1103.8 (5)
Si2—Ti_m1(1)—Ohii108.7 (2)O1ii—O6—Nb_m1(1)71.6 (4)
Si2—Ti_m1(1)—Nb_m1(1)0O2ii—O6—O357.7 (4)
Si2ii—Ti_m1(1)—O2159.0 (3)O2ii—O6—O4111.7 (8)
Si2ii—Ti_m1(1)—O2ii21.0 (3)O2ii—O6—O6vii111.2 (4)
Si2ii—Ti_m1(1)—O399.2 (3)O2ii—O6—O763.3 (4)
Si2ii—Ti_m1(1)—O3ii80.8 (3)O2ii—O6—Ohii55.3 (4)
Si2ii—Ti_m1(1)—O657.22 (14)O2ii—O6—Ohv116.6 (3)
Si2ii—Ti_m1(1)—O6ii122.78 (14)O2ii—O6—W1128.1 (3)
Si2ii—Ti_m1(1)—Oh108.7 (2)O2ii—O6—Nb_m1(1)34.2 (2)
Si2ii—Ti_m1(1)—Ohii71.3 (2)O3—O6—O461.1 (6)
Si2ii—Ti_m1(1)—Nb_m1(1)0O3—O6—O6vii91.0 (5)
O2—Ti_m1(1)—O2ii180.0 (5)O3—O6—O759.6 (5)
O2—Ti_m1(1)—O389.2 (3)O3—O6—Ohii60.8 (4)
O2—Ti_m1(1)—O3ii90.8 (3)O3—O6—Ohv148.2 (4)
O2—Ti_m1(1)—O6118.0 (4)O3—O6—W1141.8 (3)
O2—Ti_m1(1)—O6ii62.0 (4)O3—O6—Nb_m1(1)34.5 (2)
O2—Ti_m1(1)—Oh90.7 (5)O4—O6—O6vii96.9 (3)
O2—Ti_m1(1)—Ohii89.3 (5)O4—O6—O761.6 (4)
O2—Ti_m1(1)—Nb_m1(1)0O4—O6—Ohii113.8 (6)
O2ii—Ti_m1(1)—O390.8 (3)O4—O6—Ohv131.4 (8)
O2ii—Ti_m1(1)—O3ii89.2 (3)O4—O6—W186.6 (5)
O2ii—Ti_m1(1)—O662.0 (4)O4—O6—Nb_m1(1)95.6 (7)
O2ii—Ti_m1(1)—O6ii118.0 (4)O6vii—O6—O7149.0 (6)
O2ii—Ti_m1(1)—Oh89.3 (5)O6vii—O6—Ohii56.0 (4)
O2ii—Ti_m1(1)—Ohii90.7 (5)O6vii—O6—Ohv60.6 (4)
O2ii—Ti_m1(1)—Nb_m1(1)0O6vii—O6—W1114.2 (6)
O3—Ti_m1(1)—O3ii180.0 (5)O6vii—O6—Nb_m1(1)84.4 (4)
O3—Ti_m1(1)—O650.3 (5)O7—O6—Ohii109.8 (7)
O3—Ti_m1(1)—O6ii129.7 (5)O7—O6—Ohv150.3 (5)
O3—Ti_m1(1)—Oh88.0 (5)O7—O6—W188.1 (4)
O3—Ti_m1(1)—Ohii92.0 (5)O7—O6—Nb_m1(1)76.4 (5)
O3—Ti_m1(1)—Nb_m1(1)0Ohii—O6—Ohv89.7 (4)
O3ii—Ti_m1(1)—O6129.7 (5)Ohii—O6—W1157.4 (5)
O3ii—Ti_m1(1)—O6ii50.3 (5)Ohii—O6—Nb_m1(1)33.5 (3)
O3ii—Ti_m1(1)—Oh92.0 (5)Ohv—O6—W168.7 (4)
O3ii—Ti_m1(1)—Ohii88.0 (5)Ohv—O6—Nb_m1(1)121.4 (3)
O3ii—Ti_m1(1)—Nb_m1(1)0W1—O6—Nb_m1(1)161.0 (3)
O6—Ti_m1(1)—O6ii180.0 (5)Na_a—O7—Na_aiii106.1 (5)
O6—Ti_m1(1)—Oh125.0 (3)Na_a—O7—Si179.4 (6)
O6—Ti_m1(1)—Ohii55.0 (3)Na_a—O7—Si2iv77.1 (6)
O6—Ti_m1(1)—Nb_m1(1)0Na_a—O7—O1iv105.3 (5)
O6ii—Ti_m1(1)—Oh55.0 (3)Na_a—O7—O2iv44.6 (3)
O6ii—Ti_m1(1)—Ohii125.0 (3)Na_a—O7—O2ii75.7 (4)
O6ii—Ti_m1(1)—Nb_m1(1)0Na_a—O7—O3104.6 (4)
Oh—Ti_m1(1)—Ohii180.0 (5)Na_a—O7—O490.3 (6)
Oh—Ti_m1(1)—Nb_m1(1)0Na_a—O7—O5iv88.1 (6)
Ohii—Ti_m1(1)—Nb_m1(1)0Na_a—O7—O646.0 (4)
Na_aii—Ti_m1(2)—Na_ax174.2 (2)Na_a—O7—O7vi124.9 (6)
Na_aii—Ti_m1(2)—Fe_m292.91 (15)Na_a—O7—W2148.0 (4)
Na_aii—Ti_m1(2)—Si1ii62.7 (3)Na_aiii—O7—Si1117.6 (6)
Na_aii—Ti_m1(2)—Si1x112.9 (3)Na_aiii—O7—Si2iv101.0 (5)
Na_aii—Ti_m1(2)—Si257.9 (4)Na_aiii—O7—O1iv70.8 (5)
Na_aii—Ti_m1(2)—Si2xi125.4 (4)Na_aiii—O7—O2iv99.4 (5)
Na_aii—Ti_m1(2)—O159.6 (3)Na_aiii—O7—O2ii49.7 (4)
Na_aii—Ti_m1(2)—O1xi125.6 (4)Na_aiii—O7—O387.3 (6)
Na_aii—Ti_m1(2)—O269.7 (4)Na_aiii—O7—O4146.7 (7)
Na_aii—Ti_m1(2)—O2xi111.1 (4)Na_aiii—O7—O5iv131.6 (5)
Na_aii—Ti_m1(2)—O6ii45.2 (4)Na_aiii—O7—O6114.8 (4)
Na_aii—Ti_m1(2)—O6x129.6 (4)Na_aiii—O7—O7vi128.1 (7)
Na_aii—Ti_m1(2)—Oh121.2 (5)Na_aiii—O7—W242.0 (5)
Na_aii—Ti_m1(2)—Ohxi59.0 (5)Si1—O7—Si2iv139.0 (11)
Na_aii—Ti_m1(2)—Ti_m292.91 (15)Si1—O7—O1iv169.3 (4)
Na_aii—Ti_m1(2)—Mg_m292.91 (15)Si1—O7—O2iv120.3 (9)
Na_ax—Ti_m1(2)—Fe_m292.91 (15)Si1—O7—O2ii74.1 (3)
Na_ax—Ti_m1(2)—Si1ii112.9 (3)Si1—O7—O335.0 (5)
Na_ax—Ti_m1(2)—Si1x62.7 (3)Si1—O7—O436.2 (3)
Na_ax—Ti_m1(2)—Si2125.4 (4)Si1—O7—O5iv110.4 (7)
Na_ax—Ti_m1(2)—Si2xi57.9 (4)Si1—O7—O634.0 (4)
Na_ax—Ti_m1(2)—O1125.6 (4)Si1—O7—O7vi83.6 (3)
Na_ax—Ti_m1(2)—O1xi59.6 (3)Si1—O7—W2113.9 (7)
Na_ax—Ti_m1(2)—O2111.1 (4)Si2iv—O7—O1iv36.9 (5)
Na_ax—Ti_m1(2)—O2xi69.7 (4)Si2iv—O7—O2iv33.8 (3)
Na_ax—Ti_m1(2)—O6ii129.6 (4)Si2iv—O7—O2ii130.1 (3)
Na_ax—Ti_m1(2)—O6x45.2 (4)Si2iv—O7—O3170.8 (5)
Na_ax—Ti_m1(2)—Oh59.0 (5)Si2iv—O7—O4111.0 (7)
Na_ax—Ti_m1(2)—Ohxi121.2 (5)Si2iv—O7—O5iv36.4 (3)
Na_ax—Ti_m1(2)—Ti_m292.91 (15)Si2iv—O7—O6118.0 (9)
Na_ax—Ti_m1(2)—Mg_m292.91 (15)Si2iv—O7—O7vi83.0 (3)
Fe_m2—Ti_m1(2)—Si1ii134.06 (7)Si2iv—O7—W2103.7 (6)
Fe_m2—Ti_m1(2)—Si1x134.06 (7)O1iv—O7—O2iv61.9 (4)
Fe_m2—Ti_m1(2)—Si261.58 (6)O1iv—O7—O2ii116.2 (4)
Fe_m2—Ti_m1(2)—Si2xi61.58 (6)O1iv—O7—O3146.8 (9)
Fe_m2—Ti_m1(2)—O141.2 (2)O1iv—O7—O4133.3 (3)
Fe_m2—Ti_m1(2)—O1xi41.2 (2)O1iv—O7—O5iv60.8 (4)
Fe_m2—Ti_m1(2)—O282.68 (10)O1iv—O7—O6151.2 (7)
Fe_m2—Ti_m1(2)—O2xi82.68 (10)O1iv—O7—O7vi85.9 (2)
Fe_m2—Ti_m1(2)—O6ii130.9 (2)O1iv—O7—W267.2 (5)
Fe_m2—Ti_m1(2)—O6x130.9 (2)O2iv—O7—O2ii103.5 (3)
Fe_m2—Ti_m1(2)—Oh88.32 (17)O2iv—O7—O3149.2 (6)
Fe_m2—Ti_m1(2)—Ohxi88.32 (17)O2iv—O7—O4112.2 (8)
Fe_m2—Ti_m1(2)—Ti_m20.0 (5)O2iv—O7—O5iv59.1 (4)
Fe_m2—Ti_m1(2)—Mg_m20.0 (5)O2iv—O7—O689.4 (6)
Si1ii—Ti_m1(2)—Si1x91.88 (11)O2iv—O7—O7vi109.4 (4)
Si1ii—Ti_m1(2)—Si272.53 (9)O2iv—O7—W2124.6 (4)
Si1ii—Ti_m1(2)—Si2xi164.17 (9)O2ii—O7—O358.6 (2)
Si1ii—Ti_m1(2)—O194.4 (3)O2ii—O7—O4110.2 (3)
Si1ii—Ti_m1(2)—O1xi165.7 (5)O2ii—O7—O5iv162.2 (6)
Si1ii—Ti_m1(2)—O253.22 (13)O2ii—O7—O665.3 (4)
Si1ii—Ti_m1(2)—O2xi140.89 (15)O2ii—O7—O7vi146.4 (4)
Si1ii—Ti_m1(2)—O6ii19.7 (5)O2ii—O7—W280.3 (5)
Si1ii—Ti_m1(2)—O6x91.7 (3)O3—O7—O460.2 (4)
Si1ii—Ti_m1(2)—Oh75.1 (2)O3—O7—O5iv134.4 (4)
Si1ii—Ti_m1(2)—Ohxi107.3 (2)O3—O7—O660.8 (5)
Si1ii—Ti_m1(2)—Ti_m2134.06 (7)O3—O7—O7vi88.8 (2)
Si1ii—Ti_m1(2)—Mg_m2134.06 (7)O3—O7—W279.8 (5)
Si1x—Ti_m1(2)—Si2164.17 (9)O4—O7—O5iv76.5 (4)
Si1x—Ti_m1(2)—Si2xi72.53 (9)O4—O7—O657.6 (4)
Si1x—Ti_m1(2)—O1165.7 (5)O4—O7—O7vi50.7 (3)
Si1x—Ti_m1(2)—O1xi94.4 (3)O4—O7—W2118.0 (6)
Si1x—Ti_m1(2)—O2140.89 (15)O5iv—O7—O6108.2 (8)
Si1x—Ti_m1(2)—O2xi53.22 (13)O5iv—O7—O7vi50.4 (3)
Si1x—Ti_m1(2)—O6ii91.7 (3)O5iv—O7—W2111.8 (5)
Si1x—Ti_m1(2)—O6x19.7 (5)O6—O7—O7vi107.9 (4)
Si1x—Ti_m1(2)—Oh107.3 (2)O6—O7—W2136.9 (5)
Si1x—Ti_m1(2)—Ohxi75.1 (2)O7vi—O7—W286.4 (4)
Si1x—Ti_m1(2)—Ti_m2134.06 (7)Na_aiii—Oh—Na_ax48.5 (6)
Si1x—Ti_m1(2)—Mg_m2134.06 (7)Na_aiii—Oh—Ti_m1(1)90.7 (7)
Si2—Ti_m1(2)—Si2xi123.17 (10)Na_aiii—Oh—Ti_m1(2)133.8 (7)
Si2—Ti_m1(2)—O124.0 (4)Na_aiii—Oh—Si1ii128.9 (3)
Si2—Ti_m1(2)—O1xi101.4 (3)Na_aiii—Oh—Si2147.7 (6)
Si2—Ti_m1(2)—O227.30 (16)Na_aiii—Oh—O1150.3 (3)
Si2—Ti_m1(2)—O2xi140.12 (14)Na_aiii—Oh—O1xi101.6 (5)
Si2—Ti_m1(2)—O6ii72.7 (3)Na_aiii—Oh—O2132.3 (8)
Si2—Ti_m1(2)—O6x157.1 (5)Na_aiii—Oh—O2ii48.4 (4)
Si2—Ti_m1(2)—Oh72.0 (2)Na_aiii—Oh—O376.0 (5)
Si2—Ti_m1(2)—Ohxi106.4 (2)Na_aiii—Oh—O3ii104.5 (5)
Si2—Ti_m1(2)—Ti_m261.58 (6)Na_aiii—Oh—O6ii146.4 (3)
Si2—Ti_m1(2)—Mg_m261.58 (6)Na_aiii—Oh—O6x93.2 (5)
Si2xi—Ti_m1(2)—O1101.4 (3)Na_aiii—Oh—Ba88.4 (3)
Si2xi—Ti_m1(2)—O1xi24.0 (4)Na_aiii—Oh—W1iii37.3 (3)
Si2xi—Ti_m1(2)—O2140.12 (14)Na_aiii—Oh—W240.3 (3)
Si2xi—Ti_m1(2)—O2xi27.30 (16)Na_aiii—Oh—W_c88.4 (3)
Si2xi—Ti_m1(2)—O6ii157.1 (5)Na_aiii—Oh—Nb_m1(1)90.7 (7)
Si2xi—Ti_m1(2)—O6x72.7 (3)Na_ax—Oh—Ti_m1(1)137.0 (7)
Si2xi—Ti_m1(2)—Oh106.4 (2)Na_ax—Oh—Ti_m1(2)85.4 (7)
Si2xi—Ti_m1(2)—Ohxi72.0 (2)Na_ax—Oh—Si1ii124.3 (4)
Si2xi—Ti_m1(2)—Ti_m261.58 (6)Na_ax—Oh—Si2147.0 (6)
Si2xi—Ti_m1(2)—Mg_m261.58 (6)Na_ax—Oh—O1118.3 (7)
O1—Ti_m1(2)—O1xi82.4 (3)Na_ax—Oh—O1xi61.2 (5)
O1—Ti_m1(2)—O250.8 (4)Na_ax—Oh—O2176.4 (4)
O1—Ti_m1(2)—O2xi116.1 (4)Na_ax—Oh—O2ii91.0 (5)
O1—Ti_m1(2)—O6ii89.9 (3)Na_ax—Oh—O3118.1 (5)
O1—Ti_m1(2)—O6x170.7 (3)Na_ax—Oh—O3ii123.1 (3)
O1—Ti_m1(2)—Oh86.7 (5)Na_ax—Oh—O6ii114.6 (7)
O1—Ti_m1(2)—Ohxi90.7 (5)Na_ax—Oh—O6x51.2 (5)
O1—Ti_m1(2)—Ti_m241.2 (2)Na_ax—Oh—Ba88.7 (3)
O1—Ti_m1(2)—Mg_m241.2 (2)Na_ax—Oh—W1iii37.7 (3)
O1xi—Ti_m1(2)—O2116.1 (4)Na_ax—Oh—W241.0 (3)
O1xi—Ti_m1(2)—O2xi50.8 (4)Na_ax—Oh—W_c88.7 (3)
O1xi—Ti_m1(2)—O6ii170.7 (3)Na_ax—Oh—Nb_m1(1)137.0 (7)
O1xi—Ti_m1(2)—O6x89.9 (3)Ti_m1(1)—Oh—Ti_m1(2)132.1 (3)
O1xi—Ti_m1(2)—Oh90.7 (5)Ti_m1(1)—Oh—Si1ii66.8 (2)
O1xi—Ti_m1(2)—Ohxi86.7 (5)Ti_m1(1)—Oh—Si274.4 (2)
O1xi—Ti_m1(2)—Ti_m241.2 (2)Ti_m1(1)—Oh—O1104.2 (4)
O1xi—Ti_m1(2)—Mg_m241.2 (2)Ti_m1(1)—Oh—O1xi158.4 (3)
O2—Ti_m1(2)—O2xi165.36 (14)Ti_m1(1)—Oh—O245.3 (3)
O2—Ti_m1(2)—O6ii61.7 (5)Ti_m1(1)—Oh—O2ii46.0 (3)
O2—Ti_m1(2)—O6x129.9 (5)Ti_m1(1)—Oh—O346.9 (4)
O2—Ti_m1(2)—Oh52.1 (3)Ti_m1(1)—Oh—O3ii44.9 (3)
O2—Ti_m1(2)—Ohxi127.4 (3)Ti_m1(1)—Oh—O6ii91.6 (4)
O2—Ti_m1(2)—Ti_m282.68 (10)Ti_m1(1)—Oh—O6x137.1 (3)
O2—Ti_m1(2)—Mg_m282.68 (10)Ti_m1(1)—Oh—Ba105.6 (5)
O2xi—Ti_m1(2)—O6ii129.9 (5)Ti_m1(1)—Oh—W1iii102.7 (4)
O2xi—Ti_m1(2)—O6x61.7 (5)Ti_m1(1)—Oh—W2118.5 (6)
O2xi—Ti_m1(2)—Oh127.4 (3)Ti_m1(1)—Oh—W_c105.6 (5)
O2xi—Ti_m1(2)—Ohxi52.1 (3)Ti_m1(1)—Oh—Nb_m1(1)0.0 (5)
O2xi—Ti_m1(2)—Ti_m282.68 (10)Ti_m1(2)—Oh—Si1ii70.4 (2)
O2xi—Ti_m1(2)—Mg_m282.68 (10)Ti_m1(2)—Oh—Si272.7 (3)
O6ii—Ti_m1(2)—O6x98.1 (3)Ti_m1(2)—Oh—O147.7 (4)
O6ii—Ti_m1(2)—Oh94.0 (5)Ti_m1(2)—Oh—O1xi45.6 (4)
O6ii—Ti_m1(2)—Ohxi88.2 (5)Ti_m1(2)—Oh—O293.8 (4)
O6ii—Ti_m1(2)—Ti_m2130.9 (2)Ti_m1(2)—Oh—O2ii151.1 (3)
O6ii—Ti_m1(2)—Mg_m2130.9 (2)Ti_m1(2)—Oh—O3143.1 (3)
O6x—Ti_m1(2)—Oh88.2 (5)Ti_m1(2)—Oh—O3ii98.4 (4)
O6x—Ti_m1(2)—Ohxi94.0 (5)Ti_m1(2)—Oh—O6ii42.6 (4)
O6x—Ti_m1(2)—Ti_m2130.9 (2)Ti_m1(2)—Oh—O6x45.5 (4)
O6x—Ti_m1(2)—Mg_m2130.9 (2)Ti_m1(2)—Oh—Ba94.0 (4)
Oh—Ti_m1(2)—Ohxi176.6 (3)Ti_m1(2)—Oh—W1iii105.7 (4)
Oh—Ti_m1(2)—Ti_m288.32 (17)Ti_m1(2)—Oh—W2108.6 (5)
Oh—Ti_m1(2)—Mg_m288.32 (17)Ti_m1(2)—Oh—W_c94.0 (4)
Ohxi—Ti_m1(2)—Ti_m288.32 (17)Ti_m1(2)—Oh—Nb_m1(1)132.1 (3)
Ohxi—Ti_m1(2)—Mg_m288.32 (17)Si1ii—Oh—Si271.59 (13)
Ti_m2—Ti_m1(2)—Mg_m20.0 (5)Si1ii—Oh—O180.8 (2)
Ti_m1(2)—Fe_m2—Ti_m1(2)xii180.0 (5)Si1ii—Oh—O1xi116.0 (5)
Ti_m1(2)—Fe_m2—Si262.28 (5)Si1ii—Oh—O258.59 (19)
Ti_m1(2)—Fe_m2—Si2xi62.28 (5)Si1ii—Oh—O2ii88.4 (3)
Ti_m1(2)—Fe_m2—Si2xii117.72 (5)Si1ii—Oh—O3110.5 (4)
Ti_m1(2)—Fe_m2—Si2vi117.72 (5)Si1ii—Oh—O3ii28.6 (3)
Ti_m1(2)—Fe_m2—O141.5 (2)Si1ii—Oh—O6ii28.2 (3)
Ti_m1(2)—Fe_m2—O1xi41.5 (2)Si1ii—Oh—O6x77.9 (3)
Ti_m1(2)—Fe_m2—O1xii138.5 (2)Si1ii—Oh—Ba140.4 (2)
Ti_m1(2)—Fe_m2—O1vi138.5 (2)Si1ii—Oh—W1iii101.4 (2)
Ti_m1(2)—Fe_m2—O590Si1ii—Oh—W2164.2 (3)
Ti_m1(2)—Fe_m2—O5xi90Si1ii—Oh—W_c140.4 (2)
Ti_m1(2)—Fe_m2—Ba90Si1ii—Oh—Nb_m1(1)66.8 (2)
Ti_m1(2)—Fe_m2—Baxi90Si2—Oh—O130.0 (3)
Ti_m1(2)—Fe_m2—W_c90Si2—Oh—O1xi86.0 (3)
Ti_m1(2)—Fe_m2—W_cxi90Si2—Oh—O229.9 (3)
Ti_m1(2)—Fe_m2—Ti_m20Si2—Oh—O2ii119.9 (5)
Ti_m1(2)—Fe_m2—Mg_m20Si2—Oh—O372.9 (3)
Ti_m1(2)xii—Fe_m2—Si2117.72 (5)Si2—Oh—O3ii85.1 (2)
Ti_m1(2)xii—Fe_m2—Si2xi117.72 (5)Si2—Oh—O6ii64.1 (2)
Ti_m1(2)xii—Fe_m2—Si2xii62.28 (5)Si2—Oh—O6x117.3 (5)
Ti_m1(2)xii—Fe_m2—Si2vi62.28 (5)Si2—Oh—Ba69.06 (12)
Ti_m1(2)xii—Fe_m2—O1138.5 (2)Si2—Oh—W1iii173.0 (2)
Ti_m1(2)xii—Fe_m2—O1xi138.5 (2)Si2—Oh—W2123.8 (2)
Ti_m1(2)xii—Fe_m2—O1xii41.5 (2)Si2—Oh—W_c69.06 (12)
Ti_m1(2)xii—Fe_m2—O1vi41.5 (2)Si2—Oh—Nb_m1(1)74.4 (2)
Ti_m1(2)xii—Fe_m2—O590O1—Oh—O1xi57.3 (4)
Ti_m1(2)xii—Fe_m2—O5xi90O1—Oh—O259.1 (4)
Ti_m1(2)xii—Fe_m2—Ba90O1—Oh—O2ii149.9 (6)
Ti_m1(2)xii—Fe_m2—Baxi90O1—Oh—O395.4 (4)
Ti_m1(2)xii—Fe_m2—W_c90O1—Oh—O3ii104.2 (3)
Ti_m1(2)xii—Fe_m2—W_cxi90O1—Oh—O6ii60.1 (3)
Ti_m1(2)xii—Fe_m2—Ti_m20O1—Oh—O6x92.9 (6)
Ti_m1(2)xii—Fe_m2—Mg_m20O1—Oh—Ba63.0 (2)
Si2—Fe_m2—Si2xi124.57 (8)O1—Oh—W1iii151.4 (7)
Si2—Fe_m2—Si2xii180.0 (5)O1—Oh—W2110.6 (3)
Si2—Fe_m2—Si2vi55.43 (8)O1—Oh—W_c63.0 (2)
Si2—Fe_m2—O124.4 (4)O1—Oh—Nb_m1(1)104.2 (4)
Si2—Fe_m2—O1xi102.4 (3)O1xi—Oh—O2115.9 (4)
Si2—Fe_m2—O1xii155.6 (4)O1xi—Oh—O2ii149.9 (3)
Si2—Fe_m2—O1vi77.6 (3)O1xi—Oh—O3118.8 (3)
Si2—Fe_m2—O529.44 (12)O1xi—Oh—O3ii143.8 (6)
Si2—Fe_m2—O5xi150.56 (12)O1xi—Oh—O6ii87.9 (6)
Si2—Fe_m2—Ba80.24 (13)O1xi—Oh—O6x60.6 (4)
Si2—Fe_m2—Baxi99.76 (13)O1xi—Oh—Ba57.7 (3)
Si2—Fe_m2—W_c80.24 (13)O1xi—Oh—W1iii97.7 (3)
Si2—Fe_m2—W_cxi99.76 (13)O1xi—Oh—W265.3 (3)
Si2—Fe_m2—Ti_m20O1xi—Oh—W_c57.7 (3)
Si2—Fe_m2—Mg_m20O1xi—Oh—Nb_m1(1)158.4 (3)
Si2xi—Fe_m2—Si2xii55.43 (8)O2—Oh—O2ii91.3 (5)
Si2xi—Fe_m2—Si2vi180.0 (5)O2—Oh—O360.8 (4)
Si2xi—Fe_m2—O1102.4 (3)O2—Oh—O3ii60.5 (3)
Si2xi—Fe_m2—O1xi24.4 (4)O2—Oh—O6ii66.7 (4)
Si2xi—Fe_m2—O1xii77.6 (3)O2—Oh—O6x130.0 (5)
Si2xi—Fe_m2—O1vi155.6 (4)O2—Oh—Ba87.8 (2)
Si2xi—Fe_m2—O5150.56 (12)O2—Oh—W1iii145.6 (5)
Si2xi—Fe_m2—O5xi29.44 (12)O2—Oh—W2136.4 (4)
Si2xi—Fe_m2—Ba99.76 (13)O2—Oh—W_c87.8 (2)
Si2xi—Fe_m2—Baxi80.24 (13)O2—Oh—Nb_m1(1)45.3 (3)
Si2xi—Fe_m2—W_c99.76 (13)O2ii—Oh—O362.2 (5)
Si2xi—Fe_m2—W_cxi80.24 (13)O2ii—Oh—O3ii60.1 (4)
Si2xi—Fe_m2—Ti_m20O2ii—Oh—O6ii116.0 (4)
Si2xi—Fe_m2—Mg_m20O2ii—Oh—O6x112.3 (4)
Si2xii—Fe_m2—Si2vi124.57 (8)O2ii—Oh—Ba114.6 (5)
Si2xii—Fe_m2—O1155.6 (4)O2ii—Oh—W1iii58.3 (2)
Si2xii—Fe_m2—O1xi77.6 (3)O2ii—Oh—W286.4 (3)
Si2xii—Fe_m2—O1xii24.4 (4)O2ii—Oh—W_c114.6 (5)
Si2xii—Fe_m2—O1vi102.4 (3)O2ii—Oh—Nb_m1(1)46.0 (3)
Si2xii—Fe_m2—O5150.56 (12)O3—Oh—O3ii91.8 (6)
Si2xii—Fe_m2—O5xi29.44 (12)O3—Oh—O6ii127.3 (4)
Si2xii—Fe_m2—Ba99.76 (13)O3—Oh—O6x169.0 (3)
Si2xii—Fe_m2—Baxi80.24 (13)O3—Oh—Ba61.1 (3)
Si2xii—Fe_m2—W_c99.76 (13)O3—Oh—W1iii110.0 (4)
Si2xii—Fe_m2—W_cxi80.24 (13)O3—Oh—W280.1 (3)
Si2xii—Fe_m2—Ti_m20O3—Oh—W_c61.1 (3)
Si2xii—Fe_m2—Mg_m20O3—Oh—Nb_m1(1)46.9 (4)
Si2vi—Fe_m2—O177.6 (3)O3ii—Oh—O6ii56.8 (4)
Si2vi—Fe_m2—O1xi155.6 (4)O3ii—Oh—O6x93.1 (4)
Si2vi—Fe_m2—O1xii102.4 (3)O3ii—Oh—Ba146.6 (5)
Si2vi—Fe_m2—O1vi24.4 (4)O3ii—Oh—W1iii88.4 (3)
Si2vi—Fe_m2—O529.44 (12)O3ii—Oh—W2144.8 (5)
Si2vi—Fe_m2—O5xi150.56 (12)O3ii—Oh—W_c146.6 (5)
Si2vi—Fe_m2—Ba80.24 (13)O3ii—Oh—Nb_m1(1)44.9 (3)
Si2vi—Fe_m2—Baxi99.76 (13)O6ii—Oh—O6x63.4 (4)
Si2vi—Fe_m2—W_c80.24 (13)O6ii—Oh—Ba123.0 (4)
Si2vi—Fe_m2—W_cxi99.76 (13)O6ii—Oh—W1iii109.9 (3)
Si2vi—Fe_m2—Ti_m20O6ii—Oh—W2149.8 (7)
Si2vi—Fe_m2—Mg_m20O6ii—Oh—W_c123.0 (4)
O1—Fe_m2—O1xi83.1 (3)O6ii—Oh—Nb_m1(1)91.6 (4)
O1—Fe_m2—O1xii180.0 (5)O6x—Oh—Ba117.2 (5)
O1—Fe_m2—O1vi96.9 (3)O6x—Oh—W1iii60.3 (3)
O1—Fe_m2—O553.8 (4)O6x—Oh—W290.2 (3)
O1—Fe_m2—O5xi126.2 (4)O6x—Oh—W_c117.2 (5)
O1—Fe_m2—Ba93.7 (4)O6x—Oh—Nb_m1(1)137.1 (3)
O1—Fe_m2—Baxi86.3 (4)Ba—Oh—W1iii118.0 (2)
O1—Fe_m2—W_c93.7 (4)Ba—Oh—W254.71 (19)
O1—Fe_m2—W_cxi86.3 (4)Ba—Oh—W_c0.0 (5)
O1—Fe_m2—Ti_m20Ba—Oh—Nb_m1(1)105.6 (5)
O1—Fe_m2—Mg_m20W1iii—Oh—W263.2 (2)
O1xi—Fe_m2—O1xii96.9 (3)W1iii—Oh—W_c118.0 (2)
O1xi—Fe_m2—O1vi180.0 (5)W1iii—Oh—Nb_m1(1)102.7 (4)
O1xi—Fe_m2—O5126.2 (4)W2—Oh—W_c54.71 (19)
O1xi—Fe_m2—O5xi53.8 (4)W2—Oh—Nb_m1(1)118.5 (6)
O1xi—Fe_m2—Ba86.3 (4)W_c—Oh—Nb_m1(1)105.6 (5)
O1xi—Fe_m2—Baxi93.7 (4)Fe_m2—Ba—Si263.84 (12)
O1xi—Fe_m2—W_c86.3 (4)Fe_m2—Ba—Si2vi63.84 (12)
O1xi—Fe_m2—W_cxi93.7 (4)Fe_m2—Ba—O142.0 (3)
O1xi—Fe_m2—Ti_m20Fe_m2—Ba—O1xi45.6 (2)
O1xi—Fe_m2—Mg_m20Fe_m2—Ba—O1xii45.6 (2)
O1xii—Fe_m2—O1vi83.1 (3)Fe_m2—Ba—O1vi42.0 (3)
O1xii—Fe_m2—O5126.2 (4)Fe_m2—Ba—O3127.8 (2)
O1xii—Fe_m2—O5xi53.8 (4)Fe_m2—Ba—O3vi127.8 (2)
O1xii—Fe_m2—Ba86.3 (4)Fe_m2—Ba—O573.6 (4)
O1xii—Fe_m2—Baxi93.7 (4)Fe_m2—Ba—Oh86.8 (3)
O1xii—Fe_m2—W_c86.3 (4)Fe_m2—Ba—Ohvi86.8 (3)
O1xii—Fe_m2—W_cxi93.7 (4)Fe_m2—Ba—W2114.03 (18)
O1xii—Fe_m2—Ti_m20Fe_m2—Ba—W2xiv114.03 (18)
O1xii—Fe_m2—Mg_m20Fe_m2—Ba—W_c0
O1vi—Fe_m2—O553.8 (4)Fe_m2—Ba—Ti_m20.0 (5)
O1vi—Fe_m2—O5xi126.2 (4)Fe_m2—Ba—Mg_m20.0 (5)
O1vi—Fe_m2—Ba93.7 (4)Si2—Ba—Si2vi50.12 (6)
O1vi—Fe_m2—Baxi86.3 (4)Si2—Ba—O127.0 (3)
O1vi—Fe_m2—W_c93.7 (4)Si2—Ba—O1xi80.68 (17)
O1vi—Fe_m2—W_cxi86.3 (4)Si2—Ba—O1xii107.0 (2)
O1vi—Fe_m2—Ti_m20Si2—Ba—O1vi62.28 (14)
O1vi—Fe_m2—Mg_m20Si2—Ba—O366.0 (2)
O5—Fe_m2—O5xi180.0 (5)Si2—Ba—O3vi94.09 (17)
O5—Fe_m2—Ba68.6 (3)Si2—Ba—O527.93 (18)
O5—Fe_m2—Baxi111.4 (3)Si2—Ba—Oh58.49 (11)
O5—Fe_m2—W_c68.6 (3)Si2—Ba—Ohvi108.61 (12)
O5—Fe_m2—W_cxi111.4 (3)Si2—Ba—W2122.25 (18)
O5—Fe_m2—Ti_m20Si2—Ba—W2xiv172.37 (18)
O5—Fe_m2—Mg_m20Si2—Ba—W_c0
O5xi—Fe_m2—Ba111.4 (3)Si2—Ba—Ti_m263.84 (12)
O5xi—Fe_m2—Baxi68.6 (3)Si2—Ba—Mg_m263.84 (12)
O5xi—Fe_m2—W_c111.4 (3)Si2vi—Ba—O162.28 (14)
O5xi—Fe_m2—W_cxi68.6 (3)Si2vi—Ba—O1xi107.0 (2)
O5xi—Fe_m2—Ti_m20Si2vi—Ba—O1xii80.68 (17)
O5xi—Fe_m2—Mg_m20Si2vi—Ba—O1vi27.0 (3)
Ba—Fe_m2—Baxi180.0 (5)Si2vi—Ba—O394.09 (17)
Ba—Fe_m2—W_c0.0 (5)Si2vi—Ba—O3vi66.0 (2)
Ba—Fe_m2—W_cxi180.0 (5)Si2vi—Ba—O527.93 (18)
Ba—Fe_m2—Ti_m20Si2vi—Ba—Oh108.61 (12)
Ba—Fe_m2—Mg_m20Si2vi—Ba—Ohvi58.49 (11)
Baxi—Fe_m2—W_c180.0 (5)Si2vi—Ba—W2172.37 (18)
Baxi—Fe_m2—W_cxi0.0 (5)Si2vi—Ba—W2xiv122.25 (18)
Baxi—Fe_m2—Ti_m20Si2vi—Ba—W_c0
Baxi—Fe_m2—Mg_m20Si2vi—Ba—Ti_m263.84 (12)
W_c—Fe_m2—W_cxi180.0 (5)Si2vi—Ba—Mg_m263.84 (12)
W_c—Fe_m2—Ti_m20O1—Ba—O1xi54.6 (3)
W_c—Fe_m2—Mg_m20O1—Ba—O1xii87.6 (3)
W_cxi—Fe_m2—Ti_m20O1—Ba—O1vi60.31 (19)
W_cxi—Fe_m2—Mg_m20O1—Ba—O385.8 (3)
Ti_m2—Fe_m2—Mg_m20O1—Ba—O3vi119.6 (3)
Na_a—Si1—Na_aiii83.7 (5)O1—Ba—O550.6 (4)
Na_a—Si1—K_b136.1 (3)O1—Ba—Oh54.3 (2)
Na_a—Si1—Ti_m1(1)105.2 (2)O1—Ba—Ohvi114.5 (2)
Na_a—Si1—Ti_m1(2)ii60.11 (18)O1—Ba—W2110.9 (2)
Na_a—Si1—Si1vi127.5 (3)O1—Ba—W2xiv154.1 (4)
Na_a—Si1—Si2iv62.0 (2)O1—Ba—W_c0
Na_a—Si1—O2ii74.2 (4)O1—Ba—Ti_m242.0 (3)
Na_a—Si1—O3137.9 (3)O1—Ba—Mg_m242.0 (3)
Na_a—Si1—O4109.4 (8)O1xi—Ba—O1xii64.8 (3)
Na_a—Si1—O638.9 (3)O1xi—Ba—O1vi87.6 (3)
Na_a—Si1—O772.4 (6)O1xi—Ba—O3112.9 (3)
Na_a—Si1—Ohii87.3 (3)O1xi—Ba—O3vi173.0 (2)
Na_a—Si1—Nb_m1(1)105.2 (2)O1xi—Ba—O5104.8 (4)
Na_aiii—Si1—K_b131.7 (4)O1xi—Ba—Oh58.4 (4)
Na_aiii—Si1—Ti_m1(1)64.8 (2)O1xi—Ba—Ohvi122.7 (4)
Na_aiii—Si1—Ti_m1(2)ii106.9 (2)O1xi—Ba—W269.38 (19)
Na_aiii—Si1—Si1vi118.7 (3)O1xi—Ba—W2xiv103.1 (2)
Na_aiii—Si1—Si2iv57.3 (3)O1xi—Ba—W_c0
Na_aiii—Si1—O2ii41.4 (2)O1xi—Ba—Ti_m245.6 (2)
Na_aiii—Si1—O376.6 (5)O1xi—Ba—Mg_m245.6 (2)
Na_aiii—Si1—O4139.4 (5)O1xii—Ba—O1vi54.6 (3)
Na_aiii—Si1—O6108.3 (4)O1xii—Ba—O3173.0 (2)
Na_aiii—Si1—O737.9 (5)O1xii—Ba—O3vi112.9 (3)
Na_aiii—Si1—Ohii90.9 (3)O1xii—Ba—O5104.8 (4)
Na_aiii—Si1—Nb_m1(1)64.8 (2)O1xii—Ba—Oh122.7 (4)
K_b—Si1—Ti_m1(1)76.78 (13)O1xii—Ba—Ohvi58.4 (4)
K_b—Si1—Ti_m1(2)ii82.24 (11)O1xii—Ba—W2103.1 (2)
K_b—Si1—Si1vi64.03 (6)O1xii—Ba—W2xiv69.38 (19)
K_b—Si1—Si2iv153.55 (9)O1xii—Ba—W_c0
K_b—Si1—O2ii113.19 (19)O1xii—Ba—Ti_m245.6 (2)
K_b—Si1—O355.6 (4)O1xii—Ba—Mg_m245.6 (2)
K_b—Si1—O463.3 (4)O1vi—Ba—O3119.6 (3)
K_b—Si1—O698.5 (3)O1vi—Ba—O3vi85.8 (3)
K_b—Si1—O7151.1 (5)O1vi—Ba—O550.6 (4)
K_b—Si1—Ohii70.00 (11)O1vi—Ba—Oh114.5 (2)
K_b—Si1—Nb_m1(1)76.78 (13)O1vi—Ba—Ohvi54.3 (2)
Ti_m1(1)—Si1—Ti_m1(2)ii67.32 (5)O1vi—Ba—W2154.1 (4)
Ti_m1(1)—Si1—Si1vi127.2 (2)O1vi—Ba—W2xiv110.9 (2)
Ti_m1(1)—Si1—Si2iv121.44 (17)O1vi—Ba—W_c0
Ti_m1(1)—Si1—O2ii37.10 (17)O1vi—Ba—Ti_m242.0 (3)
Ti_m1(1)—Si1—O332.7 (2)O1vi—Ba—Mg_m242.0 (3)
Ti_m1(1)—Si1—O4139.1 (5)O3—Ba—O3vi68.6 (3)
Ti_m1(1)—Si1—O688.7 (5)O3—Ba—O569.0 (3)
Ti_m1(1)—Si1—O7102.7 (5)O3—Ba—Oh54.5 (4)
Ti_m1(1)—Si1—Ohii34.3 (3)O3—Ba—Ohvi122.7 (4)
Ti_m1(1)—Si1—Nb_m1(1)0.0 (5)O3—Ba—W281.57 (18)
Ti_m1(2)ii—Si1—Si1vi134.06 (18)O3—Ba—W2xiv117.5 (2)
Ti_m1(2)ii—Si1—Si2iv121.30 (15)O3—Ba—W_c0
Ti_m1(2)ii—Si1—O2ii67.3 (2)O3—Ba—Ti_m2127.8 (2)
Ti_m1(2)ii—Si1—O390.5 (3)O3—Ba—Mg_m2127.8 (2)
Ti_m1(2)ii—Si1—O4112.9 (6)O3vi—Ba—O569.0 (3)
Ti_m1(2)ii—Si1—O624.4 (4)O3vi—Ba—Oh122.7 (4)
Ti_m1(2)ii—Si1—O7124.8 (3)O3vi—Ba—Ohvi54.5 (4)
Ti_m1(2)ii—Si1—Ohii34.5 (3)O3vi—Ba—W2117.5 (2)
Ti_m1(2)ii—Si1—Nb_m1(1)67.32 (5)O3vi—Ba—W2xiv81.57 (18)
Si1vi—Si1—Si2iv89.68 (8)O3vi—Ba—W_c0
Si1vi—Si1—O2ii153.5 (4)O3vi—Ba—Ti_m2127.8 (2)
Si1vi—Si1—O394.6 (3)O3vi—Ba—Mg_m2127.8 (2)
Si1vi—Si1—O424.4 (7)O5—Ba—Oh83.72 (13)
Si1vi—Si1—O6129.3 (5)O5—Ba—Ohvi83.72 (13)
Si1vi—Si1—O796.4 (2)O5—Ba—W2145.2 (2)
Si1vi—Si1—Ohii134.02 (13)O5—Ba—W2xiv145.2 (2)
Si1vi—Si1—Nb_m1(1)127.2 (2)O5—Ba—W_c0
Si2iv—Si1—O2ii88.82 (14)O5—Ba—Ti_m273.6 (4)
Si2iv—Si1—O3128.9 (5)O5—Ba—Mg_m273.6 (4)
Si2iv—Si1—O494.2 (3)Oh—Ba—Ohvi167.10 (16)
Si2iv—Si1—O6100.7 (3)Oh—Ba—W263.8 (2)
Si2iv—Si1—O720.4 (6)Oh—Ba—W2xiv129.1 (2)
Si2iv—Si1—Ohii136.11 (12)Oh—Ba—W_c0
Si2iv—Si1—Nb_m1(1)121.44 (17)Oh—Ba—Ti_m286.8 (3)
O2ii—Si1—O366.4 (3)Oh—Ba—Mg_m286.8 (3)
O2ii—Si1—O4176.1 (6)Ohvi—Ba—W2129.1 (2)
O2ii—Si1—O676.9 (5)Ohvi—Ba—W2xiv63.8 (2)
O2ii—Si1—O774.3 (3)Ohvi—Ba—W_c0
O2ii—Si1—Ohii51.0 (2)Ohvi—Ba—Ti_m286.8 (3)
O2ii—Si1—Nb_m1(1)37.10 (17)Ohvi—Ba—Mg_m286.8 (3)
O3—Si1—O4109.7 (7)W2—Ba—W2xiv65.4 (3)
O3—Si1—O6114.7 (5)W2—Ba—W_c0
O3—Si1—O7109.0 (8)W2—Ba—Ti_m2114.03 (18)
O3—Si1—Ohii56.6 (4)W2—Ba—Mg_m2114.03 (18)
O3—Si1—Nb_m1(1)32.7 (2)W2xiv—Ba—W_c0
O4—Si1—O6104.9 (9)W2xiv—Ba—Ti_m2114.03 (18)
O4—Si1—O7107.9 (4)W2xiv—Ba—Mg_m2114.03 (18)
O4—Si1—Ohii126.9 (4)W_c—Ba—Ti_m20
O4—Si1—Nb_m1(1)139.1 (5)W_c—Ba—Mg_m20
O6—Si1—O7110.4 (5)Ti_m2—Ba—Mg_m20.0 (5)
O6—Si1—Ohii58.1 (5)Na_a—W1—Na_ai74.1 (9)
O6—Si1—Nb_m1(1)88.7 (5)Na_a—W1—K_biv126.4 (4)
O7—Si1—Ohii125.2 (3)Na_a—W1—K_bvii122.9 (4)
O7—Si1—Nb_m1(1)102.7 (5)Na_a—W1—O2iv53.0 (4)
Ohii—Si1—Nb_m1(1)34.3 (3)Na_a—W1—O2vii106.4 (6)
Na_aix—Si2—Na_aii90.2 (5)Na_a—W1—O653.0 (5)
Na_aix—Si2—Ti_m1(1)65.2 (2)Na_a—W1—O6i109.4 (6)
Na_aix—Si2—Ti_m1(2)111.3 (2)Na_a—W1—Ohiii64.8 (4)
Na_aix—Si2—Fe_m2163.1 (2)Na_a—W1—Ohv61.5 (4)
Na_aix—Si2—Si1ix64.3 (2)Na_a—W1—W2iii37.0 (6)
Na_aix—Si2—Si2vi128.8 (3)Na_ai—W1—K_biv122.9 (4)
Na_aix—Si2—O1140.7 (3)Na_ai—W1—K_bvii126.4 (4)
Na_aix—Si2—O1vi156.9 (4)Na_ai—W1—O2iv106.4 (6)
Na_aix—Si2—O239.4 (3)Na_ai—W1—O2vii53.0 (4)
Na_aix—Si2—O5108.2 (7)Na_ai—W1—O6109.4 (6)
Na_aix—Si2—O6ii81.1 (4)Na_ai—W1—O6i53.0 (5)
Na_aix—Si2—O7ix74.7 (6)Na_ai—W1—Ohiii61.5 (4)
Na_aix—Si2—Oh96.0 (3)Na_ai—W1—Ohv64.8 (4)
Na_aix—Si2—Ba131.7 (3)Na_ai—W1—W2iii37.0 (6)
Na_aix—Si2—W_c131.7 (3)K_biv—W1—K_bvii89.2 (3)
Na_aix—Si2—Nb_m1(1)65.2 (2)K_biv—W1—O2iv73.7 (2)
Na_aix—Si2—Ti_m2163.1 (2)K_biv—W1—O2vii124.5 (3)
Na_aix—Si2—Mg_m2163.1 (2)K_biv—W1—O6125.4 (3)
Na_aii—Si2—Ti_m1(1)107.7 (2)K_biv—W1—O6i70.2 (2)
Na_aii—Si2—Ti_m1(2)63.0 (2)K_biv—W1—Ohiii79.82 (11)
Na_aii—Si2—Fe_m292.8 (3)K_biv—W1—Ohv169.0 (3)
Na_aii—Si2—Si1ix68.4 (2)K_biv—W1—W2iii135.42 (15)
Na_aii—Si2—Si2vi122.4 (3)K_bvii—W1—O2iv124.5 (3)
Na_aii—Si2—O165.3 (5)K_bvii—W1—O2vii73.7 (2)
Na_aii—Si2—O1vi106.1 (4)K_bvii—W1—O670.2 (2)
Na_aii—Si2—O2104.4 (5)K_bvii—W1—O6i125.4 (3)
Na_aii—Si2—O5145.9 (7)K_bvii—W1—Ohiii169.0 (3)
Na_aii—Si2—O6ii44.3 (3)K_bvii—W1—Ohv79.82 (11)
Na_aii—Si2—O7ix48.8 (5)K_bvii—W1—W2iii135.42 (15)
Na_aii—Si2—Oh93.8 (3)O2iv—W1—O2vii157.0 (4)
Na_aii—Si2—Ba123.1 (3)O2iv—W1—O677.9 (3)
Na_aii—Si2—W_c123.1 (3)O2iv—W1—O6i98.1 (3)
Na_aii—Si2—Nb_m1(1)107.7 (2)O2iv—W1—Ohiii52.0 (4)
Na_aii—Si2—Ti_m292.8 (3)O2iv—W1—Ohv113.0 (4)
Na_aii—Si2—Mg_m292.8 (3)O2iv—W1—W2iii78.5 (2)
Ti_m1(1)—Si2—Ti_m1(2)65.93 (5)O2vii—W1—O698.1 (3)
Ti_m1(1)—Si2—Fe_m298.07 (6)O2vii—W1—O6i77.9 (3)
Ti_m1(1)—Si2—Si1ix129.30 (16)O2vii—W1—Ohiii113.0 (4)
Ti_m1(1)—Si2—Si2vi125.70 (16)O2vii—W1—Ohv52.0 (4)
Ti_m1(1)—Si2—O192.3 (4)O2vii—W1—W2iii78.5 (2)
Ti_m1(1)—Si2—O1vi122.39 (16)O6—W1—O6i160.6 (4)
Ti_m1(1)—Si2—O226.0 (2)O6—W1—Ohiii116.0 (4)
Ti_m1(1)—Si2—O5106.1 (6)O6—W1—Ohv51.0 (4)
Ti_m1(1)—Si2—O6ii64.5 (3)O6—W1—W2iii80.3 (2)
Ti_m1(1)—Si2—O7ix133.7 (3)O6i—W1—Ohiii51.0 (4)
Ti_m1(1)—Si2—Oh34.3 (3)O6i—W1—Ohv116.0 (4)
Ti_m1(1)—Si2—Ba71.22 (8)O6i—W1—W2iii80.3 (2)
Ti_m1(1)—Si2—W_c71.22 (8)Ohiii—W1—Ohv111.2 (3)
Ti_m1(1)—Si2—Nb_m1(1)0.0 (5)Ohiii—W1—W2iii55.60 (18)
Ti_m1(1)—Si2—Ti_m298.07 (6)Ohv—W1—W2iii55.60 (18)
Ti_m1(1)—Si2—Mg_m298.07 (6)Na_aiii—W2—Na_ax70.9 (9)
Ti_m1(2)—Si2—Fe_m256.13 (9)Na_aiii—W2—O1iv63.1 (5)
Ti_m1(2)—Si2—Si1ix131.29 (19)Na_aiii—W2—O1xi116.6 (5)
Ti_m1(2)—Si2—Si2vi118.42 (16)Na_aiii—W2—O751.6 (6)
Ti_m1(2)—Si2—O130.8 (2)Na_aiii—W2—O7xv121.4 (7)
Ti_m1(2)—Si2—O1vi90.9 (2)Na_aiii—W2—Oh68.5 (4)
Ti_m1(2)—Si2—O285.2 (4)Na_aiii—W2—Ohxv65.2 (4)
Ti_m1(2)—Si2—O5129.7 (4)Na_aiii—W2—Ba117.7 (3)
Ti_m1(2)—Si2—O6ii34.72 (16)Na_aiii—W2—Baxv114.5 (3)
Ti_m1(2)—Si2—O7ix111.7 (5)Na_aiii—W2—W1iii35.4 (6)
Ti_m1(2)—Si2—Oh35.3 (3)Na_aiii—W2—W2xiv144.6 (6)
Ti_m1(2)—Si2—Ba65.97 (9)Na_aiii—W2—W_c117.7 (3)
Ti_m1(2)—Si2—W_c65.97 (9)Na_aiii—W2—W_cxv114.5 (3)
Ti_m1(2)—Si2—Nb_m1(1)65.93 (5)Na_ax—W2—O1iv116.6 (5)
Ti_m1(2)—Si2—Ti_m256.13 (9)Na_ax—W2—O1xi63.1 (5)
Ti_m1(2)—Si2—Mg_m256.13 (9)Na_ax—W2—O7121.4 (7)
Fe_m2—Si2—Si1ix132.0 (2)Na_ax—W2—O7xv51.6 (6)
Fe_m2—Si2—Si2vi62.28 (10)Na_ax—W2—Oh65.2 (4)
Fe_m2—Si2—O131.1 (2)Na_ax—W2—Ohxv68.5 (4)
Fe_m2—Si2—O1vi35.28 (15)Na_ax—W2—Ba114.5 (3)
Fe_m2—Si2—O2124.0 (2)Na_ax—W2—Baxv117.7 (3)
Fe_m2—Si2—O577.9 (5)Na_ax—W2—W1iii35.4 (6)
Fe_m2—Si2—O6ii89.5 (2)Na_ax—W2—W2xiv144.6 (6)
Fe_m2—Si2—O7ix119.2 (6)Na_ax—W2—W_c114.5 (3)
Fe_m2—Si2—Oh67.2 (2)Na_ax—W2—W_cxv117.7 (3)
Fe_m2—Si2—Ba35.93 (10)O1iv—W2—O1xi179.8 (4)
Fe_m2—Si2—W_c35.93 (10)O1iv—W2—O748.4 (2)
Fe_m2—Si2—Nb_m1(1)98.07 (6)O1iv—W2—O7xv131.6 (2)
Fe_m2—Si2—Ti_m20.0 (5)O1iv—W2—Oh125.8 (4)
Fe_m2—Si2—Mg_m20.0 (5)O1iv—W2—Ohxv54.0 (3)
Si1ix—Si2—Si2vi90.32 (8)O1iv—W2—Ba124.3 (3)
Si1ix—Si2—O1125.2 (5)O1iv—W2—Baxv55.8 (2)
Si1ix—Si2—O1vi106.09 (15)O1iv—W2—W1iii89.9 (2)
Si1ix—Si2—O2103.7 (3)O1iv—W2—W2xiv90.1 (2)
Si1ix—Si2—O593.5 (3)O1iv—W2—W_c124.3 (3)
Si1ix—Si2—O6ii103.16 (17)O1iv—W2—W_cxv55.8 (2)
Si1ix—Si2—O7ix20.6 (5)O1xi—W2—O7131.6 (2)
Si1ix—Si2—Oh152.27 (13)O1xi—W2—O7xv48.4 (2)
Si1ix—Si2—Ba155.25 (8)O1xi—W2—Oh54.0 (3)
Si1ix—Si2—W_c155.25 (8)O1xi—W2—Ohxv125.8 (4)
Si1ix—Si2—Nb_m1(1)129.30 (16)O1xi—W2—Ba55.8 (2)
Si1ix—Si2—Ti_m2132.0 (2)O1xi—W2—Baxv124.3 (3)
Si1ix—Si2—Mg_m2132.0 (2)O1xi—W2—W1iii89.9 (2)
Si2vi—Si2—O190.5 (2)O1xi—W2—W2xiv90.1 (2)
Si2vi—Si2—O1vi28.2 (2)O1xi—W2—W_c55.8 (2)
Si2vi—Si2—O2133.0 (5)O1xi—W2—W_cxv124.3 (3)
Si2vi—Si2—O525.4 (7)O7—W2—O7xv172.9 (4)
Si2vi—Si2—O6ii150.0 (3)O7—W2—Oh82.8 (3)
Si2vi—Si2—O7ix97.0 (2)O7—W2—Ohxv93.8 (3)
Si2vi—Si2—Oh117.39 (12)O7—W2—Ba86.60 (18)
Si2vi—Si2—Ba64.94 (6)O7—W2—Baxv97.3 (2)
Si2vi—Si2—W_c64.94 (6)O7—W2—W1iii86.4 (2)
Si2vi—Si2—Nb_m1(1)125.70 (16)O7—W2—W2xiv93.6 (2)
Si2vi—Si2—Ti_m262.28 (10)O7—W2—W_c86.60 (18)
Si2vi—Si2—Mg_m262.28 (10)O7—W2—W_cxv97.3 (2)
O1—Si2—O1vi62.3 (3)O7xv—W2—Oh93.8 (3)
O1—Si2—O2114.9 (5)O7xv—W2—Ohxv82.8 (3)
O1—Si2—O5108.9 (6)O7xv—W2—Ba97.3 (2)
O1—Si2—O6ii59.8 (3)O7xv—W2—Baxv86.60 (18)
O1—Si2—O7ix105.5 (8)O7xv—W2—W1iii86.4 (2)
O1—Si2—Oh58.1 (5)O7xv—W2—W2xiv93.6 (2)
O1—Si2—Ba58.0 (4)O7xv—W2—W_c97.3 (2)
O1—Si2—W_c58.0 (4)O7xv—W2—W_cxv86.60 (18)
O1—Si2—Nb_m1(1)92.3 (4)Oh—W2—Ohxv122.3 (4)
O1—Si2—Ti_m231.1 (2)Oh—W2—Ba61.53 (10)
O1—Si2—Mg_m231.1 (2)Oh—W2—Baxv176.2 (4)
O1vi—Si2—O2143.4 (4)Oh—W2—W1iii61.16 (19)
O1vi—Si2—O549.7 (7)Oh—W2—W2xiv118.84 (19)
O1vi—Si2—O6ii122.0 (4)Oh—W2—W_c61.53 (10)
O1vi—Si2—O7ix103.6 (4)Oh—W2—W_cxv176.2 (4)
O1vi—Si2—Oh99.09 (19)Ohxv—W2—Ba176.2 (4)
O1vi—Si2—Ba51.27 (14)Ohxv—W2—Baxv61.53 (10)
O1vi—Si2—W_c51.27 (14)Ohxv—W2—W1iii61.16 (19)
O1vi—Si2—Nb_m1(1)122.39 (16)Ohxv—W2—W2xiv118.84 (19)
O1vi—Si2—Ti_m235.28 (15)Ohxv—W2—W_c176.2 (4)
O1vi—Si2—Mg_m235.28 (15)Ohxv—W2—W_cxv61.53 (10)
O2—Si2—O5107.9 (9)Ba—W2—Baxv114.6 (4)
O2—Si2—O6ii70.1 (5)Ba—W2—W1iii122.69 (18)
O2—Si2—O7ix111.7 (5)Ba—W2—W2xiv57.31 (18)
O2—Si2—Oh58.9 (4)Ba—W2—W_c0.0 (5)
O2—Si2—Ba94.7 (2)Ba—W2—W_cxv114.6 (4)
O2—Si2—W_c94.7 (2)Baxv—W2—W1iii122.69 (18)
O2—Si2—Nb_m1(1)26.0 (2)Baxv—W2—W2xiv57.31 (18)
O2—Si2—Ti_m2124.0 (2)Baxv—W2—W_c114.6 (4)
O2—Si2—Mg_m2124.0 (2)Baxv—W2—W_cxv0.0 (5)
O5—Si2—O6ii163.2 (3)W1iii—W2—W2xiv180.0 (5)
O5—Si2—O7ix107.7 (4)W1iii—W2—W_c122.69 (18)
O5—Si2—Oh111.8 (4)W1iii—W2—W_cxv122.69 (18)
O5—Si2—Ba64.7 (3)W2xiv—W2—W_c57.31 (18)
O5—Si2—W_c64.7 (3)W2xiv—W2—W_cxv57.31 (18)
O5—Si2—Nb_m1(1)106.1 (6)W_c—W2—W_cxv114.6 (4)
O5—Si2—Ti_m277.9 (5)Fe_m2—W_c—Si263.84 (12)
O5—Si2—Mg_m277.9 (5)Fe_m2—W_c—Si2vi63.84 (12)
O6ii—Si2—O7ix88.0 (4)Fe_m2—W_c—O142.0 (3)
O6ii—Si2—Oh52.3 (2)Fe_m2—W_c—O1xi45.6 (2)
O6ii—Si2—Ba98.61 (14)Fe_m2—W_c—O1xii45.6 (2)
O6ii—Si2—W_c98.61 (14)Fe_m2—W_c—O1vi42.0 (3)
O6ii—Si2—Nb_m1(1)64.5 (3)Fe_m2—W_c—O3127.8 (2)
O6ii—Si2—Ti_m289.5 (2)Fe_m2—W_c—O3vi127.8 (2)
O6ii—Si2—Mg_m289.5 (2)Fe_m2—W_c—O573.6 (4)
O7ix—Si2—Oh140.3 (4)Fe_m2—W_c—Oh86.8 (3)
O7ix—Si2—Ba153.4 (5)Fe_m2—W_c—Ohvi86.8 (3)
O7ix—Si2—W_c153.4 (5)Fe_m2—W_c—Ba0
O7ix—Si2—Nb_m1(1)133.7 (3)Fe_m2—W_c—W2114.03 (18)
O7ix—Si2—Ti_m2119.2 (6)Fe_m2—W_c—W2xiv114.03 (18)
O7ix—Si2—Mg_m2119.2 (6)Fe_m2—W_c—Ti_m20.0 (5)
Oh—Si2—Ba52.45 (10)Fe_m2—W_c—Mg_m20.0 (5)
Oh—Si2—W_c52.45 (10)Si2—W_c—Si2vi50.12 (6)
Oh—Si2—Nb_m1(1)34.3 (3)Si2—W_c—O127.0 (3)
Oh—Si2—Ti_m267.2 (2)Si2—W_c—O1xi80.68 (17)
Oh—Si2—Mg_m267.2 (2)Si2—W_c—O1xii107.0 (2)
Ba—Si2—W_c0.0 (5)Si2—W_c—O1vi62.28 (14)
Ba—Si2—Nb_m1(1)71.22 (8)Si2—W_c—O366.0 (2)
Ba—Si2—Ti_m235.93 (10)Si2—W_c—O3vi94.09 (17)
Ba—Si2—Mg_m235.93 (10)Si2—W_c—O527.93 (18)
W_c—Si2—Nb_m1(1)71.22 (8)Si2—W_c—Oh58.49 (11)
W_c—Si2—Ti_m235.93 (10)Si2—W_c—Ohvi108.61 (12)
W_c—Si2—Mg_m235.93 (10)Si2—W_c—Ba0
Nb_m1(1)—Si2—Ti_m298.07 (6)Si2—W_c—W2122.25 (18)
Nb_m1(1)—Si2—Mg_m298.07 (6)Si2—W_c—W2xiv172.37 (18)
Ti_m2—Si2—Mg_m20.0 (5)Si2—W_c—Ti_m263.84 (12)
Na_aii—O1—Ti_m1(2)83.6 (4)Si2—W_c—Mg_m263.84 (12)
Na_aii—O1—Fe_m2139.7 (9)Si2vi—W_c—O162.28 (14)
Na_aii—O1—Si284.5 (5)Si2vi—W_c—O1xi107.0 (2)
Na_aii—O1—Si2vi117.7 (3)Si2vi—W_c—O1xii80.68 (17)
Na_aii—O1—O1xi119.6 (6)Si2vi—W_c—O1vi27.0 (3)
Na_aii—O1—O1vi125.6 (4)Si2vi—W_c—O394.09 (17)
Na_aii—O1—O288.1 (5)Si2vi—W_c—O3vi66.0 (2)
Na_aii—O1—O5113.4 (4)Si2vi—W_c—O527.93 (18)
Na_aii—O1—O6ii50.2 (3)Si2vi—W_c—Oh108.61 (12)
Na_aii—O1—O7ix52.4 (5)Si2vi—W_c—Ohvi58.49 (11)
Na_aii—O1—Oh111.8 (3)Si2vi—W_c—Ba0
Na_aii—O1—Ohxi60.3 (5)Si2vi—W_c—W2172.37 (18)
Na_aii—O1—Ba174.5 (4)Si2vi—W_c—W2xiv122.25 (18)
Na_aii—O1—Baxi91.7 (6)Si2vi—W_c—Ti_m263.84 (12)
Na_aii—O1—W2ix39.7 (4)Si2vi—W_c—Mg_m263.84 (12)
Na_aii—O1—W_c174.5 (4)O1—W_c—O1xi54.6 (3)
Na_aii—O1—W_cxi91.7 (6)O1—W_c—O1xii87.6 (3)
Na_aii—O1—Ti_m2139.7 (9)O1—W_c—O1vi60.31 (19)
Na_aii—O1—Mg_m2139.7 (9)O1—W_c—O385.8 (3)
Ti_m1(2)—O1—Fe_m297.2 (3)O1—W_c—O3vi119.6 (3)
Ti_m1(2)—O1—Si2125.1 (6)O1—W_c—O550.6 (4)
Ti_m1(2)—O1—Si2vi158.7 (4)O1—W_c—Oh54.3 (2)
Ti_m1(2)—O1—O1xi48.8 (2)O1—W_c—Ohvi114.5 (2)
Ti_m1(2)—O1—O1vi138.8 (4)O1—W_c—Ba0
Ti_m1(2)—O1—O293.7 (4)O1—W_c—W2110.9 (2)
Ti_m1(2)—O1—O5145.5 (8)O1—W_c—W2xiv154.1 (4)
Ti_m1(2)—O1—O6ii43.6 (2)O1—W_c—Ti_m242.0 (3)
Ti_m1(2)—O1—O7ix126.7 (3)O1—W_c—Mg_m242.0 (3)
Ti_m1(2)—O1—Oh45.6 (3)O1xi—W_c—O1xii64.8 (3)
Ti_m1(2)—O1—Ohxi43.6 (3)O1xi—W_c—O1vi87.6 (3)
Ti_m1(2)—O1—Ba92.3 (2)O1xi—W_c—O3112.9 (3)
Ti_m1(2)—O1—Baxi97.9 (5)O1xi—W_c—O3vi173.0 (2)
Ti_m1(2)—O1—W2ix102.2 (5)O1xi—W_c—O5104.8 (4)
Ti_m1(2)—O1—W_c92.3 (2)O1xi—W_c—Oh58.4 (4)
Ti_m1(2)—O1—W_cxi97.9 (5)O1xi—W_c—Ohvi122.7 (4)
Ti_m1(2)—O1—Ti_m297.2 (3)O1xi—W_c—Ba0
Ti_m1(2)—O1—Mg_m297.2 (3)O1xi—W_c—W269.38 (19)
Fe_m2—O1—Si2124.5 (6)O1xi—W_c—W2xiv103.1 (2)
Fe_m2—O1—Si2vi67.09 (19)O1xi—W_c—Ti_m245.6 (2)
Fe_m2—O1—O1xi48.5 (2)O1xi—W_c—Mg_m245.6 (2)
Fe_m2—O1—O1vi41.53 (18)O1xii—W_c—O1vi54.6 (3)
Fe_m2—O1—O2131.7 (7)O1xii—W_c—O3173.0 (2)
Fe_m2—O1—O588.5 (4)O1xii—W_c—O3vi112.9 (3)
Fe_m2—O1—O6ii140.6 (4)O1xii—W_c—O5104.8 (4)
Fe_m2—O1—O7ix135.3 (3)O1xii—W_c—Oh122.7 (4)
Fe_m2—O1—Oh95.9 (3)O1xii—W_c—Ohvi58.4 (4)
Fe_m2—O1—Ohxi92.9 (5)O1xii—W_c—Ba0
Fe_m2—O1—Ba44.3 (2)O1xii—W_c—W2103.1 (2)
Fe_m2—O1—Baxi48.1 (3)O1xii—W_c—W2xiv69.38 (19)
Fe_m2—O1—W2ix102.1 (5)O1xii—W_c—Ti_m245.6 (2)
Fe_m2—O1—W_c44.3 (2)O1xii—W_c—Mg_m245.6 (2)
Fe_m2—O1—W_cxi48.1 (3)O1vi—W_c—O3119.6 (3)
Fe_m2—O1—Ti_m20.0 (5)O1vi—W_c—O3vi85.8 (3)
Fe_m2—O1—Mg_m20.0 (5)O1vi—W_c—O550.6 (4)
Si2—O1—Si2vi61.3 (3)O1vi—W_c—Oh114.5 (2)
Si2—O1—O1xi149.7 (8)O1vi—W_c—Ohvi54.3 (2)
Si2—O1—O1vi89.5 (4)O1vi—W_c—Ba0
Si2—O1—O232.5 (3)O1vi—W_c—W2154.1 (4)
Si2—O1—O536.1 (3)O1vi—W_c—W2xiv110.9 (2)
Si2—O1—O6ii90.3 (4)O1vi—W_c—Ti_m242.0 (3)
Si2—O1—O7ix37.6 (4)O1vi—W_c—Mg_m242.0 (3)
Si2—O1—Oh91.9 (7)O3—W_c—O3vi68.6 (3)
Si2—O1—Ohxi142.2 (4)O3—W_c—O569.0 (3)
Si2—O1—Ba95.0 (6)O3—W_c—Oh54.5 (4)
Si2—O1—Baxi135.8 (3)O3—W_c—Ohvi122.7 (4)
Si2—O1—W2ix101.7 (3)O3—W_c—Ba0
Si2—O1—W_c95.0 (6)O3—W_c—W281.57 (18)
Si2—O1—W_cxi135.8 (3)O3—W_c—W2xiv117.5 (2)
Si2—O1—Ti_m2124.5 (6)O3—W_c—Ti_m2127.8 (2)
Si2—O1—Mg_m2124.5 (6)O3—W_c—Mg_m2127.8 (2)
Si2vi—O1—O1xi114.1 (2)O3vi—W_c—O569.0 (3)
Si2vi—O1—O1vi28.2 (3)O3vi—W_c—Oh122.7 (4)
Si2vi—O1—O287.2 (4)O3vi—W_c—Ohvi54.5 (4)
Si2vi—O1—O528.4 (3)O3vi—W_c—Ba0
Si2vi—O1—O6ii151.3 (5)O3vi—W_c—W2117.5 (2)
Si2vi—O1—O7ix71.9 (3)O3vi—W_c—W2xiv81.57 (18)
Si2vi—O1—Oh119.1 (5)O3vi—W_c—Ti_m2127.8 (2)
Si2vi—O1—Ohxi145.8 (5)O3vi—W_c—Mg_m2127.8 (2)
Si2vi—O1—Ba66.45 (19)O5—W_c—Oh83.72 (13)
Si2vi—O1—Baxi82.48 (19)O5—W_c—Ohvi83.72 (13)
Si2vi—O1—W2ix95.4 (3)O5—W_c—Ba0
Si2vi—O1—W_c66.45 (19)O5—W_c—W2145.2 (2)
Si2vi—O1—W_cxi82.48 (19)O5—W_c—W2xiv145.2 (2)
Si2vi—O1—Ti_m267.09 (19)O5—W_c—Ti_m273.6 (4)
Si2vi—O1—Mg_m267.09 (19)O5—W_c—Mg_m273.6 (4)
O1xi—O1—O1vi90.0 (3)Oh—W_c—Ohvi167.10 (16)
O1xi—O1—O2123.6 (5)Oh—W_c—Ba0
O1xi—O1—O5127.0 (4)Oh—W_c—W263.8 (2)
O1xi—O1—O6ii92.3 (3)Oh—W_c—W2xiv129.1 (2)
O1xi—O1—O7ix171.8 (8)Oh—W_c—Ti_m286.8 (3)
O1xi—O1—Oh63.3 (4)Oh—W_c—Mg_m286.8 (3)
O1xi—O1—Ohxi59.5 (4)Ohvi—W_c—Ba0
O1xi—O1—Ba59.2 (3)Ohvi—W_c—W2129.1 (2)
O1xi—O1—Baxi66.3 (4)Ohvi—W_c—W2xiv63.8 (2)
O1xi—O1—W2ix108.6 (6)Ohvi—W_c—Ti_m286.8 (3)
O1xi—O1—W_c59.2 (3)Ohvi—W_c—Mg_m286.8 (3)
O1xi—O1—W_cxi66.3 (4)Ba—W_c—W20
O1xi—O1—Ti_m248.5 (2)Ba—W_c—W2xiv0
O1xi—O1—Mg_m248.5 (2)Ba—W_c—Ti_m20
O1vi—O1—O2113.5 (6)Ba—W_c—Mg_m20
O1vi—O1—O555.4 (4)W2—W_c—W2xiv65.4 (3)
O1vi—O1—O6ii175.7 (5)W2—W_c—Ti_m2114.03 (18)
O1vi—O1—O7ix94.1 (3)W2—W_c—Mg_m2114.03 (18)
O1vi—O1—Oh122.4 (4)W2xiv—W_c—Ti_m2114.03 (18)
O1vi—O1—Ohxi121.2 (6)W2xiv—W_c—Mg_m2114.03 (18)
O1vi—O1—Ba59.8 (2)Ti_m2—W_c—Mg_m20.0 (5)
O1vi—O1—Baxi57.6 (4)Ti_m1(1)—Nb_m1(1)—Si10
O1vi—O1—W2ix89.9 (4)Ti_m1(1)—Nb_m1(1)—Si1ii0
O1vi—O1—W_c59.8 (2)Ti_m1(1)—Nb_m1(1)—Si20
O1vi—O1—W_cxi57.6 (4)Ti_m1(1)—Nb_m1(1)—Si2ii0
O1vi—O1—Ti_m241.53 (18)Ti_m1(1)—Nb_m1(1)—O20
O1vi—O1—Mg_m241.53 (18)Ti_m1(1)—Nb_m1(1)—O2ii0
O2—O1—O558.9 (5)Ti_m1(1)—Nb_m1(1)—O30
O2—O1—O6ii68.1 (4)Ti_m1(1)—Nb_m1(1)—O3ii0
O2—O1—O7ix60.9 (4)Ti_m1(1)—Nb_m1(1)—O60
O2—O1—Oh60.8 (4)Ti_m1(1)—Nb_m1(1)—O6ii0
O2—O1—Ohxi125.3 (3)Ti_m1(1)—Nb_m1(1)—Oh0
O2—O1—Ba88.6 (5)Ti_m1(1)—Nb_m1(1)—Ohii0
O2—O1—Baxi168.3 (3)Si1—Nb_m1(1)—Si1ii180.0 (5)
O2—O1—W2ix121.2 (3)Si1—Nb_m1(1)—Si2106.35 (9)
O2—O1—W_c88.6 (5)Si1—Nb_m1(1)—Si2ii73.65 (9)
O2—O1—W_cxi168.3 (3)Si1—Nb_m1(1)—O2111.3 (3)
O2—O1—Ti_m2131.7 (7)Si1—Nb_m1(1)—O2ii68.7 (3)
O2—O1—Mg_m2131.7 (7)Si1—Nb_m1(1)—O326.1 (4)
O5—O1—O6ii125.3 (6)Si1—Nb_m1(1)—O3ii153.9 (4)
O5—O1—O7ix61.0 (4)Si1—Nb_m1(1)—O627.07 (18)
O5—O1—Oh100.0 (7)Si1—Nb_m1(1)—O6ii152.93 (18)
O5—O1—Ohxi170.5 (5)Si1—Nb_m1(1)—Oh101.0 (3)
O5—O1—Ba68.4 (3)Si1—Nb_m1(1)—Ohii79.0 (3)
O5—O1—Baxi110.8 (4)Si1ii—Nb_m1(1)—Si273.65 (9)
O5—O1—W2ix109.8 (4)Si1ii—Nb_m1(1)—Si2ii106.35 (9)
O5—O1—W_c68.4 (3)Si1ii—Nb_m1(1)—O268.7 (3)
O5—O1—W_cxi110.8 (4)Si1ii—Nb_m1(1)—O2ii111.3 (3)
O5—O1—Ti_m288.5 (4)Si1ii—Nb_m1(1)—O3153.9 (4)
O5—O1—Mg_m288.5 (4)Si1ii—Nb_m1(1)—O3ii26.1 (4)
O6ii—O1—O7ix83.1 (3)Si1ii—Nb_m1(1)—O6152.93 (18)
O6ii—O1—Oh61.9 (3)Si1ii—Nb_m1(1)—O6ii27.07 (18)
O6ii—O1—Ohxi57.4 (4)Si1ii—Nb_m1(1)—Oh79.0 (3)
O6ii—O1—Ba124.4 (4)Si1ii—Nb_m1(1)—Ohii101.0 (3)
O6ii—O1—Baxi120.2 (6)Si2—Nb_m1(1)—Si2ii180.0 (5)
O6ii—O1—W2ix86.0 (4)Si2—Nb_m1(1)—O221.0 (3)
O6ii—O1—W_c124.4 (4)Si2—Nb_m1(1)—O2ii159.0 (3)
O6ii—O1—W_cxi120.2 (6)Si2—Nb_m1(1)—O380.8 (3)
O6ii—O1—Ti_m2140.6 (4)Si2—Nb_m1(1)—O3ii99.2 (3)
O6ii—O1—Mg_m2140.6 (4)Si2—Nb_m1(1)—O6122.78 (14)
O7ix—O1—Oh119.6 (6)Si2—Nb_m1(1)—O6ii57.22 (14)
O7ix—O1—Ohxi112.4 (5)Si2—Nb_m1(1)—Oh71.3 (2)
O7ix—O1—Ba129.0 (6)Si2—Nb_m1(1)—Ohii108.7 (2)
O7ix—O1—Baxi110.2 (5)Si2ii—Nb_m1(1)—O2159.0 (3)
O7ix—O1—W2ix64.4 (4)Si2ii—Nb_m1(1)—O2ii21.0 (3)
O7ix—O1—W_c129.0 (6)Si2ii—Nb_m1(1)—O399.2 (3)
O7ix—O1—W_cxi110.2 (5)Si2ii—Nb_m1(1)—O3ii80.8 (3)
O7ix—O1—Ti_m2135.3 (3)Si2ii—Nb_m1(1)—O657.22 (14)
O7ix—O1—Mg_m2135.3 (3)Si2ii—Nb_m1(1)—O6ii122.78 (14)
Oh—O1—Ohxi89.2 (4)Si2ii—Nb_m1(1)—Oh108.7 (2)
Oh—O1—Ba62.7 (3)Si2ii—Nb_m1(1)—Ohii71.3 (2)
Oh—O1—Baxi129.5 (4)O2—Nb_m1(1)—O2ii180.0 (5)
Oh—O1—W2ix145.2 (4)O2—Nb_m1(1)—O389.2 (3)
Oh—O1—W_c62.7 (3)O2—Nb_m1(1)—O3ii90.8 (3)
Oh—O1—W_cxi129.5 (4)O2—Nb_m1(1)—O6118.0 (4)
Oh—O1—Ti_m295.9 (3)O2—Nb_m1(1)—O6ii62.0 (4)
Oh—O1—Mg_m295.9 (3)O2—Nb_m1(1)—Oh90.7 (5)
Ohxi—O1—Ba118.6 (3)O2—Nb_m1(1)—Ohii89.3 (5)
Ohxi—O1—Baxi64.0 (4)O2ii—Nb_m1(1)—O390.8 (3)
Ohxi—O1—W2ix60.7 (4)O2ii—Nb_m1(1)—O3ii89.2 (3)
Ohxi—O1—W_c118.6 (3)O2ii—Nb_m1(1)—O662.0 (4)
Ohxi—O1—W_cxi64.0 (4)O2ii—Nb_m1(1)—O6ii118.0 (4)
Ohxi—O1—Ti_m292.9 (5)O2ii—Nb_m1(1)—Oh89.3 (5)
Ohxi—O1—Mg_m292.9 (5)O2ii—Nb_m1(1)—Ohii90.7 (5)
Ba—O1—Baxi92.4 (2)O3—Nb_m1(1)—O3ii180.0 (5)
Ba—O1—W2ix145.3 (4)O3—Nb_m1(1)—O650.3 (5)
Ba—O1—W_c0.0 (5)O3—Nb_m1(1)—O6ii129.7 (5)
Ba—O1—W_cxi92.4 (2)O3—Nb_m1(1)—Oh88.0 (5)
Ba—O1—Ti_m244.3 (2)O3—Nb_m1(1)—Ohii92.0 (5)
Ba—O1—Mg_m244.3 (2)O3ii—Nb_m1(1)—O6129.7 (5)
Baxi—O1—W2ix54.8 (3)O3ii—Nb_m1(1)—O6ii50.3 (5)
Baxi—O1—W_c92.4 (2)O3ii—Nb_m1(1)—Oh92.0 (5)
Baxi—O1—W_cxi0.0 (5)O3ii—Nb_m1(1)—Ohii88.0 (5)
Baxi—O1—Ti_m248.1 (3)O6—Nb_m1(1)—O6ii180.0 (5)
Baxi—O1—Mg_m248.1 (3)O6—Nb_m1(1)—Oh125.0 (3)
W2ix—O1—W_c145.3 (4)O6—Nb_m1(1)—Ohii55.0 (3)
W2ix—O1—W_cxi54.8 (3)O6ii—Nb_m1(1)—Oh55.0 (3)
W2ix—O1—Ti_m2102.1 (5)O6ii—Nb_m1(1)—Ohii125.0 (3)
W2ix—O1—Mg_m2102.1 (5)Oh—Nb_m1(1)—Ohii180.0 (5)
W_c—O1—W_cxi92.4 (2)Ti_m1(2)—Ti_m2—Ti_m1(2)xii180.0 (5)
W_c—O1—Ti_m244.3 (2)Ti_m1(2)—Ti_m2—Fe_m20
W_c—O1—Mg_m244.3 (2)Ti_m1(2)—Ti_m2—Si262.28 (5)
W_cxi—O1—Ti_m248.1 (3)Ti_m1(2)—Ti_m2—Si2xi62.28 (5)
W_cxi—O1—Mg_m248.1 (3)Ti_m1(2)—Ti_m2—Si2xii117.72 (5)
Ti_m2—O1—Mg_m20.0 (5)Ti_m1(2)—Ti_m2—Si2vi117.72 (5)
Na_aix—O2—K_b94.1 (6)Ti_m1(2)—Ti_m2—O141.5 (2)
Na_aix—O2—Ti_m1(1)111.6 (6)Ti_m1(2)—Ti_m2—O1xi41.5 (2)
Na_aix—O2—Ti_m1(2)136.8 (6)Ti_m1(2)—Ti_m2—O1xii138.5 (2)
Na_aix—O2—Si1ii80.7 (4)Ti_m1(2)—Ti_m2—O1vi138.5 (2)
Na_aix—O2—Si2115.1 (5)Ti_m1(2)—Ti_m2—O590
Na_aix—O2—O1137.5 (7)Ti_m1(2)—Ti_m2—O5xi90
Na_aix—O2—O3126.9 (9)Ti_m1(2)—Ti_m2—Ba90
Na_aix—O2—O3ii85.5 (3)Ti_m1(2)—Ti_m2—Baxi90
Na_aix—O2—O5114.0 (4)Ti_m1(2)—Ti_m2—W_c90
Na_aix—O2—O6ii103.4 (6)Ti_m1(2)—Ti_m2—W_cxi90
Na_aix—O2—O7ix82.5 (5)Ti_m1(2)—Ti_m2—Mg_m20
Na_aix—O2—O7ii52.2 (5)Ti_m1(2)xii—Ti_m2—Fe_m20
Na_aix—O2—Oh146.0 (3)Ti_m1(2)xii—Ti_m2—Si2117.72 (5)
Na_aix—O2—Ohii71.9 (6)Ti_m1(2)xii—Ti_m2—Si2xi117.72 (5)
Na_aix—O2—W1ix42.8 (5)Ti_m1(2)xii—Ti_m2—Si2xii62.28 (5)
Na_aix—O2—Nb_m1(1)111.6 (6)Ti_m1(2)xii—Ti_m2—Si2vi62.28 (5)
K_b—O2—Ti_m1(1)94.3 (4)Ti_m1(2)xii—Ti_m2—O1138.5 (2)
K_b—O2—Ti_m1(2)128.7 (2)Ti_m1(2)xii—Ti_m2—O1xi138.5 (2)
K_b—O2—Si1ii164.4 (5)Ti_m1(2)xii—Ti_m2—O1xii41.5 (2)
K_b—O2—Si287.6 (3)Ti_m1(2)xii—Ti_m2—O1vi41.5 (2)
K_b—O2—O1106.1 (3)Ti_m1(2)xii—Ti_m2—O590
K_b—O2—O353.6 (3)Ti_m1(2)xii—Ti_m2—O5xi90
K_b—O2—O3ii133.7 (5)Ti_m1(2)xii—Ti_m2—Ba90
K_b—O2—O551.1 (5)Ti_m1(2)xii—Ti_m2—Baxi90
K_b—O2—O6ii161.9 (4)Ti_m1(2)xii—Ti_m2—W_c90
K_b—O2—O7ix101.6 (3)Ti_m1(2)xii—Ti_m2—W_cxi90
K_b—O2—O7ii146.2 (4)Ti_m1(2)xii—Ti_m2—Mg_m20
K_b—O2—Oh108.9 (3)Fe_m2—Ti_m2—Si20
K_b—O2—Ohii77.3 (4)Fe_m2—Ti_m2—Si2xi0
K_b—O2—W1ix51.4 (3)Fe_m2—Ti_m2—Si2xii0
K_b—O2—Nb_m1(1)94.3 (4)Fe_m2—Ti_m2—Si2vi0
Ti_m1(1)—O2—Ti_m1(2)75.3 (3)Fe_m2—Ti_m2—O10
Ti_m1(1)—O2—Si1ii74.2 (2)Fe_m2—Ti_m2—O1xi0
Ti_m1(1)—O2—Si2133.0 (5)Fe_m2—Ti_m2—O1xii0
Ti_m1(1)—O2—O1103.9 (4)Fe_m2—Ti_m2—O1vi0
Ti_m1(1)—O2—O345.6 (2)Fe_m2—Ti_m2—O50
Ti_m1(1)—O2—O3ii44.9 (2)Fe_m2—Ti_m2—O5xi0
Ti_m1(1)—O2—O5123.2 (3)Fe_m2—Ti_m2—Ba0
Ti_m1(1)—O2—O6ii83.9 (3)Fe_m2—Ti_m2—Baxi0
Ti_m1(1)—O2—O7ix158.0 (7)Fe_m2—Ti_m2—W_c0
Ti_m1(1)—O2—O7ii98.4 (2)Fe_m2—Ti_m2—W_cxi0
Ti_m1(1)—O2—Oh44.0 (3)Fe_m2—Ti_m2—Mg_m20
Ti_m1(1)—O2—Ohii44.7 (3)Si2—Ti_m2—Si2xi124.57 (8)
Ti_m1(1)—O2—W1ix112.6 (6)Si2—Ti_m2—Si2xii180.0 (5)
Ti_m1(1)—O2—Nb_m1(1)0.0 (5)Si2—Ti_m2—Si2vi55.43 (8)
Ti_m1(2)—O2—Si1ii59.5 (2)Si2—Ti_m2—O124.4 (4)
Ti_m1(2)—O2—Si267.5 (5)Si2—Ti_m2—O1xi102.4 (3)
Ti_m1(2)—O2—O135.5 (2)Si2—Ti_m2—O1xii155.6 (4)
Ti_m1(2)—O2—O389.4 (4)Si2—Ti_m2—O1vi77.6 (3)
Ti_m1(2)—O2—O3ii69.8 (4)Si2—Ti_m2—O529.44 (12)
Ti_m1(2)—O2—O592.8 (5)Si2—Ti_m2—O5xi150.56 (12)
Ti_m1(2)—O2—O6ii33.5 (2)Si2—Ti_m2—Ba80.24 (13)
Ti_m1(2)—O2—O7ix82.9 (5)Si2—Ti_m2—Baxi99.76 (13)
Ti_m1(2)—O2—O7ii84.9 (4)Si2—Ti_m2—W_c80.24 (13)
Ti_m1(2)—O2—Oh34.1 (4)Si2—Ti_m2—W_cxi99.76 (13)
Ti_m1(2)—O2—Ohii118.3 (3)Si2—Ti_m2—Mg_m20
Ti_m1(2)—O2—W1ix172.0 (4)Si2xi—Ti_m2—Si2xii55.43 (8)
Ti_m1(2)—O2—Nb_m1(1)75.3 (3)Si2xi—Ti_m2—Si2vi180.0 (5)
Si1ii—O2—Si2107.9 (7)Si2xi—Ti_m2—O1102.4 (3)
Si1ii—O2—O187.3 (4)Si2xi—Ti_m2—O1xi24.4 (4)
Si1ii—O2—O3118.5 (2)Si2xi—Ti_m2—O1xii77.6 (3)
Si1ii—O2—O3ii31.7 (3)Si2xi—Ti_m2—O1vi155.6 (4)
Si1ii—O2—O5144.4 (8)Si2xi—Ti_m2—O5150.56 (12)
Si1ii—O2—O6ii30.0 (3)Si2xi—Ti_m2—O5xi29.44 (12)
Si1ii—O2—O7ix92.4 (4)Si2xi—Ti_m2—Ba99.76 (13)
Si1ii—O2—O7ii31.60 (18)Si2xi—Ti_m2—Baxi80.24 (13)
Si1ii—O2—Oh70.4 (3)Si2xi—Ti_m2—W_c99.76 (13)
Si1ii—O2—Ohii87.1 (3)Si2xi—Ti_m2—W_cxi80.24 (13)
Si1ii—O2—W1ix122.7 (3)Si2xi—Ti_m2—Mg_m20
Si1ii—O2—Nb_m1(1)74.2 (2)Si2xii—Ti_m2—Si2vi124.57 (8)
Si2—O2—O132.6 (3)Si2xii—Ti_m2—O1155.6 (4)
Si2—O2—O3105.3 (3)Si2xii—Ti_m2—O1xi77.6 (3)
Si2—O2—O3ii134.0 (8)Si2xii—Ti_m2—O1xii24.4 (4)
Si2—O2—O536.6 (5)Si2xii—Ti_m2—O1vi102.4 (3)
Si2—O2—O6ii80.6 (6)Si2xii—Ti_m2—O5150.56 (12)
Si2—O2—O7ix34.5 (3)Si2xii—Ti_m2—O5xi29.44 (12)
Si2—O2—O7ii105.5 (6)Si2xii—Ti_m2—Ba99.76 (13)
Si2—O2—Oh91.2 (5)Si2xii—Ti_m2—Baxi80.24 (13)
Si2—O2—Ohii164.0 (6)Si2xii—Ti_m2—W_c99.76 (13)
Si2—O2—W1ix105.0 (4)Si2xii—Ti_m2—W_cxi80.24 (13)
Si2—O2—Nb_m1(1)133.0 (5)Si2xii—Ti_m2—Mg_m20
O1—O2—O394.6 (4)Si2vi—Ti_m2—O177.6 (3)
O1—O2—O3ii104.8 (5)Si2vi—Ti_m2—O1xi155.6 (4)
O1—O2—O559.5 (5)Si2vi—Ti_m2—O1xii102.4 (3)
O1—O2—O6ii57.3 (4)Si2vi—Ti_m2—O1vi24.4 (4)
O1—O2—O7ix57.3 (4)Si2vi—Ti_m2—O529.44 (12)
O1—O2—O7ii101.0 (6)Si2vi—Ti_m2—O5xi150.56 (12)
O1—O2—Oh60.1 (4)Si2vi—Ti_m2—Ba80.24 (13)
O1—O2—Ohii148.2 (3)Si2vi—Ti_m2—Baxi99.76 (13)
O1—O2—W1ix137.4 (3)Si2vi—Ti_m2—W_c80.24 (13)
O1—O2—Nb_m1(1)103.9 (4)Si2vi—Ti_m2—W_cxi99.76 (13)
O3—O2—O3ii90.5 (3)Si2vi—Ti_m2—Mg_m20
O3—O2—O579.7 (4)O1—Ti_m2—O1xi83.1 (3)
O3—O2—O6ii116.4 (4)O1—Ti_m2—O1xii180.0 (5)
O3—O2—O7ix138.3 (3)O1—Ti_m2—O1vi96.9 (3)
O3—O2—O7ii143.6 (3)O1—Ti_m2—O553.8 (4)
O3—O2—Oh58.6 (4)O1—Ti_m2—O5xi126.2 (4)
O3—O2—Ohii61.3 (4)O1—Ti_m2—Ba93.7 (4)
O3—O2—W1ix95.4 (5)O1—Ti_m2—Baxi86.3 (4)
O3—O2—Nb_m1(1)45.6 (2)O1—Ti_m2—W_c93.7 (4)
O3ii—O2—O5160.3 (5)O1—Ti_m2—W_cxi86.3 (4)
O3ii—O2—O6ii54.0 (4)O1—Ti_m2—Mg_m20
O3ii—O2—O7ix124.1 (5)O1xi—Ti_m2—O1xii96.9 (3)
O3ii—O2—O7ii53.9 (2)O1xi—Ti_m2—O1vi180.0 (5)
O3ii—O2—Oh60.5 (3)O1xi—Ti_m2—O5126.2 (4)
O3ii—O2—Ohii58.6 (4)O1xi—Ti_m2—O5xi53.8 (4)
O3ii—O2—W1ix116.4 (5)O1xi—Ti_m2—Ba86.3 (4)
O3ii—O2—Nb_m1(1)44.9 (2)O1xi—Ti_m2—Baxi93.7 (4)
O5—O2—O6ii115.5 (7)O1xi—Ti_m2—W_c86.3 (4)
O5—O2—O7ix59.9 (4)O1xi—Ti_m2—W_cxi93.7 (4)
O5—O2—O7ii136.3 (5)O1xi—Ti_m2—Mg_m20
O5—O2—Oh99.9 (4)O1xii—Ti_m2—O1vi83.1 (3)
O5—O2—Ohii127.8 (7)O1xii—Ti_m2—O5126.2 (4)
O5—O2—W1ix81.8 (5)O1xii—Ti_m2—O5xi53.8 (4)
O5—O2—Nb_m1(1)123.2 (3)O1xii—Ti_m2—Ba86.3 (4)
O6ii—O2—O7ix76.3 (5)O1xii—Ti_m2—Baxi93.7 (4)
O6ii—O2—O7ii51.4 (3)O1xii—Ti_m2—W_c86.3 (4)
O6ii—O2—Oh58.0 (4)O1xii—Ti_m2—W_cxi93.7 (4)
O6ii—O2—Ohii112.6 (3)O1xii—Ti_m2—Mg_m20
O6ii—O2—W1ix145.4 (3)O1vi—Ti_m2—O553.8 (4)
O6ii—O2—Nb_m1(1)83.9 (3)O1vi—Ti_m2—O5xi126.2 (4)
O7ix—O2—O7ii76.5 (4)O1vi—Ti_m2—Ba93.7 (4)
O7ix—O2—Oh115.4 (7)O1vi—Ti_m2—Baxi86.3 (4)
O7ix—O2—Ohii154.2 (4)O1vi—Ti_m2—W_c93.7 (4)
O7ix—O2—W1ix89.3 (3)O1vi—Ti_m2—W_cxi86.3 (4)
O7ix—O2—Nb_m1(1)158.0 (7)O1vi—Ti_m2—Mg_m20
O7ii—O2—Oh101.9 (4)O5—Ti_m2—O5xi180.0 (5)
O7ii—O2—Ohii90.2 (4)O5—Ti_m2—Ba68.6 (3)
O7ii—O2—W1ix94.9 (4)O5—Ti_m2—Baxi111.4 (3)
O7ii—O2—Nb_m1(1)98.4 (2)O5—Ti_m2—W_c68.6 (3)
Oh—O2—Ohii88.7 (4)O5—Ti_m2—W_cxi111.4 (3)
Oh—O2—W1ix152.7 (6)O5—Ti_m2—Mg_m20
Oh—O2—Nb_m1(1)44.0 (3)O5xi—Ti_m2—Ba111.4 (3)
Ohii—O2—W1ix69.7 (4)O5xi—Ti_m2—Baxi68.6 (3)
Ohii—O2—Nb_m1(1)44.7 (3)O5xi—Ti_m2—W_c111.4 (3)
W1ix—O2—Nb_m1(1)112.6 (6)O5xi—Ti_m2—W_cxi68.6 (3)
Na_aiii—O3—K_b170.4 (3)O5xi—Ti_m2—Mg_m20
Na_aiii—O3—Ti_m1(1)75.5 (3)Ba—Ti_m2—Baxi180.0 (5)
Na_aiii—O3—Si177.0 (4)Ba—Ti_m2—W_c0.0 (5)
Na_aiii—O3—O2113.3 (5)Ba—Ti_m2—W_cxi180.0 (5)
Na_aiii—O3—O2ii42.0 (3)Ba—Ti_m2—Mg_m20
Na_aiii—O3—O3vi116.4 (3)Baxi—Ti_m2—W_c180.0 (5)
Na_aiii—O3—O4104.0 (4)Baxi—Ti_m2—W_cxi0.0 (5)
Na_aiii—O3—O5132.7 (7)Baxi—Ti_m2—Mg_m20
Na_aiii—O3—O686.5 (5)W_c—Ti_m2—W_cxi180.0 (5)
Na_aiii—O3—O743.9 (4)W_c—Ti_m2—Mg_m20
Na_aiii—O3—Oh55.8 (4)W_cxi—Ti_m2—Mg_m20
Na_aiii—O3—Ohii100.9 (3)Ti_m1(2)—Mg_m2—Ti_m1(2)xii180.0 (5)
Na_aiii—O3—Ba80.5 (4)Ti_m1(2)—Mg_m2—Fe_m20
Na_aiii—O3—W_c80.5 (4)Ti_m1(2)—Mg_m2—Si262.28 (5)
Na_aiii—O3—Nb_m1(1)75.5 (3)Ti_m1(2)—Mg_m2—Si2xi62.28 (5)
K_b—O3—Ti_m1(1)114.1 (2)Ti_m1(2)—Mg_m2—Si2xii117.72 (5)
K_b—O3—Si196.9 (6)Ti_m1(2)—Mg_m2—Si2vi117.72 (5)
K_b—O3—O275.5 (3)Ti_m1(2)—Mg_m2—O141.5 (2)
K_b—O3—O2ii145.4 (4)Ti_m1(2)—Mg_m2—O1xi41.5 (2)
K_b—O3—O3vi55.14 (19)Ti_m1(2)—Mg_m2—O1xii138.5 (2)
K_b—O3—O467.6 (3)Ti_m1(2)—Mg_m2—O1vi138.5 (2)
K_b—O3—O549.9 (4)Ti_m1(2)—Mg_m2—O590
K_b—O3—O692.2 (5)Ti_m1(2)—Mg_m2—O5xi90
K_b—O3—O7127.9 (6)Ti_m1(2)—Mg_m2—Ba90
K_b—O3—Oh130.8 (5)Ti_m1(2)—Mg_m2—Baxi90
K_b—O3—Ohii86.9 (3)Ti_m1(2)—Mg_m2—W_c90
K_b—O3—Ba96.2 (3)Ti_m1(2)—Mg_m2—W_cxi90
K_b—O3—W_c96.2 (3)Ti_m1(2)—Mg_m2—Ti_m20
K_b—O3—Nb_m1(1)114.1 (2)Ti_m1(2)xii—Mg_m2—Fe_m20
Ti_m1(1)—O3—Si1121.2 (5)Ti_m1(2)xii—Mg_m2—Si2117.72 (5)
Ti_m1(1)—O3—O245.1 (2)Ti_m1(2)xii—Mg_m2—Si2xi117.72 (5)
Ti_m1(1)—O3—O2ii44.4 (2)Ti_m1(2)xii—Mg_m2—Si2xii62.28 (5)
Ti_m1(1)—O3—O3vi153.2 (6)Ti_m1(2)xii—Mg_m2—Si2vi62.28 (5)
Ti_m1(1)—O3—O4152.2 (8)Ti_m1(2)xii—Mg_m2—O1138.5 (2)
Ti_m1(1)—O3—O592.3 (4)Ti_m1(2)xii—Mg_m2—O1xi138.5 (2)
Ti_m1(1)—O3—O695.1 (4)Ti_m1(2)xii—Mg_m2—O1xii41.5 (2)
Ti_m1(1)—O3—O7111.5 (3)Ti_m1(2)xii—Mg_m2—O1vi41.5 (2)
Ti_m1(1)—O3—Oh45.1 (3)Ti_m1(2)xii—Mg_m2—O590
Ti_m1(1)—O3—Ohii43.1 (3)Ti_m1(2)xii—Mg_m2—O5xi90
Ti_m1(1)—O3—Ba107.0 (7)Ti_m1(2)xii—Mg_m2—Ba90
Ti_m1(1)—O3—W_c107.0 (7)Ti_m1(2)xii—Mg_m2—Baxi90
Ti_m1(1)—O3—Nb_m1(1)0.0 (5)Ti_m1(2)xii—Mg_m2—W_c90
Si1—O3—O2152.2 (7)Ti_m1(2)xii—Mg_m2—W_cxi90
Si1—O3—O2ii81.9 (4)Ti_m1(2)xii—Mg_m2—Ti_m20
Si1—O3—O3vi85.4 (4)Fe_m2—Mg_m2—Si20
Si1—O3—O435.8 (3)Fe_m2—Mg_m2—Si2xi0
Si1—O3—O5142.2 (5)Fe_m2—Mg_m2—Si2xii0
Si1—O3—O632.4 (3)Fe_m2—Mg_m2—Si2vi0
Si1—O3—O736.0 (4)Fe_m2—Mg_m2—O10
Si1—O3—Oh132.3 (4)Fe_m2—Mg_m2—O1xi0
Si1—O3—Ohii94.7 (6)Fe_m2—Mg_m2—O1xii0
Si1—O3—Ba118.2 (3)Fe_m2—Mg_m2—O1vi0
Si1—O3—W_c118.2 (3)Fe_m2—Mg_m2—O50
Si1—O3—Nb_m1(1)121.2 (5)Fe_m2—Mg_m2—O5xi0
O2—O3—O2ii89.5 (3)Fe_m2—Mg_m2—Ba0
O2—O3—O3vi110.1 (3)Fe_m2—Mg_m2—Baxi0
O2—O3—O4142.5 (4)Fe_m2—Mg_m2—W_c0
O2—O3—O548.5 (2)Fe_m2—Mg_m2—W_cxi0
O2—O3—O6120.1 (4)Fe_m2—Mg_m2—Ti_m20
O2—O3—O7155.8 (4)Si2—Mg_m2—Si2xi124.57 (8)
O2—O3—Oh60.5 (4)Si2—Mg_m2—Si2xii180.0 (5)
O2—O3—Ohii58.6 (4)Si2—Mg_m2—Si2vi55.43 (8)
O2—O3—Ba89.4 (5)Si2—Mg_m2—O124.4 (4)
O2—O3—W_c89.4 (5)Si2—Mg_m2—O1xi102.4 (3)
O2—O3—Nb_m1(1)45.1 (2)Si2—Mg_m2—O1xii155.6 (4)
O2ii—O3—O3vi157.1 (3)Si2—Mg_m2—O1vi77.6 (3)
O2ii—O3—O4117.7 (5)Si2—Mg_m2—O529.44 (12)
O2ii—O3—O5135.2 (5)Si2—Mg_m2—O5xi150.56 (12)
O2ii—O3—O668.3 (4)Si2—Mg_m2—Ba80.24 (13)
O2ii—O3—O767.5 (2)Si2—Mg_m2—Baxi99.76 (13)
O2ii—O3—Oh59.3 (4)Si2—Mg_m2—W_c80.24 (13)
O2ii—O3—Ohii59.0 (2)Si2—Mg_m2—W_cxi99.76 (13)
O2ii—O3—Ba115.0 (5)Si2—Mg_m2—Ti_m20
O2ii—O3—W_c115.0 (5)Si2xi—Mg_m2—Si2xii55.43 (8)
O2ii—O3—Nb_m1(1)44.4 (2)Si2xi—Mg_m2—Si2vi180.0 (5)
O3vi—O3—O452.2 (4)Si2xi—Mg_m2—O1102.4 (3)
O3vi—O3—O561.8 (2)Si2xi—Mg_m2—O1xi24.4 (4)
O3vi—O3—O6109.0 (5)Si2xi—Mg_m2—O1xii77.6 (3)
O3vi—O3—O791.2 (3)Si2xi—Mg_m2—O1vi155.6 (4)
O3vi—O3—Oh119.6 (6)Si2xi—Mg_m2—O5150.56 (12)
O3vi—O3—Ohii141.6 (4)Si2xi—Mg_m2—O5xi29.44 (12)
O3vi—O3—Ba55.7 (3)Si2xi—Mg_m2—Ba99.76 (13)
O3vi—O3—W_c55.7 (3)Si2xi—Mg_m2—Baxi80.24 (13)
O3vi—O3—Nb_m1(1)153.2 (6)Si2xi—Mg_m2—W_c99.76 (13)
O4—O3—O5106.7 (3)Si2xi—Mg_m2—W_cxi80.24 (13)
O4—O3—O657.3 (5)Si2xi—Mg_m2—Ti_m20
O4—O3—O760.4 (4)Si2xii—Mg_m2—Si2vi124.57 (8)
O4—O3—Oh154.9 (4)Si2xii—Mg_m2—O1155.6 (4)
O4—O3—Ohii112.0 (7)Si2xii—Mg_m2—O1xi77.6 (3)
O4—O3—Ba100.2 (4)Si2xii—Mg_m2—O1xii24.4 (4)
O4—O3—W_c100.2 (4)Si2xii—Mg_m2—O1vi102.4 (3)
O4—O3—Nb_m1(1)152.2 (8)Si2xii—Mg_m2—O5150.56 (12)
O5—O3—O6140.6 (5)Si2xii—Mg_m2—O5xi29.44 (12)
O5—O3—O7148.9 (4)Si2xii—Mg_m2—Ba99.76 (13)
O5—O3—Oh83.1 (5)Si2xii—Mg_m2—Baxi80.24 (13)
O5—O3—Ohii99.9 (3)Si2xii—Mg_m2—W_c99.76 (13)
O5—O3—Ba59.4 (3)Si2xii—Mg_m2—W_cxi80.24 (13)
O5—O3—W_c59.4 (3)Si2xii—Mg_m2—Ti_m20
O5—O3—Nb_m1(1)92.3 (4)Si2vi—Mg_m2—O177.6 (3)
O6—O3—O759.6 (4)Si2vi—Mg_m2—O1xi155.6 (4)
O6—O3—Oh127.6 (3)Si2vi—Mg_m2—O1xii102.4 (3)
O6—O3—Ohii62.4 (4)Si2vi—Mg_m2—O1vi24.4 (4)
O6—O3—Ba150.4 (3)Si2vi—Mg_m2—O529.44 (12)
O6—O3—W_c150.4 (3)Si2vi—Mg_m2—O5xi150.56 (12)
O6—O3—Nb_m1(1)95.1 (4)Si2vi—Mg_m2—Ba80.24 (13)
O7—O3—Oh99.3 (4)Si2vi—Mg_m2—Baxi99.76 (13)
O7—O3—Ohii111.2 (5)Si2vi—Mg_m2—W_c80.24 (13)
O7—O3—Ba93.5 (4)Si2vi—Mg_m2—W_cxi99.76 (13)
O7—O3—W_c93.5 (4)Si2vi—Mg_m2—Ti_m20
O7—O3—Nb_m1(1)111.5 (3)O1—Mg_m2—O1xi83.1 (3)
Oh—O3—Ohii88.2 (4)O1—Mg_m2—O1xii180.0 (5)
Oh—O3—Ba64.4 (4)O1—Mg_m2—O1vi96.9 (3)
Oh—O3—W_c64.4 (4)O1—Mg_m2—O553.8 (4)
Oh—O3—Nb_m1(1)45.1 (3)O1—Mg_m2—O5xi126.2 (4)
Ohii—O3—Ba146.1 (6)O1—Mg_m2—Ba93.7 (4)
Ohii—O3—W_c146.1 (6)O1—Mg_m2—Baxi86.3 (4)
Ohii—O3—Nb_m1(1)43.1 (3)O1—Mg_m2—W_c93.7 (4)
Ba—O3—W_c0.0 (5)O1—Mg_m2—W_cxi86.3 (4)
Ba—O3—Nb_m1(1)107.0 (7)O1—Mg_m2—Ti_m20
W_c—O3—Nb_m1(1)107.0 (7)O1xi—Mg_m2—O1xii96.9 (3)
K_b—O4—K_bvii103.0 (5)O1xi—Mg_m2—O1vi180.0 (5)
K_b—O4—Si188.0 (5)O1xi—Mg_m2—O5126.2 (4)
K_b—O4—Si1vi88.0 (5)O1xi—Mg_m2—O5xi53.8 (4)
K_b—O4—O359.2 (3)O1xi—Mg_m2—Ba86.3 (4)
K_b—O4—O3vi59.2 (3)O1xi—Mg_m2—Baxi93.7 (4)
K_b—O4—O5iv164.8 (9)O1xi—Mg_m2—W_c86.3 (4)
K_b—O4—O689.7 (3)O1xi—Mg_m2—W_cxi93.7 (4)
K_b—O4—O6vi89.7 (3)O1xi—Mg_m2—Ti_m20
K_b—O4—O7118.7 (6)O1xii—Mg_m2—O1vi83.1 (3)
K_b—O4—O7vi118.7 (6)O1xii—Mg_m2—O5126.2 (4)
K_bvii—O4—Si1114.2 (8)O1xii—Mg_m2—O5xi53.8 (4)
K_bvii—O4—Si1vi114.2 (8)O1xii—Mg_m2—Ba86.3 (4)
K_bvii—O4—O3134.5 (4)O1xii—Mg_m2—Baxi93.7 (4)
K_bvii—O4—O3vi134.5 (4)O1xii—Mg_m2—W_c86.3 (4)
K_bvii—O4—O5iv92.2 (6)O1xii—Mg_m2—W_cxi93.7 (4)
K_bvii—O4—O678.3 (6)O1xii—Mg_m2—Ti_m20
K_bvii—O4—O6vi78.3 (6)O1vi—Mg_m2—O553.8 (4)
K_bvii—O4—O7118.9 (6)O1vi—Mg_m2—O5xi126.2 (4)
K_bvii—O4—O7vi118.9 (6)O1vi—Mg_m2—Ba93.7 (4)
Si1—O4—Si1vi131.2 (15)O1vi—Mg_m2—Baxi86.3 (4)
Si1—O4—O334.5 (5)O1vi—Mg_m2—W_c93.7 (4)
Si1—O4—O3vi107.0 (11)O1vi—Mg_m2—W_cxi86.3 (4)
Si1—O4—O5iv85.7 (3)O1vi—Mg_m2—Ti_m20
Si1—O4—O636.5 (5)O5—Mg_m2—O5xi180.0 (5)
Si1—O4—O6vi167.6 (13)O5—Mg_m2—Ba68.6 (3)
Si1—O4—O735.9 (3)O5—Mg_m2—Baxi111.4 (3)
Si1—O4—O7vi110.1 (9)O5—Mg_m2—W_c68.6 (3)
Si1vi—O4—O3107.0 (11)O5—Mg_m2—W_cxi111.4 (3)
Si1vi—O4—O3vi34.5 (5)O5—Mg_m2—Ti_m20
Si1vi—O4—O5iv85.7 (3)O5xi—Mg_m2—Ba111.4 (3)
Si1vi—O4—O6167.6 (13)O5xi—Mg_m2—Baxi68.6 (3)
Si1vi—O4—O6vi36.5 (5)O5xi—Mg_m2—W_c111.4 (3)
Si1vi—O4—O7110.1 (9)O5xi—Mg_m2—W_cxi68.6 (3)
Si1vi—O4—O7vi35.9 (3)O5xi—Mg_m2—Ti_m20
O3—O4—O3vi75.7 (7)Ba—Mg_m2—Baxi180.0 (5)
O3—O4—O5iv109.6 (5)Ba—Mg_m2—W_c0.0 (5)
O3—O4—O661.6 (5)Ba—Mg_m2—W_cxi180.0 (5)
O3—O4—O6vi136.3 (8)Ba—Mg_m2—Ti_m20
O3—O4—O759.4 (4)Baxi—Mg_m2—W_c180.0 (5)
O3—O4—O7vi105.6 (9)Baxi—Mg_m2—W_cxi0.0 (5)
O3vi—O4—O5iv109.6 (5)Baxi—Mg_m2—Ti_m20
O3vi—O4—O6136.3 (8)W_c—Mg_m2—W_cxi180.0 (5)
O3vi—O4—O6vi61.6 (5)W_c—Mg_m2—Ti_m20
O3vi—O4—O7105.6 (9)W_cxi—Mg_m2—Ti_m20
O3vi—O4—O7vi59.4 (4)
Symmetry codes: (i) x+1, y, z; (ii) x+1/2, y+1/2, z+1; (iii) x+1/2, y+1/2, z; (iv) x, y, z1; (v) x+1/2, y+1/2, z; (vi) x, y, z; (vii) x+1, y, z+1; (viii) x+1, y, z+1; (ix) x, y, z+1; (x) x1/2, y+1/2, z; (xi) x, y, z+1; (xii) x, y, z+1; (xiii) x, y, z+1; (xiv) x, y, z; (xv) x, y, z.
(labu_Fe_7.21) top
Crystal data top
Ba0.7Fe0.5K2.1Mg0.05Na2Nb0.1O33Si8Ti4Z = 2
Mr = 1206.8F(000) = 1167
Monoclinic, C2/mDx = 3.202 Mg m3
Hall symbol: -C 2ySynchrotron radiation, λ = 0.414 Å
a = 13.862 (12) ÅCell parameters from 2907 reflections
b = 13.4214 (4) Åθ = 1.8–19.0°
c = 7.515 (3) ŵ = 0.85 mm1
β = 116.50 (6)°T = 293 K
V = 1251.3 (13) Å3Anhedral grain
Data collection top
ESRF ID 09
diffractometer
θmax = 19.0°, θmin = 1.8°
2907 measured reflectionsh = 78
901 independent reflectionsk = 2020
679 reflections with I > 2σ(I)l = 1010
Rint = 0.057
Refinement top
Refinement on F0 restraints
R[F2 > 2σ(F2)] = 0.0716 constraints
wR(F2) = 0.130Weighting scheme based on measured s.u.'s w = 1/(σ2(F) + 0.0120999999F2)
S = 0.97(Δ/σ)max = 0.046
901 reflectionsΔρmax = 0.94 e Å3
71 parametersΔρmin = 0.80 e Å3
Fractional atomic coordinates and isotropic or equivalent isotropic displacement parameters (Å2) top
xyzUiso*/UeqOcc. (<1)
Na_a0.4175 (16)0.2673 (6)0.0163 (12)0.033 (10)0.5
K_b0.4272 (6)00.7147 (4)0.020 (4)
Ti_m1(1)0.250.250.50.0119 (5)*0.95
Ti_m1(2)00.22129 (14)0.50.0101 (5)*
Fe_m2000.50.0243 (11)*0.5
Si10.3247 (4)0.11052 (13)0.2605 (3)0.0061 (5)*
Si20.2108 (4)0.10950 (13)0.8108 (3)0.0060 (5)*
O10.0818 (10)0.1099 (3)0.6767 (8)0.0089 (11)*
O20.2731 (10)0.1920 (4)0.7542 (7)0.0074 (11)*
O30.2741 (10)0.1187 (3)0.4156 (8)0.0083 (11)*
O40.3816 (16)00.2792 (11)0.0121 (16)*
O50.2601 (14)00.7934 (10)0.0070 (14)*
O60.4198 (11)0.1858 (4)0.2949 (8)0.0159 (13)*
O70.2269 (11)0.1225 (4)0.0364 (8)0.0095 (11)*
Oh0.0990 (10)0.2161 (3)0.3885 (7)0.0085 (11)*
Ba0.0900 (3)00.3412 (2)0.0127 (5)*0.35
W10.50.1445 (7)00.037 (13)
W200.1119 (8)00.059 (19)
W_c0.0900 (3)00.3412 (2)0.0127 (5)*0.65
Nb_m1(1)0.250.250.50.0119 (5)*0.05
Ti_m2000.50.0243 (11)*0.1
Mg_m2000.50.0243 (11)*0.05
Atomic displacement parameters (Å2) top
U11U22U33U12U13U23
Na_a0.05 (2)0.019 (3)0.028 (4)0.007 (5)0.016 (6)0.001 (3)
K_b0.010 (8)0.0343 (14)0.0127 (11)00.002 (2)0
W10.06 (3)0.022 (4)0.017 (4)00.008 (7)0
W20.10 (4)0.037 (6)0.025 (6)00.018 (10)0
Geometric parameters (Å, º) top
Na_a—Na_ai2.41 (3)Ti_m1(2)—Ohxii1.902 (13)
Na_a—K_bii4.278 (10)Ti_m1(2)—Ba3.624 (3)
Na_a—K_biii4.208 (10)Ti_m1(2)—Baxii3.624 (3)
Na_a—Ti_m1(1)ii3.530 (10)Ti_m1(2)—Ti_m22.9700 (18)
Na_a—Ti_m1(2)iv3.292 (10)Ti_m1(2)—Mg_m22.9700 (18)
Na_a—Si2iv3.106 (19)Fe_m2—O11.971 (6)
Na_a—O2ii2.321 (14)Fe_m2—O1xii1.971 (6)
Na_a—O62.349 (15)Fe_m2—O1xiv1.971 (6)
Na_a—O7v2.38 (2)Fe_m2—O1x1.971 (6)
Na_a—Bavi4.028 (10)Fe_m2—Ba2.076 (5)
Na_a—Bavii4.091 (10)Fe_m2—Baxii2.076 (5)
Na_a—W12.040 (16)Fe_m2—W_c2.076 (5)
Na_a—W2v2.019 (17)Fe_m2—W_cxii2.076 (5)
Na_a—Nb_m1(1)ii3.530 (10)Fe_m2—Ti_m20
K_b—K_biii4.505 (10)Fe_m2—Mg_m20
K_b—K_bviii3.839 (6)Si1—O31.611 (13)
K_b—Si13.398 (4)Si1—O41.657 (10)
K_b—Si1iii3.673 (11)Si1—O61.589 (13)
K_b—Si1ix3.673 (11)Si1—O71.632 (8)
K_b—Si1x3.398 (4)Si2—O11.613 (13)
K_b—Si23.690 (10)Si2—O21.575 (11)
K_b—Si2x3.690 (10)Si2—O51.650 (10)
K_b—O32.800 (9)Si2—O7xi1.618 (8)
K_b—O3x2.800 (9)Si2—Ba3.485 (4)
K_b—O4iii2.63 (2)O1—Baxii2.754 (14)
K_b—O52.63 (2)O1—Ti_m21.971 (6)
K_b—Ba4.245 (12)O1—Mg_m21.971 (6)
K_b—W1xi2.729 (7)O2—Nb_m1(1)1.952 (7)
K_b—W1ix2.729 (7)O3—Ba2.844 (13)
Ti_m1(1)—O21.952 (7)O3—Nb_m1(1)1.951 (7)
Ti_m1(1)—O2iv1.952 (7)Oh—Nb_m1(1)1.930 (13)
Ti_m1(1)—O31.951 (7)Ba—Baxv4.595 (6)
Ti_m1(1)—O3iv1.951 (7)Ba—Baxii4.152 (7)
Ti_m1(1)—Oh1.930 (13)Ba—W22.745 (6)
Ti_m1(1)—Ohiv1.930 (13)Ba—W2xvi2.745 (6)
Ti_m1(1)—Nb_m1(1)0Ba—W_c0
Ti_m1(2)—O11.985 (6)Ba—Ti_m22.076 (5)
Ti_m1(2)—O1xii1.985 (6)Ba—Mg_m22.076 (5)
Ti_m1(2)—O6iv1.907 (6)W_c—Ti_m22.076 (5)
Ti_m1(2)—O6xiii1.907 (6)W_c—Mg_m22.076 (5)
Ti_m1(2)—Oh1.902 (13)Ti_m2—Mg_m20
Na_ai—Na_a—K_bii71.9 (4)O7xi—Si2—Ba152.4 (4)
Na_ai—Na_a—K_biii75.1 (4)Ti_m1(2)—O1—Fe_m297.3 (3)
Na_ai—Na_a—Ti_m1(1)ii94.4 (5)Ti_m1(2)—O1—Si2124.3 (5)
Na_ai—Na_a—Ti_m1(2)iv103.6 (5)Ti_m1(2)—O1—Baxii98.5 (5)
Na_ai—Na_a—Si2iv142.2 (4)Ti_m1(2)—O1—Ti_m297.3 (3)
Na_ai—Na_a—O2ii114.3 (7)Ti_m1(2)—O1—Mg_m297.3 (3)
Na_ai—Na_a—O6117.1 (7)Fe_m2—O1—Si2124.2 (5)
Na_ai—Na_a—O7v138.7 (6)Fe_m2—O1—Baxii48.7 (3)
Na_ai—Na_a—Bavi74.2 (4)Fe_m2—O1—Ti_m20.0 (5)
Na_ai—Na_a—Bavii71.3 (4)Fe_m2—O1—Mg_m20.0 (5)
Na_ai—Na_a—W153.9 (6)Si2—O1—Baxii136.2 (3)
Na_ai—Na_a—W2v53.4 (6)Si2—O1—Ti_m2124.2 (5)
Na_ai—Na_a—Nb_m1(1)ii94.4 (5)Si2—O1—Mg_m2124.2 (5)
K_bii—Na_a—K_biii53.79 (14)Baxii—O1—Ti_m248.7 (3)
K_bii—Na_a—Ti_m1(1)ii61.52 (14)Baxii—O1—Mg_m248.7 (3)
K_bii—Na_a—Ti_m1(2)iv123.1 (2)Ti_m2—O1—Mg_m20.0 (5)
K_bii—Na_a—Si2iv145.8 (6)Na_axi—O2—Ti_m1(1)111.1 (6)
K_bii—Na_a—O2ii53.4 (3)Na_axi—O2—Si2116.5 (4)
K_bii—Na_a—O695.2 (3)Na_axi—O2—Nb_m1(1)111.1 (6)
K_bii—Na_a—O7v131.1 (5)Ti_m1(1)—O2—Si2132.4 (4)
K_bii—Na_a—Bavi145.2 (6)Ti_m1(1)—O2—Nb_m1(1)0.0 (5)
K_bii—Na_a—Bavii106.8 (3)Si2—O2—Nb_m1(1)132.4 (4)
K_bii—Na_a—W130.67 (19)K_b—O3—Ti_m1(1)115.6 (2)
K_bii—Na_a—W2v119.3 (7)K_b—O3—Si197.1 (5)
K_bii—Na_a—Nb_m1(1)ii61.52 (14)K_b—O3—Ba97.5 (3)
K_biii—Na_a—Ti_m1(1)ii114.6 (2)K_b—O3—Nb_m1(1)115.6 (2)
K_biii—Na_a—Ti_m1(2)iv70.00 (16)Ti_m1(1)—O3—Si1119.3 (4)
K_biii—Na_a—Si2iv121.2 (4)Ti_m1(1)—O3—Ba107.5 (6)
K_biii—Na_a—O2ii95.7 (3)Ti_m1(1)—O3—Nb_m1(1)0.0 (5)
K_biii—Na_a—O651.3 (3)Si1—O3—Ba117.5 (3)
K_biii—Na_a—O7v145.4 (7)Si1—O3—Nb_m1(1)119.3 (4)
K_biii—Na_a—Bavi109.4 (3)Ba—O3—Nb_m1(1)107.5 (6)
K_biii—Na_a—Bavii145.5 (6)K_biii—O4—Si1116.1 (7)
K_biii—Na_a—W132.87 (19)K_biii—O4—Si1x116.1 (7)
K_biii—Na_a—W2v122.1 (7)Si1—O4—Si1x127.1 (14)
K_biii—Na_a—Nb_m1(1)ii114.6 (2)K_b—O5—Si2117.0 (6)
Ti_m1(1)ii—Na_a—Ti_m1(2)iv162.0 (7)K_b—O5—Si2x117.0 (6)
Ti_m1(1)ii—Na_a—Si2iv106.0 (5)Si2—O5—Si2x125.9 (13)
Ti_m1(1)ii—Na_a—O2ii31.1 (2)Na_a—O6—Ti_m1(2)iv100.8 (4)
Ti_m1(1)ii—Na_a—O6133.6 (6)Na_a—O6—Si1118.1 (5)
Ti_m1(1)ii—Na_a—O7v76.4 (3)Ti_m1(2)iv—O6—Si1133.6 (7)
Ti_m1(1)ii—Na_a—Bavi129.7 (2)Na_av—O7—Si1118.9 (5)
Ti_m1(1)ii—Na_a—Bavii61.10 (14)Na_av—O7—Si2ii100.4 (4)
Ti_m1(1)ii—Na_a—W189.6 (3)Si1—O7—Si2ii137.2 (10)
Ti_m1(1)ii—Na_a—W2v95.7 (3)Ti_m1(1)—Oh—Ti_m1(2)131.0 (3)
Ti_m1(1)ii—Na_a—Nb_m1(1)ii0.0 (5)Ti_m1(1)—Oh—Nb_m1(1)0.0 (5)
Ti_m1(2)iv—Na_a—Si2iv59.7 (3)Ti_m1(2)—Oh—Nb_m1(1)131.0 (3)
Ti_m1(2)iv—Na_a—O2ii134.5 (8)Na_axviii—Ba—Na_axix34.5 (4)
Ti_m1(2)iv—Na_a—O634.7 (2)Na_axviii—Ba—Na_av111.07 (18)
Ti_m1(2)iv—Na_a—O7v90.4 (5)Na_axviii—Ba—Na_axiii101.7 (2)
Ti_m1(2)iv—Na_a—Bavi58.31 (14)Na_axviii—Ba—K_b125.6 (3)
Ti_m1(2)iv—Na_a—Bavii125.7 (2)Na_axviii—Ba—Ti_m1(2)129.5 (3)
Ti_m1(2)iv—Na_a—W1100.1 (3)Na_axviii—Ba—Ti_m1(2)xiv50.62 (17)
Ti_m1(2)iv—Na_a—W2v95.9 (3)Na_axviii—Ba—Fe_m290.1 (3)
Ti_m1(2)iv—Na_a—Nb_m1(1)ii162.0 (7)Na_axviii—Ba—Si2145.9 (2)
Si2iv—Na_a—O2ii98.6 (8)Na_axviii—Ba—Si2x100.01 (13)
Si2iv—Na_a—O670.0 (5)Na_axviii—Ba—O1xii96.8 (3)
Si2iv—Na_a—O7v30.8 (3)Na_axviii—Ba—O1xiv44.6 (3)
Si2iv—Na_a—Bavi68.25 (19)Na_axviii—Ba—O3142.3 (4)
Si2iv—Na_a—Bavii91.0 (2)Na_axviii—Ba—O3x85.6 (3)
Si2iv—Na_a—W1153.6 (6)Na_axviii—Ba—Baxv56.18 (14)
Si2iv—Na_a—W2v92.5 (4)Na_axviii—Ba—Baxii90.1 (3)
Si2iv—Na_a—Nb_m1(1)ii106.0 (5)Na_axviii—Ba—W287.6 (2)
O2ii—Na_a—O6102.6 (7)Na_axviii—Ba—W2xvi27.1 (3)
O2ii—Na_a—O7v77.7 (6)Na_axviii—Ba—W_c0
O2ii—Na_a—Bavi154.9 (4)Na_axviii—Ba—Ti_m290.1 (3)
O2ii—Na_a—Bavii90.9 (3)Na_axviii—Ba—Mg_m290.1 (3)
O2ii—Na_a—W183.8 (4)Na_axix—Ba—Na_av99.5 (2)
O2ii—Na_a—W2v126.5 (4)Na_axix—Ba—Na_axiii111.07 (18)
O2ii—Na_a—Nb_m1(1)ii31.1 (2)Na_axix—Ba—K_b97.6 (3)
O6—Na_a—O7v96.5 (8)Na_axix—Ba—Ti_m1(2)158.5 (2)
O6—Na_a—Bavi93.0 (3)Na_axix—Ba—Ti_m1(2)xiv71.3 (2)
O6—Na_a—Bavii157.9 (4)Na_axix—Ba—Fe_m2122.1 (3)
O6—Na_a—W183.8 (4)Na_axix—Ba—Si2147.89 (19)
O6—Na_a—W2v130.2 (5)Na_axix—Ba—Si2x101.72 (12)
O6—Na_a—Nb_m1(1)ii133.6 (6)Na_axix—Ba—O1xii127.5 (3)
O7v—Na_a—Bavi81.2 (3)Na_axix—Ba—O1xiv77.9 (3)
O7v—Na_a—Bavii69.0 (3)Na_axix—Ba—O3108.3 (4)
O7v—Na_a—W1161.1 (7)Na_axix—Ba—O3x57.3 (3)
O7v—Na_a—W2v87.0 (4)Na_axix—Ba—Baxv54.89 (13)
O7v—Na_a—Nb_m1(1)ii76.4 (3)Na_axix—Ba—Baxii122.1 (3)
Bavi—Na_a—Bavii68.93 (18)Na_axix—Ba—W286.3 (2)
Bavi—Na_a—W1117.7 (7)Na_axix—Ba—W2xvi26.0 (2)
Bavi—Na_a—W2v38.28 (17)Na_axix—Ba—W_c0
Bavi—Na_a—Nb_m1(1)ii129.7 (2)Na_axix—Ba—Ti_m2122.1 (3)
Bavii—Na_a—W1115.3 (7)Na_axix—Ba—Mg_m2122.1 (3)
Bavii—Na_a—W2v36.50 (17)Na_av—Ba—Na_axiii34.5 (4)
Bavii—Na_a—Nb_m1(1)ii61.10 (14)Na_av—Ba—K_b97.6 (3)
W1—Na_a—W2v107.3 (10)Na_av—Ba—Ti_m1(2)71.3 (2)
W1—Na_a—Nb_m1(1)ii89.6 (3)Na_av—Ba—Ti_m1(2)xiv158.5 (2)
W2v—Na_a—Nb_m1(1)ii95.7 (3)Na_av—Ba—Fe_m2122.1 (3)
Na_axi—K_b—Na_aiii32.9 (4)Na_av—Ba—Si2101.72 (12)
Na_axi—K_b—Na_aix126.21 (18)Na_av—Ba—Si2x147.89 (19)
Na_axi—K_b—Na_axvii114.0 (3)Na_av—Ba—O1xii77.9 (3)
Na_axi—K_b—K_biii120.6 (3)Na_av—Ba—O1xiv127.5 (3)
Na_axi—K_b—K_bviii62.18 (12)Na_av—Ba—O357.3 (3)
Na_axi—K_b—Si193.92 (12)Na_av—Ba—O3x108.3 (4)
Na_axi—K_b—Si1iii83.4 (3)Na_av—Ba—Baxv54.89 (13)
Na_axi—K_b—Si1ix124.2 (3)Na_av—Ba—Baxii122.1 (3)
Na_axi—K_b—Si1x143.19 (16)Na_av—Ba—W226.0 (2)
Na_axi—K_b—Si248.8 (3)Na_av—Ba—W2xvi86.3 (2)
Na_axi—K_b—Si2x90.6 (3)Na_av—Ba—W_c0
Na_axi—K_b—O375.90 (19)Na_av—Ba—Ti_m2122.1 (3)
Na_axi—K_b—O3x135.3 (4)Na_av—Ba—Mg_m2122.1 (3)
Na_axi—K_b—O4iii105.1 (3)Na_axiii—Ba—K_b125.6 (3)
Na_axi—K_b—O569.0 (3)Na_axiii—Ba—Ti_m1(2)50.62 (17)
Na_axi—K_b—Ba93.7 (3)Na_axiii—Ba—Ti_m1(2)xiv129.5 (3)
Na_axi—K_b—W1xi22.4 (2)Na_axiii—Ba—Fe_m290.1 (3)
Na_axi—K_b—W1ix105.5 (2)Na_axiii—Ba—Si2100.01 (13)
Na_aiii—K_b—Na_aix117.0 (3)Na_axiii—Ba—Si2x145.9 (2)
Na_aiii—K_b—Na_axvii126.21 (18)Na_axiii—Ba—O1xii44.6 (3)
Na_aiii—K_b—K_biii92.7 (3)Na_axiii—Ba—O1xiv96.8 (3)
Na_aiii—K_b—K_bviii64.03 (13)Na_axiii—Ba—O385.6 (3)
Na_aiii—K_b—Si190.31 (13)Na_axiii—Ba—O3x142.3 (4)
Na_aiii—K_b—Si1iii50.5 (3)Na_axiii—Ba—Baxv56.18 (14)
Na_aiii—K_b—Si1ix93.1 (3)Na_axiii—Ba—Baxii90.1 (3)
Na_aiii—K_b—Si1x138.6 (2)Na_axiii—Ba—W227.1 (3)
Na_aiii—K_b—Si281.5 (3)Na_axiii—Ba—W2xvi87.6 (2)
Na_aiii—K_b—Si2x122.1 (3)Na_axiii—Ba—W_c0
Na_aiii—K_b—O386.7 (2)Na_axiii—Ba—Ti_m290.1 (3)
Na_aiii—K_b—O3x155.91 (18)Na_axiii—Ba—Mg_m290.1 (3)
Na_aiii—K_b—O4iii72.3 (3)K_b—Ba—Ti_m1(2)102.81 (7)
Na_aiii—K_b—O5101.8 (3)K_b—Ba—Ti_m1(2)xiv102.81 (7)
Na_aiii—K_b—Ba119.6 (3)K_b—Ba—Fe_m2112.76 (12)
Na_aiii—K_b—W1xi23.9 (2)K_b—Ba—Si255.99 (13)
Na_aiii—K_b—W1ix107.3 (2)K_b—Ba—Si2x55.99 (13)
Na_aix—K_b—Na_axvii32.9 (4)K_b—Ba—O1xii134.89 (15)
Na_aix—K_b—K_biii92.7 (3)K_b—Ba—O1xiv134.89 (15)
Na_aix—K_b—K_bviii64.03 (13)K_b—Ba—O340.84 (14)
Na_aix—K_b—Si1138.6 (2)K_b—Ba—O3x40.84 (14)
Na_aix—K_b—Si1iii93.1 (3)K_b—Ba—Baxv128.87 (15)
Na_aix—K_b—Si1ix50.5 (3)K_b—Ba—Baxii112.76 (11)
Na_aix—K_b—Si1x90.31 (13)K_b—Ba—W2121.69 (16)
Na_aix—K_b—Si2122.1 (3)K_b—Ba—W2xvi121.69 (16)
Na_aix—K_b—Si2x81.5 (3)K_b—Ba—W_c0
Na_aix—K_b—O3155.91 (18)K_b—Ba—Ti_m2112.76 (12)
Na_aix—K_b—O3x86.7 (2)K_b—Ba—Mg_m2112.76 (12)
Na_aix—K_b—O4iii72.3 (3)Ti_m1(2)—Ba—Ti_m1(2)xiv110.09 (12)
Na_aix—K_b—O5101.8 (3)Ti_m1(2)—Ba—Fe_m255.05 (6)
Na_aix—K_b—Ba119.6 (3)Ti_m1(2)—Ba—Si253.22 (8)
Na_aix—K_b—W1xi107.3 (2)Ti_m1(2)—Ba—Si2x95.32 (8)
Na_aix—K_b—W1ix23.9 (2)Ti_m1(2)—Ba—O1xii32.81 (15)
Na_axvii—K_b—K_biii120.6 (3)Ti_m1(2)—Ba—O1xiv92.2 (2)
Na_axvii—K_b—K_bviii62.18 (12)Ti_m1(2)—Ba—O383.5 (2)
Na_axvii—K_b—Si1143.19 (16)Ti_m1(2)—Ba—O3x143.61 (15)
Na_axvii—K_b—Si1iii124.2 (3)Ti_m1(2)—Ba—Baxv105.80 (7)
Na_axvii—K_b—Si1ix83.4 (3)Ti_m1(2)—Ba—Baxii55.05 (6)
Na_axvii—K_b—Si1x93.92 (12)Ti_m1(2)—Ba—W277.26 (16)
Na_axvii—K_b—Si290.6 (3)Ti_m1(2)—Ba—W2xvi132.56 (18)
Na_axvii—K_b—Si2x48.8 (3)Ti_m1(2)—Ba—W_c0
Na_axvii—K_b—O3135.3 (4)Ti_m1(2)—Ba—Ti_m255.05 (6)
Na_axvii—K_b—O3x75.90 (19)Ti_m1(2)—Ba—Mg_m255.05 (6)
Na_axvii—K_b—O4iii105.1 (3)Ti_m1(2)xiv—Ba—Fe_m255.05 (6)
Na_axvii—K_b—O569.0 (3)Ti_m1(2)xiv—Ba—Si295.32 (8)
Na_axvii—K_b—Ba93.7 (3)Ti_m1(2)xiv—Ba—Si2x53.22 (8)
Na_axvii—K_b—W1xi105.5 (2)Ti_m1(2)xiv—Ba—O1xii92.2 (2)
Na_axvii—K_b—W1ix22.4 (2)Ti_m1(2)xiv—Ba—O1xiv32.81 (15)
K_biii—K_b—K_bviii128.3 (2)Ti_m1(2)xiv—Ba—O3143.61 (15)
K_biii—K_b—Si153.17 (15)Ti_m1(2)xiv—Ba—O3x83.5 (2)
K_biii—K_b—Si1iii47.77 (12)Ti_m1(2)xiv—Ba—Baxv105.80 (7)
K_biii—K_b—Si1ix47.77 (12)Ti_m1(2)xiv—Ba—Baxii55.05 (6)
K_biii—K_b—Si1x53.17 (15)Ti_m1(2)xiv—Ba—W2132.56 (18)
K_biii—K_b—Si2143.44 (9)Ti_m1(2)xiv—Ba—W2xvi77.26 (16)
K_biii—K_b—Si2x143.44 (9)Ti_m1(2)xiv—Ba—W_c0
K_biii—K_b—O381.2 (3)Ti_m1(2)xiv—Ba—Ti_m255.05 (6)
K_biii—K_b—O3x81.2 (3)Ti_m1(2)xiv—Ba—Mg_m255.05 (6)
K_biii—K_b—O4iii40.8 (2)Fe_m2—Ba—Si263.79 (12)
K_biii—K_b—O5151.7 (2)Fe_m2—Ba—Si2x63.79 (12)
K_biii—K_b—Ba103.84 (12)Fe_m2—Ba—O1xii45.53 (19)
K_biii—K_b—W1xi115.9 (2)Fe_m2—Ba—O1xiv45.53 (19)
K_biii—K_b—W1ix115.9 (2)Fe_m2—Ba—O3127.13 (19)
K_bviii—K_b—Si1153.90 (5)Fe_m2—Ba—O3x127.13 (19)
K_bviii—K_b—Si1iii85.97 (17)Fe_m2—Ba—Baxv118.37 (16)
K_bviii—K_b—Si1ix85.97 (17)Fe_m2—Ba—Baxii0.0 (5)
K_bviii—K_b—Si1x153.90 (5)Fe_m2—Ba—W2113.44 (17)
K_bviii—K_b—Si281.34 (17)Fe_m2—Ba—W2xvi113.44 (17)
K_bviii—K_b—Si2x81.34 (17)Fe_m2—Ba—W_c0
K_bviii—K_b—O3136.8 (2)Fe_m2—Ba—Ti_m20.0 (5)
K_bviii—K_b—O3x136.8 (2)Fe_m2—Ba—Mg_m20.0 (5)
K_bviii—K_b—O4iii87.6 (3)Si2—Ba—Si2x49.89 (5)
K_bviii—K_b—O580.0 (2)Si2—Ba—O1xii80.67 (17)
K_bviii—K_b—Ba127.8 (2)Si2—Ba—O1xiv106.8 (2)
K_bviii—K_b—W1xi45.30 (14)Si2—Ba—O365.24 (18)
K_bviii—K_b—W1ix45.30 (14)Si2—Ba—O3x93.08 (16)
Si1—K_b—Si1iii80.62 (17)Si2—Ba—Baxv155.04 (3)
Si1—K_b—Si1ix100.9 (2)Si2—Ba—Baxii63.79 (13)
Si1—K_b—Si1x51.77 (6)Si2—Ba—W2121.88 (19)
Si1—K_b—Si290.61 (16)Si2—Ba—W2xvi171.75 (19)
Si1—K_b—Si2x111.0 (2)Si2—Ba—W_c0
Si1—K_b—O328.1 (3)Si2—Ba—Ti_m263.79 (12)
Si1—K_b—O3x67.32 (15)Si2—Ba—Mg_m263.79 (12)
Si1—K_b—O4iii89.1 (2)Si2x—Ba—O1xii106.8 (2)
Si1—K_b—O5102.1 (2)Si2x—Ba—O1xiv80.67 (17)
Si1—K_b—Ba59.48 (14)Si2x—Ba—O393.08 (16)
Si1—K_b—W1xi108.75 (14)Si2x—Ba—O3x65.24 (18)
Si1—K_b—W1ix160.39 (16)Si2x—Ba—Baxv155.04 (3)
Si1iii—K_b—Si1ix47.64 (12)Si2x—Ba—Baxii63.79 (13)
Si1iii—K_b—Si1x100.9 (2)Si2x—Ba—W2171.75 (19)
Si1iii—K_b—Si2130.83 (8)Si2x—Ba—W2xvi121.88 (19)
Si1iii—K_b—Si2x167.31 (10)Si2x—Ba—W_c0
Si1iii—K_b—O399.7 (3)Si2x—Ba—Ti_m263.79 (12)
Si1iii—K_b—O3x128.9 (3)Si2x—Ba—Mg_m263.79 (12)
Si1iii—K_b—O4iii23.90 (7)O1xii—Ba—O1xiv64.8 (3)
Si1iii—K_b—O5152.36 (11)O1xii—Ba—O3113.0 (3)
Si1iii—K_b—Ba139.76 (10)O1xii—Ba—O3x172.1 (2)
Si1iii—K_b—W1xi70.34 (14)O1xii—Ba—Baxv85.30 (15)
Si1iii—K_b—W1ix103.7 (2)O1xii—Ba—Baxii45.53 (18)
Si1ix—K_b—Si1x80.62 (17)O1xii—Ba—W268.79 (18)
Si1ix—K_b—Si2167.31 (10)O1xii—Ba—W2xvi103.0 (2)
Si1ix—K_b—Si2x130.83 (8)O1xii—Ba—W_c0
Si1ix—K_b—O3128.9 (3)O1xii—Ba—Ti_m245.53 (19)
Si1ix—K_b—O3x99.7 (3)O1xii—Ba—Mg_m245.53 (19)
Si1ix—K_b—O4iii23.90 (7)O1xiv—Ba—O3172.1 (2)
Si1ix—K_b—O5152.36 (11)O1xiv—Ba—O3x113.0 (3)
Si1ix—K_b—Ba139.76 (10)O1xiv—Ba—Baxv85.30 (15)
Si1ix—K_b—W1xi103.7 (2)O1xiv—Ba—Baxii45.53 (18)
Si1ix—K_b—W1ix70.34 (14)O1xiv—Ba—W2103.0 (2)
Si1x—K_b—Si2111.0 (2)O1xiv—Ba—W2xvi68.79 (18)
Si1x—K_b—Si2x90.61 (16)O1xiv—Ba—W_c0
Si1x—K_b—O367.32 (15)O1xiv—Ba—Ti_m245.53 (19)
Si1x—K_b—O3x28.1 (3)O1xiv—Ba—Mg_m245.53 (19)
Si1x—K_b—O4iii89.1 (2)O3—Ba—O3x68.2 (3)
Si1x—K_b—O5102.1 (2)O3—Ba—Baxv102.25 (16)
Si1x—K_b—Ba59.48 (14)O3—Ba—Baxii127.13 (19)
Si1x—K_b—W1xi160.39 (16)O3—Ba—W282.59 (18)
Si1x—K_b—W1ix108.75 (14)O3—Ba—W2xvi119.0 (2)
Si2—K_b—Si2x46.95 (12)O3—Ba—W_c0
Si2—K_b—O362.5 (3)O3—Ba—Ti_m2127.13 (19)
Si2—K_b—O3x89.6 (3)O3—Ba—Mg_m2127.13 (19)
Si2—K_b—O4iii153.84 (11)O3x—Ba—Baxv102.25 (16)
Si2—K_b—O523.48 (7)O3x—Ba—Baxii127.13 (19)
Si2—K_b—Ba51.52 (12)O3x—Ba—W2119.0 (2)
Si2—K_b—W1xi67.11 (15)O3x—Ba—W2xvi82.59 (18)
Si2—K_b—W1ix100.2 (2)O3x—Ba—W_c0
Si2x—K_b—O389.6 (3)O3x—Ba—Ti_m2127.13 (19)
Si2x—K_b—O3x62.5 (3)O3x—Ba—Mg_m2127.13 (19)
Si2x—K_b—O4iii153.84 (11)Baxv—Ba—Baxii118.37 (14)
Si2x—K_b—O523.48 (7)Baxv—Ba—W233.17 (18)
Si2x—K_b—Ba51.52 (12)Baxv—Ba—W2xvi33.17 (18)
Si2x—K_b—W1xi100.2 (2)Baxv—Ba—W_c0
Si2x—K_b—W1ix67.11 (15)Baxv—Ba—Ti_m2118.37 (16)
O3—K_b—O3x69.4 (2)Baxv—Ba—Mg_m2118.37 (16)
O3—K_b—O4iii114.3 (4)Baxii—Ba—W2113.44 (15)
O3—K_b—O575.7 (4)Baxii—Ba—W2xvi113.44 (15)
O3—K_b—Ba41.6 (3)Baxii—Ba—W_c0
O3—K_b—W1xi96.22 (18)Baxii—Ba—Ti_m20.0 (5)
O3—K_b—W1ix156.5 (4)Baxii—Ba—Mg_m20.0 (5)
O3x—K_b—O4iii114.3 (4)W2—Ba—W2xvi66.3 (3)
O3x—K_b—O575.7 (4)W2—Ba—W_c0
O3x—K_b—Ba41.6 (3)W2—Ba—Ti_m2113.44 (17)
O3x—K_b—W1xi156.5 (4)W2—Ba—Mg_m2113.44 (17)
O3x—K_b—W1ix96.22 (18)W2xvi—Ba—W_c0
O4iii—K_b—O5167.5 (3)W2xvi—Ba—Ti_m2113.44 (17)
O4iii—K_b—Ba144.6 (2)W2xvi—Ba—Mg_m2113.44 (17)
O4iii—K_b—W1xi88.3 (2)W_c—Ba—Ti_m20
O4iii—K_b—W1ix88.3 (2)W_c—Ba—Mg_m20
O5—K_b—Ba47.9 (2)Ti_m2—Ba—Mg_m20.0 (5)
O5—K_b—W1xi83.0 (2)Na_a—W1—Na_ai72.3 (8)
O5—K_b—W1ix83.0 (2)Na_a—W1—K_bii126.9 (4)
Ba—K_b—W1xi115.6 (2)Na_a—W1—K_biii123.2 (4)
Ba—K_b—W1ix115.6 (2)Na_ai—W1—K_bii123.2 (4)
W1xi—K_b—W1ix90.6 (2)Na_ai—W1—K_biii126.9 (4)
Na_axi—Ti_m1(1)—Na_av180.0 (5)K_bii—W1—K_biii89.4 (3)
Na_axi—Ti_m1(1)—O237.8 (4)Na_av—W2—Na_axiii73.2 (8)
Na_axi—Ti_m1(1)—O2iv142.2 (4)Na_av—W2—Ba117.5 (3)
Na_axi—Ti_m1(1)—O3107.0 (2)Na_av—W2—Baxv114.6 (3)
Na_axi—Ti_m1(1)—O3iv73.0 (2)Na_axiii—W2—Ba114.6 (3)
Na_axi—Ti_m1(1)—Oh123.1 (4)Na_axiii—W2—Baxv117.5 (3)
Na_axi—Ti_m1(1)—Ohiv56.9 (4)Ba—W2—Baxv113.7 (4)
Na_axi—Ti_m1(1)—Nb_m1(1)0Fe_m2—W_c—Ba0
Na_av—Ti_m1(1)—O2142.2 (4)Fe_m2—W_c—Ti_m20.0 (5)
Na_av—Ti_m1(1)—O2iv37.8 (4)Fe_m2—W_c—Mg_m20.0 (5)
Na_av—Ti_m1(1)—O373.0 (2)Ba—W_c—Ti_m20
Na_av—Ti_m1(1)—O3iv107.0 (2)Ba—W_c—Mg_m20
Na_av—Ti_m1(1)—Oh56.9 (4)Ti_m2—W_c—Mg_m20.0 (5)
Na_av—Ti_m1(1)—Ohiv123.1 (4)Na_axi—Nb_m1(1)—Na_av180.0 (5)
Na_av—Ti_m1(1)—Nb_m1(1)0Na_axi—Nb_m1(1)—Ti_m1(1)0
O2—Ti_m1(1)—O2iv180.0 (5)Na_axi—Nb_m1(1)—O237.8 (4)
O2—Ti_m1(1)—O388.9 (3)Na_axi—Nb_m1(1)—O2iv142.2 (4)
O2—Ti_m1(1)—O3iv91.1 (3)Na_axi—Nb_m1(1)—O3107.0 (2)
O2—Ti_m1(1)—Oh90.2 (4)Na_axi—Nb_m1(1)—O3iv73.0 (2)
O2—Ti_m1(1)—Ohiv89.8 (4)Na_axi—Nb_m1(1)—Oh123.1 (4)
O2—Ti_m1(1)—Nb_m1(1)0Na_axi—Nb_m1(1)—Ohiv56.9 (4)
O2iv—Ti_m1(1)—O391.1 (3)Na_av—Nb_m1(1)—Ti_m1(1)0
O2iv—Ti_m1(1)—O3iv88.9 (3)Na_av—Nb_m1(1)—O2142.2 (4)
O2iv—Ti_m1(1)—Oh89.8 (4)Na_av—Nb_m1(1)—O2iv37.8 (4)
O2iv—Ti_m1(1)—Ohiv90.2 (4)Na_av—Nb_m1(1)—O373.0 (2)
O2iv—Ti_m1(1)—Nb_m1(1)0Na_av—Nb_m1(1)—O3iv107.0 (2)
O3—Ti_m1(1)—O3iv180.0 (5)Na_av—Nb_m1(1)—Oh56.9 (4)
O3—Ti_m1(1)—Oh87.5 (4)Na_av—Nb_m1(1)—Ohiv123.1 (4)
O3—Ti_m1(1)—Ohiv92.5 (4)Ti_m1(1)—Nb_m1(1)—O20
O3—Ti_m1(1)—Nb_m1(1)0Ti_m1(1)—Nb_m1(1)—O2iv0
O3iv—Ti_m1(1)—Oh92.5 (4)Ti_m1(1)—Nb_m1(1)—O30
O3iv—Ti_m1(1)—Ohiv87.5 (4)Ti_m1(1)—Nb_m1(1)—O3iv0
O3iv—Ti_m1(1)—Nb_m1(1)0Ti_m1(1)—Nb_m1(1)—Oh0
Oh—Ti_m1(1)—Ohiv180.0 (5)Ti_m1(1)—Nb_m1(1)—Ohiv0
Oh—Ti_m1(1)—Nb_m1(1)0O2—Nb_m1(1)—O2iv180.0 (5)
Ohiv—Ti_m1(1)—Nb_m1(1)0O2—Nb_m1(1)—O388.9 (3)
Na_aiv—Ti_m1(2)—Na_axiii174.66 (19)O2—Nb_m1(1)—O3iv91.1 (3)
Na_aiv—Ti_m1(2)—O158.9 (3)O2—Nb_m1(1)—Oh90.2 (4)
Na_aiv—Ti_m1(2)—O1xii126.0 (3)O2—Nb_m1(1)—Ohiv89.8 (4)
Na_aiv—Ti_m1(2)—O6iv44.5 (3)O2iv—Nb_m1(1)—O391.1 (3)
Na_aiv—Ti_m1(2)—O6xiii130.7 (3)O2iv—Nb_m1(1)—O3iv88.9 (3)
Na_aiv—Ti_m1(2)—Oh121.6 (4)O2iv—Nb_m1(1)—Oh89.8 (4)
Na_aiv—Ti_m1(2)—Ohxii58.6 (4)O2iv—Nb_m1(1)—Ohiv90.2 (4)
Na_aiv—Ti_m1(2)—Ba113.6 (2)O3—Nb_m1(1)—O3iv180.0 (5)
Na_aiv—Ti_m1(2)—Baxii71.1 (2)O3—Nb_m1(1)—Oh87.5 (4)
Na_aiv—Ti_m1(2)—Ti_m292.67 (13)O3—Nb_m1(1)—Ohiv92.5 (4)
Na_aiv—Ti_m1(2)—Mg_m292.67 (13)O3iv—Nb_m1(1)—Oh92.5 (4)
Na_axiii—Ti_m1(2)—O1126.0 (3)O3iv—Nb_m1(1)—Ohiv87.5 (4)
Na_axiii—Ti_m1(2)—O1xii58.9 (3)Oh—Nb_m1(1)—Ohiv180.0 (5)
Na_axiii—Ti_m1(2)—O6iv130.7 (3)Ti_m1(2)—Ti_m2—Ti_m1(2)xiv180.0 (5)
Na_axiii—Ti_m1(2)—O6xiii44.5 (3)Ti_m1(2)—Ti_m2—Fe_m20
Na_axiii—Ti_m1(2)—Oh58.6 (4)Ti_m1(2)—Ti_m2—O141.52 (18)
Na_axiii—Ti_m1(2)—Ohxii121.6 (4)Ti_m1(2)—Ti_m2—O1xii41.52 (18)
Na_axiii—Ti_m1(2)—Ba71.1 (2)Ti_m1(2)—Ti_m2—O1xiv138.48 (18)
Na_axiii—Ti_m1(2)—Baxii113.6 (2)Ti_m1(2)—Ti_m2—O1x138.48 (18)
Na_axiii—Ti_m1(2)—Ti_m292.67 (13)Ti_m1(2)—Ti_m2—Ba90
Na_axiii—Ti_m1(2)—Mg_m292.67 (13)Ti_m1(2)—Ti_m2—Baxii90
O1—Ti_m1(2)—O1xii82.3 (3)Ti_m1(2)—Ti_m2—W_c90
O1—Ti_m1(2)—O6iv89.9 (3)Ti_m1(2)—Ti_m2—W_cxii90
O1—Ti_m1(2)—O6xiii170.4 (3)Ti_m1(2)—Ti_m2—Mg_m20
O1—Ti_m1(2)—Oh87.6 (4)Ti_m1(2)xiv—Ti_m2—Fe_m20
O1—Ti_m1(2)—Ohxii89.3 (4)Ti_m1(2)xiv—Ti_m2—O1138.48 (18)
O1—Ti_m1(2)—Ba54.9 (2)Ti_m1(2)xiv—Ti_m2—O1xii138.48 (18)
O1—Ti_m1(2)—Baxii48.7 (4)Ti_m1(2)xiv—Ti_m2—O1xiv41.52 (18)
O1—Ti_m1(2)—Ti_m241.15 (18)Ti_m1(2)xiv—Ti_m2—O1x41.52 (18)
O1—Ti_m1(2)—Mg_m241.15 (18)Ti_m1(2)xiv—Ti_m2—Ba90
O1xii—Ti_m1(2)—O6iv170.4 (3)Ti_m1(2)xiv—Ti_m2—Baxii90
O1xii—Ti_m1(2)—O6xiii89.9 (3)Ti_m1(2)xiv—Ti_m2—W_c90
O1xii—Ti_m1(2)—Oh89.3 (4)Ti_m1(2)xiv—Ti_m2—W_cxii90
O1xii—Ti_m1(2)—Ohxii87.6 (4)Ti_m1(2)xiv—Ti_m2—Mg_m20
O1xii—Ti_m1(2)—Ba48.7 (4)Fe_m2—Ti_m2—O10
O1xii—Ti_m1(2)—Baxii54.9 (2)Fe_m2—Ti_m2—O1xii0
O1xii—Ti_m1(2)—Ti_m241.15 (18)Fe_m2—Ti_m2—O1xiv0
O1xii—Ti_m1(2)—Mg_m241.15 (18)Fe_m2—Ti_m2—O1x0
O6iv—Ti_m1(2)—O6xiii98.4 (3)Fe_m2—Ti_m2—Ba0
O6iv—Ti_m1(2)—Oh96.0 (5)Fe_m2—Ti_m2—Baxii0
O6iv—Ti_m1(2)—Ohxii86.7 (5)Fe_m2—Ti_m2—W_c0
O6iv—Ti_m1(2)—Ba129.8 (4)Fe_m2—Ti_m2—W_cxii0
O6iv—Ti_m1(2)—Baxii115.6 (3)Fe_m2—Ti_m2—Mg_m20
O6iv—Ti_m1(2)—Ti_m2130.82 (19)O1—Ti_m2—O1xii83.0 (3)
O6iv—Ti_m1(2)—Mg_m2130.82 (19)O1—Ti_m2—O1xiv180.0 (5)
O6xiii—Ti_m1(2)—Oh86.7 (5)O1—Ti_m2—O1x97.0 (3)
O6xiii—Ti_m1(2)—Ohxii96.0 (5)O1—Ti_m2—Ba94.3 (4)
O6xiii—Ti_m1(2)—Ba115.6 (3)O1—Ti_m2—Baxii85.7 (4)
O6xiii—Ti_m1(2)—Baxii129.8 (4)O1—Ti_m2—W_c94.3 (4)
O6xiii—Ti_m1(2)—Ti_m2130.82 (19)O1—Ti_m2—W_cxii85.7 (4)
O6xiii—Ti_m1(2)—Mg_m2130.82 (19)O1—Ti_m2—Mg_m20
Oh—Ti_m1(2)—Ohxii175.8 (2)O1xii—Ti_m2—O1xiv97.0 (3)
Oh—Ti_m1(2)—Ba53.33 (16)O1xii—Ti_m2—O1x180.0 (5)
Oh—Ti_m1(2)—Baxii122.51 (17)O1xii—Ti_m2—Ba85.7 (4)
Oh—Ti_m1(2)—Ti_m287.91 (15)O1xii—Ti_m2—Baxii94.3 (4)
Oh—Ti_m1(2)—Mg_m287.91 (15)O1xii—Ti_m2—W_c85.7 (4)
Ohxii—Ti_m1(2)—Ba122.51 (17)O1xii—Ti_m2—W_cxii94.3 (4)
Ohxii—Ti_m1(2)—Baxii53.33 (16)O1xii—Ti_m2—Mg_m20
Ohxii—Ti_m1(2)—Ti_m287.91 (15)O1xiv—Ti_m2—O1x83.0 (3)
Ohxii—Ti_m1(2)—Mg_m287.91 (15)O1xiv—Ti_m2—Ba85.7 (4)
Ba—Ti_m1(2)—Baxii69.91 (9)O1xiv—Ti_m2—Baxii94.3 (4)
Ba—Ti_m1(2)—Ti_m234.95 (6)O1xiv—Ti_m2—W_c85.7 (4)
Ba—Ti_m1(2)—Mg_m234.95 (6)O1xiv—Ti_m2—W_cxii94.3 (4)
Baxii—Ti_m1(2)—Ti_m234.95 (6)O1xiv—Ti_m2—Mg_m20
Baxii—Ti_m1(2)—Mg_m234.95 (6)O1x—Ti_m2—Ba94.3 (4)
Ti_m2—Ti_m1(2)—Mg_m20.0 (5)O1x—Ti_m2—Baxii85.7 (4)
O1—Fe_m2—O1xii83.0 (3)O1x—Ti_m2—W_c94.3 (4)
O1—Fe_m2—O1xiv180.0 (5)O1x—Ti_m2—W_cxii85.7 (4)
O1—Fe_m2—O1x97.0 (3)O1x—Ti_m2—Mg_m20
O1—Fe_m2—Ba94.3 (4)Ba—Ti_m2—Baxii180.0 (5)
O1—Fe_m2—Baxii85.7 (4)Ba—Ti_m2—W_c0.0 (5)
O1—Fe_m2—W_c94.3 (4)Ba—Ti_m2—W_cxii180.0 (5)
O1—Fe_m2—W_cxii85.7 (4)Ba—Ti_m2—Mg_m20
O1—Fe_m2—Ti_m20Baxii—Ti_m2—W_c180.0 (5)
O1—Fe_m2—Mg_m20Baxii—Ti_m2—W_cxii0.0 (5)
O1xii—Fe_m2—O1xiv97.0 (3)Baxii—Ti_m2—Mg_m20
O1xii—Fe_m2—O1x180.0 (5)W_c—Ti_m2—W_cxii180.0 (5)
O1xii—Fe_m2—Ba85.7 (4)W_c—Ti_m2—Mg_m20
O1xii—Fe_m2—Baxii94.3 (4)W_cxii—Ti_m2—Mg_m20
O1xii—Fe_m2—W_c85.7 (4)Ti_m1(2)—Mg_m2—Ti_m1(2)xiv180.0 (5)
O1xii—Fe_m2—W_cxii94.3 (4)Ti_m1(2)—Mg_m2—Fe_m20
O1xii—Fe_m2—Ti_m20Ti_m1(2)—Mg_m2—O141.52 (18)
O1xii—Fe_m2—Mg_m20Ti_m1(2)—Mg_m2—O1xii41.52 (18)
O1xiv—Fe_m2—O1x83.0 (3)Ti_m1(2)—Mg_m2—O1xiv138.48 (18)
O1xiv—Fe_m2—Ba85.7 (4)Ti_m1(2)—Mg_m2—O1x138.48 (18)
O1xiv—Fe_m2—Baxii94.3 (4)Ti_m1(2)—Mg_m2—Ba90
O1xiv—Fe_m2—W_c85.7 (4)Ti_m1(2)—Mg_m2—Baxii90
O1xiv—Fe_m2—W_cxii94.3 (4)Ti_m1(2)—Mg_m2—W_c90
O1xiv—Fe_m2—Ti_m20Ti_m1(2)—Mg_m2—W_cxii90
O1xiv—Fe_m2—Mg_m20Ti_m1(2)—Mg_m2—Ti_m20
O1x—Fe_m2—Ba94.3 (4)Ti_m1(2)xiv—Mg_m2—Fe_m20
O1x—Fe_m2—Baxii85.7 (4)Ti_m1(2)xiv—Mg_m2—O1138.48 (18)
O1x—Fe_m2—W_c94.3 (4)Ti_m1(2)xiv—Mg_m2—O1xii138.48 (18)
O1x—Fe_m2—W_cxii85.7 (4)Ti_m1(2)xiv—Mg_m2—O1xiv41.52 (18)
O1x—Fe_m2—Ti_m20Ti_m1(2)xiv—Mg_m2—O1x41.52 (18)
O1x—Fe_m2—Mg_m20Ti_m1(2)xiv—Mg_m2—Ba90
Ba—Fe_m2—Baxii180.0 (5)Ti_m1(2)xiv—Mg_m2—Baxii90
Ba—Fe_m2—W_c0.0 (5)Ti_m1(2)xiv—Mg_m2—W_c90
Ba—Fe_m2—W_cxii180.0 (5)Ti_m1(2)xiv—Mg_m2—W_cxii90
Ba—Fe_m2—Ti_m20Ti_m1(2)xiv—Mg_m2—Ti_m20
Ba—Fe_m2—Mg_m20Fe_m2—Mg_m2—O10
Baxii—Fe_m2—W_c180.0 (5)Fe_m2—Mg_m2—O1xii0
Baxii—Fe_m2—W_cxii0.0 (5)Fe_m2—Mg_m2—O1xiv0
Baxii—Fe_m2—Ti_m20Fe_m2—Mg_m2—O1x0
Baxii—Fe_m2—Mg_m20Fe_m2—Mg_m2—Ba0
W_c—Fe_m2—W_cxii180.0 (5)Fe_m2—Mg_m2—Baxii0
W_c—Fe_m2—Ti_m20Fe_m2—Mg_m2—W_c0
W_c—Fe_m2—Mg_m20Fe_m2—Mg_m2—W_cxii0
W_cxii—Fe_m2—Ti_m20Fe_m2—Mg_m2—Ti_m20
W_cxii—Fe_m2—Mg_m20O1—Mg_m2—O1xii83.0 (3)
Ti_m2—Fe_m2—Mg_m20O1—Mg_m2—O1xiv180.0 (5)
K_b—Si1—K_biii79.06 (17)O1—Mg_m2—O1x97.0 (3)
K_b—Si1—O354.9 (3)O1—Mg_m2—Ba94.3 (4)
K_b—Si1—O463.5 (4)O1—Mg_m2—Baxii85.7 (4)
K_b—Si1—O699.8 (3)O1—Mg_m2—W_c94.3 (4)
K_b—Si1—O7149.6 (5)O1—Mg_m2—W_cxii85.7 (4)
K_biii—Si1—O3133.7 (3)O1—Mg_m2—Ti_m20
K_biii—Si1—O440.0 (7)O1xii—Mg_m2—O1xiv97.0 (3)
K_biii—Si1—O663.8 (4)O1xii—Mg_m2—O1x180.0 (5)
K_biii—Si1—O7114.9 (5)O1xii—Mg_m2—Ba85.7 (4)
O3—Si1—O4110.2 (6)O1xii—Mg_m2—Baxii94.3 (4)
O3—Si1—O6115.9 (4)O1xii—Mg_m2—W_c85.7 (4)
O3—Si1—O7108.1 (7)O1xii—Mg_m2—W_cxii94.3 (4)
O4—Si1—O6103.1 (8)O1xii—Mg_m2—Ti_m20
O4—Si1—O7108.7 (4)O1xiv—Mg_m2—O1x83.0 (3)
O6—Si1—O7110.6 (5)O1xiv—Mg_m2—Ba85.7 (4)
Na_aiv—Si2—K_b164.0 (3)O1xiv—Mg_m2—Baxii94.3 (4)
Na_aiv—Si2—O165.0 (4)O1xiv—Mg_m2—W_c85.7 (4)
Na_aiv—Si2—O2103.0 (4)O1xiv—Mg_m2—W_cxii94.3 (4)
Na_aiv—Si2—O5147.3 (6)O1xiv—Mg_m2—Ti_m20
Na_aiv—Si2—O7xi48.8 (4)O1x—Mg_m2—Ba94.3 (4)
Na_aiv—Si2—Ba122.8 (3)O1x—Mg_m2—Baxii85.7 (4)
K_b—Si2—O1130.6 (3)O1x—Mg_m2—W_c94.3 (4)
K_b—Si2—O268.6 (4)O1x—Mg_m2—W_cxii85.7 (4)
K_b—Si2—O539.5 (6)O1x—Mg_m2—Ti_m20
K_b—Si2—O7xi120.3 (5)Ba—Mg_m2—Baxii180.0 (5)
K_b—Si2—Ba72.49 (14)Ba—Mg_m2—W_c0.0 (5)
O1—Si2—O2114.7 (4)Ba—Mg_m2—W_cxii180.0 (5)
O1—Si2—O5109.7 (5)Ba—Mg_m2—Ti_m20
O1—Si2—O7xi104.5 (7)Baxii—Mg_m2—W_c180.0 (5)
O1—Si2—Ba58.1 (3)Baxii—Mg_m2—W_cxii0.0 (5)
O2—Si2—O5107.9 (8)Baxii—Mg_m2—Ti_m20
O2—Si2—O7xi111.8 (4)W_c—Mg_m2—W_cxii180.0 (5)
O2—Si2—Ba95.5 (2)W_c—Mg_m2—Ti_m20
O5—Si2—O7xi108.1 (4)W_cxii—Mg_m2—Ti_m20
O5—Si2—Ba64.7 (3)
Symmetry codes: (i) x+1, y, z; (ii) x, y, z1; (iii) x+1, y, z+1; (iv) x+1/2, y+1/2, z+1; (v) x+1/2, y+1/2, z; (vi) x+1/2, y+1/2, z; (vii) x+1/2, y+1/2, z; (viii) x+1, y, z+2; (ix) x+1, y, z+1; (x) x, y, z; (xi) x, y, z+1; (xii) x, y, z+1; (xiii) x1/2, y+1/2, z; (xiv) x, y, z+1; (xv) x, y, z; (xvi) x, y, z; (xvii) x, y, z+1; (xviii) x1/2, y1/2, z; (xix) x+1/2, y1/2, z.
(labu-Fe_10.01) top
Crystal data top
Ba0.7Fe0.5K2.1Mg0.05Na2Nb0.1O33Si8Ti4Z = 2
Mr = 1206.8F(000) = 1167
Monoclinic, C2/mDx = 3.292 Mg m3
Hall symbol: -C 2ySynchrotron radiation, λ = 0.414 Å
a = 13.739 (12) ÅCell parameters from 2971 reflections
b = 13.3221 (7) Åθ = 1.8–19.1°
c = 7.419 (2) ŵ = 0.87 mm1
β = 116.33 (5)°T = 293 K
V = 1217.1 (12) Å3Anhedral grain
Data collection top
ESRF ID 09
diffractometer
θmax = 19.1°, θmin = 1.8°
2971 measured reflectionsh = 87
877 independent reflectionsk = 2020
687 reflections with I > 2σ(I)l = 1010
Rint = 0.051
Refinement top
Refinement on F0 restraints
R[F2 > 2σ(F2)] = 0.0746 constraints
wR(F2) = 0.137Weighting scheme based on measured s.u.'s w = 1/(σ2(F) + 0.0120999999F2)
S = 1.06(Δ/σ)max = 0.043
877 reflectionsΔρmax = 0.97 e Å3
71 parametersΔρmin = 0.95 e Å3
Fractional atomic coordinates and isotropic or equivalent isotropic displacement parameters (Å2) top
xyzUiso*/UeqOcc. (<1)
Na_a0.4191 (15)0.2682 (5)0.0155 (12)0.025 (9)0.5
K_b0.4289 (5)00.7197 (4)0.020 (4)
Ti_m1(1)0.250.250.50.0141 (5)*0.95
Ti_m1(2)00.21989 (14)0.50.0132 (6)*
Fe_m2000.50.0255 (11)*0.5
Si10.3268 (4)0.11032 (13)0.2634 (3)0.0085 (5)*
Si20.2112 (4)0.10905 (13)0.8133 (3)0.0079 (5)*
O10.0815 (11)0.1091 (3)0.6797 (8)0.0087 (11)*
O20.2729 (10)0.1943 (4)0.7576 (7)0.0090 (11)*
O30.2783 (11)0.1182 (3)0.4237 (8)0.0100 (11)*
O40.3827 (16)00.2844 (11)0.0129 (16)*
O50.2628 (15)00.7928 (11)0.0117 (16)*
O60.4212 (11)0.1868 (4)0.2938 (9)0.0177 (14)*
O70.2253 (11)0.1196 (3)0.0393 (8)0.0106 (11)*
Oh0.0972 (10)0.2129 (4)0.3873 (8)0.0112 (11)*
Ba0.0917 (3)00.3401 (2)0.0137 (5)*0.35
W10.50.1440 (7)00.056 (13)
W200.1078 (7)00.038 (17)
W_c0.0917 (3)00.3401 (2)0.0137 (5)*0.65
Nb_m1(1)0.250.250.50.0141 (5)*0.05
Ti_m2000.50.0255 (11)*0.1
Mg_m2000.50.0255 (11)*0.05
Atomic displacement parameters (Å2) top
U11U22U33U12U13U23
Na_a0.02 (2)0.019 (3)0.034 (4)0.008 (5)0.008 (6)0.003 (3)
K_b0.014 (8)0.0331 (14)0.0129 (11)00.0057 (19)0
W10.09 (3)0.027 (5)0.016 (4)00.009 (8)0
W20.05 (4)0.032 (5)0.034 (6)00.023 (9)0
Geometric parameters (Å, º) top
Na_a—Na_ai2.33 (3)Ti_m1(2)—Ba3.592 (3)
Na_a—K_bii4.226 (10)Ti_m1(2)—Baxiii3.592 (3)
Na_a—K_biii4.165 (10)Ti_m1(2)—Ti_m22.9294 (19)
Na_a—Ti_m1(1)ii3.493 (10)Ti_m1(2)—Mg_m22.9294 (19)
Na_a—Ti_m1(2)iv3.262 (10)Fe_m2—O11.954 (6)
Na_a—Si2iv3.084 (18)Fe_m2—O1xiii1.954 (6)
Na_a—O2ii2.294 (14)Fe_m2—O1xv1.954 (6)
Na_a—O62.321 (15)Fe_m2—O1x1.954 (6)
Na_a—O7v2.37 (2)Fe_m2—Ba2.079 (5)
Na_a—Bavi3.987 (10)Fe_m2—Baxiii2.079 (5)
Na_a—Bavii4.021 (10)Fe_m2—W_c2.079 (5)
Na_a—W12.025 (16)Fe_m2—W_cxiii2.079 (5)
Na_a—W2v2.022 (16)Fe_m2—Ti_m20
Na_a—Nb_m1(1)ii3.493 (10)Fe_m2—Mg_m20
K_b—K_biii4.484 (9)Si1—O31.604 (13)
K_b—K_bviii3.729 (6)Si1—O41.634 (10)
K_b—Si13.373 (4)Si1—O61.585 (13)
K_b—Si1iii3.616 (10)Si1—O71.633 (8)
K_b—Si1ix3.616 (10)Si2—O11.610 (13)
K_b—Si1x3.373 (4)Si2—O21.577 (11)
K_b—Si23.657 (10)Si2—O51.652 (11)
K_b—Si2x3.657 (10)Si2—O7xi1.607 (8)
K_b—O32.749 (9)Si2—Ba3.467 (4)
K_b—O3x2.749 (9)O1—Baxiii2.736 (14)
K_b—O4iii2.60 (2)O1—Ti_m21.954 (6)
K_b—O52.57 (2)O1—Mg_m21.954 (6)
K_b—Ba4.221 (12)O2—Nb_m1(1)1.942 (7)
K_b—W1xi2.675 (7)O3—Ba2.833 (14)
K_b—W1ix2.675 (7)O3—Nb_m1(1)1.936 (7)
Ti_m1(1)—O21.942 (7)Oh—Ba2.855 (5)
Ti_m1(1)—O2iv1.942 (7)Oh—Nb_m1(1)1.948 (13)
Ti_m1(1)—O31.936 (7)Ba—Baxvi4.532 (6)
Ti_m1(1)—O3iv1.936 (7)Ba—Baxiii4.157 (7)
Ti_m1(1)—Oh1.948 (13)Ba—W22.683 (6)
Ti_m1(1)—Ohiv1.948 (13)Ba—W2xvii2.683 (6)
Ti_m1(1)—Ba3.865 (3)Ba—W_c0
Ti_m1(1)—Baxii3.865 (3)Ba—Nb_m1(1)3.865 (3)
Ti_m1(1)—Nb_m1(1)0Ba—Nb_m1(1)xviii3.865 (3)
Ti_m1(2)—O11.971 (6)Ba—Ti_m22.079 (5)
Ti_m1(2)—O1xiii1.971 (6)Ba—Mg_m22.079 (5)
Ti_m1(2)—O6iv1.895 (6)W_c—Ti_m22.079 (5)
Ti_m1(2)—O6xiv1.895 (6)W_c—Mg_m22.079 (5)
Ti_m1(2)—Oh1.866 (13)Ti_m2—Mg_m20
Ti_m1(2)—Ohxiii1.866 (13)
Na_ai—Na_a—K_bii72.4 (4)Na_axx—Ba—Nb_m1(1)162.89 (19)
Na_ai—Na_a—K_biii75.3 (4)Na_axx—Ba—Nb_m1(1)xviii67.7 (2)
Na_ai—Na_a—Ti_m1(1)ii95.3 (5)Na_axx—Ba—Ti_m289.8 (3)
Na_ai—Na_a—Ti_m1(2)iv103.6 (5)Na_axx—Ba—Mg_m289.8 (3)
Na_ai—Na_a—Si2iv142.5 (4)Na_axxi—Ba—Na_av100.3 (2)
Na_ai—Na_a—O2ii116.0 (7)Na_axxi—Ba—Na_axiv111.06 (18)
Na_ai—Na_a—O6116.8 (7)Na_axxi—Ba—K_b98.5 (3)
Na_ai—Na_a—O7v138.1 (6)Na_axxi—Ba—Ti_m1(1)135.7 (3)
Na_ai—Na_a—Bavi73.9 (4)Na_axxi—Ba—Ti_m1(1)xviii52.54 (14)
Na_ai—Na_a—Bavii72.3 (4)Na_axxi—Ba—Ti_m1(2)157.9 (2)
Na_ai—Na_a—W154.8 (5)Na_axxi—Ba—Ti_m1(2)xv71.0 (2)
Na_ai—Na_a—W2v54.8 (5)Na_axxi—Ba—Fe_m2121.3 (3)
Na_ai—Na_a—Nb_m1(1)ii95.3 (5)Na_axxi—Ba—Si2148.14 (18)
K_bii—Na_a—K_biii52.76 (13)Na_axxi—Ba—Si2x101.87 (12)
K_bii—Na_a—Ti_m1(1)ii62.07 (14)Na_axxi—Ba—O1xiii126.5 (3)
K_bii—Na_a—Ti_m1(2)iv122.7 (2)Na_axxi—Ba—O1xv77.2 (3)
K_bii—Na_a—Si2iv145.1 (5)Na_axxi—Ba—O3109.7 (4)
K_bii—Na_a—O2ii54.7 (3)Na_axxi—Ba—O3x58.9 (3)
K_bii—Na_a—O694.3 (3)Na_axxi—Ba—Oh146.6 (2)
K_bii—Na_a—O7v131.4 (5)Na_axxi—Ba—Ohx46.3 (2)
K_bii—Na_a—Bavi145.2 (6)Na_axxi—Ba—Baxvi55.17 (13)
K_bii—Na_a—Bavii108.0 (3)Na_axxi—Ba—Baxiii121.3 (3)
K_bii—Na_a—W130.11 (18)Na_axxi—Ba—W285.9 (2)
K_bii—Na_a—W2v121.1 (7)Na_axxi—Ba—W2xvii26.7 (2)
K_bii—Na_a—Nb_m1(1)ii62.07 (14)Na_axxi—Ba—W_c0
K_biii—Na_a—Ti_m1(1)ii114.1 (2)Na_axxi—Ba—Nb_m1(1)135.7 (3)
K_biii—Na_a—Ti_m1(2)iv70.58 (16)Na_axxi—Ba—Nb_m1(1)xviii52.54 (14)
K_biii—Na_a—Si2iv121.5 (4)Na_axxi—Ba—Ti_m2121.3 (3)
K_biii—Na_a—O2ii95.5 (3)Na_axxi—Ba—Mg_m2121.3 (3)
K_biii—Na_a—O651.2 (3)Na_av—Ba—Na_axiv33.9 (4)
K_biii—Na_a—O7v145.9 (7)Na_av—Ba—K_b98.5 (3)
K_biii—Na_a—Bavi109.9 (3)Na_av—Ba—Ti_m1(1)52.54 (14)
K_biii—Na_a—Bavii146.4 (6)Na_av—Ba—Ti_m1(1)xviii135.7 (3)
K_biii—Na_a—W132.07 (19)Na_av—Ba—Ti_m1(2)71.0 (2)
K_biii—Na_a—W2v123.7 (7)Na_av—Ba—Ti_m1(2)xv157.9 (2)
K_biii—Na_a—Nb_m1(1)ii114.1 (2)Na_av—Ba—Fe_m2121.3 (3)
Ti_m1(1)ii—Na_a—Ti_m1(2)iv161.1 (7)Na_av—Ba—Si2101.87 (12)
Ti_m1(1)ii—Na_a—Si2iv105.2 (5)Na_av—Ba—Si2x148.14 (18)
Ti_m1(1)ii—Na_a—O2ii31.3 (2)Na_av—Ba—O1xiii77.2 (3)
Ti_m1(1)ii—Na_a—O6132.9 (6)Na_av—Ba—O1xv126.5 (3)
Ti_m1(1)ii—Na_a—O7v75.9 (3)Na_av—Ba—O358.9 (3)
Ti_m1(1)ii—Na_a—Bavi130.1 (2)Na_av—Ba—O3x109.7 (4)
Ti_m1(1)ii—Na_a—Bavii61.44 (14)Na_av—Ba—Oh46.3 (2)
Ti_m1(1)ii—Na_a—W189.8 (3)Na_av—Ba—Ohx146.6 (2)
Ti_m1(1)ii—Na_a—W2v96.3 (3)Na_av—Ba—Baxvi55.17 (13)
Ti_m1(1)ii—Na_a—Nb_m1(1)ii0.0 (5)Na_av—Ba—Baxiii121.3 (3)
Ti_m1(2)iv—Na_a—Si2iv59.8 (3)Na_av—Ba—W226.7 (2)
Ti_m1(2)iv—Na_a—O2ii133.2 (8)Na_av—Ba—W2xvii85.9 (2)
Ti_m1(2)iv—Na_a—O634.8 (2)Na_av—Ba—W_c0
Ti_m1(2)iv—Na_a—O7v90.5 (5)Na_av—Ba—Nb_m1(1)52.54 (14)
Ti_m1(2)iv—Na_a—Bavi58.39 (14)Na_av—Ba—Nb_m1(1)xviii135.7 (3)
Ti_m1(2)iv—Na_a—Bavii125.5 (2)Na_av—Ba—Ti_m2121.3 (3)
Ti_m1(2)iv—Na_a—W1100.1 (3)Na_av—Ba—Mg_m2121.3 (3)
Ti_m1(2)iv—Na_a—W2v95.5 (3)Na_axiv—Ba—K_b125.9 (2)
Ti_m1(2)iv—Na_a—Nb_m1(1)ii161.1 (7)Na_axiv—Ba—Ti_m1(1)67.7 (2)
Si2iv—Na_a—O2ii96.7 (7)Na_axiv—Ba—Ti_m1(1)xviii162.89 (19)
Si2iv—Na_a—O670.2 (5)Na_axiv—Ba—Ti_m1(2)50.66 (17)
Si2iv—Na_a—O7v30.9 (3)Na_axiv—Ba—Ti_m1(2)xv129.0 (3)
Si2iv—Na_a—Bavi68.84 (19)Na_axiv—Ba—Fe_m289.8 (3)
Si2iv—Na_a—Bavii90.2 (2)Na_axiv—Ba—Si2100.07 (13)
Si2iv—Na_a—W1152.9 (6)Na_axiv—Ba—Si2x145.5 (2)
Si2iv—Na_a—W2v91.4 (4)Na_axiv—Ba—O1xiii44.4 (3)
Si2iv—Na_a—Nb_m1(1)ii105.2 (5)Na_axiv—Ba—O1xv96.2 (3)
O2ii—Na_a—O6101.6 (7)Na_axiv—Ba—O386.5 (3)
O2ii—Na_a—O7v76.7 (6)Na_axiv—Ba—O3x143.2 (4)
O2ii—Na_a—Bavi154.6 (4)Na_axiv—Ba—Oh44.01 (19)
O2ii—Na_a—Bavii91.1 (3)Na_axiv—Ba—Ohx145.1 (3)
O2ii—Na_a—W184.3 (4)Na_axiv—Ba—Baxvi55.89 (13)
O2ii—Na_a—W2v127.1 (4)Na_axiv—Ba—Baxiii89.8 (3)
O2ii—Na_a—Nb_m1(1)ii31.3 (2)Na_axiv—Ba—W227.3 (2)
O6—Na_a—O7v97.3 (8)Na_axiv—Ba—W2xvii86.6 (2)
O6—Na_a—Bavi93.2 (3)Na_axiv—Ba—W_c0
O6—Na_a—Bavii157.6 (4)Na_axiv—Ba—Nb_m1(1)67.7 (2)
O6—Na_a—W183.0 (4)Na_axiv—Ba—Nb_m1(1)xviii162.89 (19)
O6—Na_a—W2v129.9 (4)Na_axiv—Ba—Ti_m289.8 (3)
O6—Na_a—Nb_m1(1)ii132.9 (6)Na_axiv—Ba—Mg_m289.8 (3)
O7v—Na_a—Bavi81.0 (3)K_b—Ba—Ti_m1(1)59.58 (6)
O7v—Na_a—Bavii67.6 (3)K_b—Ba—Ti_m1(1)xviii59.58 (6)
O7v—Na_a—W1160.7 (7)K_b—Ba—Ti_m1(2)102.80 (7)
O7v—Na_a—W2v85.1 (4)K_b—Ba—Ti_m1(2)xv102.80 (7)
O7v—Na_a—Nb_m1(1)ii75.9 (3)K_b—Ba—Fe_m2112.51 (11)
Bavi—Na_a—Bavii68.94 (17)K_b—Ba—Si255.78 (13)
Bavi—Na_a—W1118.2 (7)K_b—Ba—Si2x55.78 (13)
Bavi—Na_a—W2v37.54 (17)K_b—Ba—O1xiii134.98 (14)
Bavi—Na_a—Nb_m1(1)ii130.1 (2)K_b—Ba—O1xv134.98 (14)
Bavii—Na_a—W1116.9 (7)K_b—Ba—O340.12 (14)
Bavii—Na_a—W2v36.57 (17)K_b—Ba—O3x40.12 (14)
Bavii—Na_a—Nb_m1(1)ii61.44 (14)K_b—Ba—Oh87.5 (2)
W1—Na_a—W2v109.6 (10)K_b—Ba—Ohx87.5 (2)
W1—Na_a—Nb_m1(1)ii89.8 (3)K_b—Ba—Baxvi130.29 (15)
W2v—Na_a—Nb_m1(1)ii96.3 (3)K_b—Ba—Baxiii112.51 (11)
Na_axi—K_b—Na_aiii32.3 (4)K_b—Ba—W2123.11 (16)
Na_axi—K_b—Na_aix127.24 (17)K_b—Ba—W2xvii123.11 (16)
Na_axi—K_b—Na_axix115.4 (3)K_b—Ba—W_c0
Na_axi—K_b—K_biii120.1 (2)K_b—Ba—Nb_m1(1)59.58 (6)
Na_axi—K_b—K_bviii62.78 (12)K_b—Ba—Nb_m1(1)xviii59.58 (6)
Na_axi—K_b—Si193.32 (12)K_b—Ba—Ti_m2112.51 (11)
Na_axi—K_b—Si1iii83.2 (3)K_b—Ba—Mg_m2112.51 (11)
Na_axi—K_b—Si1ix124.6 (3)Ti_m1(1)—Ba—Ti_m1(1)xviii119.01 (12)
Na_axi—K_b—Si1x142.63 (16)Ti_m1(1)—Ba—Ti_m1(2)55.11 (4)
Na_axi—K_b—Si249.4 (3)Ti_m1(1)—Ba—Ti_m1(2)xv146.45 (6)
Na_axi—K_b—Si2x91.2 (3)Ti_m1(1)—Ba—Fe_m2103.05 (5)
Na_axi—K_b—O375.20 (19)Ti_m1(1)—Ba—Si251.60 (7)
Na_axi—K_b—O3x135.5 (4)Ti_m1(1)—Ba—Si2x95.80 (8)
Na_axi—K_b—O4iii105.5 (3)Ti_m1(1)—Ba—O1xiii85.21 (18)
Na_axi—K_b—O569.8 (3)Ti_m1(1)—Ba—O1xv146.3 (2)
Na_axi—K_b—Ba93.9 (3)Ti_m1(1)—Ba—O328.7 (2)
Na_axi—K_b—W1xi22.3 (2)Ti_m1(1)—Ba—O3x94.6 (2)
Na_axi—K_b—W1ix106.7 (2)Ti_m1(1)—Ba—Oh29.0 (3)
Na_aiii—K_b—Na_aix118.2 (3)Ti_m1(1)—Ba—Ohx146.9 (2)
Na_aiii—K_b—Na_axix127.24 (17)Ti_m1(1)—Ba—Baxvi107.52 (6)
Na_aiii—K_b—K_biii93.1 (3)Ti_m1(1)—Ba—Baxiii103.05 (6)
Na_aiii—K_b—K_bviii64.46 (13)Ti_m1(1)—Ba—W278.05 (17)
Na_aiii—K_b—Si189.88 (13)Ti_m1(1)—Ba—W2xvii135.68 (17)
Na_aiii—K_b—Si1iii51.1 (3)Ti_m1(1)—Ba—W_c0
Na_aiii—K_b—Si1ix93.9 (3)Ti_m1(1)—Ba—Nb_m1(1)0.0 (5)
Na_aiii—K_b—Si1x138.2 (2)Ti_m1(1)—Ba—Nb_m1(1)xviii119.01 (12)
Na_aiii—K_b—Si281.4 (3)Ti_m1(1)—Ba—Ti_m2103.05 (5)
Na_aiii—K_b—Si2x122.2 (3)Ti_m1(1)—Ba—Mg_m2103.05 (5)
Na_aiii—K_b—O385.8 (2)Ti_m1(1)xviii—Ba—Ti_m1(2)146.45 (6)
Na_aiii—K_b—O3x155.60 (18)Ti_m1(1)xviii—Ba—Ti_m1(2)xv55.11 (4)
Na_aiii—K_b—O4iii73.3 (3)Ti_m1(1)xviii—Ba—Fe_m2103.05 (5)
Na_aiii—K_b—O5101.9 (3)Ti_m1(1)xviii—Ba—Si295.80 (8)
Na_aiii—K_b—Ba119.1 (2)Ti_m1(1)xviii—Ba—Si2x51.60 (7)
Na_aiii—K_b—W1xi23.7 (2)Ti_m1(1)xviii—Ba—O1xiii146.3 (2)
Na_aiii—K_b—W1ix108.3 (2)Ti_m1(1)xviii—Ba—O1xv85.21 (18)
Na_aix—K_b—Na_axix32.3 (4)Ti_m1(1)xviii—Ba—O394.6 (2)
Na_aix—K_b—K_biii93.1 (3)Ti_m1(1)xviii—Ba—O3x28.7 (2)
Na_aix—K_b—K_bviii64.46 (13)Ti_m1(1)xviii—Ba—Oh146.9 (2)
Na_aix—K_b—Si1138.2 (2)Ti_m1(1)xviii—Ba—Ohx29.0 (3)
Na_aix—K_b—Si1iii93.9 (3)Ti_m1(1)xviii—Ba—Baxvi107.52 (6)
Na_aix—K_b—Si1ix51.1 (3)Ti_m1(1)xviii—Ba—Baxiii103.05 (6)
Na_aix—K_b—Si1x89.88 (13)Ti_m1(1)xviii—Ba—W2135.68 (17)
Na_aix—K_b—Si2122.2 (3)Ti_m1(1)xviii—Ba—W2xvii78.05 (17)
Na_aix—K_b—Si2x81.4 (3)Ti_m1(1)xviii—Ba—W_c0
Na_aix—K_b—O3155.60 (18)Ti_m1(1)xviii—Ba—Nb_m1(1)119.01 (12)
Na_aix—K_b—O3x85.8 (2)Ti_m1(1)xviii—Ba—Nb_m1(1)xviii0.0 (5)
Na_aix—K_b—O4iii73.3 (3)Ti_m1(1)xviii—Ba—Ti_m2103.05 (5)
Na_aix—K_b—O5101.9 (3)Ti_m1(1)xviii—Ba—Mg_m2103.05 (5)
Na_aix—K_b—Ba119.1 (2)Ti_m1(2)—Ba—Ti_m1(2)xv109.28 (12)
Na_aix—K_b—W1xi108.3 (2)Ti_m1(2)—Ba—Fe_m254.64 (6)
Na_aix—K_b—W1ix23.7 (2)Ti_m1(2)—Ba—Si253.26 (8)
Na_axix—K_b—K_biii120.1 (2)Ti_m1(2)—Ba—Si2x94.90 (9)
Na_axix—K_b—K_bviii62.78 (12)Ti_m1(2)—Ba—O1xiii32.91 (15)
Na_axix—K_b—Si1142.63 (16)Ti_m1(2)—Ba—O1xv91.5 (2)
Na_axix—K_b—Si1iii124.6 (3)Ti_m1(2)—Ba—O383.7 (2)
Na_axix—K_b—Si1ix83.2 (3)Ti_m1(2)—Ba—O3x142.85 (14)
Na_axix—K_b—Si1x93.32 (12)Ti_m1(2)—Ba—Oh31.0 (3)
Na_axix—K_b—Si291.2 (3)Ti_m1(2)—Ba—Ohx139.8 (3)
Na_axix—K_b—Si2x49.4 (3)Ti_m1(2)—Ba—Baxvi105.34 (7)
Na_axix—K_b—O3135.5 (4)Ti_m1(2)—Ba—Baxiii54.64 (6)
Na_axix—K_b—O3x75.20 (19)Ti_m1(2)—Ba—W277.69 (16)
Na_axix—K_b—O4iii105.5 (3)Ti_m1(2)—Ba—W2xvii131.29 (17)
Na_axix—K_b—O569.8 (3)Ti_m1(2)—Ba—W_c0
Na_axix—K_b—Ba93.9 (3)Ti_m1(2)—Ba—Nb_m1(1)55.11 (4)
Na_axix—K_b—W1xi106.7 (2)Ti_m1(2)—Ba—Nb_m1(1)xviii146.45 (6)
Na_axix—K_b—W1ix22.3 (2)Ti_m1(2)—Ba—Ti_m254.64 (6)
K_biii—K_b—K_bviii129.0 (2)Ti_m1(2)—Ba—Mg_m254.64 (6)
K_biii—K_b—Si152.51 (15)Ti_m1(2)xv—Ba—Fe_m254.64 (6)
K_biii—K_b—Si1iii47.75 (11)Ti_m1(2)xv—Ba—Si294.90 (9)
K_biii—K_b—Si1ix47.75 (11)Ti_m1(2)xv—Ba—Si2x53.26 (8)
K_biii—K_b—Si1x52.51 (15)Ti_m1(2)xv—Ba—O1xiii91.5 (2)
K_biii—K_b—Si2142.64 (9)Ti_m1(2)xv—Ba—O1xv32.91 (15)
K_biii—K_b—Si2x142.64 (9)Ti_m1(2)xv—Ba—O3142.85 (14)
K_biii—K_b—O380.5 (3)Ti_m1(2)xv—Ba—O3x83.7 (2)
K_biii—K_b—O3x80.5 (3)Ti_m1(2)xv—Ba—Oh139.8 (3)
K_biii—K_b—O4iii40.1 (2)Ti_m1(2)xv—Ba—Ohx31.0 (3)
K_biii—K_b—O5150.2 (2)Ti_m1(2)xv—Ba—Baxvi105.34 (7)
K_biii—K_b—Ba102.60 (11)Ti_m1(2)xv—Ba—Baxiii54.64 (6)
K_biii—K_b—W1xi116.0 (2)Ti_m1(2)xv—Ba—W2131.29 (17)
K_biii—K_b—W1ix116.0 (2)Ti_m1(2)xv—Ba—W2xvii77.69 (16)
K_bviii—K_b—Si1153.94 (5)Ti_m1(2)xv—Ba—W_c0
K_bviii—K_b—Si1iii86.68 (17)Ti_m1(2)xv—Ba—Nb_m1(1)146.45 (6)
K_bviii—K_b—Si1ix86.68 (17)Ti_m1(2)xv—Ba—Nb_m1(1)xviii55.11 (4)
K_bviii—K_b—Si1x153.94 (5)Ti_m1(2)xv—Ba—Ti_m254.64 (6)
K_bviii—K_b—Si281.75 (17)Ti_m1(2)xv—Ba—Mg_m254.64 (6)
K_bviii—K_b—Si2x81.75 (17)Fe_m2—Ba—Si263.70 (12)
K_bviii—K_b—O3136.7 (2)Fe_m2—Ba—Si2x63.70 (12)
K_bviii—K_b—O3x136.7 (2)Fe_m2—Ba—O1xiii45.39 (18)
K_bviii—K_b—O4iii88.9 (2)Fe_m2—Ba—O1xv45.39 (18)
K_bviii—K_b—O580.8 (2)Fe_m2—Ba—O3126.4 (2)
K_bviii—K_b—Ba128.4 (2)Fe_m2—Ba—O3x126.4 (2)
K_bviii—K_b—W1xi45.81 (15)Fe_m2—Ba—Oh85.4 (3)
K_bviii—K_b—W1ix45.81 (15)Fe_m2—Ba—Ohx85.4 (3)
Si1—K_b—Si1iii79.86 (17)Fe_m2—Ba—Baxvi117.19 (16)
Si1—K_b—Si1ix100.3 (2)Fe_m2—Ba—Baxiii0.0 (5)
Si1—K_b—Si1x51.67 (6)Fe_m2—Ba—W2112.71 (17)
Si1—K_b—Si290.37 (16)Fe_m2—Ba—W2xvii112.71 (17)
Si1—K_b—Si2x110.7 (2)Fe_m2—Ba—W_c0
Si1—K_b—O328.1 (3)Fe_m2—Ba—Nb_m1(1)103.05 (5)
Si1—K_b—O3x67.48 (15)Fe_m2—Ba—Nb_m1(1)xviii103.05 (5)
Si1—K_b—O4iii87.8 (2)Fe_m2—Ba—Ti_m20.0 (5)
Si1—K_b—O5101.5 (3)Fe_m2—Ba—Mg_m20.0 (5)
Si1—K_b—Ba59.04 (14)Si2—Ba—Si2x49.55 (5)
Si1—K_b—W1xi108.28 (15)Si2—Ba—O1xiii80.91 (16)
Si1—K_b—W1ix159.82 (17)Si2—Ba—O1xv106.7 (2)
Si1iii—K_b—Si1ix47.97 (12)Si2—Ba—O364.49 (19)
Si1iii—K_b—Si1x100.3 (2)Si2—Ba—O3x92.02 (16)
Si1iii—K_b—Si2131.05 (8)Si2—Ba—Oh58.98 (11)
Si1iii—K_b—Si2x168.43 (10)Si2—Ba—Ohx108.50 (12)
Si1iii—K_b—O398.8 (3)Si2—Ba—Baxvi155.15 (4)
Si1iii—K_b—O3x128.2 (3)Si2—Ba—Baxiii63.70 (13)
Si1iii—K_b—O4iii24.11 (7)Si2—Ba—W2122.83 (18)
Si1iii—K_b—O5152.97 (11)Si2—Ba—W2xvii172.21 (18)
Si1iii—K_b—Ba138.62 (10)Si2—Ba—W_c0
Si1iii—K_b—W1xi70.62 (14)Si2—Ba—Nb_m1(1)51.60 (7)
Si1iii—K_b—W1ix104.5 (2)Si2—Ba—Nb_m1(1)xviii95.80 (8)
Si1ix—K_b—Si1x79.86 (17)Si2—Ba—Ti_m263.70 (12)
Si1ix—K_b—Si2168.43 (10)Si2—Ba—Mg_m263.70 (12)
Si1ix—K_b—Si2x131.05 (8)Si2x—Ba—O1xiii106.7 (2)
Si1ix—K_b—O3128.2 (3)Si2x—Ba—O1xv80.91 (16)
Si1ix—K_b—O3x98.8 (3)Si2x—Ba—O392.02 (16)
Si1ix—K_b—O4iii24.11 (7)Si2x—Ba—O3x64.49 (19)
Si1ix—K_b—O5152.97 (11)Si2x—Ba—Oh108.50 (12)
Si1ix—K_b—Ba138.62 (10)Si2x—Ba—Ohx58.98 (11)
Si1ix—K_b—W1xi104.5 (2)Si2x—Ba—Baxvi155.15 (4)
Si1ix—K_b—W1ix70.62 (14)Si2x—Ba—Baxiii63.70 (13)
Si1x—K_b—Si2110.7 (2)Si2x—Ba—W2172.21 (18)
Si1x—K_b—Si2x90.37 (16)Si2x—Ba—W2xvii122.83 (18)
Si1x—K_b—O367.48 (15)Si2x—Ba—W_c0
Si1x—K_b—O3x28.1 (3)Si2x—Ba—Nb_m1(1)95.80 (8)
Si1x—K_b—O4iii87.8 (2)Si2x—Ba—Nb_m1(1)xviii51.60 (7)
Si1x—K_b—O5101.5 (3)Si2x—Ba—Ti_m263.70 (12)
Si1x—K_b—Ba59.04 (14)Si2x—Ba—Mg_m263.70 (12)
Si1x—K_b—W1xi159.82 (17)O1xiii—Ba—O1xv64.2 (3)
Si1x—K_b—W1ix108.28 (15)O1xiii—Ba—O3113.4 (3)
Si2—K_b—Si2x46.81 (12)O1xiii—Ba—O3x171.1 (2)
Si2—K_b—O362.3 (3)O1xiii—Ba—Oh56.9 (3)
Si2—K_b—O3x89.4 (4)O1xiii—Ba—Ohx120.6 (4)
Si2—K_b—O4iii154.63 (10)O1xiii—Ba—Baxvi84.22 (15)
Si2—K_b—O523.41 (7)O1xiii—Ba—Baxiii45.39 (18)
Si2—K_b—Ba51.61 (12)O1xiii—Ba—W268.32 (18)
Si2—K_b—W1xi67.37 (14)O1xiii—Ba—W2xvii101.5 (2)
Si2—K_b—W1ix100.7 (2)O1xiii—Ba—W_c0
Si2x—K_b—O389.4 (4)O1xiii—Ba—Nb_m1(1)85.21 (18)
Si2x—K_b—O3x62.3 (3)O1xiii—Ba—Nb_m1(1)xviii146.3 (2)
Si2x—K_b—O4iii154.63 (10)O1xiii—Ba—Ti_m245.39 (18)
Si2x—K_b—O523.41 (7)O1xiii—Ba—Mg_m245.39 (18)
Si2x—K_b—Ba51.61 (12)O1xv—Ba—O3171.1 (2)
Si2x—K_b—W1xi100.7 (2)O1xv—Ba—O3x113.4 (3)
Si2x—K_b—W1ix67.37 (14)O1xv—Ba—Oh120.6 (4)
O3—K_b—O3x69.9 (2)O1xv—Ba—Ohx56.9 (3)
O3—K_b—O4iii113.0 (4)O1xv—Ba—Baxvi84.22 (15)
O3—K_b—O575.2 (4)O1xv—Ba—Baxiii45.39 (18)
O3—K_b—Ba41.6 (3)O1xv—Ba—W2101.5 (2)
O3—K_b—W1xi95.53 (19)O1xv—Ba—W2xvii68.32 (18)
O3—K_b—W1ix156.6 (4)O1xv—Ba—W_c0
O3x—K_b—O4iii113.0 (4)O1xv—Ba—Nb_m1(1)146.3 (2)
O3x—K_b—O575.2 (4)O1xv—Ba—Nb_m1(1)xviii85.21 (18)
O3x—K_b—Ba41.6 (3)O1xv—Ba—Ti_m245.39 (18)
O3x—K_b—W1xi156.6 (4)O1xv—Ba—Mg_m245.39 (18)
O3x—K_b—W1ix95.53 (19)O3—Ba—O3x67.6 (3)
O4iii—K_b—O5169.7 (3)O3—Ba—Oh56.5 (3)
O4iii—K_b—Ba142.7 (2)O3—Ba—Ohx123.6 (3)
O4iii—K_b—W1xi89.2 (2)O3—Ba—Baxvi104.24 (16)
O4iii—K_b—W1ix89.2 (2)O3—Ba—Baxiii126.4 (2)
O5—K_b—Ba47.6 (2)O3—Ba—W284.84 (18)
O5—K_b—W1xi83.6 (2)O3—Ba—W2xvii120.4 (2)
O5—K_b—W1ix83.6 (2)O3—Ba—W_c0
Ba—K_b—W1xi115.7 (2)O3—Ba—Nb_m1(1)28.7 (2)
Ba—K_b—W1ix115.7 (2)O3—Ba—Nb_m1(1)xviii94.6 (2)
W1xi—K_b—W1ix91.6 (2)O3—Ba—Ti_m2126.4 (2)
Na_axi—Ti_m1(1)—Na_av180.0 (5)O3—Ba—Mg_m2126.4 (2)
Na_axi—Ti_m1(1)—O237.8 (4)O3x—Ba—Oh123.6 (3)
Na_axi—Ti_m1(1)—O2iv142.2 (4)O3x—Ba—Ohx56.5 (3)
Na_axi—Ti_m1(1)—O3105.1 (3)O3x—Ba—Baxvi104.24 (16)
Na_axi—Ti_m1(1)—O3iv74.9 (3)O3x—Ba—Baxiii126.4 (2)
Na_axi—Ti_m1(1)—Oh123.7 (4)O3x—Ba—W2120.4 (2)
Na_axi—Ti_m1(1)—Ohiv56.3 (4)O3x—Ba—W2xvii84.84 (18)
Na_axi—Ti_m1(1)—Ba113.98 (18)O3x—Ba—W_c0
Na_axi—Ti_m1(1)—Baxii66.02 (18)O3x—Ba—Nb_m1(1)94.6 (2)
Na_axi—Ti_m1(1)—Nb_m1(1)0O3x—Ba—Nb_m1(1)xviii28.7 (2)
Na_av—Ti_m1(1)—O2142.2 (4)O3x—Ba—Ti_m2126.4 (2)
Na_av—Ti_m1(1)—O2iv37.8 (4)O3x—Ba—Mg_m2126.4 (2)
Na_av—Ti_m1(1)—O374.9 (3)Oh—Ba—Ohx167.0 (2)
Na_av—Ti_m1(1)—O3iv105.1 (3)Oh—Ba—Baxvi96.19 (11)
Na_av—Ti_m1(1)—Oh56.3 (4)Oh—Ba—Baxiii85.4 (3)
Na_av—Ti_m1(1)—Ohiv123.7 (4)Oh—Ba—W263.9 (2)
Na_av—Ti_m1(1)—Ba66.02 (18)Oh—Ba—W2xvii128.5 (2)
Na_av—Ti_m1(1)—Baxii113.98 (18)Oh—Ba—W_c0
Na_av—Ti_m1(1)—Nb_m1(1)0Oh—Ba—Nb_m1(1)29.0 (3)
O2—Ti_m1(1)—O2iv180.0 (5)Oh—Ba—Nb_m1(1)xviii146.9 (2)
O2—Ti_m1(1)—O388.6 (3)Oh—Ba—Ti_m285.4 (3)
O2—Ti_m1(1)—O3iv91.4 (3)Oh—Ba—Mg_m285.4 (3)
O2—Ti_m1(1)—Oh89.9 (4)Ohx—Ba—Baxvi96.19 (11)
O2—Ti_m1(1)—Ohiv90.1 (4)Ohx—Ba—Baxiii85.4 (3)
O2—Ti_m1(1)—Ba78.2 (2)Ohx—Ba—W2128.5 (2)
O2—Ti_m1(1)—Baxii101.8 (2)Ohx—Ba—W2xvii63.9 (2)
O2—Ti_m1(1)—Nb_m1(1)0Ohx—Ba—W_c0
O2iv—Ti_m1(1)—O391.4 (3)Ohx—Ba—Nb_m1(1)146.9 (2)
O2iv—Ti_m1(1)—O3iv88.6 (3)Ohx—Ba—Nb_m1(1)xviii29.0 (3)
O2iv—Ti_m1(1)—Oh90.1 (4)Ohx—Ba—Ti_m285.4 (3)
O2iv—Ti_m1(1)—Ohiv89.9 (4)Ohx—Ba—Mg_m285.4 (3)
O2iv—Ti_m1(1)—Ba101.8 (2)Baxvi—Ba—Baxiii117.19 (14)
O2iv—Ti_m1(1)—Baxii78.2 (2)Baxvi—Ba—W232.36 (17)
O2iv—Ti_m1(1)—Nb_m1(1)0Baxvi—Ba—W2xvii32.36 (17)
O3—Ti_m1(1)—O3iv180.0 (5)Baxvi—Ba—W_c0
O3—Ti_m1(1)—Oh87.8 (5)Baxvi—Ba—Nb_m1(1)107.52 (6)
O3—Ti_m1(1)—Ohiv92.2 (5)Baxvi—Ba—Nb_m1(1)xviii107.52 (6)
O3—Ti_m1(1)—Ba44.6 (4)Baxvi—Ba—Ti_m2117.19 (16)
O3—Ti_m1(1)—Baxii135.4 (4)Baxvi—Ba—Mg_m2117.19 (16)
O3—Ti_m1(1)—Nb_m1(1)0Baxiii—Ba—W2112.71 (15)
O3iv—Ti_m1(1)—Oh92.2 (5)Baxiii—Ba—W2xvii112.71 (15)
O3iv—Ti_m1(1)—Ohiv87.8 (5)Baxiii—Ba—W_c0
O3iv—Ti_m1(1)—Ba135.4 (4)Baxiii—Ba—Nb_m1(1)103.05 (6)
O3iv—Ti_m1(1)—Baxii44.6 (4)Baxiii—Ba—Nb_m1(1)xviii103.05 (6)
O3iv—Ti_m1(1)—Nb_m1(1)0Baxiii—Ba—Ti_m20.0 (5)
Oh—Ti_m1(1)—Ohiv180.0 (5)Baxiii—Ba—Mg_m20.0 (5)
Oh—Ti_m1(1)—Ba45.35 (19)W2—Ba—W2xvii64.7 (2)
Oh—Ti_m1(1)—Baxii134.65 (19)W2—Ba—W_c0
Oh—Ti_m1(1)—Nb_m1(1)0W2—Ba—Nb_m1(1)78.05 (17)
Ohiv—Ti_m1(1)—Ba134.65 (19)W2—Ba—Nb_m1(1)xviii135.68 (17)
Ohiv—Ti_m1(1)—Baxii45.35 (19)W2—Ba—Ti_m2112.71 (17)
Ohiv—Ti_m1(1)—Nb_m1(1)0W2—Ba—Mg_m2112.71 (17)
Ba—Ti_m1(1)—Baxii180.0 (5)W2xvii—Ba—W_c0
Ba—Ti_m1(1)—Nb_m1(1)0W2xvii—Ba—Nb_m1(1)135.68 (17)
Baxii—Ti_m1(1)—Nb_m1(1)0W2xvii—Ba—Nb_m1(1)xviii78.05 (17)
Na_aiv—Ti_m1(2)—Na_axiv174.43 (19)W2xvii—Ba—Ti_m2112.71 (17)
Na_aiv—Ti_m1(2)—O158.5 (3)W2xvii—Ba—Mg_m2112.71 (17)
Na_aiv—Ti_m1(2)—O1xiii126.5 (3)W_c—Ba—Nb_m1(1)0
Na_aiv—Ti_m1(2)—O6iv44.3 (3)W_c—Ba—Nb_m1(1)xviii0
Na_aiv—Ti_m1(2)—O6xiv130.7 (3)W_c—Ba—Ti_m20
Na_aiv—Ti_m1(2)—Oh122.3 (4)W_c—Ba—Mg_m20
Na_aiv—Ti_m1(2)—Ohxiii58.0 (4)Nb_m1(1)—Ba—Nb_m1(1)xviii119.01 (12)
Na_aiv—Ti_m1(2)—Ba113.9 (2)Nb_m1(1)—Ba—Ti_m2103.05 (5)
Na_aiv—Ti_m1(2)—Baxiii70.9 (2)Nb_m1(1)—Ba—Mg_m2103.05 (5)
Na_aiv—Ti_m1(2)—Ti_m292.78 (13)Nb_m1(1)xviii—Ba—Ti_m2103.05 (5)
Na_aiv—Ti_m1(2)—Mg_m292.78 (13)Nb_m1(1)xviii—Ba—Mg_m2103.05 (5)
Na_axiv—Ti_m1(2)—O1126.5 (3)Ti_m2—Ba—Mg_m20.0 (5)
Na_axiv—Ti_m1(2)—O1xiii58.5 (3)Na_a—W1—Na_ai70.4 (8)
Na_axiv—Ti_m1(2)—O6iv130.7 (3)Na_a—W1—K_bii127.6 (3)
Na_axiv—Ti_m1(2)—O6xiv44.3 (3)Na_a—W1—K_biii124.2 (4)
Na_axiv—Ti_m1(2)—Oh58.0 (4)Na_ai—W1—K_bii124.2 (4)
Na_axiv—Ti_m1(2)—Ohxiii122.3 (4)Na_ai—W1—K_biii127.6 (3)
Na_axiv—Ti_m1(2)—Ba70.9 (2)K_bii—W1—K_biii88.4 (3)
Na_axiv—Ti_m1(2)—Baxiii113.9 (2)Na_av—W2—Na_axiv70.5 (8)
Na_axiv—Ti_m1(2)—Ti_m292.78 (13)Na_av—W2—Ba116.7 (3)
Na_axiv—Ti_m1(2)—Mg_m292.78 (13)Na_av—W2—Baxvi115.1 (3)
O1—Ti_m1(2)—O1xiii83.0 (3)Na_axiv—W2—Ba115.1 (3)
O1—Ti_m1(2)—O6iv89.8 (3)Na_axiv—W2—Baxvi116.7 (3)
O1—Ti_m1(2)—O6xiv170.9 (3)Ba—W2—Baxvi115.3 (3)
O1—Ti_m1(2)—Oh87.8 (4)Fe_m2—W_c—Ba0
O1—Ti_m1(2)—Ohxiii87.9 (5)Fe_m2—W_c—Ti_m20.0 (5)
O1—Ti_m1(2)—Ba55.6 (2)Fe_m2—W_c—Mg_m20.0 (5)
O1—Ti_m1(2)—Baxiii48.9 (4)Ba—W_c—Ti_m20
O1—Ti_m1(2)—Ti_m241.50 (18)Ba—W_c—Mg_m20
O1—Ti_m1(2)—Mg_m241.50 (18)Ti_m2—W_c—Mg_m20.0 (5)
O1xiii—Ti_m1(2)—O6iv170.9 (3)Na_axi—Nb_m1(1)—Na_av180.0 (5)
O1xiii—Ti_m1(2)—O6xiv89.8 (3)Na_axi—Nb_m1(1)—Ti_m1(1)0
O1xiii—Ti_m1(2)—Oh87.9 (5)Na_axi—Nb_m1(1)—O237.8 (4)
O1xiii—Ti_m1(2)—Ohxiii87.8 (4)Na_axi—Nb_m1(1)—O2iv142.2 (4)
O1xiii—Ti_m1(2)—Ba48.9 (4)Na_axi—Nb_m1(1)—O3105.1 (3)
O1xiii—Ti_m1(2)—Baxiii55.6 (2)Na_axi—Nb_m1(1)—O3iv74.9 (3)
O1xiii—Ti_m1(2)—Ti_m241.50 (18)Na_axi—Nb_m1(1)—Oh123.7 (4)
O1xiii—Ti_m1(2)—Mg_m241.50 (18)Na_axi—Nb_m1(1)—Ohiv56.3 (4)
O6iv—Ti_m1(2)—O6xiv98.0 (3)Na_axi—Nb_m1(1)—Ba113.98 (18)
O6iv—Ti_m1(2)—Oh97.4 (5)Na_axi—Nb_m1(1)—Baxii66.02 (18)
O6iv—Ti_m1(2)—Ohxiii86.4 (5)Na_av—Nb_m1(1)—Ti_m1(1)0
O6iv—Ti_m1(2)—Ba130.1 (4)Na_av—Nb_m1(1)—O2142.2 (4)
O6iv—Ti_m1(2)—Baxiii115.3 (3)Na_av—Nb_m1(1)—O2iv37.8 (4)
O6iv—Ti_m1(2)—Ti_m2131.02 (19)Na_av—Nb_m1(1)—O374.9 (3)
O6iv—Ti_m1(2)—Mg_m2131.02 (19)Na_av—Nb_m1(1)—O3iv105.1 (3)
O6xiv—Ti_m1(2)—Oh86.4 (5)Na_av—Nb_m1(1)—Oh56.3 (4)
O6xiv—Ti_m1(2)—Ohxiii97.4 (5)Na_av—Nb_m1(1)—Ohiv123.7 (4)
O6xiv—Ti_m1(2)—Ba115.3 (3)Na_av—Nb_m1(1)—Ba66.02 (18)
O6xiv—Ti_m1(2)—Baxiii130.1 (4)Na_av—Nb_m1(1)—Baxii113.98 (18)
O6xiv—Ti_m1(2)—Ti_m2131.02 (19)Ti_m1(1)—Nb_m1(1)—O20
O6xiv—Ti_m1(2)—Mg_m2131.02 (19)Ti_m1(1)—Nb_m1(1)—O2iv0
Oh—Ti_m1(2)—Ohxiii174.3 (2)Ti_m1(1)—Nb_m1(1)—O30
Oh—Ti_m1(2)—Ba52.11 (17)Ti_m1(1)—Nb_m1(1)—O3iv0
Oh—Ti_m1(2)—Baxiii122.21 (18)Ti_m1(1)—Nb_m1(1)—Oh0
Oh—Ti_m1(2)—Ti_m287.15 (16)Ti_m1(1)—Nb_m1(1)—Ohiv0
Oh—Ti_m1(2)—Mg_m287.15 (16)Ti_m1(1)—Nb_m1(1)—Ba0
Ohxiii—Ti_m1(2)—Ba122.21 (18)Ti_m1(1)—Nb_m1(1)—Baxii0
Ohxiii—Ti_m1(2)—Baxiii52.11 (17)O2—Nb_m1(1)—O2iv180.0 (5)
Ohxiii—Ti_m1(2)—Ti_m287.15 (16)O2—Nb_m1(1)—O388.6 (3)
Ohxiii—Ti_m1(2)—Mg_m287.15 (16)O2—Nb_m1(1)—O3iv91.4 (3)
Ba—Ti_m1(2)—Baxiii70.72 (9)O2—Nb_m1(1)—Oh89.9 (4)
Ba—Ti_m1(2)—Ti_m235.36 (6)O2—Nb_m1(1)—Ohiv90.1 (4)
Ba—Ti_m1(2)—Mg_m235.36 (6)O2—Nb_m1(1)—Ba78.2 (2)
Baxiii—Ti_m1(2)—Ti_m235.36 (6)O2—Nb_m1(1)—Baxii101.8 (2)
Baxiii—Ti_m1(2)—Mg_m235.36 (6)O2iv—Nb_m1(1)—O391.4 (3)
Ti_m2—Ti_m1(2)—Mg_m20.0 (5)O2iv—Nb_m1(1)—O3iv88.6 (3)
O1—Fe_m2—O1xiii83.9 (3)O2iv—Nb_m1(1)—Oh90.1 (4)
O1—Fe_m2—O1xv180.0 (5)O2iv—Nb_m1(1)—Ohiv89.9 (4)
O1—Fe_m2—O1x96.1 (3)O2iv—Nb_m1(1)—Ba101.8 (2)
O1—Fe_m2—Ba94.6 (4)O2iv—Nb_m1(1)—Baxii78.2 (2)
O1—Fe_m2—Baxiii85.4 (4)O3—Nb_m1(1)—O3iv180.0 (5)
O1—Fe_m2—W_c94.6 (4)O3—Nb_m1(1)—Oh87.8 (5)
O1—Fe_m2—W_cxiii85.4 (4)O3—Nb_m1(1)—Ohiv92.2 (5)
O1—Fe_m2—Ti_m20O3—Nb_m1(1)—Ba44.6 (4)
O1—Fe_m2—Mg_m20O3—Nb_m1(1)—Baxii135.4 (4)
O1xiii—Fe_m2—O1xv96.1 (3)O3iv—Nb_m1(1)—Oh92.2 (5)
O1xiii—Fe_m2—O1x180.0 (5)O3iv—Nb_m1(1)—Ohiv87.8 (5)
O1xiii—Fe_m2—Ba85.4 (4)O3iv—Nb_m1(1)—Ba135.4 (4)
O1xiii—Fe_m2—Baxiii94.6 (4)O3iv—Nb_m1(1)—Baxii44.6 (4)
O1xiii—Fe_m2—W_c85.4 (4)Oh—Nb_m1(1)—Ohiv180.0 (5)
O1xiii—Fe_m2—W_cxiii94.6 (4)Oh—Nb_m1(1)—Ba45.35 (19)
O1xiii—Fe_m2—Ti_m20Oh—Nb_m1(1)—Baxii134.65 (19)
O1xiii—Fe_m2—Mg_m20Ohiv—Nb_m1(1)—Ba134.65 (19)
O1xv—Fe_m2—O1x83.9 (3)Ohiv—Nb_m1(1)—Baxii45.35 (19)
O1xv—Fe_m2—Ba85.4 (4)Ba—Nb_m1(1)—Baxii180.0 (5)
O1xv—Fe_m2—Baxiii94.6 (4)Ti_m1(2)—Ti_m2—Ti_m1(2)xv180.0 (5)
O1xv—Fe_m2—W_c85.4 (4)Ti_m1(2)—Ti_m2—Fe_m20
O1xv—Fe_m2—W_cxiii94.6 (4)Ti_m1(2)—Ti_m2—O141.96 (18)
O1xv—Fe_m2—Ti_m20Ti_m1(2)—Ti_m2—O1xiii41.96 (18)
O1xv—Fe_m2—Mg_m20Ti_m1(2)—Ti_m2—O1xv138.04 (18)
O1x—Fe_m2—Ba94.6 (4)Ti_m1(2)—Ti_m2—O1x138.04 (18)
O1x—Fe_m2—Baxiii85.4 (4)Ti_m1(2)—Ti_m2—Ba90
O1x—Fe_m2—W_c94.6 (4)Ti_m1(2)—Ti_m2—Baxiii90
O1x—Fe_m2—W_cxiii85.4 (4)Ti_m1(2)—Ti_m2—W_c90
O1x—Fe_m2—Ti_m20Ti_m1(2)—Ti_m2—W_cxiii90
O1x—Fe_m2—Mg_m20Ti_m1(2)—Ti_m2—Mg_m20
Ba—Fe_m2—Baxiii180.0 (5)Ti_m1(2)xv—Ti_m2—Fe_m20
Ba—Fe_m2—W_c0.0 (5)Ti_m1(2)xv—Ti_m2—O1138.04 (18)
Ba—Fe_m2—W_cxiii180.0 (5)Ti_m1(2)xv—Ti_m2—O1xiii138.04 (18)
Ba—Fe_m2—Ti_m20Ti_m1(2)xv—Ti_m2—O1xv41.96 (18)
Ba—Fe_m2—Mg_m20Ti_m1(2)xv—Ti_m2—O1x41.96 (18)
Baxiii—Fe_m2—W_c180.0 (5)Ti_m1(2)xv—Ti_m2—Ba90
Baxiii—Fe_m2—W_cxiii0.0 (5)Ti_m1(2)xv—Ti_m2—Baxiii90
Baxiii—Fe_m2—Ti_m20Ti_m1(2)xv—Ti_m2—W_c90
Baxiii—Fe_m2—Mg_m20Ti_m1(2)xv—Ti_m2—W_cxiii90
W_c—Fe_m2—W_cxiii180.0 (5)Ti_m1(2)xv—Ti_m2—Mg_m20
W_c—Fe_m2—Ti_m20Fe_m2—Ti_m2—O10
W_c—Fe_m2—Mg_m20Fe_m2—Ti_m2—O1xiii0
W_cxiii—Fe_m2—Ti_m20Fe_m2—Ti_m2—O1xv0
W_cxiii—Fe_m2—Mg_m20Fe_m2—Ti_m2—O1x0
Ti_m2—Fe_m2—Mg_m20Fe_m2—Ti_m2—Ba0
K_b—Si1—K_biii79.74 (16)Fe_m2—Ti_m2—Baxiii0
K_b—Si1—O353.8 (3)Fe_m2—Ti_m2—W_c0
K_b—Si1—O462.9 (4)Fe_m2—Ti_m2—W_cxiii0
K_b—Si1—O6100.8 (3)Fe_m2—Ti_m2—Mg_m20
K_b—Si1—O7147.4 (5)O1—Ti_m2—O1xiii83.9 (3)
K_biii—Si1—O3133.3 (3)O1—Ti_m2—O1xv180.0 (5)
K_biii—Si1—O440.6 (7)O1—Ti_m2—O1x96.1 (3)
K_biii—Si1—O664.3 (4)O1—Ti_m2—Ba94.6 (4)
K_biii—Si1—O7115.2 (5)O1—Ti_m2—Baxiii85.4 (4)
O3—Si1—O4108.7 (6)O1—Ti_m2—W_c94.6 (4)
O3—Si1—O6115.9 (5)O1—Ti_m2—W_cxiii85.4 (4)
O3—Si1—O7107.6 (7)O1—Ti_m2—Mg_m20
O4—Si1—O6104.1 (8)O1xiii—Ti_m2—O1xv96.1 (3)
O4—Si1—O7108.5 (4)O1xiii—Ti_m2—O1x180.0 (5)
O6—Si1—O7111.8 (5)O1xiii—Ti_m2—Ba85.4 (4)
Na_aiv—Si2—K_b164.1 (3)O1xiii—Ti_m2—Baxiii94.6 (4)
Na_aiv—Si2—O164.3 (4)O1xiii—Ti_m2—W_c85.4 (4)
Na_aiv—Si2—O2101.8 (4)O1xiii—Ti_m2—W_cxiii94.6 (4)
Na_aiv—Si2—O5148.7 (6)O1xiii—Ti_m2—Mg_m20
Na_aiv—Si2—O7xi49.2 (4)O1xv—Ti_m2—O1x83.9 (3)
Na_aiv—Si2—Ba122.6 (3)O1xv—Ti_m2—Ba85.4 (4)
K_b—Si2—O1131.2 (3)O1xv—Ti_m2—Baxiii94.6 (4)
K_b—Si2—O269.9 (4)O1xv—Ti_m2—W_c85.4 (4)
K_b—Si2—O538.1 (7)O1xv—Ti_m2—W_cxiii94.6 (4)
K_b—Si2—O7xi120.2 (5)O1xv—Ti_m2—Mg_m20
K_b—Si2—Ba72.61 (14)O1x—Ti_m2—Ba94.6 (4)
O1—Si2—O2114.5 (4)O1x—Ti_m2—Baxiii85.4 (4)
O1—Si2—O5110.2 (6)O1x—Ti_m2—W_c94.6 (4)
O1—Si2—O7xi103.3 (7)O1x—Ti_m2—W_cxiii85.4 (4)
O1—Si2—Ba58.6 (3)O1x—Ti_m2—Mg_m20
O2—Si2—O5107.9 (8)Ba—Ti_m2—Baxiii180.0 (5)
O2—Si2—O7xi112.4 (4)Ba—Ti_m2—W_c0.0 (5)
O2—Si2—Ba96.0 (2)Ba—Ti_m2—W_cxiii180.0 (5)
O5—Si2—O7xi108.3 (4)Ba—Ti_m2—Mg_m20
O5—Si2—Ba64.4 (3)Baxiii—Ti_m2—W_c180.0 (5)
O7xi—Si2—Ba151.3 (4)Baxiii—Ti_m2—W_cxiii0.0 (5)
Ti_m1(2)—O1—Fe_m296.5 (3)Baxiii—Ti_m2—Mg_m20
Ti_m1(2)—O1—Si2123.9 (5)W_c—Ti_m2—W_cxiii180.0 (5)
Ti_m1(2)—O1—Baxiii98.2 (5)W_c—Ti_m2—Mg_m20
Ti_m1(2)—O1—Ti_m296.5 (3)W_cxiii—Ti_m2—Mg_m20
Ti_m1(2)—O1—Mg_m296.5 (3)Ti_m1(2)—Mg_m2—Ti_m1(2)xv180.0 (5)
Fe_m2—O1—Si2124.2 (5)Ti_m1(2)—Mg_m2—Fe_m20
Fe_m2—O1—Baxiii49.2 (3)Ti_m1(2)—Mg_m2—O141.96 (18)
Fe_m2—O1—Ti_m20.0 (5)Ti_m1(2)—Mg_m2—O1xiii41.96 (18)
Fe_m2—O1—Mg_m20.0 (5)Ti_m1(2)—Mg_m2—O1xv138.04 (18)
Si2—O1—Baxiii137.1 (3)Ti_m1(2)—Mg_m2—O1x138.04 (18)
Si2—O1—Ti_m2124.2 (5)Ti_m1(2)—Mg_m2—Ba90
Si2—O1—Mg_m2124.2 (5)Ti_m1(2)—Mg_m2—Baxiii90
Baxiii—O1—Ti_m249.2 (3)Ti_m1(2)—Mg_m2—W_c90
Baxiii—O1—Mg_m249.2 (3)Ti_m1(2)—Mg_m2—W_cxiii90
Ti_m2—O1—Mg_m20.0 (5)Ti_m1(2)—Mg_m2—Ti_m20
Na_axi—O2—Ti_m1(1)110.9 (6)Ti_m1(2)xv—Mg_m2—Fe_m20
Na_axi—O2—Si2117.7 (4)Ti_m1(2)xv—Mg_m2—O1138.04 (18)
Na_axi—O2—Nb_m1(1)110.9 (6)Ti_m1(2)xv—Mg_m2—O1xiii138.04 (18)
Ti_m1(1)—O2—Si2131.5 (4)Ti_m1(2)xv—Mg_m2—O1xv41.96 (18)
Ti_m1(1)—O2—Nb_m1(1)0.0 (5)Ti_m1(2)xv—Mg_m2—O1x41.96 (18)
Si2—O2—Nb_m1(1)131.5 (4)Ti_m1(2)xv—Mg_m2—Ba90
K_b—O3—Ti_m1(1)117.6 (2)Ti_m1(2)xv—Mg_m2—Baxiii90
K_b—O3—Si198.1 (6)Ti_m1(2)xv—Mg_m2—W_c90
K_b—O3—Ba98.3 (3)Ti_m1(2)xv—Mg_m2—W_cxiii90
K_b—O3—Nb_m1(1)117.6 (2)Ti_m1(2)xv—Mg_m2—Ti_m20
Ti_m1(1)—O3—Si1118.7 (4)Fe_m2—Mg_m2—O10
Ti_m1(1)—O3—Ba106.8 (6)Fe_m2—Mg_m2—O1xiii0
Ti_m1(1)—O3—Nb_m1(1)0.0 (5)Fe_m2—Mg_m2—O1xv0
Si1—O3—Ba115.8 (3)Fe_m2—Mg_m2—O1x0
Si1—O3—Nb_m1(1)118.7 (4)Fe_m2—Mg_m2—Ba0
Ba—O3—Nb_m1(1)106.8 (6)Fe_m2—Mg_m2—Baxiii0
K_biii—O4—Si1115.3 (7)Fe_m2—Mg_m2—W_c0
K_biii—O4—Si1x115.3 (7)Fe_m2—Mg_m2—W_cxiii0
Si1—O4—Si1x128.2 (14)Fe_m2—Mg_m2—Ti_m20
K_b—O5—Si2118.5 (7)O1—Mg_m2—O1xiii83.9 (3)
K_b—O5—Si2x118.5 (7)O1—Mg_m2—O1xv180.0 (5)
Si2—O5—Si2x123.1 (13)O1—Mg_m2—O1x96.1 (3)
Na_a—O6—Ti_m1(2)iv100.9 (4)O1—Mg_m2—Ba94.6 (4)
Na_a—O6—Si1119.2 (5)O1—Mg_m2—Baxiii85.4 (4)
Ti_m1(2)iv—O6—Si1132.4 (7)O1—Mg_m2—W_c94.6 (4)
Na_av—O7—Si1119.6 (5)O1—Mg_m2—W_cxiii85.4 (4)
Na_av—O7—Si2ii99.9 (4)O1—Mg_m2—Ti_m20
Si1—O7—Si2ii135.2 (10)O1xiii—Mg_m2—O1xv96.1 (3)
Ti_m1(1)—Oh—Ti_m1(2)130.1 (3)O1xiii—Mg_m2—O1x180.0 (5)
Ti_m1(1)—Oh—Ba105.6 (4)O1xiii—Mg_m2—Ba85.4 (4)
Ti_m1(1)—Oh—Nb_m1(1)0.0 (5)O1xiii—Mg_m2—Baxiii94.6 (4)
Ti_m1(2)—Oh—Ba96.9 (3)O1xiii—Mg_m2—W_c85.4 (4)
Ti_m1(2)—Oh—Nb_m1(1)130.1 (3)O1xiii—Mg_m2—W_cxiii94.6 (4)
Ba—Oh—Nb_m1(1)105.6 (4)O1xiii—Mg_m2—Ti_m20
Na_axx—Ba—Na_axxi33.9 (4)O1xv—Mg_m2—O1x83.9 (3)
Na_axx—Ba—Na_av111.06 (18)O1xv—Mg_m2—Ba85.4 (4)
Na_axx—Ba—Na_axiv101.5 (2)O1xv—Mg_m2—Baxiii94.6 (4)
Na_axx—Ba—K_b125.9 (2)O1xv—Mg_m2—W_c85.4 (4)
Na_axx—Ba—Ti_m1(1)162.89 (19)O1xv—Mg_m2—W_cxiii94.6 (4)
Na_axx—Ba—Ti_m1(1)xviii67.7 (2)O1xv—Mg_m2—Ti_m20
Na_axx—Ba—Ti_m1(2)129.0 (3)O1x—Mg_m2—Ba94.6 (4)
Na_axx—Ba—Ti_m1(2)xv50.66 (17)O1x—Mg_m2—Baxiii85.4 (4)
Na_axx—Ba—Fe_m289.8 (3)O1x—Mg_m2—W_c94.6 (4)
Na_axx—Ba—Si2145.5 (2)O1x—Mg_m2—W_cxiii85.4 (4)
Na_axx—Ba—Si2x100.07 (13)O1x—Mg_m2—Ti_m20
Na_axx—Ba—O1xiii96.2 (3)Ba—Mg_m2—Baxiii180.0 (5)
Na_axx—Ba—O1xv44.4 (3)Ba—Mg_m2—W_c0.0 (5)
Na_axx—Ba—O3143.2 (4)Ba—Mg_m2—W_cxiii180.0 (5)
Na_axx—Ba—O3x86.5 (3)Ba—Mg_m2—Ti_m20
Na_axx—Ba—Oh145.1 (3)Baxiii—Mg_m2—W_c180.0 (5)
Na_axx—Ba—Ohx44.01 (19)Baxiii—Mg_m2—W_cxiii0.0 (5)
Na_axx—Ba—Baxvi55.89 (13)Baxiii—Mg_m2—Ti_m20
Na_axx—Ba—Baxiii89.8 (3)W_c—Mg_m2—W_cxiii180.0 (5)
Na_axx—Ba—W286.6 (2)W_c—Mg_m2—Ti_m20
Na_axx—Ba—W2xvii27.3 (2)W_cxiii—Mg_m2—Ti_m20
Na_axx—Ba—W_c0
Symmetry codes: (i) x+1, y, z; (ii) x, y, z1; (iii) x+1, y, z+1; (iv) x+1/2, y+1/2, z+1; (v) x+1/2, y+1/2, z; (vi) x+1/2, y+1/2, z; (vii) x+1/2, y+1/2, z; (viii) x+1, y, z+2; (ix) x+1, y, z+1; (x) x, y, z; (xi) x, y, z+1; (xii) x+1/2, y+1/2, z+1; (xiii) x, y, z+1; (xiv) x1/2, y+1/2, z; (xv) x, y, z+1; (xvi) x, y, z; (xvii) x, y, z; (xviii) x+1/2, y1/2, z+1; (xix) x, y, z+1; (xx) x1/2, y1/2, z; (xxi) x+1/2, y1/2, z.
(labu-Fe_12.59) top
Crystal data top
Ba0.7Fe0.5K2.1Mg0.05Na2Nb0.1O33Si8Ti4Z = 2
Mr = 1206.8F(000) = 1167
Monoclinic, C2/mDx = 3.370 Mg m3
Hall symbol: -C 2ySynchrotron radiation, λ = 0.414 Å
a = 13.645 (8) ÅCell parameters from 2849 reflections
b = 13.2460 (7) Åθ = 1.8–19.0°
c = 7.3265 (17) ŵ = 0.89 mm1
β = 116.11 (4)°T = 293 K
V = 1189.0 (8) Å3Anhedral grain
Data collection top
ESRF ID 09
diffractometer
θmax = 19.0°, θmin = 1.8°
2849 measured reflectionsh = 87
857 independent reflectionsk = 2020
595 reflections with I > 2σ(I)l = 1010
Rint = 0.049
Refinement top
Refinement on F0 restraints
R[F2 > 2σ(F2)] = 0.0756 constraints
wR(F2) = 0.132Weighting scheme based on measured s.u.'s w = 1/(σ2(F) + 0.0100000007F2)
S = 1.04(Δ/σ)max = 0.049
857 reflectionsΔρmax = 0.99 e Å3
68 parametersΔρmin = 1.04 e Å3
Fractional atomic coordinates and isotropic or equivalent isotropic displacement parameters (Å2) top
xyzUiso*/UeqOcc. (<1)
Na_a0.4184 (17)0.2701 (6)0.0103 (14)0.029 (11)0.5
K_b0.4306 (6)00.7244 (4)0.028 (4)
Ti_m1(1)0.250.250.50.0151 (6)*0.95
Ti_m1(2)00.21864 (16)0.50.0139 (6)*
Fe_m2000.50.0250 (12)*0.5
Si10.3284 (5)0.10984 (15)0.2667 (3)0.0082 (6)*
Si20.2109 (4)0.10896 (14)0.8159 (3)0.0074 (6)*
O10.0799 (11)0.1076 (4)0.6810 (9)0.0100 (13)*
O20.2721 (11)0.1962 (4)0.7605 (9)0.0105 (12)*
O30.2829 (12)0.1170 (4)0.4316 (9)0.0106 (12)*
O40.3859 (16)00.2875 (12)0.0091 (16)*
O50.2617 (16)00.7953 (12)0.0090 (16)*
O60.4212 (12)0.1889 (5)0.2901 (10)0.0182 (15)*
O70.2246 (12)0.1179 (4)0.0454 (9)0.0111 (13)*
Oh0.0983 (11)0.2117 (4)0.3840 (9)0.0102 (12)*
Ba0.0943 (4)00.3384 (3)0.0142 (5)*0.35
W10.50.1448 (8)00.055 (15)
W200.1075 (7)00.028 (3)*
W_c0.0943 (4)00.3384 (3)0.0142 (5)*0.65
Nb_m1(1)0.250.250.50.0151 (6)*0.05
Ti_m2000.50.0250 (12)*0.1
Mg_m2000.50.0250 (12)*0.05
Atomic displacement parameters (Å2) top
U11U22U33U12U13U23
Na_a0.02 (2)0.023 (4)0.034 (5)0.006 (5)0.007 (8)0.001 (3)
K_b0.030 (10)0.0337 (16)0.0119 (12)00.003 (2)0
W10.10 (4)0.029 (5)0.019 (5)00.009 (9)0
Geometric parameters (Å, º) top
Na_a—Na_ai2.30 (3)Ti_m1(2)—Ba3.576 (3)
Na_a—K_bii4.186 (11)Ti_m1(2)—Baxiii3.576 (3)
Na_a—K_biii4.159 (10)Ti_m1(2)—Ti_m22.896 (2)
Na_a—Ti_m1(1)ii3.430 (10)Ti_m1(2)—Mg_m22.896 (2)
Na_a—Ti_m1(2)iv3.259 (10)Fe_m2—O11.925 (6)
Na_a—Si2iv3.05 (2)Fe_m2—O1xiii1.925 (6)
Na_a—O2ii2.253 (16)Fe_m2—O1xv1.925 (6)
Na_a—O62.301 (16)Fe_m2—O1x1.925 (6)
Na_a—O7v2.34 (2)Fe_m2—Ba2.097 (5)
Na_a—Bavi3.967 (11)Fe_m2—Baxiii2.097 (5)
Na_a—Bavii3.929 (11)Fe_m2—W_c2.097 (5)
Na_a—W12.018 (17)Fe_m2—W_cxiii2.097 (5)
Na_a—W2v1.987 (17)Fe_m2—Ti_m20
Na_a—Nb_m1(1)ii3.430 (10)Fe_m2—Mg_m20
K_b—K_biii4.459 (10)Si1—O31.586 (15)
K_b—K_bviii3.628 (5)Si1—O41.628 (10)
K_b—Si13.345 (4)Si1—O61.593 (14)
K_b—Si1iii3.571 (10)Si1—O71.620 (9)
K_b—Si1ix3.571 (10)Si2—O11.618 (14)
K_b—Si1x3.345 (4)Si2—O21.580 (12)
K_b—Si23.645 (10)Si2—O51.636 (11)
K_b—Si2x3.645 (10)Si2—O7xi1.613 (9)
K_b—O32.694 (9)Si2—Ba3.457 (4)
K_b—O3x2.694 (9)O1—Baxiii2.721 (14)
K_b—O4iii2.54 (2)O1—Ti_m21.925 (6)
K_b—O52.58 (2)O1—Mg_m21.925 (6)
K_b—Ba4.199 (10)O2—Nb_m1(1)1.932 (7)
K_b—W1xi2.640 (8)O3—Ba2.818 (15)
K_b—W1ix2.640 (8)O3—Nb_m1(1)1.937 (8)
Ti_m1(1)—O21.932 (7)Oh—Ba2.821 (5)
Ti_m1(1)—O2iv1.932 (7)Oh—Nb_m1(1)1.928 (13)
Ti_m1(1)—O31.937 (8)Ba—Baxvi4.470 (5)
Ti_m1(1)—O3iv1.937 (8)Ba—Baxiii4.194 (7)
Ti_m1(1)—Oh1.928 (13)Ba—W22.650 (6)
Ti_m1(1)—Ohiv1.928 (13)Ba—W2xvii2.650 (6)
Ti_m1(1)—Ba3.830 (3)Ba—W_c0
Ti_m1(1)—Baxii3.830 (3)Ba—Nb_m1(1)3.830 (3)
Ti_m1(1)—Nb_m1(1)0Ba—Nb_m1(1)xviii3.830 (3)
Ti_m1(2)—O11.960 (6)Ba—Ti_m22.097 (5)
Ti_m1(2)—O1xiii1.960 (6)Ba—Mg_m22.097 (5)
Ti_m1(2)—O6iv1.888 (7)W_c—Ti_m22.097 (5)
Ti_m1(2)—O6xiv1.888 (7)W_c—Mg_m22.097 (5)
Ti_m1(2)—Oh1.879 (14)Ti_m2—Mg_m20
Ti_m1(2)—Ohxiii1.879 (14)
Na_ai—Na_a—K_bii73.4 (4)Na_axx—Ba—Nb_m1(1)163.04 (19)
Na_ai—Na_a—K_biii74.7 (4)Na_axx—Ba—Nb_m1(1)xviii68.2 (2)
Na_ai—Na_a—Ti_m1(1)ii97.6 (5)Na_axx—Ba—Ti_m289.1 (3)
Na_ai—Na_a—Ti_m1(2)iv101.6 (5)Na_axx—Ba—Mg_m289.1 (3)
Na_ai—Na_a—Si2iv141.6 (5)Na_axxi—Ba—Na_av101.6 (2)
Na_ai—Na_a—O2ii119.0 (8)Na_axxi—Ba—Na_axiv111.0 (2)
Na_ai—Na_a—O6115.0 (7)Na_axxi—Ba—K_b99.2 (3)
Na_ai—Na_a—O7v138.3 (6)Na_axxi—Ba—Ti_m1(1)136.9 (3)
Na_ai—Na_a—Bavi72.2 (4)Na_axxi—Ba—Ti_m1(1)xviii52.45 (16)
Na_ai—Na_a—Bavii74.0 (4)Na_axxi—Ba—Ti_m1(2)157.5 (3)
Na_ai—Na_a—W155.3 (6)Na_axxi—Ba—Ti_m1(2)xv70.6 (2)
Na_ai—Na_a—W2v54.7 (6)Na_axxi—Ba—Fe_m2120.3 (3)
Na_ai—Na_a—Nb_m1(1)ii97.6 (5)Na_axxi—Ba—Si2148.25 (19)
K_bii—Na_a—K_biii51.54 (14)Na_axxi—Ba—Si2x101.73 (14)
K_bii—Na_a—Ti_m1(1)ii62.83 (16)Na_axxi—Ba—O1xiii125.8 (3)
K_bii—Na_a—Ti_m1(2)iv121.4 (2)Na_axxi—Ba—O1xv76.9 (4)
K_bii—Na_a—Si2iv144.7 (6)Na_axxi—Ba—O3111.0 (4)
K_bii—Na_a—O2ii55.8 (4)Na_axxi—Ba—O3x60.4 (3)
K_bii—Na_a—O693.3 (3)Na_axxi—Ba—Oh147.2 (3)
K_bii—Na_a—O7v131.9 (5)Na_axxi—Ba—Ohx45.6 (2)
K_bii—Na_a—Bavi144.4 (6)Na_axxi—Ba—Baxvi55.92 (15)
K_bii—Na_a—Bavii109.7 (3)Na_axxi—Ba—Baxiii120.3 (3)
K_bii—Na_a—W130.1 (2)Na_axxi—Ba—W286.8 (2)
K_bii—Na_a—W2v122.2 (8)Na_axxi—Ba—W2xvii27.2 (3)
K_bii—Na_a—Nb_m1(1)ii62.83 (16)Na_axxi—Ba—W_c0
K_biii—Na_a—Ti_m1(1)ii113.5 (2)Na_axxi—Ba—Nb_m1(1)136.9 (3)
K_biii—Na_a—Ti_m1(2)iv70.48 (17)Na_axxi—Ba—Nb_m1(1)xviii52.45 (16)
K_biii—Na_a—Si2iv121.1 (4)Na_axxi—Ba—Ti_m2120.3 (3)
K_biii—Na_a—O2ii94.9 (3)Na_axxi—Ba—Mg_m2120.3 (3)
K_biii—Na_a—O651.0 (4)Na_av—Ba—Na_axiv33.8 (5)
K_biii—Na_a—O7v146.2 (8)Na_av—Ba—K_b99.2 (3)
K_biii—Na_a—Bavi109.5 (3)Na_av—Ba—Ti_m1(1)52.45 (16)
K_biii—Na_a—Bavii147.3 (6)Na_av—Ba—Ti_m1(1)xviii136.9 (3)
K_biii—Na_a—W130.9 (2)Na_av—Ba—Ti_m1(2)70.6 (2)
K_biii—Na_a—W2v123.3 (8)Na_av—Ba—Ti_m1(2)xv157.5 (3)
K_biii—Na_a—Nb_m1(1)ii113.5 (2)Na_av—Ba—Fe_m2120.3 (3)
Ti_m1(1)ii—Na_a—Ti_m1(2)iv160.7 (8)Na_av—Ba—Si2101.73 (14)
Ti_m1(1)ii—Na_a—Si2iv105.3 (5)Na_av—Ba—Si2x148.25 (19)
Ti_m1(1)ii—Na_a—O2ii32.0 (3)Na_av—Ba—O1xiii76.9 (4)
Ti_m1(1)ii—Na_a—O6132.5 (7)Na_av—Ba—O1xv125.8 (3)
Ti_m1(1)ii—Na_a—O7v75.6 (4)Na_av—Ba—O360.4 (3)
Ti_m1(1)ii—Na_a—Bavi131.0 (3)Na_av—Ba—O3x111.0 (4)
Ti_m1(1)ii—Na_a—Bavii62.28 (16)Na_av—Ba—Oh45.6 (2)
Ti_m1(1)ii—Na_a—W190.7 (3)Na_av—Ba—Ohx147.2 (3)
Ti_m1(1)ii—Na_a—W2v98.0 (4)Na_av—Ba—Baxvi55.92 (15)
Ti_m1(1)ii—Na_a—Nb_m1(1)ii0.0 (5)Na_av—Ba—Baxiii120.3 (3)
Ti_m1(2)iv—Na_a—Si2iv59.7 (3)Na_av—Ba—W227.2 (3)
Ti_m1(2)iv—Na_a—O2ii131.7 (8)Na_av—Ba—W2xvii86.8 (2)
Ti_m1(2)iv—Na_a—O634.6 (2)Na_av—Ba—W_c0
Ti_m1(2)iv—Na_a—O7v91.0 (5)Na_av—Ba—Nb_m1(1)52.45 (16)
Ti_m1(2)iv—Na_a—Bavi58.34 (15)Na_av—Ba—Nb_m1(1)xviii136.9 (3)
Ti_m1(2)iv—Na_a—Bavii125.2 (2)Na_av—Ba—Ti_m2120.3 (3)
Ti_m1(2)iv—Na_a—W198.7 (3)Na_av—Ba—Mg_m2120.3 (3)
Ti_m1(2)iv—Na_a—W2v94.5 (3)Na_axiv—Ba—K_b126.8 (3)
Ti_m1(2)iv—Na_a—Nb_m1(1)ii160.7 (8)Na_axiv—Ba—Ti_m1(1)68.2 (2)
Si2iv—Na_a—O2ii95.7 (8)Na_axiv—Ba—Ti_m1(1)xviii163.04 (19)
Si2iv—Na_a—O670.0 (6)Na_axiv—Ba—Ti_m1(2)50.87 (19)
Si2iv—Na_a—O7v31.5 (3)Na_axiv—Ba—Ti_m1(2)xv127.8 (3)
Si2iv—Na_a—Bavi69.5 (2)Na_axiv—Ba—Fe_m289.1 (3)
Si2iv—Na_a—Bavii89.8 (2)Na_axiv—Ba—Si2100.31 (15)
Si2iv—Na_a—W1151.5 (6)Na_axiv—Ba—Si2x145.1 (2)
Si2iv—Na_a—W2v91.4 (4)Na_axiv—Ba—O1xiii44.3 (4)
Si2iv—Na_a—Nb_m1(1)ii105.3 (5)Na_axiv—Ba—O1xv95.1 (4)
O2ii—Na_a—O6100.5 (8)Na_axiv—Ba—O388.2 (3)
O2ii—Na_a—O7v76.2 (7)Na_axiv—Ba—O3x144.4 (4)
O2ii—Na_a—Bavi155.4 (5)Na_axiv—Ba—Oh44.3 (2)
O2ii—Na_a—Bavii92.2 (3)Na_axiv—Ba—Ohx144.1 (3)
O2ii—Na_a—W185.3 (4)Na_axiv—Ba—Baxvi55.13 (15)
O2ii—Na_a—W2v129.4 (5)Na_axiv—Ba—Baxiii89.1 (3)
O2ii—Na_a—Nb_m1(1)ii32.0 (3)Na_axiv—Ba—W226.5 (3)
O6—Na_a—O7v97.9 (9)Na_axiv—Ba—W2xvii86.0 (2)
O6—Na_a—Bavi92.9 (3)Na_axiv—Ba—W_c0
O6—Na_a—Bavii157.0 (5)Na_axiv—Ba—Nb_m1(1)68.2 (2)
O6—Na_a—W181.7 (4)Na_axiv—Ba—Nb_m1(1)xviii163.04 (19)
O6—Na_a—W2v128.7 (5)Na_axiv—Ba—Ti_m289.1 (3)
O6—Na_a—Nb_m1(1)ii132.5 (7)Na_axiv—Ba—Mg_m289.1 (3)
O7v—Na_a—Bavi81.6 (3)K_b—Ba—Ti_m1(1)59.91 (6)
O7v—Na_a—Bavii66.5 (4)K_b—Ba—Ti_m1(1)xviii59.91 (6)
O7v—Na_a—W1161.1 (8)K_b—Ba—Ti_m1(2)102.88 (7)
O7v—Na_a—W2v85.1 (5)K_b—Ba—Ti_m1(2)xv102.88 (7)
O7v—Na_a—Nb_m1(1)ii75.6 (4)K_b—Ba—Fe_m2112.34 (11)
Bavi—Na_a—Bavii68.95 (19)K_b—Ba—Si255.86 (13)
Bavi—Na_a—W1117.2 (7)K_b—Ba—Si2x55.86 (13)
Bavi—Na_a—W2v36.57 (18)K_b—Ba—O1xiii134.91 (16)
Bavi—Na_a—Nb_m1(1)ii131.0 (3)K_b—Ba—O1xv134.91 (16)
Bavii—Na_a—W1118.7 (7)K_b—Ba—O339.31 (15)
Bavii—Na_a—W2v37.63 (19)K_b—Ba—O3x39.31 (15)
Bavii—Na_a—Nb_m1(1)ii62.28 (16)K_b—Ba—Oh87.8 (2)
W1—Na_a—W2v110.0 (11)K_b—Ba—Ohx87.8 (2)
W1—Na_a—Nb_m1(1)ii90.7 (3)K_b—Ba—Baxvi132.22 (16)
W2v—Na_a—Nb_m1(1)ii98.0 (4)K_b—Ba—Baxiii112.34 (11)
Na_axi—K_b—Na_aiii32.0 (4)K_b—Ba—W2124.52 (17)
Na_axi—K_b—Na_aix128.46 (19)K_b—Ba—W2xvii124.52 (17)
Na_axi—K_b—Na_axix117.5 (3)K_b—Ba—W_c0
Na_axi—K_b—K_biii119.5 (3)K_b—Ba—Nb_m1(1)59.91 (6)
Na_axi—K_b—K_bviii63.85 (14)K_b—Ba—Nb_m1(1)xviii59.91 (6)
Na_axi—K_b—Si192.24 (14)K_b—Ba—Ti_m2112.34 (11)
Na_axi—K_b—Si1iii83.2 (3)K_b—Ba—Mg_m2112.34 (11)
Na_axi—K_b—Si1ix125.3 (3)Ti_m1(1)—Ba—Ti_m1(1)xviii119.69 (12)
Na_axi—K_b—Si1x141.49 (18)Ti_m1(1)—Ba—Ti_m1(2)55.17 (3)
Na_axi—K_b—Si249.7 (3)Ti_m1(1)—Ba—Ti_m1(2)xv146.05 (7)
Na_axi—K_b—Si2x91.7 (3)Ti_m1(1)—Ba—Fe_m2102.73 (6)
Na_axi—K_b—O374.1 (2)Ti_m1(1)—Ba—Si251.73 (7)
Na_axi—K_b—O3x135.2 (5)Ti_m1(1)—Ba—Si2x95.89 (8)
Na_axi—K_b—O4iii105.9 (3)Ti_m1(1)—Ba—O1xiii85.21 (19)
Na_axi—K_b—O570.3 (3)Ti_m1(1)—Ba—O1xv145.3 (2)
Na_axi—K_b—Ba93.7 (3)Ti_m1(1)—Ba—O329.1 (2)
Na_axi—K_b—W1xi22.5 (3)Ti_m1(1)—Ba—O3x94.4 (2)
Na_axi—K_b—W1ix108.5 (2)Ti_m1(1)—Ba—Oh29.0 (3)
Na_aiii—K_b—Na_aix118.7 (3)Ti_m1(1)—Ba—Ohx147.5 (3)
Na_aiii—K_b—Na_axix128.46 (19)Ti_m1(1)—Ba—Baxvi108.24 (6)
Na_aiii—K_b—K_biii93.5 (3)Ti_m1(1)—Ba—Baxiii102.73 (6)
Na_aiii—K_b—K_bviii64.61 (15)Ti_m1(1)—Ba—W278.43 (17)
Na_aiii—K_b—Si189.81 (14)Ti_m1(1)—Ba—W2xvii136.77 (18)
Na_aiii—K_b—Si1iii51.5 (3)Ti_m1(1)—Ba—W_c0
Na_aiii—K_b—Si1ix94.5 (3)Ti_m1(1)—Ba—Nb_m1(1)0.0 (5)
Na_aiii—K_b—Si1x138.1 (2)Ti_m1(1)—Ba—Nb_m1(1)xviii119.69 (12)
Na_aiii—K_b—Si281.5 (3)Ti_m1(1)—Ba—Ti_m2102.73 (6)
Na_aiii—K_b—Si2x122.2 (3)Ti_m1(1)—Ba—Mg_m2102.73 (6)
Na_aiii—K_b—O385.4 (2)Ti_m1(1)xviii—Ba—Ti_m1(2)146.05 (7)
Na_aiii—K_b—O3x155.5 (2)Ti_m1(1)xviii—Ba—Ti_m1(2)xv55.17 (3)
Na_aiii—K_b—O4iii73.9 (3)Ti_m1(1)xviii—Ba—Fe_m2102.73 (6)
Na_aiii—K_b—O5102.1 (3)Ti_m1(1)xviii—Ba—Si295.89 (8)
Na_aiii—K_b—Ba119.0 (3)Ti_m1(1)xviii—Ba—Si2x51.73 (7)
Na_aiii—K_b—W1xi23.1 (3)Ti_m1(1)xviii—Ba—O1xiii145.3 (2)
Na_aiii—K_b—W1ix109.3 (2)Ti_m1(1)xviii—Ba—O1xv85.21 (19)
Na_aix—K_b—Na_axix32.0 (4)Ti_m1(1)xviii—Ba—O394.4 (2)
Na_aix—K_b—K_biii93.5 (3)Ti_m1(1)xviii—Ba—O3x29.1 (2)
Na_aix—K_b—K_bviii64.61 (15)Ti_m1(1)xviii—Ba—Oh147.5 (3)
Na_aix—K_b—Si1138.1 (2)Ti_m1(1)xviii—Ba—Ohx29.0 (3)
Na_aix—K_b—Si1iii94.5 (3)Ti_m1(1)xviii—Ba—Baxvi108.24 (6)
Na_aix—K_b—Si1ix51.5 (3)Ti_m1(1)xviii—Ba—Baxiii102.73 (6)
Na_aix—K_b—Si1x89.81 (14)Ti_m1(1)xviii—Ba—W2136.77 (18)
Na_aix—K_b—Si2122.2 (3)Ti_m1(1)xviii—Ba—W2xvii78.43 (17)
Na_aix—K_b—Si2x81.5 (3)Ti_m1(1)xviii—Ba—W_c0
Na_aix—K_b—O3155.5 (2)Ti_m1(1)xviii—Ba—Nb_m1(1)119.69 (12)
Na_aix—K_b—O3x85.4 (2)Ti_m1(1)xviii—Ba—Nb_m1(1)xviii0.0 (5)
Na_aix—K_b—O4iii73.9 (3)Ti_m1(1)xviii—Ba—Ti_m2102.73 (6)
Na_aix—K_b—O5102.1 (3)Ti_m1(1)xviii—Ba—Mg_m2102.73 (6)
Na_aix—K_b—Ba119.0 (3)Ti_m1(2)—Ba—Ti_m1(2)xv108.19 (13)
Na_aix—K_b—W1xi109.3 (2)Ti_m1(2)—Ba—Fe_m254.09 (7)
Na_aix—K_b—W1ix23.1 (3)Ti_m1(2)—Ba—Si253.08 (8)
Na_axix—K_b—K_biii119.5 (3)Ti_m1(2)—Ba—Si2x94.34 (9)
Na_axix—K_b—K_bviii63.85 (14)Ti_m1(2)—Ba—O1xiii32.84 (16)
Na_axix—K_b—Si1141.49 (18)Ti_m1(2)—Ba—O1xv90.5 (2)
Na_axix—K_b—Si1iii125.3 (3)Ti_m1(2)—Ba—O384.1 (2)
Na_axix—K_b—Si1ix83.2 (3)Ti_m1(2)—Ba—O3x142.04 (15)
Na_axix—K_b—Si1x92.24 (14)Ti_m1(2)—Ba—Oh31.4 (3)
Na_axix—K_b—Si291.7 (3)Ti_m1(2)—Ba—Ohx139.2 (3)
Na_axix—K_b—Si2x49.7 (3)Ti_m1(2)—Ba—Baxvi104.59 (7)
Na_axix—K_b—O3135.2 (5)Ti_m1(2)—Ba—Baxiii54.09 (7)
Na_axix—K_b—O3x74.1 (2)Ti_m1(2)—Ba—W277.13 (16)
Na_axix—K_b—O4iii105.9 (3)Ti_m1(2)—Ba—W2xvii130.37 (18)
Na_axix—K_b—O570.3 (3)Ti_m1(2)—Ba—W_c0
Na_axix—K_b—Ba93.7 (3)Ti_m1(2)—Ba—Nb_m1(1)55.17 (3)
Na_axix—K_b—W1xi108.5 (2)Ti_m1(2)—Ba—Nb_m1(1)xviii146.05 (7)
Na_axix—K_b—W1ix22.5 (3)Ti_m1(2)—Ba—Ti_m254.09 (7)
K_biii—K_b—K_bviii129.6 (3)Ti_m1(2)—Ba—Mg_m254.09 (7)
K_biii—K_b—Si152.11 (15)Ti_m1(2)xv—Ba—Fe_m254.09 (7)
K_biii—K_b—Si1iii47.67 (12)Ti_m1(2)xv—Ba—Si294.34 (9)
K_biii—K_b—Si1ix47.67 (12)Ti_m1(2)xv—Ba—Si2x53.08 (8)
K_biii—K_b—Si1x52.11 (15)Ti_m1(2)xv—Ba—O1xiii90.5 (2)
K_biii—K_b—Si2141.84 (10)Ti_m1(2)xv—Ba—O1xv32.84 (16)
K_biii—K_b—Si2x141.84 (10)Ti_m1(2)xv—Ba—O3142.04 (15)
K_biii—K_b—O379.9 (3)Ti_m1(2)xv—Ba—O3x84.1 (2)
K_biii—K_b—O3x79.9 (3)Ti_m1(2)xv—Ba—Oh139.2 (3)
K_biii—K_b—O4iii39.7 (2)Ti_m1(2)xv—Ba—Ohx31.4 (3)
K_biii—K_b—O5149.0 (2)Ti_m1(2)xv—Ba—Baxvi104.59 (7)
K_biii—K_b—Ba101.33 (12)Ti_m1(2)xv—Ba—Baxiii54.09 (7)
K_biii—K_b—W1xi116.0 (2)Ti_m1(2)xv—Ba—W2130.37 (18)
K_biii—K_b—W1ix116.0 (2)Ti_m1(2)xv—Ba—W2xvii77.13 (16)
K_bviii—K_b—Si1154.01 (5)Ti_m1(2)xv—Ba—W_c0
K_bviii—K_b—Si1iii87.37 (18)Ti_m1(2)xv—Ba—Nb_m1(1)146.05 (7)
K_bviii—K_b—Si1ix87.37 (18)Ti_m1(2)xv—Ba—Nb_m1(1)xviii55.17 (3)
K_bviii—K_b—Si1x154.01 (5)Ti_m1(2)xv—Ba—Ti_m254.09 (7)
K_bviii—K_b—Si282.19 (18)Ti_m1(2)xv—Ba—Mg_m254.09 (7)
K_bviii—K_b—Si2x82.19 (18)Fe_m2—Ba—Si263.40 (12)
K_bviii—K_b—O3136.7 (3)Fe_m2—Ba—Si2x63.40 (12)
K_bviii—K_b—O3x136.7 (3)Fe_m2—Ba—O1xiii44.8 (2)
K_bviii—K_b—O4iii89.9 (3)Fe_m2—Ba—O1xv44.8 (2)
K_bviii—K_b—O581.4 (3)Fe_m2—Ba—O3125.8 (2)
K_bviii—K_b—Ba129.1 (3)Fe_m2—Ba—O3x125.8 (2)
K_bviii—K_b—W1xi46.59 (17)Fe_m2—Ba—Oh85.3 (3)
K_bviii—K_b—W1ix46.59 (17)Fe_m2—Ba—Ohx85.3 (3)
Si1—K_b—Si1iii79.36 (17)Fe_m2—Ba—Baxvi115.44 (16)
Si1—K_b—Si1ix99.8 (2)Fe_m2—Ba—Baxiii0.0 (5)
Si1—K_b—Si1x51.56 (7)Fe_m2—Ba—W2111.24 (18)
Si1—K_b—Si289.91 (17)Fe_m2—Ba—W2xvii111.24 (18)
Si1—K_b—Si2x110.1 (2)Fe_m2—Ba—W_c0
Si1—K_b—O327.9 (3)Fe_m2—Ba—Nb_m1(1)102.73 (6)
Si1—K_b—O3x67.44 (17)Fe_m2—Ba—Nb_m1(1)xviii102.73 (6)
Si1—K_b—O4iii87.0 (3)Fe_m2—Ba—Ti_m20.0 (5)
Si1—K_b—O5100.8 (3)Fe_m2—Ba—Mg_m20.0 (5)
Si1—K_b—Ba58.34 (14)Si2—Ba—Si2x49.35 (5)
Si1—K_b—W1xi107.56 (17)Si2—Ba—O1xiii80.61 (17)
Si1—K_b—W1ix159.01 (19)Si2—Ba—O1xv105.9 (2)
Si1iii—K_b—Si1ix48.09 (14)Si2—Ba—O363.9 (2)
Si1iii—K_b—Si1x99.8 (2)Si2—Ba—O3x91.15 (17)
Si1iii—K_b—Si2131.36 (8)Si2—Ba—Oh59.27 (12)
Si1iii—K_b—Si2x169.54 (11)Si2—Ba—Ohx108.59 (13)
Si1iii—K_b—O398.1 (4)Si2—Ba—Baxvi155.01 (5)
Si1iii—K_b—O3x127.5 (4)Si2—Ba—Baxiii63.40 (13)
Si1iii—K_b—O4iii24.20 (8)Si2—Ba—W2122.69 (18)
Si1iii—K_b—O5153.51 (11)Si2—Ba—W2xvii171.40 (19)
Si1iii—K_b—Ba137.49 (10)Si2—Ba—W_c0
Si1iii—K_b—W1xi70.88 (15)Si2—Ba—Nb_m1(1)51.73 (7)
Si1iii—K_b—W1ix105.3 (2)Si2—Ba—Nb_m1(1)xviii95.89 (8)
Si1ix—K_b—Si1x79.36 (17)Si2—Ba—Ti_m263.40 (12)
Si1ix—K_b—Si2169.54 (11)Si2—Ba—Mg_m263.40 (12)
Si1ix—K_b—Si2x131.36 (8)Si2x—Ba—O1xiii105.9 (2)
Si1ix—K_b—O3127.5 (4)Si2x—Ba—O1xv80.61 (17)
Si1ix—K_b—O3x98.1 (4)Si2x—Ba—O391.15 (17)
Si1ix—K_b—O4iii24.20 (8)Si2x—Ba—O3x63.9 (2)
Si1ix—K_b—O5153.51 (11)Si2x—Ba—Oh108.59 (13)
Si1ix—K_b—Ba137.49 (10)Si2x—Ba—Ohx59.27 (12)
Si1ix—K_b—W1xi105.3 (2)Si2x—Ba—Baxvi155.01 (5)
Si1ix—K_b—W1ix70.88 (15)Si2x—Ba—Baxiii63.40 (13)
Si1x—K_b—Si2110.1 (2)Si2x—Ba—W2171.40 (19)
Si1x—K_b—Si2x89.91 (17)Si2x—Ba—W2xvii122.69 (18)
Si1x—K_b—O367.44 (17)Si2x—Ba—W_c0
Si1x—K_b—O3x27.9 (3)Si2x—Ba—Nb_m1(1)95.89 (8)
Si1x—K_b—O4iii87.0 (3)Si2x—Ba—Nb_m1(1)xviii51.73 (7)
Si1x—K_b—O5100.8 (3)Si2x—Ba—Ti_m263.40 (12)
Si1x—K_b—Ba58.34 (14)Si2x—Ba—Mg_m263.40 (12)
Si1x—K_b—W1xi159.01 (19)O1xiii—Ba—O1xv63.2 (3)
Si1x—K_b—W1ix107.56 (17)O1xiii—Ba—O3114.1 (3)
Si2—K_b—Si2x46.65 (13)O1xiii—Ba—O3x169.8 (2)
Si2—K_b—O362.0 (3)O1xiii—Ba—Oh57.1 (4)
Si2—K_b—O3x89.2 (4)O1xiii—Ba—Ohx119.8 (4)
Si2—K_b—O4iii155.22 (10)O1xiii—Ba—Baxvi83.04 (16)
Si2—K_b—O523.33 (7)O1xiii—Ba—Baxiii44.82 (19)
Si2—K_b—Ba51.72 (12)O1xiii—Ba—W267.44 (19)
Si2—K_b—W1xi67.60 (15)O1xiii—Ba—W2xvii100.3 (2)
Si2—K_b—W1ix101.2 (2)O1xiii—Ba—W_c0
Si2x—K_b—O389.2 (4)O1xiii—Ba—Nb_m1(1)85.21 (19)
Si2x—K_b—O3x62.0 (3)O1xiii—Ba—Nb_m1(1)xviii145.3 (2)
Si2x—K_b—O4iii155.22 (10)O1xiii—Ba—Ti_m244.8 (2)
Si2x—K_b—O523.33 (7)O1xiii—Ba—Mg_m244.8 (2)
Si2x—K_b—Ba51.72 (12)O1xv—Ba—O3169.8 (2)
Si2x—K_b—W1xi101.2 (2)O1xv—Ba—O3x114.1 (3)
Si2x—K_b—W1ix67.60 (15)O1xv—Ba—Oh119.8 (4)
O3—K_b—O3x70.2 (2)O1xv—Ba—Ohx57.1 (4)
O3—K_b—O4iii112.1 (4)O1xv—Ba—Baxvi83.04 (16)
O3—K_b—O574.8 (4)O1xv—Ba—Baxiii44.82 (19)
O3—K_b—Ba41.5 (3)O1xv—Ba—W2100.3 (2)
O3—K_b—W1xi94.7 (2)O1xv—Ba—W2xvii67.44 (19)
O3—K_b—W1ix156.6 (5)O1xv—Ba—W_c0
O3x—K_b—O4iii112.1 (4)O1xv—Ba—Nb_m1(1)145.3 (2)
O3x—K_b—O574.8 (4)O1xv—Ba—Nb_m1(1)xviii85.21 (19)
O3x—K_b—Ba41.5 (3)O1xv—Ba—Ti_m244.8 (2)
O3x—K_b—W1xi156.6 (5)O1xv—Ba—Mg_m244.8 (2)
O3x—K_b—W1ix94.7 (2)O3—Ba—O3x66.7 (3)
O4iii—K_b—O5171.3 (3)O3—Ba—Oh57.1 (4)
O4iii—K_b—Ba141.0 (2)O3—Ba—Ohx123.4 (4)
O4iii—K_b—W1xi89.9 (2)O3—Ba—Baxvi106.69 (18)
O4iii—K_b—W1ix89.9 (2)O3—Ba—Baxiii125.8 (2)
O5—K_b—Ba47.6 (2)O3—Ba—W286.94 (19)
O5—K_b—W1xi84.1 (2)O3—Ba—W2xvii122.5 (3)
O5—K_b—W1ix84.1 (2)O3—Ba—W_c0
Ba—K_b—W1xi115.7 (2)O3—Ba—Nb_m1(1)29.1 (2)
Ba—K_b—W1ix115.7 (2)O3—Ba—Nb_m1(1)xviii94.4 (2)
W1xi—K_b—W1ix93.2 (3)O3—Ba—Ti_m2125.8 (2)
Na_axi—Ti_m1(1)—Na_av180.0 (5)O3—Ba—Mg_m2125.8 (2)
Na_axi—Ti_m1(1)—O238.2 (4)O3x—Ba—Oh123.4 (4)
Na_axi—Ti_m1(1)—O2iv141.8 (4)O3x—Ba—Ohx57.1 (4)
Na_axi—Ti_m1(1)—O3103.4 (3)O3x—Ba—Baxvi106.69 (18)
Na_axi—Ti_m1(1)—O3iv76.6 (3)O3x—Ba—Baxiii125.8 (2)
Na_axi—Ti_m1(1)—Oh125.1 (5)O3x—Ba—W2122.5 (3)
Na_axi—Ti_m1(1)—Ohiv54.9 (5)O3x—Ba—W2xvii86.94 (19)
Na_axi—Ti_m1(1)—Ba114.7 (2)O3x—Ba—W_c0
Na_axi—Ti_m1(1)—Baxii65.3 (2)O3x—Ba—Nb_m1(1)94.4 (2)
Na_axi—Ti_m1(1)—Nb_m1(1)0O3x—Ba—Nb_m1(1)xviii29.1 (2)
Na_av—Ti_m1(1)—O2141.8 (4)O3x—Ba—Ti_m2125.8 (2)
Na_av—Ti_m1(1)—O2iv38.2 (4)O3x—Ba—Mg_m2125.8 (2)
Na_av—Ti_m1(1)—O376.6 (3)Oh—Ba—Ohx167.2 (2)
Na_av—Ti_m1(1)—O3iv103.4 (3)Oh—Ba—Baxvi95.91 (12)
Na_av—Ti_m1(1)—Oh54.9 (5)Oh—Ba—Baxiii85.3 (3)
Na_av—Ti_m1(1)—Ohiv125.1 (5)Oh—Ba—W263.4 (2)
Na_av—Ti_m1(1)—Ba65.3 (2)Oh—Ba—W2xvii128.4 (2)
Na_av—Ti_m1(1)—Baxii114.7 (2)Oh—Ba—W_c0
Na_av—Ti_m1(1)—Nb_m1(1)0Oh—Ba—Nb_m1(1)29.0 (3)
O2—Ti_m1(1)—O2iv180.0 (5)Oh—Ba—Nb_m1(1)xviii147.5 (3)
O2—Ti_m1(1)—O388.1 (3)Oh—Ba—Ti_m285.3 (3)
O2—Ti_m1(1)—O3iv91.9 (3)Oh—Ba—Mg_m285.3 (3)
O2—Ti_m1(1)—Oh90.5 (4)Ohx—Ba—Baxvi95.91 (12)
O2—Ti_m1(1)—Ohiv89.5 (4)Ohx—Ba—Baxiii85.3 (3)
O2—Ti_m1(1)—Ba79.1 (2)Ohx—Ba—W2128.4 (2)
O2—Ti_m1(1)—Baxii100.9 (2)Ohx—Ba—W2xvii63.4 (2)
O2—Ti_m1(1)—Nb_m1(1)0Ohx—Ba—W_c0
O2iv—Ti_m1(1)—O391.9 (3)Ohx—Ba—Nb_m1(1)147.5 (3)
O2iv—Ti_m1(1)—O3iv88.1 (3)Ohx—Ba—Nb_m1(1)xviii29.0 (3)
O2iv—Ti_m1(1)—Oh89.5 (4)Ohx—Ba—Ti_m285.3 (3)
O2iv—Ti_m1(1)—Ohiv90.5 (4)Ohx—Ba—Mg_m285.3 (3)
O2iv—Ti_m1(1)—Ba100.9 (2)Baxvi—Ba—Baxiii115.44 (14)
O2iv—Ti_m1(1)—Baxii79.1 (2)Baxvi—Ba—W232.50 (17)
O2iv—Ti_m1(1)—Nb_m1(1)0Baxvi—Ba—W2xvii32.50 (17)
O3—Ti_m1(1)—O3iv180.0 (5)Baxvi—Ba—W_c0
O3—Ti_m1(1)—Oh88.4 (5)Baxvi—Ba—Nb_m1(1)108.24 (6)
O3—Ti_m1(1)—Ohiv91.6 (5)Baxvi—Ba—Nb_m1(1)xviii108.24 (6)
O3—Ti_m1(1)—Ba45.1 (5)Baxvi—Ba—Ti_m2115.44 (16)
O3—Ti_m1(1)—Baxii134.9 (5)Baxvi—Ba—Mg_m2115.44 (16)
O3—Ti_m1(1)—Nb_m1(1)0Baxiii—Ba—W2111.24 (15)
O3iv—Ti_m1(1)—Oh91.6 (5)Baxiii—Ba—W2xvii111.24 (15)
O3iv—Ti_m1(1)—Ohiv88.4 (5)Baxiii—Ba—W_c0
O3iv—Ti_m1(1)—Ba134.9 (5)Baxiii—Ba—Nb_m1(1)102.73 (6)
O3iv—Ti_m1(1)—Baxii45.1 (5)Baxiii—Ba—Nb_m1(1)xviii102.73 (6)
O3iv—Ti_m1(1)—Nb_m1(1)0Baxiii—Ba—Ti_m20.0 (5)
Oh—Ti_m1(1)—Ohiv180.0 (5)Baxiii—Ba—Mg_m20.0 (5)
Oh—Ti_m1(1)—Ba45.1 (2)W2—Ba—W2xvii65.0 (2)
Oh—Ti_m1(1)—Baxii134.9 (2)W2—Ba—W_c0
Oh—Ti_m1(1)—Nb_m1(1)0W2—Ba—Nb_m1(1)78.43 (17)
Ohiv—Ti_m1(1)—Ba134.9 (2)W2—Ba—Nb_m1(1)xviii136.77 (18)
Ohiv—Ti_m1(1)—Baxii45.1 (2)W2—Ba—Ti_m2111.24 (18)
Ohiv—Ti_m1(1)—Nb_m1(1)0W2—Ba—Mg_m2111.24 (18)
Ba—Ti_m1(1)—Baxii180.0 (5)W2xvii—Ba—W_c0
Ba—Ti_m1(1)—Nb_m1(1)0W2xvii—Ba—Nb_m1(1)136.77 (18)
Baxii—Ti_m1(1)—Nb_m1(1)0W2xvii—Ba—Nb_m1(1)xviii78.43 (17)
Na_aiv—Ti_m1(2)—Na_axiv174.8 (2)W2xvii—Ba—Ti_m2111.24 (18)
Na_aiv—Ti_m1(2)—O158.0 (3)W2xvii—Ba—Mg_m2111.24 (18)
Na_aiv—Ti_m1(2)—O1xiii126.7 (3)W_c—Ba—Nb_m1(1)0
Na_aiv—Ti_m1(2)—O6iv43.7 (4)W_c—Ba—Nb_m1(1)xviii0
Na_aiv—Ti_m1(2)—O6xiv131.5 (4)W_c—Ba—Ti_m20
Na_aiv—Ti_m1(2)—Oh122.3 (5)W_c—Ba—Mg_m20
Na_aiv—Ti_m1(2)—Ohxiii58.0 (5)Nb_m1(1)—Ba—Nb_m1(1)xviii119.69 (12)
Na_aiv—Ti_m1(2)—Ba113.8 (2)Nb_m1(1)—Ba—Ti_m2102.73 (6)
Na_aiv—Ti_m1(2)—Baxiii70.8 (2)Nb_m1(1)—Ba—Mg_m2102.73 (6)
Na_aiv—Ti_m1(2)—Ti_m292.62 (15)Nb_m1(1)xviii—Ba—Ti_m2102.73 (6)
Na_aiv—Ti_m1(2)—Mg_m292.62 (15)Nb_m1(1)xviii—Ba—Mg_m2102.73 (6)
Na_axiv—Ti_m1(2)—O1126.7 (3)Ti_m2—Ba—Mg_m20.0 (5)
Na_axiv—Ti_m1(2)—O1xiii58.0 (3)Na_a—W1—Na_ai69.4 (9)
Na_axiv—Ti_m1(2)—O6iv131.5 (4)Na_a—W1—K_bii127.4 (4)
Na_axiv—Ti_m1(2)—O6xiv43.7 (4)Na_a—W1—K_biii125.9 (4)
Na_axiv—Ti_m1(2)—Oh58.0 (5)Na_ai—W1—K_bii125.9 (4)
Na_axiv—Ti_m1(2)—Ohxiii122.3 (5)Na_ai—W1—K_biii127.4 (4)
Na_axiv—Ti_m1(2)—Ba70.8 (2)K_bii—W1—K_biii86.8 (3)
Na_axiv—Ti_m1(2)—Baxiii113.8 (2)Na_av—W2—Na_axiv70.6 (9)
Na_axiv—Ti_m1(2)—Ti_m292.62 (15)Na_av—W2—Ba115.1 (3)
Na_axiv—Ti_m1(2)—Mg_m292.62 (15)Na_av—W2—Baxvi116.9 (3)
O1—Ti_m1(2)—O1xiii82.7 (3)Na_axiv—W2—Ba116.9 (3)
O1—Ti_m1(2)—O6iv89.3 (3)Na_axiv—W2—Baxvi115.1 (3)
O1—Ti_m1(2)—O6xiv170.4 (3)Ba—W2—Baxvi115.0 (3)
O1—Ti_m1(2)—Oh88.5 (5)Fe_m2—W_c—Ba0
O1—Ti_m1(2)—Ohxiii87.3 (5)Fe_m2—W_c—Ti_m20.0 (5)
O1—Ti_m1(2)—Ba56.1 (3)Fe_m2—W_c—Mg_m20.0 (5)
O1—Ti_m1(2)—Baxiii48.8 (4)Ba—W_c—Ti_m20
O1—Ti_m1(2)—Ti_m241.33 (19)Ba—W_c—Mg_m20
O1—Ti_m1(2)—Mg_m241.33 (19)Ti_m2—W_c—Mg_m20.0 (5)
O1xiii—Ti_m1(2)—O6iv170.4 (3)Na_axi—Nb_m1(1)—Na_av180.0 (5)
O1xiii—Ti_m1(2)—O6xiv89.3 (3)Na_axi—Nb_m1(1)—Ti_m1(1)0
O1xiii—Ti_m1(2)—Oh87.3 (5)Na_axi—Nb_m1(1)—O238.2 (4)
O1xiii—Ti_m1(2)—Ohxiii88.5 (5)Na_axi—Nb_m1(1)—O2iv141.8 (4)
O1xiii—Ti_m1(2)—Ba48.8 (4)Na_axi—Nb_m1(1)—O3103.4 (3)
O1xiii—Ti_m1(2)—Baxiii56.1 (3)Na_axi—Nb_m1(1)—O3iv76.6 (3)
O1xiii—Ti_m1(2)—Ti_m241.33 (19)Na_axi—Nb_m1(1)—Oh125.1 (5)
O1xiii—Ti_m1(2)—Mg_m241.33 (19)Na_axi—Nb_m1(1)—Ohiv54.9 (5)
O6iv—Ti_m1(2)—O6xiv99.1 (3)Na_axi—Nb_m1(1)—Ba114.7 (2)
O6iv—Ti_m1(2)—Oh97.8 (6)Na_axi—Nb_m1(1)—Baxii65.3 (2)
O6iv—Ti_m1(2)—Ohxiii85.9 (5)Na_av—Nb_m1(1)—Ti_m1(1)0
O6iv—Ti_m1(2)—Ba129.5 (4)Na_av—Nb_m1(1)—O2141.8 (4)
O6iv—Ti_m1(2)—Baxiii114.5 (3)Na_av—Nb_m1(1)—O2iv38.2 (4)
O6iv—Ti_m1(2)—Ti_m2130.4 (2)Na_av—Nb_m1(1)—O376.6 (3)
O6iv—Ti_m1(2)—Mg_m2130.4 (2)Na_av—Nb_m1(1)—O3iv103.4 (3)
O6xiv—Ti_m1(2)—Oh85.9 (5)Na_av—Nb_m1(1)—Oh54.9 (5)
O6xiv—Ti_m1(2)—Ohxiii97.8 (6)Na_av—Nb_m1(1)—Ohiv125.1 (5)
O6xiv—Ti_m1(2)—Ba114.5 (3)Na_av—Nb_m1(1)—Ba65.3 (2)
O6xiv—Ti_m1(2)—Baxiii129.5 (4)Na_av—Nb_m1(1)—Baxii114.7 (2)
O6xiv—Ti_m1(2)—Ti_m2130.4 (2)Ti_m1(1)—Nb_m1(1)—O20
O6xiv—Ti_m1(2)—Mg_m2130.4 (2)Ti_m1(1)—Nb_m1(1)—O2iv0
Oh—Ti_m1(2)—Ohxiii174.4 (3)Ti_m1(1)—Nb_m1(1)—O30
Oh—Ti_m1(2)—Ba51.55 (18)Ti_m1(1)—Nb_m1(1)—O3iv0
Oh—Ti_m1(2)—Baxiii122.84 (19)Ti_m1(1)—Nb_m1(1)—Oh0
Oh—Ti_m1(2)—Ti_m287.19 (17)Ti_m1(1)—Nb_m1(1)—Ohiv0
Oh—Ti_m1(2)—Mg_m287.19 (17)Ti_m1(1)—Nb_m1(1)—Ba0
Ohxiii—Ti_m1(2)—Ba122.84 (19)Ti_m1(1)—Nb_m1(1)—Baxii0
Ohxiii—Ti_m1(2)—Baxiii51.55 (18)O2—Nb_m1(1)—O2iv180.0 (5)
Ohxiii—Ti_m1(2)—Ti_m287.19 (17)O2—Nb_m1(1)—O388.1 (3)
Ohxiii—Ti_m1(2)—Mg_m287.19 (17)O2—Nb_m1(1)—O3iv91.9 (3)
Ba—Ti_m1(2)—Baxiii71.81 (10)O2—Nb_m1(1)—Oh90.5 (4)
Ba—Ti_m1(2)—Ti_m235.91 (7)O2—Nb_m1(1)—Ohiv89.5 (4)
Ba—Ti_m1(2)—Mg_m235.91 (7)O2—Nb_m1(1)—Ba79.1 (2)
Baxiii—Ti_m1(2)—Ti_m235.91 (7)O2—Nb_m1(1)—Baxii100.9 (2)
Baxiii—Ti_m1(2)—Mg_m235.91 (7)O2iv—Nb_m1(1)—O391.9 (3)
Ti_m2—Ti_m1(2)—Mg_m20.0 (5)O2iv—Nb_m1(1)—O3iv88.1 (3)
O1—Fe_m2—O1xiii84.5 (3)O2iv—Nb_m1(1)—Oh89.5 (4)
O1—Fe_m2—O1xv180.0 (5)O2iv—Nb_m1(1)—Ohiv90.5 (4)
O1—Fe_m2—O1x95.5 (3)O2iv—Nb_m1(1)—Ba100.9 (2)
O1—Fe_m2—Ba95.0 (4)O2iv—Nb_m1(1)—Baxii79.1 (2)
O1—Fe_m2—Baxiii85.0 (4)O3—Nb_m1(1)—O3iv180.0 (5)
O1—Fe_m2—W_c95.0 (4)O3—Nb_m1(1)—Oh88.4 (5)
O1—Fe_m2—W_cxiii85.0 (4)O3—Nb_m1(1)—Ohiv91.6 (5)
O1—Fe_m2—Ti_m20O3—Nb_m1(1)—Ba45.1 (5)
O1—Fe_m2—Mg_m20O3—Nb_m1(1)—Baxii134.9 (5)
O1xiii—Fe_m2—O1xv95.5 (3)O3iv—Nb_m1(1)—Oh91.6 (5)
O1xiii—Fe_m2—O1x180.0 (5)O3iv—Nb_m1(1)—Ohiv88.4 (5)
O1xiii—Fe_m2—Ba85.0 (4)O3iv—Nb_m1(1)—Ba134.9 (5)
O1xiii—Fe_m2—Baxiii95.0 (4)O3iv—Nb_m1(1)—Baxii45.1 (5)
O1xiii—Fe_m2—W_c85.0 (4)Oh—Nb_m1(1)—Ohiv180.0 (5)
O1xiii—Fe_m2—W_cxiii95.0 (4)Oh—Nb_m1(1)—Ba45.1 (2)
O1xiii—Fe_m2—Ti_m20Oh—Nb_m1(1)—Baxii134.9 (2)
O1xiii—Fe_m2—Mg_m20Ohiv—Nb_m1(1)—Ba134.9 (2)
O1xv—Fe_m2—O1x84.5 (3)Ohiv—Nb_m1(1)—Baxii45.1 (2)
O1xv—Fe_m2—Ba85.0 (4)Ba—Nb_m1(1)—Baxii180.0 (5)
O1xv—Fe_m2—Baxiii95.0 (4)Ti_m1(2)—Ti_m2—Ti_m1(2)xv180.0 (5)
O1xv—Fe_m2—W_c85.0 (4)Ti_m1(2)—Ti_m2—Fe_m20
O1xv—Fe_m2—W_cxiii95.0 (4)Ti_m1(2)—Ti_m2—O142.25 (19)
O1xv—Fe_m2—Ti_m20Ti_m1(2)—Ti_m2—O1xiii42.25 (19)
O1xv—Fe_m2—Mg_m20Ti_m1(2)—Ti_m2—O1xv137.75 (19)
O1x—Fe_m2—Ba95.0 (4)Ti_m1(2)—Ti_m2—O1x137.75 (19)
O1x—Fe_m2—Baxiii85.0 (4)Ti_m1(2)—Ti_m2—Ba90
O1x—Fe_m2—W_c95.0 (4)Ti_m1(2)—Ti_m2—Baxiii90
O1x—Fe_m2—W_cxiii85.0 (4)Ti_m1(2)—Ti_m2—W_c90
O1x—Fe_m2—Ti_m20Ti_m1(2)—Ti_m2—W_cxiii90
O1x—Fe_m2—Mg_m20Ti_m1(2)—Ti_m2—Mg_m20
Ba—Fe_m2—Baxiii180.0 (5)Ti_m1(2)xv—Ti_m2—Fe_m20
Ba—Fe_m2—W_c0.0 (5)Ti_m1(2)xv—Ti_m2—O1137.75 (19)
Ba—Fe_m2—W_cxiii180.0 (5)Ti_m1(2)xv—Ti_m2—O1xiii137.75 (19)
Ba—Fe_m2—Ti_m20Ti_m1(2)xv—Ti_m2—O1xv42.25 (19)
Ba—Fe_m2—Mg_m20Ti_m1(2)xv—Ti_m2—O1x42.25 (19)
Baxiii—Fe_m2—W_c180.0 (5)Ti_m1(2)xv—Ti_m2—Ba90
Baxiii—Fe_m2—W_cxiii0.0 (5)Ti_m1(2)xv—Ti_m2—Baxiii90
Baxiii—Fe_m2—Ti_m20Ti_m1(2)xv—Ti_m2—W_c90
Baxiii—Fe_m2—Mg_m20Ti_m1(2)xv—Ti_m2—W_cxiii90
W_c—Fe_m2—W_cxiii180.0 (5)Ti_m1(2)xv—Ti_m2—Mg_m20
W_c—Fe_m2—Ti_m20Fe_m2—Ti_m2—O10
W_c—Fe_m2—Mg_m20Fe_m2—Ti_m2—O1xiii0
W_cxiii—Fe_m2—Ti_m20Fe_m2—Ti_m2—O1xv0
W_cxiii—Fe_m2—Mg_m20Fe_m2—Ti_m2—O1x0
Ti_m2—Fe_m2—Mg_m20Fe_m2—Ti_m2—Ba0
K_b—Si1—K_biii80.22 (18)Fe_m2—Ti_m2—Baxiii0
K_b—Si1—O352.6 (4)Fe_m2—Ti_m2—W_c0
K_b—Si1—O463.0 (4)Fe_m2—Ti_m2—W_cxiii0
K_b—Si1—O6102.5 (3)Fe_m2—Ti_m2—Mg_m20
K_b—Si1—O7145.8 (5)O1—Ti_m2—O1xiii84.5 (3)
K_biii—Si1—O3132.6 (4)O1—Ti_m2—O1xv180.0 (5)
K_biii—Si1—O439.8 (7)O1—Ti_m2—O1x95.5 (3)
K_biii—Si1—O665.4 (5)O1—Ti_m2—Ba95.0 (4)
K_biii—Si1—O7116.0 (6)O1—Ti_m2—Baxiii85.0 (4)
O3—Si1—O4108.4 (6)O1—Ti_m2—W_c95.0 (4)
O3—Si1—O6115.9 (5)O1—Ti_m2—W_cxiii85.0 (4)
O3—Si1—O7107.2 (8)O1—Ti_m2—Mg_m20
O4—Si1—O6104.5 (9)O1xiii—Ti_m2—O1xv95.5 (3)
O4—Si1—O7109.0 (4)O1xiii—Ti_m2—O1x180.0 (5)
O6—Si1—O7111.6 (5)O1xiii—Ti_m2—Ba85.0 (4)
Na_aiv—Si2—K_b163.7 (3)O1xiii—Ti_m2—Baxiii95.0 (4)
Na_aiv—Si2—O164.8 (5)O1xiii—Ti_m2—W_c85.0 (4)
Na_aiv—Si2—O2101.1 (5)O1xiii—Ti_m2—W_cxiii95.0 (4)
Na_aiv—Si2—O5148.1 (7)O1xiii—Ti_m2—Mg_m20
Na_aiv—Si2—O7xi49.3 (5)O1xv—Ti_m2—O1x84.5 (3)
Na_aiv—Si2—Ba123.3 (3)O1xv—Ti_m2—Ba85.0 (4)
K_b—Si2—O1131.3 (4)O1xv—Ti_m2—Baxiii95.0 (4)
K_b—Si2—O270.8 (5)O1xv—Ti_m2—W_c85.0 (4)
K_b—Si2—O538.6 (7)O1xv—Ti_m2—W_cxiii95.0 (4)
K_b—Si2—O7xi119.6 (5)O1xv—Ti_m2—Mg_m20
K_b—Si2—Ba72.43 (14)O1x—Ti_m2—Ba95.0 (4)
O1—Si2—O2114.7 (5)O1x—Ti_m2—Baxiii85.0 (4)
O1—Si2—O5109.4 (6)O1x—Ti_m2—W_c95.0 (4)
O1—Si2—O7xi103.1 (8)O1x—Ti_m2—W_cxiii85.0 (4)
O1—Si2—Ba59.0 (4)O1x—Ti_m2—Mg_m20
O2—Si2—O5109.1 (9)Ba—Ti_m2—Baxiii180.0 (5)
O2—Si2—O7xi112.5 (4)Ba—Ti_m2—W_c0.0 (5)
O2—Si2—Ba96.0 (3)Ba—Ti_m2—W_cxiii180.0 (5)
O5—Si2—O7xi107.6 (4)Ba—Ti_m2—Mg_m20
O5—Si2—Ba64.1 (3)Baxiii—Ti_m2—W_c180.0 (5)
O7xi—Si2—Ba151.2 (5)Baxiii—Ti_m2—W_cxiii0.0 (5)
Ti_m1(2)—O1—Fe_m296.4 (3)Baxiii—Ti_m2—Mg_m20
Ti_m1(2)—O1—Si2122.7 (6)W_c—Ti_m2—W_cxiii180.0 (5)
Ti_m1(2)—O1—Baxiii98.3 (5)W_c—Ti_m2—Mg_m20
Ti_m1(2)—O1—Ti_m296.4 (3)W_cxiii—Ti_m2—Mg_m20
Ti_m1(2)—O1—Mg_m296.4 (3)Ti_m1(2)—Mg_m2—Ti_m1(2)xv180.0 (5)
Fe_m2—O1—Si2124.6 (6)Ti_m1(2)—Mg_m2—Fe_m20
Fe_m2—O1—Baxiii50.2 (3)Ti_m1(2)—Mg_m2—O142.25 (19)
Fe_m2—O1—Ti_m20.0 (5)Ti_m1(2)—Mg_m2—O1xiii42.25 (19)
Fe_m2—O1—Mg_m20.0 (5)Ti_m1(2)—Mg_m2—O1xv137.75 (19)
Si2—O1—Baxiii138.0 (3)Ti_m1(2)—Mg_m2—O1x137.75 (19)
Si2—O1—Ti_m2124.6 (6)Ti_m1(2)—Mg_m2—Ba90
Si2—O1—Mg_m2124.6 (6)Ti_m1(2)—Mg_m2—Baxiii90
Baxiii—O1—Ti_m250.2 (3)Ti_m1(2)—Mg_m2—W_c90
Baxiii—O1—Mg_m250.2 (3)Ti_m1(2)—Mg_m2—W_cxiii90
Ti_m2—O1—Mg_m20.0 (5)Ti_m1(2)—Mg_m2—Ti_m20
Na_axi—O2—Ti_m1(1)109.8 (6)Ti_m1(2)xv—Mg_m2—Fe_m20
Na_axi—O2—Si2119.2 (5)Ti_m1(2)xv—Mg_m2—O1137.75 (19)
Na_axi—O2—Nb_m1(1)109.8 (6)Ti_m1(2)xv—Mg_m2—O1xiii137.75 (19)
Ti_m1(1)—O2—Si2130.8 (4)Ti_m1(2)xv—Mg_m2—O1xv42.25 (19)
Ti_m1(1)—O2—Nb_m1(1)0.0 (5)Ti_m1(2)xv—Mg_m2—O1x42.25 (19)
Si2—O2—Nb_m1(1)130.8 (4)Ti_m1(2)xv—Mg_m2—Ba90
K_b—O3—Ti_m1(1)119.6 (3)Ti_m1(2)xv—Mg_m2—Baxiii90
K_b—O3—Si199.5 (7)Ti_m1(2)xv—Mg_m2—W_c90
K_b—O3—Ba99.2 (3)Ti_m1(2)xv—Mg_m2—W_cxiii90
K_b—O3—Nb_m1(1)119.6 (3)Ti_m1(2)xv—Mg_m2—Ti_m20
Ti_m1(1)—O3—Si1117.7 (4)Fe_m2—Mg_m2—O10
Ti_m1(1)—O3—Ba105.8 (7)Fe_m2—Mg_m2—O1xiii0
Ti_m1(1)—O3—Nb_m1(1)0.0 (5)Fe_m2—Mg_m2—O1xv0
Si1—O3—Ba113.9 (3)Fe_m2—Mg_m2—O1x0
Si1—O3—Nb_m1(1)117.7 (4)Fe_m2—Mg_m2—Ba0
Ba—O3—Nb_m1(1)105.8 (7)Fe_m2—Mg_m2—Baxiii0
K_biii—O4—Si1116.0 (7)Fe_m2—Mg_m2—W_c0
K_biii—O4—Si1x116.0 (7)Fe_m2—Mg_m2—W_cxiii0
Si1—O4—Si1x126.7 (14)Fe_m2—Mg_m2—Ti_m20
K_b—O5—Si2118.1 (7)O1—Mg_m2—O1xiii84.5 (3)
K_b—O5—Si2x118.1 (7)O1—Mg_m2—O1xv180.0 (5)
Si2—O5—Si2x123.8 (14)O1—Mg_m2—O1x95.5 (3)
Na_a—O6—Ti_m1(2)iv101.7 (5)O1—Mg_m2—Ba95.0 (4)
Na_a—O6—Si1120.7 (6)O1—Mg_m2—Baxiii85.0 (4)
Ti_m1(2)iv—O6—Si1130.9 (8)O1—Mg_m2—W_c95.0 (4)
Na_av—O7—Si1120.7 (5)O1—Mg_m2—W_cxiii85.0 (4)
Na_av—O7—Si2ii99.2 (5)O1—Mg_m2—Ti_m20
Si1—O7—Si2ii133.4 (11)O1xiii—Mg_m2—O1xv95.5 (3)
Ti_m1(1)—Oh—Ti_m1(2)129.0 (3)O1xiii—Mg_m2—O1x180.0 (5)
Ti_m1(1)—Oh—Ba105.9 (4)O1xiii—Mg_m2—Ba85.0 (4)
Ti_m1(1)—Oh—Nb_m1(1)0.0 (5)O1xiii—Mg_m2—Baxiii95.0 (4)
Ti_m1(2)—Oh—Ba97.0 (4)O1xiii—Mg_m2—W_c85.0 (4)
Ti_m1(2)—Oh—Nb_m1(1)129.0 (3)O1xiii—Mg_m2—W_cxiii95.0 (4)
Ba—Oh—Nb_m1(1)105.9 (4)O1xiii—Mg_m2—Ti_m20
Na_axx—Ba—Na_axxi33.8 (5)O1xv—Mg_m2—O1x84.5 (3)
Na_axx—Ba—Na_av111.0 (2)O1xv—Mg_m2—Ba85.0 (4)
Na_axx—Ba—Na_axiv100.3 (2)O1xv—Mg_m2—Baxiii95.0 (4)
Na_axx—Ba—K_b126.8 (3)O1xv—Mg_m2—W_c85.0 (4)
Na_axx—Ba—Ti_m1(1)163.04 (19)O1xv—Mg_m2—W_cxiii95.0 (4)
Na_axx—Ba—Ti_m1(1)xviii68.2 (2)O1xv—Mg_m2—Ti_m20
Na_axx—Ba—Ti_m1(2)127.8 (3)O1x—Mg_m2—Ba95.0 (4)
Na_axx—Ba—Ti_m1(2)xv50.87 (19)O1x—Mg_m2—Baxiii85.0 (4)
Na_axx—Ba—Fe_m289.1 (3)O1x—Mg_m2—W_c95.0 (4)
Na_axx—Ba—Si2145.1 (2)O1x—Mg_m2—W_cxiii85.0 (4)
Na_axx—Ba—Si2x100.31 (15)O1x—Mg_m2—Ti_m20
Na_axx—Ba—O1xiii95.1 (4)Ba—Mg_m2—Baxiii180.0 (5)
Na_axx—Ba—O1xv44.3 (4)Ba—Mg_m2—W_c0.0 (5)
Na_axx—Ba—O3144.4 (4)Ba—Mg_m2—W_cxiii180.0 (5)
Na_axx—Ba—O3x88.2 (3)Ba—Mg_m2—Ti_m20
Na_axx—Ba—Oh144.1 (3)Baxiii—Mg_m2—W_c180.0 (5)
Na_axx—Ba—Ohx44.3 (2)Baxiii—Mg_m2—W_cxiii0.0 (5)
Na_axx—Ba—Baxvi55.13 (15)Baxiii—Mg_m2—Ti_m20
Na_axx—Ba—Baxiii89.1 (3)W_c—Mg_m2—W_cxiii180.0 (5)
Na_axx—Ba—W286.0 (2)W_c—Mg_m2—Ti_m20
Na_axx—Ba—W2xvii26.5 (3)W_cxiii—Mg_m2—Ti_m20
Na_axx—Ba—W_c0
Symmetry codes: (i) x+1, y, z; (ii) x, y, z1; (iii) x+1, y, z+1; (iv) x+1/2, y+1/2, z+1; (v) x+1/2, y+1/2, z; (vi) x+1/2, y+1/2, z; (vii) x+1/2, y+1/2, z; (viii) x+1, y, z+2; (ix) x+1, y, z+1; (x) x, y, z; (xi) x, y, z+1; (xii) x+1/2, y+1/2, z+1; (xiii) x, y, z+1; (xiv) x1/2, y+1/2, z; (xv) x, y, z+1; (xvi) x, y, z; (xvii) x, y, z; (xviii) x+1/2, y1/2, z+1; (xix) x, y, z+1; (xx) x1/2, y1/2, z; (xxi) x+1/2, y1/2, z.
(labu-Fe_16.3) top
Crystal data top
Ba0.7Fe0.5K2.1Mg0.05Na2Nb0.1O33Si8Ti4Z = 2
Mr = 1206.8F(000) = 1167
Monoclinic, C2/mDx = 3.476 Mg m3
Hall symbol: -C 2ySynchrotron radiation, λ = 0.414 Å
a = 13.535 (8) ÅCell parameters from 2728 reflections
b = 13.1485 (5) Åθ = 1.8–19.0°
c = 7.2026 (17) ŵ = 0.92 mm1
β = 115.94 (4)°T = 293 K
V = 1152.7 (8) Å3Anhedral grain
Data collection top
ESRF ID 09
diffractometer
θmax = 19.0°, θmin = 1.8°
2728 measured reflectionsh = 87
776 independent reflectionsk = 2020
501 reflections with I > 2σ(I)l = 910
Rint = 0.047
Refinement top
Refinement on F0 restraints
R[F2 > 2σ(F2)] = 0.0936 constraints
wR(F2) = 0.148Weighting scheme based on measured s.u.'s w = 1/(σ2(F) + 0.0100000007F2)
S = 1.11(Δ/σ)max = 0.048
776 reflectionsΔρmax = 1.08 e Å3
57 parametersΔρmin = 1.32 e Å3
Fractional atomic coordinates and isotropic or equivalent isotropic displacement parameters (Å2) top
xyzUiso*/UeqOcc. (<1)
Na_a0.418 (2)0.2704 (8)0.0128 (17)0.035 (3)*0.5
K_b0.4358 (9)00.7315 (7)0.0362 (12)*
Ti_m1(1)0.250.250.50.0196 (7)*0.95
Ti_m1(2)00.2177 (2)0.50.0181 (7)*
Fe_m2000.50.0309 (16)*0.5
Si10.3307 (6)0.10970 (19)0.2709 (4)0.0113 (7)*
Si20.2104 (5)0.10875 (18)0.8196 (4)0.0103 (7)*
O10.0805 (14)0.1047 (5)0.6816 (11)0.0149 (17)*
O20.2704 (14)0.1987 (5)0.7670 (11)0.0145 (16)*
O30.2876 (15)0.1156 (5)0.4395 (11)0.0141 (15)*
O40.3877 (19)00.2925 (15)0.013 (2)*
O50.272 (2)00.7986 (16)0.016 (2)*
O60.4180 (16)0.1883 (7)0.2876 (13)0.024 (2)*
O70.2200 (15)0.1143 (5)0.0522 (11)0.0145 (16)*
Oh0.0981 (14)0.2098 (5)0.3825 (11)0.0118 (15)*
Ba0.0963 (5)00.3344 (4)0.0179 (7)*0.35
W10.50.1435 (11)00.038 (4)*
W200.1077 (9)00.033 (3)*
W_c0.0963 (5)00.3344 (4)0.0179 (7)*0.65
Nb_m1(1)0.250.250.50.0196 (7)*0.05
Ti_m2000.50.0309 (16)*0.1
Mg_m2000.50.0309 (16)*0.05
Atomic displacement parameters (Å2) top
U11U22U33U12U13U23
???????
Geometric parameters (Å, º) top
Na_a—Na_ai2.30 (4)Ti_m1(2)—Oh1.864 (18)
Na_a—K_bii4.150 (14)Ti_m1(2)—Ohxiii1.864 (18)
Na_a—K_biii4.093 (13)Ti_m1(2)—Ba3.560 (4)
Na_a—Ti_m1(1)ii3.397 (12)Ti_m1(2)—Baxiii3.560 (4)
Na_a—Ti_m1(2)iv3.188 (13)Ti_m1(2)—Ti_m22.862 (3)
Na_a—Si2iv2.98 (2)Ti_m1(2)—Mg_m22.862 (3)
Na_a—O2ii2.22 (2)Fe_m2—O11.883 (8)
Na_a—O62.26 (2)Fe_m2—O1xiii1.883 (8)
Na_a—O7v2.29 (3)Fe_m2—O1xv1.883 (8)
Na_a—Bavi3.925 (14)Fe_m2—O1x1.883 (8)
Na_a—Bavii3.870 (13)Fe_m2—Ba2.117 (6)
Na_a—W12.03 (2)Fe_m2—Baxiii2.117 (6)
Na_a—W2v1.97 (2)Fe_m2—W_c2.117 (6)
Na_a—Nb_m1(1)ii3.397 (12)Fe_m2—W_cxiii2.117 (6)
K_b—K_biii4.384 (15)Fe_m2—Ti_m20
K_b—K_bviii3.478 (7)Fe_m2—Mg_m20
K_b—Si13.314 (5)Si1—O31.562 (18)
K_b—Si1iii3.481 (14)Si1—O41.611 (12)
K_b—Si1ix3.481 (14)Si1—O61.535 (19)
K_b—Si1x3.314 (5)Si1—O71.633 (12)
K_b—Si23.667 (14)Si2—O11.597 (17)
K_b—Si2x3.667 (14)Si2—O21.572 (15)
K_b—O32.657 (12)Si2—O7xi1.625 (12)
K_b—O3x2.657 (12)Si2—Ba3.452 (4)
K_b—O4iii2.47 (3)O1—Baxiii2.720 (18)
K_b—O52.46 (3)O1—Ti_m21.883 (8)
K_b—Ba4.218 (13)O1—Mg_m21.883 (8)
K_b—W1xi2.566 (12)O2—Nb_m1(1)1.941 (10)
K_b—W1ix2.566 (12)O3—Ba2.806 (18)
Ti_m1(1)—O21.941 (10)O3—Nb_m1(1)1.941 (10)
Ti_m1(1)—O2iv1.941 (10)Oh—Ba2.778 (6)
Ti_m1(1)—O31.941 (10)Oh—Nb_m1(1)1.923 (17)
Ti_m1(1)—O3iv1.941 (10)Ba—Baxvi4.360 (5)
Ti_m1(1)—Oh1.923 (17)Ba—Baxiii4.234 (9)
Ti_m1(1)—Ohiv1.923 (17)Ba—W22.600 (7)
Ti_m1(1)—Ba3.793 (3)Ba—W2xvii2.600 (7)
Ti_m1(1)—Baxii3.793 (3)Ba—W_c0
Ti_m1(1)—Nb_m1(1)0Ba—Nb_m1(1)3.793 (3)
Ti_m1(2)—Fe_m22.862 (3)Ba—Nb_m1(1)xviii3.793 (3)
Ti_m1(2)—O11.964 (8)Ba—Ti_m22.117 (6)
Ti_m1(2)—O1xiii1.964 (8)Ba—Mg_m22.117 (6)
Ti_m1(2)—O6iv1.901 (9)W_c—Ti_m22.117 (6)
Ti_m1(2)—O6xiv1.901 (9)Ti_m2—Mg_m20
Na_ai—Na_a—K_bii72.4 (5)Ti_m1(2)—Oh—Nb_m1(1)128.4 (4)
Na_ai—Na_a—K_biii75.2 (6)Ba—Oh—Nb_m1(1)106.1 (6)
Na_ai—Na_a—Ti_m1(1)ii97.1 (6)Na_axx—Ba—Na_axxi34.3 (6)
Na_ai—Na_a—Ti_m1(2)iv101.9 (7)Na_axx—Ba—Na_av112.0 (3)
Na_ai—Na_a—Si2iv141.9 (6)Na_axx—Ba—Na_axiv100.6 (3)
Na_ai—Na_a—O2ii120.0 (9)Na_axx—Ba—K_b127.3 (3)
Na_ai—Na_a—O6116.2 (10)Na_axx—Ba—Ti_m1(1)164.4 (2)
Na_ai—Na_a—O7v135.4 (8)Na_axx—Ba—Ti_m1(1)xviii68.3 (3)
Na_ai—Na_a—Bavi71.5 (5)Na_axx—Ba—Ti_m1(2)126.6 (4)
Na_ai—Na_a—Bavii74.2 (6)Na_axx—Ba—Ti_m1(2)xv50.1 (2)
Na_ai—Na_a—W155.4 (8)Na_axx—Ba—Fe_m287.8 (4)
Na_ai—Na_a—W2v54.3 (8)Na_axx—Ba—Si2143.4 (3)
Na_ai—Na_a—Nb_m1(1)ii97.1 (6)Na_axx—Ba—Si2x99.56 (19)
K_bii—Na_a—K_biii49.92 (18)Na_axx—Ba—O1xiii93.6 (5)
K_bii—Na_a—Ti_m1(1)ii63.6 (2)Na_axx—Ba—O1xv44.3 (5)
K_bii—Na_a—Ti_m1(2)iv120.9 (3)Na_axx—Ba—O3146.3 (5)
K_bii—Na_a—Si2iv145.5 (8)Na_axx—Ba—O3x89.9 (4)
K_bii—Na_a—O2ii58.1 (5)Na_axx—Ba—Oh143.8 (4)
K_bii—Na_a—O692.3 (4)Na_axx—Ba—Ohx43.9 (3)
K_bii—Na_a—O7v133.1 (6)Na_axx—Ba—Baxvi55.39 (18)
K_bii—Na_a—Bavi142.7 (8)Na_axx—Ba—Baxiii87.8 (4)
K_bii—Na_a—Bavii110.5 (4)Na_axx—Ba—W286.7 (3)
K_bii—Na_a—W128.8 (3)Na_axx—Ba—W2xvii26.4 (3)
K_bii—Na_a—W2v121.4 (10)Na_axx—Ba—W_c0
K_bii—Na_a—Nb_m1(1)ii63.6 (2)Na_axx—Ba—Nb_m1(1)164.4 (2)
K_biii—Na_a—Ti_m1(1)ii112.5 (3)Na_axx—Ba—Nb_m1(1)xviii68.3 (3)
K_biii—Na_a—Ti_m1(2)iv71.4 (2)Na_axx—Ba—Ti_m287.8 (4)
K_biii—Na_a—Si2iv122.3 (5)Na_axx—Ba—Mg_m287.8 (4)
K_biii—Na_a—O2ii94.5 (4)Na_axxi—Ba—Na_av102.5 (3)
K_biii—Na_a—O651.3 (5)Na_axxi—Ba—Na_axiv112.0 (3)
K_biii—Na_a—O7v149.0 (10)Na_axxi—Ba—K_b99.8 (4)
K_biii—Na_a—Bavi110.6 (4)Na_axxi—Ba—Ti_m1(1)138.2 (4)
K_biii—Na_a—Bavii147.8 (8)Na_axxi—Ba—Ti_m1(1)xviii52.6 (2)
K_biii—Na_a—W130.6 (3)Na_axxi—Ba—Ti_m1(2)157.1 (4)
K_biii—Na_a—W2v123.8 (10)Na_axxi—Ba—Ti_m1(2)xv70.5 (3)
K_biii—Na_a—Nb_m1(1)ii112.5 (3)Na_axxi—Ba—Fe_m2119.6 (4)
Ti_m1(1)ii—Na_a—Ti_m1(2)iv161.0 (10)Na_axxi—Ba—Si2148.3 (2)
Ti_m1(1)ii—Na_a—Si2iv104.5 (6)Na_axxi—Ba—Si2x101.82 (17)
Ti_m1(1)ii—Na_a—O2ii32.6 (4)Na_axxi—Ba—O1xiii124.9 (4)
Ti_m1(1)ii—Na_a—O6131.2 (9)Na_axxi—Ba—O1xv77.4 (5)
Ti_m1(1)ii—Na_a—O7v74.4 (4)Na_axxi—Ba—O3112.1 (5)
Ti_m1(1)ii—Na_a—Bavi130.5 (4)Na_axxi—Ba—O3x62.1 (4)
Ti_m1(1)ii—Na_a—Bavii62.5 (2)Na_axxi—Ba—Oh148.2 (3)
Ti_m1(1)ii—Na_a—W190.3 (4)Na_axxi—Ba—Ohx45.7 (3)
Ti_m1(1)ii—Na_a—W2v97.8 (5)Na_axxi—Ba—Baxvi56.58 (19)
Ti_m1(1)ii—Na_a—Nb_m1(1)ii0.0 (5)Na_axxi—Ba—Baxiii119.6 (4)
Ti_m1(2)iv—Na_a—Si2iv60.7 (4)Na_axxi—Ba—W287.9 (3)
Ti_m1(2)iv—Na_a—O2ii131.0 (11)Na_axxi—Ba—W2xvii27.5 (3)
Ti_m1(2)iv—Na_a—O636.0 (3)Na_axxi—Ba—W_c0
Ti_m1(2)iv—Na_a—O7v93.0 (7)Na_axxi—Ba—Nb_m1(1)138.2 (4)
Ti_m1(2)iv—Na_a—Bavi59.0 (2)Na_axxi—Ba—Nb_m1(1)xviii52.6 (2)
Ti_m1(2)iv—Na_a—Bavii124.6 (3)Na_axxi—Ba—Ti_m2119.6 (4)
Ti_m1(2)iv—Na_a—W199.0 (4)Na_axxi—Ba—Mg_m2119.6 (4)
Ti_m1(2)iv—Na_a—W2v94.6 (4)Na_av—Ba—Na_axiv34.3 (6)
Ti_m1(2)iv—Na_a—Nb_m1(1)ii161.0 (10)Na_av—Ba—K_b99.8 (4)
Si2iv—Na_a—O2ii93.8 (10)Na_av—Ba—Ti_m1(1)52.6 (2)
Si2iv—Na_a—O671.0 (8)Na_av—Ba—Ti_m1(1)xviii138.2 (4)
Si2iv—Na_a—O7v32.8 (4)Na_av—Ba—Ti_m1(2)70.5 (3)
Si2iv—Na_a—Bavi70.5 (3)Na_av—Ba—Ti_m1(2)xv157.1 (4)
Si2iv—Na_a—Bavii88.4 (3)Na_av—Ba—Fe_m2119.6 (4)
Si2iv—Na_a—W1152.4 (8)Na_av—Ba—Si2101.82 (17)
Si2iv—Na_a—W2v91.4 (5)Na_av—Ba—Si2x148.3 (2)
Si2iv—Na_a—Nb_m1(1)ii104.5 (6)Na_av—Ba—O1xiii77.4 (5)
O2ii—Na_a—O698.6 (10)Na_av—Ba—O1xv124.9 (4)
O2ii—Na_a—O7v75.4 (8)Na_av—Ba—O362.1 (4)
O2ii—Na_a—Bavi154.7 (6)Na_av—Ba—O3x112.1 (5)
O2ii—Na_a—Bavii92.5 (4)Na_av—Ba—Oh45.7 (3)
O2ii—Na_a—W186.2 (5)Na_av—Ba—Ohx148.2 (3)
O2ii—Na_a—W2v129.5 (6)Na_av—Ba—Baxvi56.58 (19)
O2ii—Na_a—Nb_m1(1)ii32.6 (4)Na_av—Ba—Baxiii119.6 (4)
O6—Na_a—O7v100.4 (12)Na_av—Ba—W227.5 (3)
O6—Na_a—Bavi95.0 (4)Na_av—Ba—W2xvii87.9 (3)
O6—Na_a—Bavii157.1 (7)Na_av—Ba—W_c0
O6—Na_a—W181.7 (6)Na_av—Ba—Nb_m1(1)52.6 (2)
O6—Na_a—W2v130.2 (6)Na_av—Ba—Nb_m1(1)xviii138.2 (4)
O6—Na_a—Nb_m1(1)ii131.2 (9)Na_av—Ba—Ti_m2119.6 (4)
O7v—Na_a—Bavi81.2 (4)Na_av—Ba—Mg_m2119.6 (4)
O7v—Na_a—Bavii63.0 (5)Na_axiv—Ba—K_b127.3 (3)
O7v—Na_a—W1161.6 (9)Na_axiv—Ba—Ti_m1(1)68.3 (3)
O7v—Na_a—W2v83.0 (6)Na_axiv—Ba—Ti_m1(1)xviii164.4 (2)
O7v—Na_a—Nb_m1(1)ii74.4 (4)Na_axiv—Ba—Ti_m1(2)50.1 (2)
Bavi—Na_a—Bavii68.0 (2)Na_axiv—Ba—Ti_m1(2)xv126.6 (4)
Bavi—Na_a—W1117.0 (9)Na_axiv—Ba—Fe_m287.8 (4)
Bavi—Na_a—W2v35.9 (2)Na_axiv—Ba—Si299.56 (19)
Bavi—Na_a—Nb_m1(1)ii130.5 (4)Na_axiv—Ba—Si2x143.4 (3)
Bavii—Na_a—W1119.2 (9)Na_axiv—Ba—O1xiii44.3 (5)
Bavii—Na_a—W2v37.5 (2)Na_axiv—Ba—O1xv93.6 (5)
Bavii—Na_a—Nb_m1(1)ii62.5 (2)Na_axiv—Ba—O389.9 (4)
W1—Na_a—W2v109.8 (14)Na_axiv—Ba—O3x146.3 (5)
W1—Na_a—Nb_m1(1)ii90.3 (4)Na_axiv—Ba—Oh43.9 (3)
W2v—Na_a—Nb_m1(1)ii97.8 (5)Na_axiv—Ba—Ohx143.8 (4)
Na_axi—K_b—Na_aiii32.4 (6)Na_axiv—Ba—Baxvi55.39 (18)
Na_axi—K_b—Na_aix130.1 (3)Na_axiv—Ba—Baxiii87.8 (4)
Na_axi—K_b—Na_axix117.9 (4)Na_axiv—Ba—W226.4 (3)
Na_axi—K_b—K_biii119.8 (3)Na_axiv—Ba—W2xvii86.7 (3)
Na_axi—K_b—K_bviii64.19 (18)Na_axiv—Ba—W_c0
Na_axi—K_b—Si191.42 (18)Na_axiv—Ba—Nb_m1(1)68.3 (3)
Na_axi—K_b—Si1iii83.9 (4)Na_axiv—Ba—Nb_m1(1)xviii164.4 (2)
Na_axi—K_b—Si1ix127.1 (4)Na_axiv—Ba—Ti_m287.8 (4)
Na_axi—K_b—Si1x140.4 (2)Na_axiv—Ba—Mg_m287.8 (4)
Na_axi—K_b—Si249.6 (4)K_b—Ba—Ti_m1(1)60.12 (7)
Na_axi—K_b—Si2x91.2 (4)K_b—Ba—Ti_m1(1)xviii60.12 (7)
Na_axi—K_b—O373.3 (3)K_b—Ba—Ti_m1(2)102.87 (9)
Na_axi—K_b—O3x133.8 (6)K_b—Ba—Ti_m1(2)xv102.87 (9)
Na_axi—K_b—O4iii107.3 (4)K_b—Ba—Fe_m2111.99 (16)
Na_axi—K_b—O569.9 (4)K_b—Ba—Si256.05 (17)
Na_axi—K_b—Ba93.0 (4)K_b—Ba—Si2x56.05 (17)
Na_axi—K_b—W1xi22.3 (3)K_b—Ba—O1xiii134.9 (2)
Na_axi—K_b—W1ix109.6 (3)K_b—Ba—O1xv134.9 (2)
Na_aiii—K_b—Na_aix120.6 (4)K_b—Ba—O338.19 (19)
Na_aiii—K_b—Na_axix130.1 (3)K_b—Ba—O3x38.19 (19)
Na_aiii—K_b—K_biii93.9 (4)K_b—Ba—Oh88.2 (3)
Na_aiii—K_b—K_bviii65.89 (19)K_b—Ba—Ohx88.2 (3)
Na_aiii—K_b—Si189.06 (18)K_b—Ba—Baxvi134.1 (2)
Na_aiii—K_b—Si1iii51.8 (4)K_b—Ba—Baxiii111.99 (15)
Na_aiii—K_b—Si1ix95.8 (5)K_b—Ba—W2125.7 (2)
Na_aiii—K_b—Si1x137.7 (3)K_b—Ba—W2xvii125.7 (2)
Na_aiii—K_b—Si281.8 (4)K_b—Ba—W_c0
Na_aiii—K_b—Si2x122.4 (4)K_b—Ba—Nb_m1(1)60.12 (7)
Na_aiii—K_b—O384.7 (3)K_b—Ba—Nb_m1(1)xviii60.12 (7)
Na_aiii—K_b—O3x154.3 (3)K_b—Ba—Ti_m2111.99 (16)
Na_aiii—K_b—O4iii74.9 (4)K_b—Ba—Mg_m2111.99 (16)
Na_aiii—K_b—O5102.1 (4)Ti_m1(1)—Ba—Ti_m1(1)xviii120.15 (15)
Na_aiii—K_b—Ba118.2 (3)Ti_m1(1)—Ba—Ti_m1(2)55.16 (4)
Na_aiii—K_b—W1xi23.7 (4)Ti_m1(1)—Ba—Ti_m1(2)xv145.32 (9)
Na_aiii—K_b—W1ix111.2 (3)Ti_m1(1)—Ba—Fe_m2102.18 (7)
Na_aix—K_b—Na_axix32.4 (6)Ti_m1(1)—Ba—Si251.82 (8)
Na_aix—K_b—K_biii93.9 (4)Ti_m1(1)—Ba—Si2x95.73 (9)
Na_aix—K_b—K_bviii65.89 (19)Ti_m1(1)—Ba—O1xiii85.8 (2)
Na_aix—K_b—Si1137.7 (3)Ti_m1(1)—Ba—O1xv143.5 (3)
Na_aix—K_b—Si1iii95.8 (5)Ti_m1(1)—Ba—O329.7 (3)
Na_aix—K_b—Si1ix51.8 (4)Ti_m1(1)—Ba—O3x94.0 (3)
Na_aix—K_b—Si1x89.06 (18)Ti_m1(1)—Ba—Oh29.2 (4)
Na_aix—K_b—Si2122.4 (4)Ti_m1(1)—Ba—Ohx147.9 (3)
Na_aix—K_b—Si2x81.8 (4)Ti_m1(1)—Ba—Baxvi109.15 (7)
Na_aix—K_b—O3154.3 (3)Ti_m1(1)—Ba—Baxiii102.18 (8)
Na_aix—K_b—O3x84.7 (3)Ti_m1(1)—Ba—W278.6 (2)
Na_aix—K_b—O4iii74.9 (4)Ti_m1(1)—Ba—W2xvii138.3 (2)
Na_aix—K_b—O5102.1 (4)Ti_m1(1)—Ba—W_c0
Na_aix—K_b—Ba118.2 (3)Ti_m1(1)—Ba—Nb_m1(1)0.0 (5)
Na_aix—K_b—W1xi111.2 (3)Ti_m1(1)—Ba—Nb_m1(1)xviii120.15 (15)
Na_aix—K_b—W1ix23.7 (4)Ti_m1(1)—Ba—Ti_m2102.18 (7)
Na_axix—K_b—K_biii119.8 (3)Ti_m1(1)—Ba—Mg_m2102.18 (7)
Na_axix—K_b—K_bviii64.19 (18)Ti_m1(1)xviii—Ba—Ti_m1(2)145.32 (9)
Na_axix—K_b—Si1140.4 (2)Ti_m1(1)xviii—Ba—Ti_m1(2)xv55.16 (4)
Na_axix—K_b—Si1iii127.1 (4)Ti_m1(1)xviii—Ba—Fe_m2102.18 (7)
Na_axix—K_b—Si1ix83.9 (4)Ti_m1(1)xviii—Ba—Si295.73 (9)
Na_axix—K_b—Si1x91.42 (18)Ti_m1(1)xviii—Ba—Si2x51.82 (8)
Na_axix—K_b—Si291.2 (4)Ti_m1(1)xviii—Ba—O1xiii143.5 (3)
Na_axix—K_b—Si2x49.6 (4)Ti_m1(1)xviii—Ba—O1xv85.8 (2)
Na_axix—K_b—O3133.8 (6)Ti_m1(1)xviii—Ba—O394.0 (3)
Na_axix—K_b—O3x73.3 (3)Ti_m1(1)xviii—Ba—O3x29.7 (3)
Na_axix—K_b—O4iii107.3 (4)Ti_m1(1)xviii—Ba—Oh147.9 (3)
Na_axix—K_b—O569.9 (4)Ti_m1(1)xviii—Ba—Ohx29.2 (4)
Na_axix—K_b—Ba93.0 (4)Ti_m1(1)xviii—Ba—Baxvi109.15 (7)
Na_axix—K_b—W1xi109.6 (3)Ti_m1(1)xviii—Ba—Baxiii102.18 (8)
Na_axix—K_b—W1ix22.3 (3)Ti_m1(1)xviii—Ba—W2138.3 (2)
K_biii—K_b—K_bviii132.4 (4)Ti_m1(1)xviii—Ba—W2xvii78.6 (2)
K_biii—K_b—Si151.5 (2)Ti_m1(1)xviii—Ba—W_c0
K_biii—K_b—Si1iii48.16 (18)Ti_m1(1)xviii—Ba—Nb_m1(1)120.15 (15)
K_biii—K_b—Si1ix48.16 (18)Ti_m1(1)xviii—Ba—Nb_m1(1)xviii0.0 (5)
K_biii—K_b—Si1x51.5 (2)Ti_m1(1)xviii—Ba—Ti_m2102.18 (7)
K_biii—K_b—Si2140.22 (15)Ti_m1(1)xviii—Ba—Mg_m2102.18 (7)
K_biii—K_b—Si2x140.22 (15)Ti_m1(2)—Ba—Ti_m1(2)xv107.03 (16)
K_biii—K_b—O379.1 (4)Ti_m1(2)—Ba—Fe_m253.51 (8)
K_biii—K_b—O3x79.1 (4)Ti_m1(2)—Ba—Si252.77 (10)
K_biii—K_b—O4iii39.6 (3)Ti_m1(2)—Ba—Si2x93.50 (12)
K_biii—K_b—O5147.0 (3)Ti_m1(2)—Ba—O1xiii33.1 (2)
K_biii—K_b—Ba99.28 (17)Ti_m1(2)—Ba—O1xv88.7 (3)
K_biii—K_b—W1xi117.2 (3)Ti_m1(2)—Ba—O384.5 (3)
K_biii—K_b—W1ix117.2 (3)Ti_m1(2)—Ba—O3x140.80 (18)
K_bviii—K_b—Si1154.16 (6)Ti_m1(2)—Ba—Oh31.2 (4)
K_bviii—K_b—Si1iii89.6 (3)Ti_m1(2)—Ba—Ohx137.8 (4)
K_bviii—K_b—Si1ix89.6 (3)Ti_m1(2)—Ba—Baxvi103.92 (10)
K_bviii—K_b—Si1x154.16 (6)Ti_m1(2)—Ba—Baxiii53.51 (8)
K_bviii—K_b—Si281.8 (3)Ti_m1(2)—Ba—W276.3 (2)
K_bviii—K_b—Si2x81.8 (3)Ti_m1(2)—Ba—W2xvii129.8 (2)
K_bviii—K_b—O3135.8 (4)Ti_m1(2)—Ba—W_c0
K_bviii—K_b—O3x135.8 (4)Ti_m1(2)—Ba—Nb_m1(1)55.16 (4)
K_bviii—K_b—O4iii92.8 (4)Ti_m1(2)—Ba—Nb_m1(1)xviii145.32 (9)
K_bviii—K_b—O580.6 (4)Ti_m1(2)—Ba—Ti_m253.51 (8)
K_bviii—K_b—Ba128.3 (4)Ti_m1(2)—Ba—Mg_m253.51 (8)
K_bviii—K_b—W1xi47.3 (2)Ti_m1(2)xv—Ba—Fe_m253.51 (8)
K_bviii—K_b—W1ix47.3 (2)Ti_m1(2)xv—Ba—Si293.50 (12)
Si1—K_b—Si1iii78.9 (2)Ti_m1(2)xv—Ba—Si2x52.77 (10)
Si1—K_b—Si1ix99.7 (3)Ti_m1(2)xv—Ba—O1xiii88.7 (3)
Si1—K_b—Si1x51.61 (10)Ti_m1(2)xv—Ba—O1xv33.1 (2)
Si1—K_b—Si288.8 (2)Ti_m1(2)xv—Ba—O3140.80 (18)
Si1—K_b—Si2x108.5 (3)Ti_m1(2)xv—Ba—O3x84.5 (3)
Si1—K_b—O327.6 (4)Ti_m1(2)xv—Ba—Oh137.8 (4)
Si1—K_b—O3x67.2 (2)Ti_m1(2)xv—Ba—Ohx31.2 (4)
Si1—K_b—O4iii86.2 (3)Ti_m1(2)xv—Ba—Baxvi103.92 (10)
Si1—K_b—O599.6 (4)Ti_m1(2)xv—Ba—Baxiii53.51 (8)
Si1—K_b—Ba57.19 (19)Ti_m1(2)xv—Ba—W2129.8 (2)
Si1—K_b—W1xi106.9 (2)Ti_m1(2)xv—Ba—W2xvii76.3 (2)
Si1—K_b—W1ix158.4 (3)Ti_m1(2)xv—Ba—W_c0
Si1iii—K_b—Si1ix49.0 (2)Ti_m1(2)xv—Ba—Nb_m1(1)145.32 (9)
Si1iii—K_b—Si1x99.7 (3)Ti_m1(2)xv—Ba—Nb_m1(1)xviii55.16 (4)
Si1iii—K_b—Si2131.70 (9)Ti_m1(2)xv—Ba—Ti_m253.51 (8)
Si1iii—K_b—Si2x171.22 (16)Ti_m1(2)xv—Ba—Mg_m253.51 (8)
Si1iii—K_b—O397.6 (4)Fe_m2—Ba—Si262.78 (14)
Si1iii—K_b—O3x127.3 (5)Fe_m2—Ba—Si2x62.78 (14)
Si1iii—K_b—O4iii24.69 (11)Fe_m2—Ba—O1xiii43.7 (2)
Si1iii—K_b—O5153.72 (15)Fe_m2—Ba—O1xv43.7 (2)
Si1iii—K_b—Ba135.94 (15)Fe_m2—Ba—O3124.8 (3)
Si1iii—K_b—W1xi71.9 (2)Fe_m2—Ba—O3x124.8 (3)
Si1iii—K_b—W1ix107.4 (3)Fe_m2—Ba—Oh84.5 (4)
Si1ix—K_b—Si1x78.9 (2)Fe_m2—Ba—Ohx84.5 (4)
Si1ix—K_b—Si2171.22 (16)Fe_m2—Ba—Baxvi113.9 (2)
Si1ix—K_b—Si2x131.70 (9)Fe_m2—Ba—Baxiii0.0 (5)
Si1ix—K_b—O3127.3 (5)Fe_m2—Ba—W2109.8 (2)
Si1ix—K_b—O3x97.6 (4)Fe_m2—Ba—W2xvii109.8 (2)
Si1ix—K_b—O4iii24.69 (11)Fe_m2—Ba—W_c0
Si1ix—K_b—O5153.72 (15)Fe_m2—Ba—Nb_m1(1)102.18 (7)
Si1ix—K_b—Ba135.94 (15)Fe_m2—Ba—Nb_m1(1)xviii102.18 (7)
Si1ix—K_b—W1xi107.4 (3)Fe_m2—Ba—Ti_m20.0 (5)
Si1ix—K_b—W1ix71.9 (2)Fe_m2—Ba—Mg_m20.0 (5)
Si1x—K_b—Si2108.5 (3)Si2—Ba—Si2x48.93 (7)
Si1x—K_b—Si2x88.8 (2)Si2—Ba—O1xiii80.1 (2)
Si1x—K_b—O367.2 (2)Si2—Ba—O1xv104.4 (3)
Si1x—K_b—O3x27.6 (4)Si2—Ba—O363.3 (3)
Si1x—K_b—O4iii86.2 (3)Si2—Ba—O3x90.0 (2)
Si1x—K_b—O599.6 (4)Si2—Ba—Oh59.14 (15)
Si1x—K_b—Ba57.19 (19)Si2—Ba—Ohx108.02 (16)
Si1x—K_b—W1xi158.4 (3)Si2—Ba—Baxvi154.78 (7)
Si1x—K_b—W1ix106.9 (2)Si2—Ba—Baxiii62.78 (16)
Si2—K_b—Si2x45.90 (17)Si2—Ba—W2122.2 (2)
Si2—K_b—O361.1 (4)Si2—Ba—W2xvii169.8 (2)
Si2—K_b—O3x87.9 (5)Si2—Ba—W_c0
Si2—K_b—O4iii156.29 (12)Si2—Ba—Nb_m1(1)51.82 (8)
Si2—K_b—O522.95 (10)Si2—Ba—Nb_m1(1)xviii95.73 (9)
Si2—K_b—Ba51.35 (17)Si2—Ba—Ti_m262.78 (14)
Si2—K_b—W1xi67.4 (2)Si2—Ba—Mg_m262.78 (14)
Si2—K_b—W1ix100.9 (3)Si2x—Ba—O1xiii104.4 (3)
Si2x—K_b—O387.9 (5)Si2x—Ba—O1xv80.1 (2)
Si2x—K_b—O3x61.1 (4)Si2x—Ba—O390.0 (2)
Si2x—K_b—O4iii156.29 (12)Si2x—Ba—O3x63.3 (3)
Si2x—K_b—O522.95 (10)Si2x—Ba—Oh108.02 (16)
Si2x—K_b—Ba51.35 (17)Si2x—Ba—Ohx59.14 (15)
Si2x—K_b—W1xi100.9 (3)Si2x—Ba—Baxvi154.78 (7)
Si2x—K_b—W1ix67.4 (2)Si2x—Ba—Baxiii62.78 (16)
O3—K_b—O3x69.8 (3)Si2x—Ba—W2169.8 (2)
O3—K_b—O4iii111.3 (5)Si2x—Ba—W2xvii122.2 (2)
O3—K_b—O574.0 (5)Si2x—Ba—W_c0
O3—K_b—Ba40.8 (4)Si2x—Ba—Nb_m1(1)95.73 (9)
O3—K_b—W1xi93.8 (3)Si2x—Ba—Nb_m1(1)xviii51.82 (8)
O3—K_b—W1ix155.0 (6)Si2x—Ba—Ti_m262.78 (14)
O3x—K_b—O4iii111.3 (5)Si2x—Ba—Mg_m262.78 (14)
O3x—K_b—O574.0 (5)O1xiii—Ba—O1xv60.8 (4)
O3x—K_b—Ba40.8 (4)O1xiii—Ba—O3115.4 (4)
O3x—K_b—W1xi155.0 (6)O1xiii—Ba—O3x167.6 (3)
O3x—K_b—W1ix93.8 (3)O1xiii—Ba—Oh57.5 (5)
O4iii—K_b—O5173.4 (4)O1xiii—Ba—Ohx117.9 (5)
O4iii—K_b—Ba138.8 (3)O1xiii—Ba—Baxvi82.16 (19)
O4iii—K_b—W1xi91.9 (3)O1xiii—Ba—Baxiii43.7 (2)
O4iii—K_b—W1ix91.9 (3)O1xiii—Ba—W267.0 (2)
O5—K_b—Ba47.7 (3)O1xiii—Ba—W2xvii99.3 (3)
O5—K_b—W1xi83.7 (3)O1xiii—Ba—W_c0
O5—K_b—W1ix83.7 (3)O1xiii—Ba—Nb_m1(1)85.8 (2)
Ba—K_b—W1xi114.9 (3)O1xiii—Ba—Nb_m1(1)xviii143.5 (3)
Ba—K_b—W1ix114.9 (3)O1xiii—Ba—Ti_m243.7 (2)
W1xi—K_b—W1ix94.7 (4)O1xiii—Ba—Mg_m243.7 (2)
Na_axi—Ti_m1(1)—Na_av180.0 (5)O1xv—Ba—O3167.6 (3)
Na_axi—Ti_m1(1)—O238.1 (6)O1xv—Ba—O3x115.4 (4)
Na_axi—Ti_m1(1)—O2iv141.9 (6)O1xv—Ba—Oh117.9 (5)
Na_axi—Ti_m1(1)—O3101.5 (4)O1xv—Ba—Ohx57.5 (5)
Na_axi—Ti_m1(1)—O3iv78.5 (4)O1xv—Ba—Baxvi82.16 (19)
Na_axi—Ti_m1(1)—Oh125.4 (6)O1xv—Ba—Baxiii43.7 (2)
Na_axi—Ti_m1(1)—Ohiv54.6 (6)O1xv—Ba—W299.3 (3)
Na_axi—Ti_m1(1)—Ba115.1 (3)O1xv—Ba—W2xvii67.0 (2)
Na_axi—Ti_m1(1)—Baxii64.9 (3)O1xv—Ba—W_c0
Na_axi—Ti_m1(1)—Nb_m1(1)0O1xv—Ba—Nb_m1(1)143.5 (3)
Na_av—Ti_m1(1)—O2141.9 (6)O1xv—Ba—Nb_m1(1)xviii85.8 (2)
Na_av—Ti_m1(1)—O2iv38.1 (6)O1xv—Ba—Ti_m243.7 (2)
Na_av—Ti_m1(1)—O378.5 (4)O1xv—Ba—Mg_m243.7 (2)
Na_av—Ti_m1(1)—O3iv101.5 (4)O3—Ba—O3x65.6 (4)
Na_av—Ti_m1(1)—Oh54.6 (6)O3—Ba—Oh58.1 (5)
Na_av—Ti_m1(1)—Ohiv125.4 (6)O3—Ba—Ohx123.2 (5)
Na_av—Ti_m1(1)—Ba64.9 (3)O3—Ba—Baxvi109.5 (2)
Na_av—Ti_m1(1)—Baxii115.1 (3)O3—Ba—Baxiii124.8 (3)
Na_av—Ti_m1(1)—Nb_m1(1)0O3—Ba—W289.1 (2)
O2—Ti_m1(1)—O2iv180.0 (5)O3—Ba—W2xvii125.1 (3)
O2—Ti_m1(1)—O388.2 (4)O3—Ba—W_c0
O2—Ti_m1(1)—O3iv91.8 (4)O3—Ba—Nb_m1(1)29.7 (3)
O2—Ti_m1(1)—Oh90.1 (6)O3—Ba—Nb_m1(1)xviii94.0 (3)
O2—Ti_m1(1)—Ohiv89.9 (6)O3—Ba—Ti_m2124.8 (3)
O2—Ti_m1(1)—Ba80.3 (3)O3—Ba—Mg_m2124.8 (3)
O2—Ti_m1(1)—Baxii99.7 (3)O3x—Ba—Oh123.2 (5)
O2—Ti_m1(1)—Nb_m1(1)0O3x—Ba—Ohx58.1 (5)
O2iv—Ti_m1(1)—O391.8 (4)O3x—Ba—Baxvi109.5 (2)
O2iv—Ti_m1(1)—O3iv88.2 (4)O3x—Ba—Baxiii124.8 (3)
O2iv—Ti_m1(1)—Oh89.9 (6)O3x—Ba—W2125.1 (3)
O2iv—Ti_m1(1)—Ohiv90.1 (6)O3x—Ba—W2xvii89.1 (2)
O2iv—Ti_m1(1)—Ba99.7 (3)O3x—Ba—W_c0
O2iv—Ti_m1(1)—Baxii80.3 (3)O3x—Ba—Nb_m1(1)94.0 (3)
O2iv—Ti_m1(1)—Nb_m1(1)0O3x—Ba—Nb_m1(1)xviii29.7 (3)
O3—Ti_m1(1)—O3iv180.0 (5)O3x—Ba—Ti_m2124.8 (3)
O3—Ti_m1(1)—Oh89.2 (6)O3x—Ba—Mg_m2124.8 (3)
O3—Ti_m1(1)—Ohiv90.8 (6)Oh—Ba—Ohx166.1 (3)
O3—Ti_m1(1)—Ba45.7 (6)Oh—Ba—Baxvi96.09 (15)
O3—Ti_m1(1)—Baxii134.3 (6)Oh—Ba—Baxiii84.5 (4)
O3—Ti_m1(1)—Nb_m1(1)0Oh—Ba—W263.1 (3)
O3iv—Ti_m1(1)—Oh90.8 (6)Oh—Ba—W2xvii129.0 (3)
O3iv—Ti_m1(1)—Ohiv89.2 (6)Oh—Ba—W_c0
O3iv—Ti_m1(1)—Ba134.3 (6)Oh—Ba—Nb_m1(1)29.2 (4)
O3iv—Ti_m1(1)—Baxii45.7 (6)Oh—Ba—Nb_m1(1)xviii147.9 (3)
O3iv—Ti_m1(1)—Nb_m1(1)0Oh—Ba—Ti_m284.5 (4)
Oh—Ti_m1(1)—Ohiv180.0 (5)Oh—Ba—Mg_m284.5 (4)
Oh—Ti_m1(1)—Ba44.7 (3)Ohx—Ba—Baxvi96.09 (15)
Oh—Ti_m1(1)—Baxii135.3 (3)Ohx—Ba—Baxiii84.5 (4)
Oh—Ti_m1(1)—Nb_m1(1)0Ohx—Ba—W2129.0 (3)
Ohiv—Ti_m1(1)—Ba135.3 (3)Ohx—Ba—W2xvii63.1 (3)
Ohiv—Ti_m1(1)—Baxii44.7 (3)Ohx—Ba—W_c0
Ohiv—Ti_m1(1)—Nb_m1(1)0Ohx—Ba—Nb_m1(1)147.9 (3)
Ba—Ti_m1(1)—Baxii180.0 (5)Ohx—Ba—Nb_m1(1)xviii29.2 (4)
Ba—Ti_m1(1)—Nb_m1(1)0Ohx—Ba—Ti_m284.5 (4)
Baxii—Ti_m1(1)—Nb_m1(1)0Ohx—Ba—Mg_m284.5 (4)
Na_aiv—Ti_m1(2)—Na_axiv174.4 (3)Baxvi—Ba—Baxiii113.86 (17)
Na_aiv—Ti_m1(2)—Fe_m292.8 (2)Baxvi—Ba—W233.0 (2)
Na_aiv—Ti_m1(2)—O158.7 (4)Baxvi—Ba—W2xvii33.0 (2)
Na_aiv—Ti_m1(2)—O1xiii126.5 (4)Baxvi—Ba—W_c0
Na_aiv—Ti_m1(2)—O6iv44.2 (5)Baxvi—Ba—Nb_m1(1)109.15 (7)
Na_aiv—Ti_m1(2)—O6xiv130.8 (5)Baxvi—Ba—Nb_m1(1)xviii109.15 (7)
Na_aiv—Ti_m1(2)—Oh122.0 (6)Baxvi—Ba—Ti_m2113.9 (2)
Na_aiv—Ti_m1(2)—Ohxiii58.4 (6)Baxvi—Ba—Mg_m2113.9 (2)
Na_aiv—Ti_m1(2)—Ba114.0 (3)Baxiii—Ba—W2109.83 (19)
Na_aiv—Ti_m1(2)—Baxiii70.9 (3)Baxiii—Ba—W2xvii109.83 (19)
Na_aiv—Ti_m1(2)—Ti_m292.8 (2)Baxiii—Ba—W_c0
Na_aiv—Ti_m1(2)—Mg_m292.8 (2)Baxiii—Ba—Nb_m1(1)102.18 (8)
Na_axiv—Ti_m1(2)—Fe_m292.8 (2)Baxiii—Ba—Nb_m1(1)xviii102.18 (8)
Na_axiv—Ti_m1(2)—O1126.5 (4)Baxiii—Ba—Ti_m20.0 (5)
Na_axiv—Ti_m1(2)—O1xiii58.7 (4)Baxiii—Ba—Mg_m20.0 (5)
Na_axiv—Ti_m1(2)—O6iv130.8 (5)W2—Ba—W2xvii66.0 (3)
Na_axiv—Ti_m1(2)—O6xiv44.2 (5)W2—Ba—W_c0
Na_axiv—Ti_m1(2)—Oh58.4 (6)W2—Ba—Nb_m1(1)78.6 (2)
Na_axiv—Ti_m1(2)—Ohxiii122.0 (6)W2—Ba—Nb_m1(1)xviii138.3 (2)
Na_axiv—Ti_m1(2)—Ba70.9 (3)W2—Ba—Ti_m2109.8 (2)
Na_axiv—Ti_m1(2)—Baxiii114.0 (3)W2—Ba—Mg_m2109.8 (2)
Na_axiv—Ti_m1(2)—Ti_m292.8 (2)W2xvii—Ba—W_c0
Na_axiv—Ti_m1(2)—Mg_m292.8 (2)W2xvii—Ba—Nb_m1(1)138.3 (2)
Fe_m2—Ti_m1(2)—O140.9 (2)W2xvii—Ba—Nb_m1(1)xviii78.6 (2)
Fe_m2—Ti_m1(2)—O1xiii40.9 (2)W2xvii—Ba—Ti_m2109.8 (2)
Fe_m2—Ti_m1(2)—O6iv130.5 (3)W2xvii—Ba—Mg_m2109.8 (2)
Fe_m2—Ti_m1(2)—O6xiv130.5 (3)W_c—Ba—Nb_m1(1)0
Fe_m2—Ti_m1(2)—Oh86.8 (2)W_c—Ba—Nb_m1(1)xviii0
Fe_m2—Ti_m1(2)—Ohxiii86.8 (2)W_c—Ba—Ti_m20
Fe_m2—Ti_m1(2)—Ba36.49 (8)W_c—Ba—Mg_m20
Fe_m2—Ti_m1(2)—Baxiii36.49 (8)Nb_m1(1)—Ba—Nb_m1(1)xviii120.15 (15)
Fe_m2—Ti_m1(2)—Ti_m20.0 (5)Nb_m1(1)—Ba—Ti_m2102.18 (7)
Fe_m2—Ti_m1(2)—Mg_m20.0 (5)Nb_m1(1)—Ba—Mg_m2102.18 (7)
O1—Ti_m1(2)—O1xiii81.7 (4)Nb_m1(1)xviii—Ba—Ti_m2102.18 (7)
O1—Ti_m1(2)—O6iv89.8 (4)Nb_m1(1)xviii—Ba—Mg_m2102.18 (7)
O1—Ti_m1(2)—O6xiv170.4 (4)Ti_m2—Ba—Mg_m20.0 (5)
O1—Ti_m1(2)—Oh87.8 (6)Na_a—W1—Na_ai69.1 (11)
O1—Ti_m1(2)—Ohxiii87.3 (6)Na_a—W1—K_bii128.9 (5)
O1—Ti_m1(2)—Ba55.7 (3)Na_a—W1—K_biii125.7 (5)
O1—Ti_m1(2)—Baxiii49.2 (5)Na_ai—W1—K_bii125.7 (5)
O1—Ti_m1(2)—Ti_m240.9 (2)Na_ai—W1—K_biii128.9 (5)
O1—Ti_m1(2)—Mg_m240.9 (2)K_bii—W1—K_biii85.3 (5)
O1xiii—Ti_m1(2)—O6iv170.4 (4)Na_av—W2—Na_axiv71.3 (11)
O1xiii—Ti_m1(2)—O6xiv89.8 (4)Na_av—W2—Ba114.9 (4)
O1xiii—Ti_m1(2)—Oh87.3 (6)Na_av—W2—Baxvi117.6 (4)
O1xiii—Ti_m1(2)—Ohxiii87.8 (6)Na_axiv—W2—Ba117.6 (4)
O1xiii—Ti_m1(2)—Ba49.2 (5)Na_axiv—W2—Baxvi114.9 (4)
O1xiii—Ti_m1(2)—Baxiii55.7 (3)Ba—W2—Baxvi114.0 (4)
O1xiii—Ti_m1(2)—Ti_m240.9 (2)Fe_m2—W_c—Ba0
O1xiii—Ti_m1(2)—Mg_m240.9 (2)Fe_m2—W_c—Ti_m20.0 (5)
O6iv—Ti_m1(2)—O6xiv98.9 (4)Ba—W_c—Ti_m20
O6iv—Ti_m1(2)—Oh96.9 (7)Na_axi—Nb_m1(1)—Na_av180.0 (5)
O6iv—Ti_m1(2)—Ohxiii87.2 (7)Na_axi—Nb_m1(1)—Ti_m1(1)0
O6iv—Ti_m1(2)—Ba128.4 (6)Na_axi—Nb_m1(1)—O238.1 (6)
O6iv—Ti_m1(2)—Baxiii115.0 (4)Na_axi—Nb_m1(1)—O2iv141.9 (6)
O6iv—Ti_m1(2)—Ti_m2130.5 (3)Na_axi—Nb_m1(1)—O3101.5 (4)
O6iv—Ti_m1(2)—Mg_m2130.5 (3)Na_axi—Nb_m1(1)—O3iv78.5 (4)
O6xiv—Ti_m1(2)—Oh87.2 (7)Na_axi—Nb_m1(1)—Oh125.4 (6)
O6xiv—Ti_m1(2)—Ohxiii96.9 (7)Na_axi—Nb_m1(1)—Ohiv54.6 (6)
O6xiv—Ti_m1(2)—Ba115.0 (4)Na_axi—Nb_m1(1)—Ba115.1 (3)
O6xiv—Ti_m1(2)—Baxiii128.4 (6)Na_axi—Nb_m1(1)—Baxii64.9 (3)
O6xiv—Ti_m1(2)—Ti_m2130.5 (3)Na_av—Nb_m1(1)—Ti_m1(1)0
O6xiv—Ti_m1(2)—Mg_m2130.5 (3)Na_av—Nb_m1(1)—O2141.9 (6)
Oh—Ti_m1(2)—Ohxiii173.6 (3)Na_av—Nb_m1(1)—O2iv38.1 (6)
Oh—Ti_m1(2)—Ba50.6 (2)Na_av—Nb_m1(1)—O378.5 (4)
Oh—Ti_m1(2)—Baxiii123.0 (2)Na_av—Nb_m1(1)—O3iv101.5 (4)
Oh—Ti_m1(2)—Ti_m286.8 (2)Na_av—Nb_m1(1)—Oh54.6 (6)
Oh—Ti_m1(2)—Mg_m286.8 (2)Na_av—Nb_m1(1)—Ohiv125.4 (6)
Ohxiii—Ti_m1(2)—Ba123.0 (2)Na_av—Nb_m1(1)—Ba64.9 (3)
Ohxiii—Ti_m1(2)—Baxiii50.6 (2)Na_av—Nb_m1(1)—Baxii115.1 (3)
Ohxiii—Ti_m1(2)—Ti_m286.8 (2)Ti_m1(1)—Nb_m1(1)—O20
Ohxiii—Ti_m1(2)—Mg_m286.8 (2)Ti_m1(1)—Nb_m1(1)—O2iv0
Ba—Ti_m1(2)—Baxiii72.97 (12)Ti_m1(1)—Nb_m1(1)—O30
Ba—Ti_m1(2)—Ti_m236.49 (8)Ti_m1(1)—Nb_m1(1)—O3iv0
Ba—Ti_m1(2)—Mg_m236.49 (8)Ti_m1(1)—Nb_m1(1)—Oh0
Baxiii—Ti_m1(2)—Ti_m236.49 (8)Ti_m1(1)—Nb_m1(1)—Ohiv0
Baxiii—Ti_m1(2)—Mg_m236.49 (8)Ti_m1(1)—Nb_m1(1)—Ba0
Ti_m2—Ti_m1(2)—Mg_m20.0 (5)Ti_m1(1)—Nb_m1(1)—Baxii0
Ti_m1(2)—Fe_m2—Ti_m1(2)xv180.0 (5)O2—Nb_m1(1)—O2iv180.0 (5)
Ti_m1(2)—Fe_m2—O143.0 (2)O2—Nb_m1(1)—O388.2 (4)
Ti_m1(2)—Fe_m2—O1xiii43.0 (2)O2—Nb_m1(1)—O3iv91.8 (4)
Ti_m1(2)—Fe_m2—O1xv137.0 (2)O2—Nb_m1(1)—Oh90.1 (6)
Ti_m1(2)—Fe_m2—O1x137.0 (2)O2—Nb_m1(1)—Ohiv89.9 (6)
Ti_m1(2)—Fe_m2—Ba90O2—Nb_m1(1)—Ba80.3 (3)
Ti_m1(2)—Fe_m2—Baxiii90O2—Nb_m1(1)—Baxii99.7 (3)
Ti_m1(2)—Fe_m2—W_c90O2iv—Nb_m1(1)—O391.8 (4)
Ti_m1(2)—Fe_m2—W_cxiii90O2iv—Nb_m1(1)—O3iv88.2 (4)
Ti_m1(2)—Fe_m2—Ti_m20O2iv—Nb_m1(1)—Oh89.9 (6)
Ti_m1(2)—Fe_m2—Mg_m20O2iv—Nb_m1(1)—Ohiv90.1 (6)
Ti_m1(2)xv—Fe_m2—O1137.0 (2)O2iv—Nb_m1(1)—Ba99.7 (3)
Ti_m1(2)xv—Fe_m2—O1xiii137.0 (2)O2iv—Nb_m1(1)—Baxii80.3 (3)
Ti_m1(2)xv—Fe_m2—O1xv43.0 (2)O3—Nb_m1(1)—O3iv180.0 (5)
Ti_m1(2)xv—Fe_m2—O1x43.0 (2)O3—Nb_m1(1)—Oh89.2 (6)
Ti_m1(2)xv—Fe_m2—Ba90O3—Nb_m1(1)—Ohiv90.8 (6)
Ti_m1(2)xv—Fe_m2—Baxiii90O3—Nb_m1(1)—Ba45.7 (6)
Ti_m1(2)xv—Fe_m2—W_c90O3—Nb_m1(1)—Baxii134.3 (6)
Ti_m1(2)xv—Fe_m2—W_cxiii90O3iv—Nb_m1(1)—Oh90.8 (6)
Ti_m1(2)xv—Fe_m2—Ti_m20O3iv—Nb_m1(1)—Ohiv89.2 (6)
Ti_m1(2)xv—Fe_m2—Mg_m20O3iv—Nb_m1(1)—Ba134.3 (6)
O1—Fe_m2—O1xiii86.0 (4)O3iv—Nb_m1(1)—Baxii45.7 (6)
O1—Fe_m2—O1xv180.0 (5)Oh—Nb_m1(1)—Ohiv180.0 (5)
O1—Fe_m2—O1x94.0 (4)Oh—Nb_m1(1)—Ba44.7 (3)
O1—Fe_m2—Ba94.5 (6)Oh—Nb_m1(1)—Baxii135.3 (3)
O1—Fe_m2—Baxiii85.5 (6)Ohiv—Nb_m1(1)—Ba135.3 (3)
O1—Fe_m2—W_c94.5 (6)Ohiv—Nb_m1(1)—Baxii44.7 (3)
O1—Fe_m2—W_cxiii85.5 (6)Ba—Nb_m1(1)—Baxii180.0 (5)
O1—Fe_m2—Ti_m20Ti_m1(2)—Ti_m2—Ti_m1(2)xv180.0 (5)
O1—Fe_m2—Mg_m20Ti_m1(2)—Ti_m2—Fe_m20
O1xiii—Fe_m2—O1xv94.0 (4)Ti_m1(2)—Ti_m2—O143.0 (2)
O1xiii—Fe_m2—O1x180.0 (5)Ti_m1(2)—Ti_m2—O1xiii43.0 (2)
O1xiii—Fe_m2—Ba85.5 (6)Ti_m1(2)—Ti_m2—O1xv137.0 (2)
O1xiii—Fe_m2—Baxiii94.5 (6)Ti_m1(2)—Ti_m2—O1x137.0 (2)
O1xiii—Fe_m2—W_c85.5 (6)Ti_m1(2)—Ti_m2—Ba90
O1xiii—Fe_m2—W_cxiii94.5 (6)Ti_m1(2)—Ti_m2—Baxiii90
O1xiii—Fe_m2—Ti_m20Ti_m1(2)—Ti_m2—W_c90
O1xiii—Fe_m2—Mg_m20Ti_m1(2)—Ti_m2—W_cxiii90
O1xv—Fe_m2—O1x86.0 (4)Ti_m1(2)—Ti_m2—Mg_m20
O1xv—Fe_m2—Ba85.5 (6)Ti_m1(2)xv—Ti_m2—Fe_m20
O1xv—Fe_m2—Baxiii94.5 (6)Ti_m1(2)xv—Ti_m2—O1137.0 (2)
O1xv—Fe_m2—W_c85.5 (6)Ti_m1(2)xv—Ti_m2—O1xiii137.0 (2)
O1xv—Fe_m2—W_cxiii94.5 (6)Ti_m1(2)xv—Ti_m2—O1xv43.0 (2)
O1xv—Fe_m2—Ti_m20Ti_m1(2)xv—Ti_m2—O1x43.0 (2)
O1xv—Fe_m2—Mg_m20Ti_m1(2)xv—Ti_m2—Ba90
O1x—Fe_m2—Ba94.5 (6)Ti_m1(2)xv—Ti_m2—Baxiii90
O1x—Fe_m2—Baxiii85.5 (6)Ti_m1(2)xv—Ti_m2—W_c90
O1x—Fe_m2—W_c94.5 (6)Ti_m1(2)xv—Ti_m2—W_cxiii90
O1x—Fe_m2—W_cxiii85.5 (6)Ti_m1(2)xv—Ti_m2—Mg_m20
O1x—Fe_m2—Ti_m20Fe_m2—Ti_m2—O10
O1x—Fe_m2—Mg_m20Fe_m2—Ti_m2—O1xiii0
Ba—Fe_m2—Baxiii180.0 (5)Fe_m2—Ti_m2—O1xv0
Ba—Fe_m2—W_c0.0 (5)Fe_m2—Ti_m2—O1x0
Ba—Fe_m2—W_cxiii180.0 (5)Fe_m2—Ti_m2—Ba0
Ba—Fe_m2—Ti_m20Fe_m2—Ti_m2—Baxiii0
Ba—Fe_m2—Mg_m20Fe_m2—Ti_m2—W_c0
Baxiii—Fe_m2—W_c180.0 (5)Fe_m2—Ti_m2—W_cxiii0
Baxiii—Fe_m2—W_cxiii0.0 (5)Fe_m2—Ti_m2—Mg_m20
Baxiii—Fe_m2—Ti_m20O1—Ti_m2—O1xiii86.0 (4)
Baxiii—Fe_m2—Mg_m20O1—Ti_m2—O1xv180.0 (5)
W_c—Fe_m2—W_cxiii180.0 (5)O1—Ti_m2—O1x94.0 (4)
W_c—Fe_m2—Ti_m20O1—Ti_m2—Ba94.5 (6)
W_c—Fe_m2—Mg_m20O1—Ti_m2—Baxiii85.5 (6)
W_cxiii—Fe_m2—Ti_m20O1—Ti_m2—W_c94.5 (6)
W_cxiii—Fe_m2—Mg_m20O1—Ti_m2—W_cxiii85.5 (6)
Ti_m2—Fe_m2—Mg_m20O1—Ti_m2—Mg_m20
K_b—Si1—K_biii80.3 (2)O1xiii—Ti_m2—O1xv94.0 (4)
K_b—Si1—O352.1 (5)O1xiii—Ti_m2—O1x180.0 (5)
K_b—Si1—O462.4 (5)O1xiii—Ti_m2—Ba85.5 (6)
K_b—Si1—O6103.7 (4)O1xiii—Ti_m2—Baxiii94.5 (6)
K_b—Si1—O7142.4 (6)O1xiii—Ti_m2—W_c85.5 (6)
K_biii—Si1—O3132.3 (5)O1xiii—Ti_m2—W_cxiii94.5 (6)
K_biii—Si1—O439.8 (9)O1xiii—Ti_m2—Mg_m20
K_biii—Si1—O667.0 (7)O1xv—Ti_m2—O1x86.0 (4)
K_biii—Si1—O7117.6 (6)O1xv—Ti_m2—Ba85.5 (6)
O3—Si1—O4107.2 (8)O1xv—Ti_m2—Baxiii94.5 (6)
O3—Si1—O6116.3 (7)O1xv—Ti_m2—W_c85.5 (6)
O3—Si1—O7104.5 (10)O1xv—Ti_m2—W_cxiii94.5 (6)
O4—Si1—O6106.0 (11)O1xv—Ti_m2—Mg_m20
O4—Si1—O7109.0 (5)O1x—Ti_m2—Ba94.5 (6)
O6—Si1—O7113.6 (6)O1x—Ti_m2—Baxiii85.5 (6)
Na_aiv—Si2—K_b163.2 (4)O1x—Ti_m2—W_c94.5 (6)
Na_aiv—Si2—O165.8 (6)O1x—Ti_m2—W_cxiii85.5 (6)
Na_aiv—Si2—O298.7 (7)O1x—Ti_m2—Mg_m20
Na_aiv—Si2—O7xi49.8 (6)Ba—Ti_m2—Baxiii180.0 (5)
Na_aiv—Si2—Ba123.4 (4)Ba—Ti_m2—W_c0.0 (5)
K_b—Si2—O1130.7 (5)Ba—Ti_m2—W_cxiii180.0 (5)
K_b—Si2—O272.2 (6)Ba—Ti_m2—Mg_m20
K_b—Si2—O7xi119.9 (6)Baxiii—Ti_m2—W_c180.0 (5)
K_b—Si2—Ba72.59 (17)Baxiii—Ti_m2—W_cxiii0.0 (5)
O1—Si2—O2114.8 (6)Baxiii—Ti_m2—Mg_m20
O1—Si2—O7xi102.3 (9)W_c—Ti_m2—W_cxiii180.0 (5)
O1—Si2—Ba58.2 (5)W_c—Ti_m2—Mg_m20
O2—Si2—O7xi113.4 (5)W_cxiii—Ti_m2—Mg_m20
O2—Si2—Ba96.7 (3)Ti_m1(2)—Mg_m2—Ti_m1(2)xv180.0 (5)
O7xi—Si2—Ba149.5 (6)Ti_m1(2)—Mg_m2—Fe_m20
Ti_m1(2)—O1—Fe_m296.1 (4)Ti_m1(2)—Mg_m2—O143.0 (2)
Ti_m1(2)—O1—Si2121.9 (7)Ti_m1(2)—Mg_m2—O1xiii43.0 (2)
Ti_m1(2)—O1—Baxiii97.6 (7)Ti_m1(2)—Mg_m2—O1xv137.0 (2)
Ti_m1(2)—O1—Ti_m296.1 (4)Ti_m1(2)—Mg_m2—O1x137.0 (2)
Ti_m1(2)—O1—Mg_m296.1 (4)Ti_m1(2)—Mg_m2—Ba90
Fe_m2—O1—Si2127.0 (8)Ti_m1(2)—Mg_m2—Baxiii90
Fe_m2—O1—Baxiii50.9 (4)Ti_m1(2)—Mg_m2—Ti_m20
Fe_m2—O1—Ti_m20.0 (5)Ti_m1(2)xv—Mg_m2—Fe_m20
Fe_m2—O1—Mg_m20.0 (5)Ti_m1(2)xv—Mg_m2—O1137.0 (2)
Si2—O1—Baxiii138.7 (4)Ti_m1(2)xv—Mg_m2—O1xiii137.0 (2)
Si2—O1—Ti_m2127.0 (8)Ti_m1(2)xv—Mg_m2—O1xv43.0 (2)
Si2—O1—Mg_m2127.0 (8)Ti_m1(2)xv—Mg_m2—O1x43.0 (2)
Baxiii—O1—Ti_m250.9 (4)Ti_m1(2)xv—Mg_m2—Ba90
Baxiii—O1—Mg_m250.9 (4)Ti_m1(2)xv—Mg_m2—Baxiii90
Ti_m2—O1—Mg_m20.0 (5)Ti_m1(2)xv—Mg_m2—Ti_m20
Na_axi—O2—Ti_m1(1)109.3 (8)Fe_m2—Mg_m2—O10
Na_axi—O2—Si2120.6 (6)Fe_m2—Mg_m2—O1xiii0
Na_axi—O2—Nb_m1(1)109.3 (8)Fe_m2—Mg_m2—O1xv0
Ti_m1(1)—O2—Si2129.5 (5)Fe_m2—Mg_m2—O1x0
Ti_m1(1)—O2—Nb_m1(1)0.0 (5)Fe_m2—Mg_m2—Ba0
Si2—O2—Nb_m1(1)129.5 (5)Fe_m2—Mg_m2—Baxiii0
K_b—O3—Ti_m1(1)121.6 (3)Fe_m2—Mg_m2—Ti_m20
K_b—O3—Si1100.2 (8)O1—Mg_m2—O1xiii86.0 (4)
K_b—O3—Ba101.0 (4)O1—Mg_m2—O1xv180.0 (5)
K_b—O3—Nb_m1(1)121.6 (3)O1—Mg_m2—O1x94.0 (4)
Ti_m1(1)—O3—Si1116.3 (5)O1—Mg_m2—Ba94.5 (6)
Ti_m1(1)—O3—Ba104.6 (8)O1—Mg_m2—Baxiii85.5 (6)
Ti_m1(1)—O3—Nb_m1(1)0.0 (5)O1—Mg_m2—Ti_m20
Si1—O3—Ba112.2 (4)O1xiii—Mg_m2—O1xv94.0 (4)
Si1—O3—Nb_m1(1)116.3 (5)O1xiii—Mg_m2—O1x180.0 (5)
Ba—O3—Nb_m1(1)104.6 (8)O1xiii—Mg_m2—Ba85.5 (6)
K_biii—O4—Si1115.5 (9)O1xiii—Mg_m2—Baxiii94.5 (6)
K_biii—O4—Si1x115.5 (9)O1xiii—Mg_m2—Ti_m20
Si1—O4—Si1x127.1 (17)O1xv—Mg_m2—O1x86.0 (4)
Na_a—O6—Ti_m1(2)iv99.8 (7)O1xv—Mg_m2—Ba85.5 (6)
Na_a—O6—Si1123.4 (7)O1xv—Mg_m2—Baxiii94.5 (6)
Ti_m1(2)iv—O6—Si1131.2 (10)O1xv—Mg_m2—Ti_m20
Na_av—O7—Si1123.0 (6)O1x—Mg_m2—Ba94.5 (6)
Na_av—O7—Si2ii97.4 (6)O1x—Mg_m2—Baxiii85.5 (6)
Si1—O7—Si2ii128.2 (13)O1x—Mg_m2—Ti_m20
Ti_m1(1)—Oh—Ti_m1(2)128.4 (4)Ba—Mg_m2—Baxiii180.0 (5)
Ti_m1(1)—Oh—Ba106.1 (6)Ba—Mg_m2—Ti_m20
Ti_m1(1)—Oh—Nb_m1(1)0.0 (5)Baxiii—Mg_m2—Ti_m20
Ti_m1(2)—Oh—Ba98.2 (5)
Symmetry codes: (i) x+1, y, z; (ii) x, y, z1; (iii) x+1, y, z+1; (iv) x+1/2, y+1/2, z+1; (v) x+1/2, y+1/2, z; (vi) x+1/2, y+1/2, z; (vii) x+1/2, y+1/2, z; (viii) x+1, y, z+2; (ix) x+1, y, z+1; (x) x, y, z; (xi) x, y, z+1; (xii) x+1/2, y+1/2, z+1; (xiii) x, y, z+1; (xiv) x1/2, y+1/2, z; (xv) x, y, z+1; (xvi) x, y, z; (xvii) x, y, z; (xviii) x+1/2, y1/2, z+1; (xix) x, y, z+1; (xx) x1/2, y1/2, z; (xxi) x+1/2, y1/2, z.
(labu_Fe_20.0) top
Crystal data top
Ba0.7Fe0.5K2.1Mg0.05Na2Nb0.1O33Si8Ti4Z = 2
Mr = 1206.8F(000) = 1167
Monoclinic, C2/mDx = 3.569 Mg m3
Hall symbol: -C 2ySynchrotron radiation, λ = 0.414 Å
a = 13.442 (9) ÅCell parameters from 2573 reflections
b = 13.0636 (12) Åθ = 1.9–19.0°
c = 7.102 (2) ŵ = 0.94 mm1
β = 115.81 (5)°T = 293 K
V = 1122.7 (10) Å3Anhedral grain
Data collection top
ESRF ID 09
diffractometer
θmax = 19.0°, θmin = 1.9°
2573 measured reflectionsh = 88
757 independent reflectionsk = 2020
391 reflections with I > 2σ(I)l = 910
Rint = 0.052
Refinement top
Refinement on F0 restraints
R[F2 > 2σ(F2)] = 0.1196 constraints
wR(F2) = 0.189Weighting scheme based on measured s.u.'s w = 1/(σ2(F) + 0.0143999998F2)
S = 1.06(Δ/σ)max = 0.049
757 reflectionsΔρmax = 1.31 e Å3
57 parametersΔρmin = 1.43 e Å3
Fractional atomic coordinates and isotropic or equivalent isotropic displacement parameters (Å2) top
xyzUiso*/UeqOcc. (<1)
Na_a0.420 (3)0.2724 (13)0.012 (3)0.049 (5)*0.5
K_b0.4366 (16)00.7391 (13)0.059 (2)*
Ti_m1(1)0.250.250.50.0273 (11)*0.95
Ti_m1(2)00.2160 (3)0.50.0249 (11)*
Fe_m2000.50.040 (2)*0.5
Si10.3319 (8)0.1094 (3)0.2753 (6)0.0182 (10)*
Si20.2110 (7)0.1086 (3)0.8213 (6)0.0161 (10)*
O10.0777 (18)0.1032 (7)0.6867 (15)0.017 (2)*
O20.268 (2)0.2013 (7)0.7695 (16)0.022 (2)*
O30.295 (2)0.1143 (8)0.4513 (17)0.024 (3)*
O40.394 (3)00.294 (2)0.017 (3)*
O50.267 (3)00.803 (2)0.018 (3)*
O60.420 (2)0.1899 (9)0.2847 (18)0.030 (3)*
O70.2190 (19)0.1122 (6)0.0565 (14)0.013 (2)*
Oh0.0989 (19)0.2082 (7)0.3806 (15)0.016 (2)*
Ba0.0980 (7)00.3342 (5)0.0223 (9)*0.35
W10.50.1468 (16)00.047 (5)*
W200.1058 (13)00.036 (5)*
W_c0.0980 (7)00.3342 (5)0.0223 (9)*0.65
Nb_m1(1)0.250.250.50.0273 (11)*0.05
Ti_m2000.50.040 (2)*0.1
Mg_m2000.50.040 (2)*0.05
Atomic displacement parameters (Å2) top
U11U22U33U12U13U23
???????
Geometric parameters (Å, º) top
Na_a—Na_ai2.23 (6)Ti_m1(2)—Ohxiii1.87 (2)
Na_a—K_bii4.10 (2)Ti_m1(2)—Ba3.526 (6)
Na_a—K_biii4.07 (2)Ti_m1(2)—Baxiii3.526 (6)
Na_a—Ti_m1(1)ii3.359 (18)Ti_m1(2)—Ti_m22.821 (4)
Na_a—Ti_m1(2)iv3.156 (19)Ti_m1(2)—Mg_m22.821 (4)
Na_a—Si2iv2.96 (4)Fe_m2—O11.860 (10)
Na_a—O2ii2.22 (3)Fe_m2—O1xiii1.860 (10)
Na_a—O62.22 (3)Fe_m2—O1xv1.860 (10)
Na_a—O7v2.28 (4)Fe_m2—O1x1.860 (10)
Na_a—Bavi3.88 (2)Fe_m2—Ba2.115 (8)
Na_a—Bavii3.80 (2)Fe_m2—Baxiii2.115 (8)
Na_a—W11.98 (3)Fe_m2—W_c2.115 (8)
Na_a—W2v1.94 (3)Fe_m2—W_cxiii2.115 (8)
Na_a—Nb_m1(1)ii3.359 (18)Fe_m2—Ti_m20
K_b—K_biii4.41 (3)Fe_m2—Mg_m20
K_b—K_bviii3.337 (12)Si1—O31.54 (2)
K_b—Si13.292 (9)Si1—O41.630 (18)
K_b—Si1iii3.47 (2)Si1—O61.57 (3)
K_b—Si1ix3.47 (2)Si1—O71.633 (16)
K_b—Si1x3.292 (9)Si2—O11.62 (2)
K_b—Si23.62 (2)Si2—O21.560 (19)
K_b—Si2x3.62 (2)Si2—O51.64 (2)
K_b—O32.580 (17)Si2—O7xi1.627 (15)
K_b—O3x2.580 (17)Si2—Ba3.422 (6)
K_b—O4iii2.39 (4)O1—Baxiii2.67 (2)
K_b—O52.51 (4)O1—Ti_m21.860 (10)
K_b—Ba4.19 (2)O1—Mg_m21.860 (10)
K_b—W1xi2.542 (17)O2—Nb_m1(1)1.930 (14)
K_b—W1ix2.542 (17)O3—Ba2.83 (3)
Ti_m1(1)—O21.930 (14)O3—Nb_m1(1)1.950 (15)
Ti_m1(1)—O2iv1.930 (14)Oh—Ba2.739 (9)
Ti_m1(1)—O31.950 (15)Oh—Nb_m1(1)1.91 (2)
Ti_m1(1)—O3iv1.950 (15)Ba—Baxvi4.312 (7)
Ti_m1(1)—Oh1.91 (2)Ba—Baxiii4.229 (12)
Ti_m1(1)—Ohiv1.91 (2)Ba—W22.561 (10)
Ti_m1(1)—Ba3.759 (4)Ba—W2xvii2.561 (10)
Ti_m1(1)—Baxii3.759 (4)Ba—W_c0
Ti_m1(1)—Nb_m1(1)0Ba—Nb_m1(1)3.759 (4)
Ti_m1(2)—Fe_m22.821 (4)Ba—Nb_m1(1)xviii3.759 (4)
Ti_m1(2)—O11.953 (11)Ba—Ti_m22.115 (8)
Ti_m1(2)—O1xiii1.953 (11)Ba—Mg_m22.115 (8)
Ti_m1(2)—O6iv1.889 (13)W_c—Ti_m22.115 (8)
Ti_m1(2)—O6xiv1.889 (13)W_c—Mg_m22.115 (8)
Ti_m1(2)—Oh1.87 (2)Ti_m2—Mg_m20
Na_ai—Na_a—K_bii73.3 (9)Na_axx—Ba—Ti_m1(1)xviii68.3 (4)
Na_ai—Na_a—K_biii75.1 (8)Na_axx—Ba—Ti_m1(2)125.9 (6)
Na_ai—Na_a—Ti_m1(1)ii98.2 (10)Na_axx—Ba—Ti_m1(2)xv50.2 (4)
Na_ai—Na_a—Ti_m1(2)iv101.7 (10)Na_axx—Ba—Fe_m287.4 (6)
Na_ai—Na_a—Si2iv142.4 (9)Na_axx—Ba—Si2143.4 (5)
Na_ai—Na_a—O2ii122.3 (14)Na_axx—Ba—Si2x99.6 (3)
Na_ai—Na_a—O6115.5 (14)Na_axx—Ba—O1xiii92.9 (6)
Na_ai—Na_a—O7v135.4 (12)Na_axx—Ba—O1xv43.6 (6)
Na_ai—Na_a—Bavi71.1 (8)Na_axx—Ba—O3146.7 (8)
Na_ai—Na_a—Bavii75.1 (9)Na_axx—Ba—O3x91.5 (6)
Na_ai—Na_a—W155.8 (12)Na_axx—Ba—Oh143.3 (6)
Na_ai—Na_a—W2v55.0 (11)Na_axx—Ba—Ohx43.9 (4)
Na_ai—Na_a—Nb_m1(1)ii98.2 (10)Na_axx—Ba—Baxvi54.9 (3)
K_bii—Na_a—K_biii48.2 (3)Na_axx—Ba—Baxiii87.4 (6)
K_bii—Na_a—Ti_m1(1)ii64.2 (3)Na_axx—Ba—W286.0 (4)
K_bii—Na_a—Ti_m1(2)iv119.8 (5)Na_axx—Ba—W2xvii26.2 (5)
K_bii—Na_a—Si2iv144.1 (11)Na_axx—Ba—W_c0
K_bii—Na_a—O2ii59.5 (7)Na_axx—Ba—Nb_m1(1)164.3 (3)
K_bii—Na_a—O690.7 (6)Na_axx—Ba—Nb_m1(1)xviii68.3 (4)
K_bii—Na_a—O7v132.9 (9)Na_axx—Ba—Ti_m287.4 (6)
K_bii—Na_a—Bavi142.8 (11)Na_axx—Ba—Mg_m287.4 (6)
K_bii—Na_a—Bavii112.0 (6)Na_axxi—Ba—Na_av103.1 (5)
K_bii—Na_a—W128.5 (4)Na_axxi—Ba—Na_axiv111.7 (4)
K_bii—Na_a—W2v123.0 (15)Na_axxi—Ba—K_b100.8 (6)
K_bii—Na_a—Nb_m1(1)ii64.2 (3)Na_axxi—Ba—Ti_m1(1)139.1 (6)
K_biii—Na_a—Ti_m1(1)ii111.4 (5)Na_axxi—Ba—Ti_m1(1)xviii52.8 (3)
K_biii—Na_a—Ti_m1(2)iv72.2 (4)Na_axxi—Ba—Ti_m1(2)156.2 (5)
K_biii—Na_a—Si2iv122.5 (8)Na_axxi—Ba—Ti_m1(2)xv70.2 (5)
K_biii—Na_a—O2ii94.2 (6)Na_axxi—Ba—Fe_m2118.7 (6)
K_biii—Na_a—O651.2 (8)Na_axxi—Ba—Si2148.6 (3)
K_biii—Na_a—O7v149.3 (15)Na_axxi—Ba—Si2x101.8 (3)
K_biii—Na_a—Bavi111.1 (6)Na_axxi—Ba—O1xiii123.7 (6)
K_biii—Na_a—Bavii148.3 (12)Na_axxi—Ba—O1xv76.3 (7)
K_biii—Na_a—W129.7 (5)Na_axxi—Ba—O3113.1 (8)
K_biii—Na_a—W2v124.7 (15)Na_axxi—Ba—O3x64.2 (5)
K_biii—Na_a—Nb_m1(1)ii111.4 (5)Na_axxi—Ba—Oh148.3 (5)
Ti_m1(1)ii—Na_a—Ti_m1(2)iv159.9 (14)Na_axxi—Ba—Ohx45.2 (4)
Ti_m1(1)ii—Na_a—Si2iv103.7 (9)Na_axxi—Ba—Baxvi56.7 (3)
Ti_m1(1)ii—Na_a—O2ii33.2 (5)Na_axxi—Ba—Baxiii118.7 (6)
Ti_m1(1)ii—Na_a—O6130.2 (13)Na_axxi—Ba—W287.8 (4)
Ti_m1(1)ii—Na_a—O7v73.7 (6)Na_axxi—Ba—W2xvii27.8 (5)
Ti_m1(1)ii—Na_a—Bavi131.3 (6)Na_axxi—Ba—W_c0
Ti_m1(1)ii—Na_a—Bavii63.0 (3)Na_axxi—Ba—Nb_m1(1)139.1 (6)
Ti_m1(1)ii—Na_a—W190.5 (6)Na_axxi—Ba—Nb_m1(1)xviii52.8 (3)
Ti_m1(1)ii—Na_a—W2v98.8 (7)Na_axxi—Ba—Ti_m2118.7 (6)
Ti_m1(1)ii—Na_a—Nb_m1(1)ii0.0 (5)Na_axxi—Ba—Mg_m2118.7 (6)
Ti_m1(2)iv—Na_a—Si2iv60.8 (5)Na_av—Ba—Na_axiv33.8 (9)
Ti_m1(2)iv—Na_a—O2ii129.0 (16)Na_av—Ba—K_b100.8 (6)
Ti_m1(2)iv—Na_a—O636.1 (4)Na_av—Ba—Ti_m1(1)52.8 (3)
Ti_m1(2)iv—Na_a—O7v93.3 (10)Na_av—Ba—Ti_m1(1)xviii139.1 (6)
Ti_m1(2)iv—Na_a—Bavi59.1 (3)Na_av—Ba—Ti_m1(2)70.2 (5)
Ti_m1(2)iv—Na_a—Bavii124.6 (5)Na_av—Ba—Ti_m1(2)xv156.2 (5)
Ti_m1(2)iv—Na_a—W198.9 (7)Na_av—Ba—Fe_m2118.7 (6)
Ti_m1(2)iv—Na_a—W2v94.4 (6)Na_av—Ba—Si2101.8 (3)
Ti_m1(2)iv—Na_a—Nb_m1(1)ii159.9 (14)Na_av—Ba—Si2x148.6 (3)
Si2iv—Na_a—O2ii91.3 (14)Na_av—Ba—O1xiii76.3 (7)
Si2iv—Na_a—O671.3 (11)Na_av—Ba—O1xv123.7 (6)
Si2iv—Na_a—O7v33.1 (6)Na_av—Ba—O364.2 (5)
Si2iv—Na_a—Bavi71.5 (4)Na_av—Ba—O3x113.1 (8)
Si2iv—Na_a—Bavii88.1 (5)Na_av—Ba—Oh45.2 (4)
Si2iv—Na_a—W1151.7 (13)Na_av—Ba—Ohx148.3 (5)
Si2iv—Na_a—W2v91.4 (8)Na_av—Ba—Baxvi56.7 (3)
Si2iv—Na_a—Nb_m1(1)ii103.7 (9)Na_av—Ba—Baxiii118.7 (6)
O2ii—Na_a—O697.2 (14)Na_av—Ba—W227.8 (5)
O2ii—Na_a—O7v73.7 (12)Na_av—Ba—W2xvii87.8 (4)
O2ii—Na_a—Bavi154.3 (10)Na_av—Ba—W_c0
O2ii—Na_a—Bavii92.8 (6)Na_av—Ba—Nb_m1(1)52.8 (3)
O2ii—Na_a—W187.4 (8)Na_av—Ba—Nb_m1(1)xviii139.1 (6)
O2ii—Na_a—W2v130.5 (9)Na_av—Ba—Ti_m2118.7 (6)
O2ii—Na_a—Nb_m1(1)ii33.2 (5)Na_av—Ba—Mg_m2118.7 (6)
O6—Na_a—O7v101.4 (17)Na_axiv—Ba—K_b127.7 (5)
O6—Na_a—Bavi95.2 (6)Na_axiv—Ba—Ti_m1(1)68.3 (4)
O6—Na_a—Bavii157.2 (10)Na_axiv—Ba—Ti_m1(1)xviii164.3 (3)
O6—Na_a—W180.8 (8)Na_axiv—Ba—Ti_m1(2)50.2 (4)
O6—Na_a—W2v130.2 (10)Na_axiv—Ba—Ti_m1(2)xv125.9 (6)
O6—Na_a—Nb_m1(1)ii130.2 (13)Na_axiv—Ba—Fe_m287.4 (6)
O7v—Na_a—Bavi81.8 (6)Na_axiv—Ba—Si299.6 (3)
O7v—Na_a—Bavii62.0 (6)Na_axiv—Ba—Si2x143.4 (5)
O7v—Na_a—W1161.1 (13)Na_axiv—Ba—O1xiii43.6 (6)
O7v—Na_a—W2v82.4 (8)Na_axiv—Ba—O1xv92.9 (6)
O7v—Na_a—Nb_m1(1)ii73.7 (6)Na_axiv—Ba—O391.5 (6)
Bavi—Na_a—Bavii68.3 (4)Na_axiv—Ba—O3x146.7 (8)
Bavi—Na_a—W1116.9 (13)Na_axiv—Ba—Oh43.9 (4)
Bavi—Na_a—W2v35.6 (3)Na_axiv—Ba—Ohx143.3 (6)
Bavi—Na_a—Nb_m1(1)ii131.3 (6)Na_axiv—Ba—Baxvi54.9 (3)
Bavii—Na_a—W1120.2 (14)Na_axiv—Ba—Baxiii87.4 (6)
Bavii—Na_a—W2v37.9 (4)Na_axiv—Ba—W226.2 (5)
Bavii—Na_a—Nb_m1(1)ii63.0 (3)Na_axiv—Ba—W2xvii86.0 (4)
W1—Na_a—W2v111 (2)Na_axiv—Ba—W_c0
W1—Na_a—Nb_m1(1)ii90.5 (6)Na_axiv—Ba—Nb_m1(1)68.3 (4)
W2v—Na_a—Nb_m1(1)ii98.8 (7)Na_axiv—Ba—Nb_m1(1)xviii164.3 (3)
Na_axi—K_b—Na_aiii31.7 (8)Na_axiv—Ba—Ti_m287.4 (6)
Na_axi—K_b—Na_aix131.8 (4)Na_axiv—Ba—Mg_m287.4 (6)
Na_axi—K_b—Na_axix120.3 (6)K_b—Ba—Ti_m1(1)60.37 (10)
Na_axi—K_b—K_biii118.8 (5)K_b—Ba—Ti_m1(1)xviii60.37 (10)
Na_axi—K_b—K_bviii65.3 (3)K_b—Ba—Ti_m1(2)102.88 (15)
Na_axi—K_b—Si190.5 (3)K_b—Ba—Ti_m1(2)xv102.88 (15)
Na_axi—K_b—Si1iii83.7 (6)K_b—Ba—Fe_m2111.8 (3)
Na_axi—K_b—Si1ix127.3 (7)K_b—Ba—Si255.6 (3)
Na_axi—K_b—Si1x139.6 (4)K_b—Ba—Si2x55.6 (3)
Na_axi—K_b—Si250.4 (6)K_b—Ba—O1xiii135.1 (3)
Na_axi—K_b—Si2x92.4 (7)K_b—Ba—O1xv135.1 (3)
Na_axi—K_b—O372.4 (4)K_b—Ba—O337.0 (3)
Na_axi—K_b—O3x134.6 (9)K_b—Ba—O3x37.0 (3)
Na_axi—K_b—O4iii107.3 (7)K_b—Ba—Oh88.3 (4)
Na_axi—K_b—O571.0 (6)K_b—Ba—Ohx88.3 (4)
Na_axi—K_b—Ba93.3 (6)K_b—Ba—Baxvi135.7 (3)
Na_axi—K_b—W1xi21.8 (5)K_b—Ba—Baxiii111.8 (2)
Na_axi—K_b—W1ix112.3 (5)K_b—Ba—W2127.0 (3)
Na_aiii—K_b—Na_aix122.1 (6)K_b—Ba—W2xvii127.0 (3)
Na_aiii—K_b—Na_axix131.8 (4)K_b—Ba—W_c0
Na_aiii—K_b—K_biii93.8 (6)K_b—Ba—Nb_m1(1)60.37 (10)
Na_aiii—K_b—K_bviii66.5 (3)K_b—Ba—Nb_m1(1)xviii60.37 (10)
Na_aiii—K_b—Si188.3 (3)K_b—Ba—Ti_m2111.8 (3)
Na_aiii—K_b—Si1iii52.4 (6)K_b—Ba—Mg_m2111.8 (3)
Na_aiii—K_b—Si1ix96.4 (7)Ti_m1(1)—Ba—Ti_m1(1)xviii120.6 (2)
Na_aiii—K_b—Si1x136.9 (5)Ti_m1(1)—Ba—Ti_m1(2)55.35 (5)
Na_aiii—K_b—Si281.9 (6)Ti_m1(1)—Ba—Ti_m1(2)xv145.26 (12)
Na_aiii—K_b—Si2x123.0 (7)Ti_m1(1)—Ba—Fe_m2102.18 (10)
Na_aiii—K_b—O383.4 (4)Ti_m1(1)—Ba—Si251.81 (12)
Na_aiii—K_b—O3x153.9 (4)Ti_m1(1)—Ba—Si2x95.85 (13)
Na_aiii—K_b—O4iii75.6 (7)Ti_m1(1)—Ba—O1xiii85.8 (3)
Na_aiii—K_b—O5102.6 (7)Ti_m1(1)—Ba—O1xv143.5 (4)
Na_aiii—K_b—Ba117.8 (5)Ti_m1(1)—Ba—O330.4 (4)
Na_aiii—K_b—W1xi22.8 (5)Ti_m1(1)—Ba—O3x93.2 (4)
Na_aiii—K_b—W1ix113.4 (5)Ti_m1(1)—Ba—Oh29.1 (5)
Na_aix—K_b—Na_axix31.7 (8)Ti_m1(1)—Ba—Ohx148.4 (4)
Na_aix—K_b—K_biii93.8 (6)Ti_m1(1)—Ba—Baxvi109.46 (9)
Na_aix—K_b—K_bviii66.5 (3)Ti_m1(1)—Ba—Baxiii102.18 (11)
Na_aix—K_b—Si1136.9 (5)Ti_m1(1)—Ba—W279.1 (3)
Na_aix—K_b—Si1iii96.4 (7)Ti_m1(1)—Ba—W2xvii138.5 (3)
Na_aix—K_b—Si1ix52.4 (6)Ti_m1(1)—Ba—W_c0
Na_aix—K_b—Si1x88.3 (3)Ti_m1(1)—Ba—Nb_m1(1)0.0 (5)
Na_aix—K_b—Si2123.0 (7)Ti_m1(1)—Ba—Nb_m1(1)xviii120.6 (2)
Na_aix—K_b—Si2x81.9 (6)Ti_m1(1)—Ba—Ti_m2102.18 (10)
Na_aix—K_b—O3153.9 (4)Ti_m1(1)—Ba—Mg_m2102.18 (10)
Na_aix—K_b—O3x83.4 (4)Ti_m1(1)xviii—Ba—Ti_m1(2)145.26 (12)
Na_aix—K_b—O4iii75.6 (7)Ti_m1(1)xviii—Ba—Ti_m1(2)xv55.35 (5)
Na_aix—K_b—O5102.6 (7)Ti_m1(1)xviii—Ba—Fe_m2102.18 (10)
Na_aix—K_b—Ba117.8 (5)Ti_m1(1)xviii—Ba—Si295.85 (13)
Na_aix—K_b—W1xi113.4 (5)Ti_m1(1)xviii—Ba—Si2x51.81 (12)
Na_aix—K_b—W1ix22.8 (5)Ti_m1(1)xviii—Ba—O1xiii143.5 (4)
Na_axix—K_b—K_biii118.8 (5)Ti_m1(1)xviii—Ba—O1xv85.8 (3)
Na_axix—K_b—K_bviii65.3 (3)Ti_m1(1)xviii—Ba—O393.2 (4)
Na_axix—K_b—Si1139.6 (4)Ti_m1(1)xviii—Ba—O3x30.4 (4)
Na_axix—K_b—Si1iii127.3 (7)Ti_m1(1)xviii—Ba—Oh148.4 (4)
Na_axix—K_b—Si1ix83.7 (6)Ti_m1(1)xviii—Ba—Ohx29.1 (5)
Na_axix—K_b—Si1x90.5 (3)Ti_m1(1)xviii—Ba—Baxvi109.46 (9)
Na_axix—K_b—Si292.4 (7)Ti_m1(1)xviii—Ba—Baxiii102.18 (11)
Na_axix—K_b—Si2x50.4 (6)Ti_m1(1)xviii—Ba—W2138.5 (3)
Na_axix—K_b—O3134.6 (9)Ti_m1(1)xviii—Ba—W2xvii79.1 (3)
Na_axix—K_b—O3x72.4 (4)Ti_m1(1)xviii—Ba—W_c0
Na_axix—K_b—O4iii107.3 (7)Ti_m1(1)xviii—Ba—Nb_m1(1)120.6 (2)
Na_axix—K_b—O571.0 (6)Ti_m1(1)xviii—Ba—Nb_m1(1)xviii0.0 (5)
Na_axix—K_b—Ba93.3 (6)Ti_m1(1)xviii—Ba—Ti_m2102.18 (10)
Na_axix—K_b—W1xi112.3 (5)Ti_m1(1)xviii—Ba—Mg_m2102.18 (10)
Na_axix—K_b—W1ix21.8 (5)Ti_m1(2)—Ba—Ti_m1(2)xv106.3 (2)
K_biii—K_b—K_bviii132.3 (7)Ti_m1(2)—Ba—Fe_m253.15 (12)
K_biii—K_b—Si151.0 (3)Ti_m1(2)—Ba—Si252.90 (14)
K_biii—K_b—Si1iii47.5 (3)Ti_m1(2)—Ba—Si2x93.45 (16)
K_biii—K_b—Si1ix47.5 (3)Ti_m1(2)—Ba—O1xiii33.2 (3)
K_biii—K_b—Si1x51.0 (3)Ti_m1(2)—Ba—O1xv88.4 (4)
K_biii—K_b—Si2139.1 (3)Ti_m1(2)—Ba—O385.2 (4)
K_biii—K_b—Si2x139.1 (3)Ti_m1(2)—Ba—O3x139.6 (3)
K_biii—K_b—O377.9 (7)Ti_m1(2)—Ba—Oh31.6 (5)
K_biii—K_b—O3x77.9 (7)Ti_m1(2)—Ba—Ohx137.5 (5)
K_biii—K_b—O4iii38.7 (4)Ti_m1(2)—Ba—Baxvi103.27 (13)
K_biii—K_b—O5145.5 (5)Ti_m1(2)—Ba—Baxiii53.15 (12)
K_biii—K_b—Ba98.0 (3)Ti_m1(2)—Ba—W276.2 (3)
K_biii—K_b—W1xi116.2 (6)Ti_m1(2)—Ba—W2xvii128.7 (3)
K_biii—K_b—W1ix116.2 (6)Ti_m1(2)—Ba—W_c0
K_bviii—K_b—Si1154.19 (11)Ti_m1(2)—Ba—Nb_m1(1)55.35 (5)
K_bviii—K_b—Si1iii90.1 (5)Ti_m1(2)—Ba—Nb_m1(1)xviii145.26 (12)
K_bviii—K_b—Si1ix90.1 (5)Ti_m1(2)—Ba—Ti_m253.15 (12)
K_bviii—K_b—Si1x154.19 (11)Ti_m1(2)—Ba—Mg_m253.15 (12)
K_bviii—K_b—Si283.1 (5)Ti_m1(2)xv—Ba—Fe_m253.15 (12)
K_bviii—K_b—Si2x83.1 (5)Ti_m1(2)xv—Ba—Si293.45 (16)
K_bviii—K_b—O3136.4 (6)Ti_m1(2)xv—Ba—Si2x52.90 (14)
K_bviii—K_b—O3x136.4 (6)Ti_m1(2)xv—Ba—O1xiii88.4 (4)
K_bviii—K_b—O4iii93.6 (7)Ti_m1(2)xv—Ba—O1xv33.2 (3)
K_bviii—K_b—O582.2 (6)Ti_m1(2)xv—Ba—O3139.6 (3)
K_bviii—K_b—Ba129.7 (7)Ti_m1(2)xv—Ba—O3x85.2 (4)
K_bviii—K_b—W1xi49.0 (3)Ti_m1(2)xv—Ba—Oh137.5 (5)
K_bviii—K_b—W1ix49.0 (3)Ti_m1(2)xv—Ba—Ohx31.6 (5)
Si1—K_b—Si1iii77.9 (4)Ti_m1(2)xv—Ba—Baxvi103.27 (13)
Si1—K_b—Si1ix98.5 (5)Ti_m1(2)xv—Ba—Baxiii53.15 (12)
Si1—K_b—Si1x51.47 (16)Ti_m1(2)xv—Ba—W2128.7 (3)
Si1—K_b—Si288.2 (4)Ti_m1(2)xv—Ba—W2xvii76.2 (3)
Si1—K_b—Si2x108.0 (5)Ti_m1(2)xv—Ba—W_c0
Si1—K_b—O327.1 (6)Ti_m1(2)xv—Ba—Nb_m1(1)145.26 (12)
Si1—K_b—O3x67.2 (3)Ti_m1(2)xv—Ba—Nb_m1(1)xviii55.35 (5)
Si1—K_b—O4iii84.9 (5)Ti_m1(2)xv—Ba—Ti_m253.15 (12)
Si1—K_b—O598.8 (6)Ti_m1(2)xv—Ba—Mg_m253.15 (12)
Si1—K_b—Ba56.7 (3)Fe_m2—Ba—Si263.1 (2)
Si1—K_b—W1xi105.3 (3)Fe_m2—Ba—Si2x63.1 (2)
Si1—K_b—W1ix156.7 (4)Fe_m2—Ba—O1xiii43.9 (3)
Si1iii—K_b—Si1ix48.7 (3)Fe_m2—Ba—O1xv43.9 (3)
Si1iii—K_b—Si1x98.5 (5)Fe_m2—Ba—O3124.4 (4)
Si1iii—K_b—Si2132.02 (13)Fe_m2—Ba—O3x124.4 (4)
Si1iii—K_b—Si2x173.1 (3)Fe_m2—Ba—Oh84.5 (5)
Si1iii—K_b—O395.9 (7)Fe_m2—Ba—Ohx84.5 (5)
Si1iii—K_b—O3x125.4 (8)Fe_m2—Ba—Baxvi112.5 (3)
Si1iii—K_b—O4iii24.58 (18)Fe_m2—Ba—Baxiii0.0 (5)
Si1iii—K_b—O5154.5 (2)Fe_m2—Ba—W2108.8 (3)
Si1iii—K_b—Ba134.4 (2)Fe_m2—Ba—W2xvii108.8 (3)
Si1iii—K_b—W1xi72.0 (4)Fe_m2—Ba—W_c0
Si1iii—K_b—W1ix108.2 (6)Fe_m2—Ba—Nb_m1(1)102.18 (10)
Si1ix—K_b—Si1x77.9 (4)Fe_m2—Ba—Nb_m1(1)xviii102.18 (10)
Si1ix—K_b—Si2173.1 (3)Fe_m2—Ba—Ti_m20.0 (5)
Si1ix—K_b—Si2x132.02 (13)Fe_m2—Ba—Mg_m20.0 (5)
Si1ix—K_b—O3125.4 (8)Si2—Ba—Si2x48.98 (10)
Si1ix—K_b—O3x95.9 (7)Si2—Ba—O1xiii80.8 (3)
Si1ix—K_b—O4iii24.58 (18)Si2—Ba—O1xv105.0 (4)
Si1ix—K_b—O5154.5 (2)Si2—Ba—O362.4 (4)
Si1ix—K_b—Ba134.4 (2)Si2—Ba—O3x88.6 (3)
Si1ix—K_b—W1xi108.2 (6)Si2—Ba—Oh59.3 (2)
Si1ix—K_b—W1ix72.0 (4)Si2—Ba—Ohx108.3 (2)
Si1x—K_b—Si2108.0 (5)Si2—Ba—Baxvi154.50 (11)
Si1x—K_b—Si2x88.2 (4)Si2—Ba—Baxiii63.1 (2)
Si1x—K_b—O367.2 (3)Si2—Ba—W2122.4 (3)
Si1x—K_b—O3x27.1 (6)Si2—Ba—W2xvii169.6 (3)
Si1x—K_b—O4iii84.9 (5)Si2—Ba—W_c0
Si1x—K_b—O598.8 (6)Si2—Ba—Nb_m1(1)51.81 (12)
Si1x—K_b—Ba56.7 (3)Si2—Ba—Nb_m1(1)xviii95.85 (13)
Si1x—K_b—W1xi156.7 (4)Si2—Ba—Ti_m263.1 (2)
Si1x—K_b—W1ix105.3 (3)Si2—Ba—Mg_m263.1 (2)
Si2—K_b—Si2x46.2 (3)Si2x—Ba—O1xiii105.0 (4)
Si2—K_b—O361.2 (7)Si2x—Ba—O1xv80.8 (3)
Si2—K_b—O3x88.4 (8)Si2x—Ba—O388.6 (3)
Si2—K_b—O4iii156.60 (18)Si2x—Ba—O3x62.4 (4)
Si2—K_b—O523.09 (16)Si2x—Ba—Oh108.3 (2)
Si2—K_b—Ba51.3 (3)Si2x—Ba—Ohx59.3 (2)
Si2—K_b—W1xi68.0 (4)Si2x—Ba—Baxvi154.50 (11)
Si2—K_b—W1ix102.5 (6)Si2x—Ba—Baxiii63.1 (2)
Si2x—K_b—O388.4 (8)Si2x—Ba—W2169.6 (3)
Si2x—K_b—O3x61.2 (7)Si2x—Ba—W2xvii122.4 (3)
Si2x—K_b—O4iii156.60 (18)Si2x—Ba—W_c0
Si2x—K_b—O523.09 (16)Si2x—Ba—Nb_m1(1)95.85 (13)
Si2x—K_b—Ba51.3 (3)Si2x—Ba—Nb_m1(1)xviii51.81 (12)
Si2x—K_b—W1xi102.5 (6)Si2x—Ba—Ti_m263.1 (2)
Si2x—K_b—W1ix68.0 (4)Si2x—Ba—Mg_m263.1 (2)
O3—K_b—O3x70.7 (5)O1xiii—Ba—O1xv60.7 (5)
O3—K_b—O4iii109.3 (8)O1xiii—Ba—O3116.2 (5)
O3—K_b—O574.0 (8)O1xiii—Ba—O3x167.2 (4)
O3—K_b—Ba41.3 (6)O1xiii—Ba—Oh57.5 (6)
O3—K_b—W1xi92.2 (4)O1xiii—Ba—Ohx117.8 (7)
O3—K_b—W1ix155.7 (10)O1xiii—Ba—Baxvi80.6 (3)
O3x—K_b—O4iii109.3 (8)O1xiii—Ba—Baxiii43.9 (3)
O3x—K_b—O574.0 (8)O1xiii—Ba—W265.8 (3)
O3x—K_b—Ba41.3 (6)O1xiii—Ba—W2xvii97.8 (4)
O3x—K_b—W1xi155.7 (10)O1xiii—Ba—W_c0
O3x—K_b—W1ix92.2 (4)O1xiii—Ba—Nb_m1(1)85.8 (3)
O4iii—K_b—O5175.8 (6)O1xiii—Ba—Nb_m1(1)xviii143.5 (4)
O4iii—K_b—Ba136.7 (5)O1xiii—Ba—Ti_m243.9 (3)
O4iii—K_b—W1xi92.4 (6)O1xiii—Ba—Mg_m243.9 (3)
O4iii—K_b—W1ix92.4 (6)O1xv—Ba—O3167.2 (4)
O5—K_b—Ba47.4 (4)O1xv—Ba—O3x116.2 (5)
O5—K_b—W1xi84.9 (5)O1xv—Ba—Oh117.8 (7)
O5—K_b—W1ix84.9 (5)O1xv—Ba—Ohx57.5 (6)
Ba—K_b—W1xi114.8 (5)O1xv—Ba—Baxvi80.6 (3)
Ba—K_b—W1ix114.8 (5)O1xv—Ba—Baxiii43.9 (3)
W1xi—K_b—W1ix97.9 (5)O1xv—Ba—W297.8 (4)
Na_axi—Ti_m1(1)—Na_av180.0 (5)O1xv—Ba—W2xvii65.8 (3)
Na_axi—Ti_m1(1)—O239.0 (8)O1xv—Ba—W_c0
Na_axi—Ti_m1(1)—O2iv141.0 (8)O1xv—Ba—Nb_m1(1)143.5 (4)
Na_axi—Ti_m1(1)—O398.9 (5)O1xv—Ba—Nb_m1(1)xviii85.8 (3)
Na_axi—Ti_m1(1)—O3iv81.1 (5)O1xv—Ba—Ti_m243.9 (3)
Na_axi—Ti_m1(1)—Oh126.6 (8)O1xv—Ba—Mg_m243.9 (3)
Na_axi—Ti_m1(1)—Ohiv53.4 (8)O3—Ba—O3x63.8 (5)
Na_axi—Ti_m1(1)—Ba115.8 (4)O3—Ba—Oh59.0 (6)
Na_axi—Ti_m1(1)—Baxii64.2 (4)O3—Ba—Ohx122.3 (6)
Na_axi—Ti_m1(1)—Nb_m1(1)0O3—Ba—Baxvi111.6 (3)
Na_av—Ti_m1(1)—O2141.0 (8)O3—Ba—Baxiii124.4 (4)
Na_av—Ti_m1(1)—O2iv39.0 (8)O3—Ba—W291.4 (3)
Na_av—Ti_m1(1)—O381.1 (5)O3—Ba—W2xvii126.6 (5)
Na_av—Ti_m1(1)—O3iv98.9 (5)O3—Ba—W_c0
Na_av—Ti_m1(1)—Oh53.4 (8)O3—Ba—Nb_m1(1)30.4 (4)
Na_av—Ti_m1(1)—Ohiv126.6 (8)O3—Ba—Nb_m1(1)xviii93.2 (4)
Na_av—Ti_m1(1)—Ba64.2 (4)O3—Ba—Ti_m2124.4 (4)
Na_av—Ti_m1(1)—Baxii115.8 (4)O3—Ba—Mg_m2124.4 (4)
Na_av—Ti_m1(1)—Nb_m1(1)0O3x—Ba—Oh122.3 (6)
O2—Ti_m1(1)—O2iv180.0 (5)O3x—Ba—Ohx59.0 (6)
O2—Ti_m1(1)—O387.7 (6)O3x—Ba—Baxvi111.6 (3)
O2—Ti_m1(1)—O3iv92.3 (6)O3x—Ba—Baxiii124.4 (4)
O2—Ti_m1(1)—Oh89.8 (8)O3x—Ba—W2126.6 (5)
O2—Ti_m1(1)—Ohiv90.2 (8)O3x—Ba—W2xvii91.4 (3)
O2—Ti_m1(1)—Ba80.8 (4)O3x—Ba—W_c0
O2—Ti_m1(1)—Baxii99.2 (4)O3x—Ba—Nb_m1(1)93.2 (4)
O2—Ti_m1(1)—Nb_m1(1)0O3x—Ba—Nb_m1(1)xviii30.4 (4)
O2iv—Ti_m1(1)—O392.3 (6)O3x—Ba—Ti_m2124.4 (4)
O2iv—Ti_m1(1)—O3iv87.7 (6)O3x—Ba—Mg_m2124.4 (4)
O2iv—Ti_m1(1)—Oh90.2 (8)Oh—Ba—Ohx166.4 (5)
O2iv—Ti_m1(1)—Ohiv89.8 (8)Oh—Ba—Baxvi95.8 (2)
O2iv—Ti_m1(1)—Ba99.2 (4)Oh—Ba—Baxiii84.5 (5)
O2iv—Ti_m1(1)—Baxii80.8 (4)Oh—Ba—W263.2 (4)
O2iv—Ti_m1(1)—Nb_m1(1)0Oh—Ba—W2xvii128.4 (4)
O3—Ti_m1(1)—O3iv180.0 (5)Oh—Ba—W_c0
O3—Ti_m1(1)—Oh90.6 (8)Oh—Ba—Nb_m1(1)29.1 (5)
O3—Ti_m1(1)—Ohiv89.4 (8)Oh—Ba—Nb_m1(1)xviii148.4 (4)
O3—Ti_m1(1)—Ba47.3 (8)Oh—Ba—Ti_m284.5 (5)
O3—Ti_m1(1)—Baxii132.7 (8)Oh—Ba—Mg_m284.5 (5)
O3—Ti_m1(1)—Nb_m1(1)0Ohx—Ba—Baxvi95.8 (2)
O3iv—Ti_m1(1)—Oh89.4 (8)Ohx—Ba—Baxiii84.5 (5)
O3iv—Ti_m1(1)—Ohiv90.6 (8)Ohx—Ba—W2128.4 (4)
O3iv—Ti_m1(1)—Ba132.7 (8)Ohx—Ba—W2xvii63.2 (4)
O3iv—Ti_m1(1)—Baxii47.3 (8)Ohx—Ba—W_c0
O3iv—Ti_m1(1)—Nb_m1(1)0Ohx—Ba—Nb_m1(1)148.4 (4)
Oh—Ti_m1(1)—Ohiv180.0 (5)Ohx—Ba—Nb_m1(1)xviii29.1 (5)
Oh—Ti_m1(1)—Ba44.3 (4)Ohx—Ba—Ti_m284.5 (5)
Oh—Ti_m1(1)—Baxii135.7 (4)Ohx—Ba—Mg_m284.5 (5)
Oh—Ti_m1(1)—Nb_m1(1)0Baxvi—Ba—Baxiii112.5 (2)
Ohiv—Ti_m1(1)—Ba135.7 (4)Baxvi—Ba—W232.7 (3)
Ohiv—Ti_m1(1)—Baxii44.3 (4)Baxvi—Ba—W2xvii32.7 (3)
Ohiv—Ti_m1(1)—Nb_m1(1)0Baxvi—Ba—W_c0
Ba—Ti_m1(1)—Baxii180.0 (5)Baxvi—Ba—Nb_m1(1)109.46 (9)
Ba—Ti_m1(1)—Nb_m1(1)0Baxvi—Ba—Nb_m1(1)xviii109.46 (9)
Baxii—Ti_m1(1)—Nb_m1(1)0Baxvi—Ba—Ti_m2112.5 (3)
Na_aiv—Ti_m1(2)—Na_axiv174.5 (5)Baxvi—Ba—Mg_m2112.5 (3)
Na_aiv—Ti_m1(2)—Fe_m292.8 (3)Baxiii—Ba—W2108.8 (3)
Na_aiv—Ti_m1(2)—O157.6 (5)Baxiii—Ba—W2xvii108.8 (3)
Na_aiv—Ti_m1(2)—O1xiii127.5 (6)Baxiii—Ba—W_c0
Na_aiv—Ti_m1(2)—O6iv43.7 (7)Baxiii—Ba—Nb_m1(1)102.18 (11)
Na_aiv—Ti_m1(2)—O6xiv131.3 (7)Baxiii—Ba—Nb_m1(1)xviii102.18 (11)
Na_aiv—Ti_m1(2)—Oh122.2 (8)Baxiii—Ba—Ti_m20.0 (5)
Na_aiv—Ti_m1(2)—Ohxiii58.2 (8)Baxiii—Ba—Mg_m20.0 (5)
Na_aiv—Ti_m1(2)—Ba114.0 (5)W2—Ba—W2xvii65.3 (4)
Na_aiv—Ti_m1(2)—Baxiii70.7 (5)W2—Ba—W_c0
Na_aiv—Ti_m1(2)—Ti_m292.8 (3)W2—Ba—Nb_m1(1)79.1 (3)
Na_aiv—Ti_m1(2)—Mg_m292.8 (3)W2—Ba—Nb_m1(1)xviii138.5 (3)
Na_axiv—Ti_m1(2)—Fe_m292.8 (3)W2—Ba—Ti_m2108.8 (3)
Na_axiv—Ti_m1(2)—O1127.5 (6)W2—Ba—Mg_m2108.8 (3)
Na_axiv—Ti_m1(2)—O1xiii57.6 (5)W2xvii—Ba—W_c0
Na_axiv—Ti_m1(2)—O6iv131.3 (7)W2xvii—Ba—Nb_m1(1)138.5 (3)
Na_axiv—Ti_m1(2)—O6xiv43.7 (7)W2xvii—Ba—Nb_m1(1)xviii79.1 (3)
Na_axiv—Ti_m1(2)—Oh58.2 (8)W2xvii—Ba—Ti_m2108.8 (3)
Na_axiv—Ti_m1(2)—Ohxiii122.2 (8)W2xvii—Ba—Mg_m2108.8 (3)
Na_axiv—Ti_m1(2)—Ba70.7 (5)W_c—Ba—Nb_m1(1)0
Na_axiv—Ti_m1(2)—Baxiii114.0 (5)W_c—Ba—Nb_m1(1)xviii0
Na_axiv—Ti_m1(2)—Ti_m292.8 (3)W_c—Ba—Ti_m20
Na_axiv—Ti_m1(2)—Mg_m292.8 (3)W_c—Ba—Mg_m20
Fe_m2—Ti_m1(2)—O141.0 (3)Nb_m1(1)—Ba—Nb_m1(1)xviii120.6 (2)
Fe_m2—Ti_m1(2)—O1xiii41.0 (3)Nb_m1(1)—Ba—Ti_m2102.18 (10)
Fe_m2—Ti_m1(2)—O6iv130.6 (4)Nb_m1(1)—Ba—Mg_m2102.18 (10)
Fe_m2—Ti_m1(2)—O6xiv130.6 (4)Nb_m1(1)xviii—Ba—Ti_m2102.18 (10)
Fe_m2—Ti_m1(2)—Oh86.9 (3)Nb_m1(1)xviii—Ba—Mg_m2102.18 (10)
Fe_m2—Ti_m1(2)—Ohxiii86.9 (3)Ti_m2—Ba—Mg_m20.0 (5)
Fe_m2—Ti_m1(2)—Ba36.85 (12)Na_a—W1—Na_ai68.4 (16)
Fe_m2—Ti_m1(2)—Baxiii36.85 (12)Na_a—W1—K_bii129.7 (8)
Fe_m2—Ti_m1(2)—Ti_m20.0 (5)Na_a—W1—K_biii127.5 (8)
Fe_m2—Ti_m1(2)—Mg_m20.0 (5)Na_ai—W1—K_bii127.5 (8)
O1—Ti_m1(2)—O1xiii82.0 (5)Na_ai—W1—K_biii129.7 (8)
O1—Ti_m1(2)—O6iv89.7 (5)K_bii—W1—K_biii82.1 (7)
O1—Ti_m1(2)—O6xiv170.9 (5)Na_av—W2—Na_axiv70.0 (16)
O1—Ti_m1(2)—Oh89.5 (8)Na_av—W2—Ba114.2 (6)
O1—Ti_m1(2)—Ohxiii85.8 (8)Na_av—W2—Baxvi118.3 (6)
O1—Ti_m1(2)—Ba57.0 (5)Na_axiv—W2—Ba118.3 (6)
O1—Ti_m1(2)—Baxiii48.5 (7)Na_axiv—W2—Baxvi114.2 (6)
O1—Ti_m1(2)—Ti_m241.0 (3)Ba—W2—Baxvi114.7 (6)
O1—Ti_m1(2)—Mg_m241.0 (3)Fe_m2—W_c—Ba0
O1xiii—Ti_m1(2)—O6iv170.9 (5)Fe_m2—W_c—Ti_m20.0 (5)
O1xiii—Ti_m1(2)—O6xiv89.7 (5)Fe_m2—W_c—Mg_m20.0 (5)
O1xiii—Ti_m1(2)—Oh85.8 (8)Ba—W_c—Ti_m20
O1xiii—Ti_m1(2)—Ohxiii89.5 (8)Ba—W_c—Mg_m20
O1xiii—Ti_m1(2)—Ba48.5 (7)Ti_m2—W_c—Mg_m20.0 (5)
O1xiii—Ti_m1(2)—Baxiii57.0 (5)Na_axi—Nb_m1(1)—Na_av180.0 (5)
O1xiii—Ti_m1(2)—Ti_m241.0 (3)Na_axi—Nb_m1(1)—Ti_m1(1)0
O1xiii—Ti_m1(2)—Mg_m241.0 (3)Na_axi—Nb_m1(1)—O239.0 (8)
O6iv—Ti_m1(2)—O6xiv98.8 (6)Na_axi—Nb_m1(1)—O2iv141.0 (8)
O6iv—Ti_m1(2)—Oh98.0 (10)Na_axi—Nb_m1(1)—O398.9 (5)
O6iv—Ti_m1(2)—Ohxiii86.1 (9)Na_axi—Nb_m1(1)—O3iv81.1 (5)
O6iv—Ti_m1(2)—Ba129.0 (8)Na_axi—Nb_m1(1)—Oh126.6 (8)
O6iv—Ti_m1(2)—Baxiii114.4 (6)Na_axi—Nb_m1(1)—Ohiv53.4 (8)
O6iv—Ti_m1(2)—Ti_m2130.6 (4)Na_axi—Nb_m1(1)—Ba115.8 (4)
O6iv—Ti_m1(2)—Mg_m2130.6 (4)Na_axi—Nb_m1(1)—Baxii64.2 (4)
O6xiv—Ti_m1(2)—Oh86.1 (9)Na_av—Nb_m1(1)—Ti_m1(1)0
O6xiv—Ti_m1(2)—Ohxiii98.0 (10)Na_av—Nb_m1(1)—O2141.0 (8)
O6xiv—Ti_m1(2)—Ba114.4 (6)Na_av—Nb_m1(1)—O2iv39.0 (8)
O6xiv—Ti_m1(2)—Baxiii129.0 (8)Na_av—Nb_m1(1)—O381.1 (5)
O6xiv—Ti_m1(2)—Ti_m2130.6 (4)Na_av—Nb_m1(1)—O3iv98.9 (5)
O6xiv—Ti_m1(2)—Mg_m2130.6 (4)Na_av—Nb_m1(1)—Oh53.4 (8)
Oh—Ti_m1(2)—Ohxiii173.7 (5)Na_av—Nb_m1(1)—Ohiv126.6 (8)
Oh—Ti_m1(2)—Ba50.3 (3)Na_av—Nb_m1(1)—Ba64.2 (4)
Oh—Ti_m1(2)—Baxiii123.5 (3)Na_av—Nb_m1(1)—Baxii115.8 (4)
Oh—Ti_m1(2)—Ti_m286.9 (3)Ti_m1(1)—Nb_m1(1)—O20
Oh—Ti_m1(2)—Mg_m286.9 (3)Ti_m1(1)—Nb_m1(1)—O2iv0
Ohxiii—Ti_m1(2)—Ba123.5 (3)Ti_m1(1)—Nb_m1(1)—O30
Ohxiii—Ti_m1(2)—Baxiii50.3 (3)Ti_m1(1)—Nb_m1(1)—O3iv0
Ohxiii—Ti_m1(2)—Ti_m286.9 (3)Ti_m1(1)—Nb_m1(1)—Oh0
Ohxiii—Ti_m1(2)—Mg_m286.9 (3)Ti_m1(1)—Nb_m1(1)—Ohiv0
Ba—Ti_m1(2)—Baxiii73.71 (17)Ti_m1(1)—Nb_m1(1)—Ba0
Ba—Ti_m1(2)—Ti_m236.85 (12)Ti_m1(1)—Nb_m1(1)—Baxii0
Ba—Ti_m1(2)—Mg_m236.85 (12)O2—Nb_m1(1)—O2iv180.0 (5)
Baxiii—Ti_m1(2)—Ti_m236.85 (12)O2—Nb_m1(1)—O387.7 (6)
Baxiii—Ti_m1(2)—Mg_m236.85 (12)O2—Nb_m1(1)—O3iv92.3 (6)
Ti_m2—Ti_m1(2)—Mg_m20.0 (5)O2—Nb_m1(1)—Oh89.8 (8)
Ti_m1(2)—Fe_m2—Ti_m1(2)xv180.0 (5)O2—Nb_m1(1)—Ohiv90.2 (8)
Ti_m1(2)—Fe_m2—O143.6 (3)O2—Nb_m1(1)—Ba80.8 (4)
Ti_m1(2)—Fe_m2—O1xiii43.6 (3)O2—Nb_m1(1)—Baxii99.2 (4)
Ti_m1(2)—Fe_m2—O1xv136.4 (3)O2iv—Nb_m1(1)—O392.3 (6)
Ti_m1(2)—Fe_m2—O1x136.4 (3)O2iv—Nb_m1(1)—O3iv87.7 (6)
Ti_m1(2)—Fe_m2—Ba90O2iv—Nb_m1(1)—Oh90.2 (8)
Ti_m1(2)—Fe_m2—Baxiii90O2iv—Nb_m1(1)—Ohiv89.8 (8)
Ti_m1(2)—Fe_m2—W_c90O2iv—Nb_m1(1)—Ba99.2 (4)
Ti_m1(2)—Fe_m2—W_cxiii90O2iv—Nb_m1(1)—Baxii80.8 (4)
Ti_m1(2)—Fe_m2—Ti_m20O3—Nb_m1(1)—O3iv180.0 (5)
Ti_m1(2)—Fe_m2—Mg_m20O3—Nb_m1(1)—Oh90.6 (8)
Ti_m1(2)xv—Fe_m2—O1136.4 (3)O3—Nb_m1(1)—Ohiv89.4 (8)
Ti_m1(2)xv—Fe_m2—O1xiii136.4 (3)O3—Nb_m1(1)—Ba47.3 (8)
Ti_m1(2)xv—Fe_m2—O1xv43.6 (3)O3—Nb_m1(1)—Baxii132.7 (8)
Ti_m1(2)xv—Fe_m2—O1x43.6 (3)O3iv—Nb_m1(1)—Oh89.4 (8)
Ti_m1(2)xv—Fe_m2—Ba90O3iv—Nb_m1(1)—Ohiv90.6 (8)
Ti_m1(2)xv—Fe_m2—Baxiii90O3iv—Nb_m1(1)—Ba132.7 (8)
Ti_m1(2)xv—Fe_m2—W_c90O3iv—Nb_m1(1)—Baxii47.3 (8)
Ti_m1(2)xv—Fe_m2—W_cxiii90Oh—Nb_m1(1)—Ohiv180.0 (5)
Ti_m1(2)xv—Fe_m2—Ti_m20Oh—Nb_m1(1)—Ba44.3 (4)
Ti_m1(2)xv—Fe_m2—Mg_m20Oh—Nb_m1(1)—Baxii135.7 (4)
O1—Fe_m2—O1xiii87.1 (4)Ohiv—Nb_m1(1)—Ba135.7 (4)
O1—Fe_m2—O1xv180.0 (5)Ohiv—Nb_m1(1)—Baxii44.3 (4)
O1—Fe_m2—O1x92.9 (4)Ba—Nb_m1(1)—Baxii180.0 (5)
O1—Fe_m2—Ba96.0 (7)Ti_m1(2)—Ti_m2—Ti_m1(2)xv180.0 (5)
O1—Fe_m2—Baxiii84.0 (7)Ti_m1(2)—Ti_m2—Fe_m20
O1—Fe_m2—W_c96.0 (7)Ti_m1(2)—Ti_m2—O143.6 (3)
O1—Fe_m2—W_cxiii84.0 (7)Ti_m1(2)—Ti_m2—O1xiii43.6 (3)
O1—Fe_m2—Ti_m20Ti_m1(2)—Ti_m2—O1xv136.4 (3)
O1—Fe_m2—Mg_m20Ti_m1(2)—Ti_m2—O1x136.4 (3)
O1xiii—Fe_m2—O1xv92.9 (4)Ti_m1(2)—Ti_m2—Ba90
O1xiii—Fe_m2—O1x180.0 (5)Ti_m1(2)—Ti_m2—Baxiii90
O1xiii—Fe_m2—Ba84.0 (7)Ti_m1(2)—Ti_m2—W_c90
O1xiii—Fe_m2—Baxiii96.0 (7)Ti_m1(2)—Ti_m2—W_cxiii90
O1xiii—Fe_m2—W_c84.0 (7)Ti_m1(2)—Ti_m2—Mg_m20
O1xiii—Fe_m2—W_cxiii96.0 (7)Ti_m1(2)xv—Ti_m2—Fe_m20
O1xiii—Fe_m2—Ti_m20Ti_m1(2)xv—Ti_m2—O1136.4 (3)
O1xiii—Fe_m2—Mg_m20Ti_m1(2)xv—Ti_m2—O1xiii136.4 (3)
O1xv—Fe_m2—O1x87.1 (4)Ti_m1(2)xv—Ti_m2—O1xv43.6 (3)
O1xv—Fe_m2—Ba84.0 (7)Ti_m1(2)xv—Ti_m2—O1x43.6 (3)
O1xv—Fe_m2—Baxiii96.0 (7)Ti_m1(2)xv—Ti_m2—Ba90
O1xv—Fe_m2—W_c84.0 (7)Ti_m1(2)xv—Ti_m2—Baxiii90
O1xv—Fe_m2—W_cxiii96.0 (7)Ti_m1(2)xv—Ti_m2—W_c90
O1xv—Fe_m2—Ti_m20Ti_m1(2)xv—Ti_m2—W_cxiii90
O1xv—Fe_m2—Mg_m20Ti_m1(2)xv—Ti_m2—Mg_m20
O1x—Fe_m2—Ba96.0 (7)Fe_m2—Ti_m2—O10
O1x—Fe_m2—Baxiii84.0 (7)Fe_m2—Ti_m2—O1xiii0
O1x—Fe_m2—W_c96.0 (7)Fe_m2—Ti_m2—O1xv0
O1x—Fe_m2—W_cxiii84.0 (7)Fe_m2—Ti_m2—O1x0
O1x—Fe_m2—Ti_m20Fe_m2—Ti_m2—Ba0
O1x—Fe_m2—Mg_m20Fe_m2—Ti_m2—Baxiii0
Ba—Fe_m2—Baxiii180.0 (5)Fe_m2—Ti_m2—W_c0
Ba—Fe_m2—W_c0.0 (5)Fe_m2—Ti_m2—W_cxiii0
Ba—Fe_m2—W_cxiii180.0 (5)Fe_m2—Ti_m2—Mg_m20
Ba—Fe_m2—Ti_m20O1—Ti_m2—O1xiii87.1 (4)
Ba—Fe_m2—Mg_m20O1—Ti_m2—O1xv180.0 (5)
Baxiii—Fe_m2—W_c180.0 (5)O1—Ti_m2—O1x92.9 (4)
Baxiii—Fe_m2—W_cxiii0.0 (5)O1—Ti_m2—Ba96.0 (7)
Baxiii—Fe_m2—Ti_m20O1—Ti_m2—Baxiii84.0 (7)
Baxiii—Fe_m2—Mg_m20O1—Ti_m2—W_c96.0 (7)
W_c—Fe_m2—W_cxiii180.0 (5)O1—Ti_m2—W_cxiii84.0 (7)
W_c—Fe_m2—Ti_m20O1—Ti_m2—Mg_m20
W_c—Fe_m2—Mg_m20O1xiii—Ti_m2—O1xv92.9 (4)
W_cxiii—Fe_m2—Ti_m20O1xiii—Ti_m2—O1x180.0 (5)
W_cxiii—Fe_m2—Mg_m20O1xiii—Ti_m2—Ba84.0 (7)
Ti_m2—Fe_m2—Mg_m20O1xiii—Ti_m2—Baxiii96.0 (7)
K_b—Si1—K_biii81.5 (4)O1xiii—Ti_m2—W_c84.0 (7)
K_b—Si1—O349.7 (8)O1xiii—Ti_m2—W_cxiii96.0 (7)
K_b—Si1—O463.6 (6)O1xiii—Ti_m2—Mg_m20
K_b—Si1—O6105.2 (6)O1xv—Ti_m2—O1x87.1 (4)
K_b—Si1—O7141.0 (8)O1xv—Ti_m2—Ba84.0 (7)
K_biii—Si1—O3131.0 (8)O1xv—Ti_m2—Baxiii96.0 (7)
K_biii—Si1—O437.6 (12)O1xv—Ti_m2—W_c84.0 (7)
K_biii—Si1—O666.6 (9)O1xv—Ti_m2—W_cxiii96.0 (7)
K_biii—Si1—O7117.1 (8)O1xv—Ti_m2—Mg_m20
O3—Si1—O4107.7 (10)O1x—Ti_m2—Ba96.0 (7)
O3—Si1—O6116.6 (9)O1x—Ti_m2—Baxiii84.0 (7)
O3—Si1—O7106.0 (13)O1x—Ti_m2—W_c96.0 (7)
O4—Si1—O6103.5 (15)O1x—Ti_m2—W_cxiii84.0 (7)
O4—Si1—O7109.2 (7)O1x—Ti_m2—Mg_m20
O6—Si1—O7113.5 (8)Ba—Ti_m2—Baxiii180.0 (5)
Na_aiv—Si2—K_b163.4 (6)Ba—Ti_m2—W_c0.0 (5)
Na_aiv—Si2—O164.0 (8)Ba—Ti_m2—W_cxiii180.0 (5)
Na_aiv—Si2—O297.2 (9)Ba—Ti_m2—Mg_m20
Na_aiv—Si2—O5149.6 (11)Baxiii—Ti_m2—W_c180.0 (5)
Na_aiv—Si2—O7xi50.0 (8)Baxiii—Ti_m2—W_cxiii0.0 (5)
Na_aiv—Si2—Ba122.9 (5)Baxiii—Ti_m2—Mg_m20
K_b—Si2—O1132.5 (6)W_c—Ti_m2—W_cxiii180.0 (5)
K_b—Si2—O274.6 (9)W_c—Ti_m2—Mg_m20
K_b—Si2—O537.0 (12)W_cxiii—Ti_m2—Mg_m20
K_b—Si2—O7xi119.5 (8)Ti_m1(2)—Mg_m2—Ti_m1(2)xv180.0 (5)
K_b—Si2—Ba73.1 (3)Ti_m1(2)—Mg_m2—Fe_m20
O1—Si2—O2115.1 (8)Ti_m1(2)—Mg_m2—O143.6 (3)
O1—Si2—O5110.0 (10)Ti_m1(2)—Mg_m2—O1xiii43.6 (3)
O1—Si2—O7xi99.7 (11)Ti_m1(2)—Mg_m2—O1xv136.4 (3)
O1—Si2—Ba59.8 (6)Ti_m1(2)—Mg_m2—O1x136.4 (3)
O2—Si2—O5111.4 (15)Ti_m1(2)—Mg_m2—Ba90
O2—Si2—O7xi113.6 (7)Ti_m1(2)—Mg_m2—Baxiii90
O2—Si2—Ba97.5 (5)Ti_m1(2)—Mg_m2—W_c90
O5—Si2—O7xi106.3 (8)Ti_m1(2)—Mg_m2—W_cxiii90
O5—Si2—Ba64.9 (5)Ti_m1(2)—Mg_m2—Ti_m20
O7xi—Si2—Ba148.4 (7)Ti_m1(2)xv—Mg_m2—Fe_m20
Ti_m1(2)—O1—Fe_m295.4 (5)Ti_m1(2)xv—Mg_m2—O1136.4 (3)
Ti_m1(2)—O1—Si2119.6 (9)Ti_m1(2)xv—Mg_m2—O1xiii136.4 (3)
Ti_m1(2)—O1—Baxiii98.3 (8)Ti_m1(2)xv—Mg_m2—O1xv43.6 (3)
Ti_m1(2)—O1—Ti_m295.4 (5)Ti_m1(2)xv—Mg_m2—O1x43.6 (3)
Ti_m1(2)—O1—Mg_m295.4 (5)Ti_m1(2)xv—Mg_m2—Ba90
Fe_m2—O1—Si2125.8 (10)Ti_m1(2)xv—Mg_m2—Baxiii90
Fe_m2—O1—Baxiii52.1 (5)Ti_m1(2)xv—Mg_m2—W_c90
Fe_m2—O1—Ti_m20.0 (5)Ti_m1(2)xv—Mg_m2—W_cxiii90
Fe_m2—O1—Mg_m20.0 (5)Ti_m1(2)xv—Mg_m2—Ti_m20
Si2—O1—Baxiii141.1 (6)Fe_m2—Mg_m2—O10
Si2—O1—Ti_m2125.8 (10)Fe_m2—Mg_m2—O1xiii0
Si2—O1—Mg_m2125.8 (10)Fe_m2—Mg_m2—O1xv0
Baxiii—O1—Ti_m252.1 (5)Fe_m2—Mg_m2—O1x0
Baxiii—O1—Mg_m252.1 (5)Fe_m2—Mg_m2—Ba0
Ti_m2—O1—Mg_m20.0 (5)Fe_m2—Mg_m2—Baxiii0
Na_axi—O2—Ti_m1(1)107.8 (12)Fe_m2—Mg_m2—W_c0
Na_axi—O2—Si2121.5 (8)Fe_m2—Mg_m2—W_cxiii0
Na_axi—O2—Nb_m1(1)107.8 (12)Fe_m2—Mg_m2—Ti_m20
Ti_m1(1)—O2—Si2128.9 (7)O1—Mg_m2—O1xiii87.1 (4)
Ti_m1(1)—O2—Nb_m1(1)0.0 (5)O1—Mg_m2—O1xv180.0 (5)
Si2—O2—Nb_m1(1)128.9 (7)O1—Mg_m2—O1x92.9 (4)
K_b—O3—Ti_m1(1)124.3 (5)O1—Mg_m2—Ba96.0 (7)
K_b—O3—Si1103.2 (13)O1—Mg_m2—Baxiii84.0 (7)
K_b—O3—Ba101.7 (6)O1—Mg_m2—W_c96.0 (7)
K_b—O3—Nb_m1(1)124.3 (5)O1—Mg_m2—W_cxiii84.0 (7)
Ti_m1(1)—O3—Si1114.6 (7)O1—Mg_m2—Ti_m20
Ti_m1(1)—O3—Ba102.3 (11)O1xiii—Mg_m2—O1xv92.9 (4)
Ti_m1(1)—O3—Nb_m1(1)0.0 (5)O1xiii—Mg_m2—O1x180.0 (5)
Si1—O3—Ba109.5 (7)O1xiii—Mg_m2—Ba84.0 (7)
Si1—O3—Nb_m1(1)114.6 (7)O1xiii—Mg_m2—Baxiii96.0 (7)
Ba—O3—Nb_m1(1)102.3 (11)O1xiii—Mg_m2—W_c84.0 (7)
K_biii—O4—Si1117.8 (12)O1xiii—Mg_m2—W_cxiii96.0 (7)
K_biii—O4—Si1x117.8 (12)O1xiii—Mg_m2—Ti_m20
Si1—O4—Si1x123 (2)O1xv—Mg_m2—O1x87.1 (4)
K_b—O5—Si2119.9 (12)O1xv—Mg_m2—Ba84.0 (7)
K_b—O5—Si2x119.9 (12)O1xv—Mg_m2—Baxiii96.0 (7)
Si2—O5—Si2x120 (2)O1xv—Mg_m2—W_c84.0 (7)
Na_a—O6—Ti_m1(2)iv100.2 (9)O1xv—Mg_m2—W_cxiii96.0 (7)
Na_a—O6—Si1125.2 (10)O1xv—Mg_m2—Ti_m20
Ti_m1(2)iv—O6—Si1128.5 (13)O1x—Mg_m2—Ba96.0 (7)
Na_av—O7—Si1123.5 (8)O1x—Mg_m2—Baxiii84.0 (7)
Na_av—O7—Si2ii96.8 (8)O1x—Mg_m2—W_c96.0 (7)
Si1—O7—Si2ii126.5 (17)O1x—Mg_m2—W_cxiii84.0 (7)
Ti_m1(1)—Oh—Ti_m1(2)127.9 (5)O1x—Mg_m2—Ti_m20
Ti_m1(1)—Oh—Ba106.6 (8)Ba—Mg_m2—Baxiii180.0 (5)
Ti_m1(1)—Oh—Nb_m1(1)0.0 (5)Ba—Mg_m2—W_c0.0 (5)
Ti_m1(2)—Oh—Ba98.2 (7)Ba—Mg_m2—W_cxiii180.0 (5)
Ti_m1(2)—Oh—Nb_m1(1)127.9 (5)Ba—Mg_m2—Ti_m20
Ba—Oh—Nb_m1(1)106.6 (8)Baxiii—Mg_m2—W_c180.0 (5)
Na_axx—Ba—Na_axxi33.8 (9)Baxiii—Mg_m2—W_cxiii0.0 (5)
Na_axx—Ba—Na_av111.7 (4)Baxiii—Mg_m2—Ti_m20
Na_axx—Ba—Na_axiv100.1 (5)W_c—Mg_m2—W_cxiii180.0 (5)
Na_axx—Ba—K_b127.7 (5)W_c—Mg_m2—Ti_m20
Na_axx—Ba—Ti_m1(1)164.3 (3)W_cxiii—Mg_m2—Ti_m20
Symmetry codes: (i) x+1, y, z; (ii) x, y, z1; (iii) x+1, y, z+1; (iv) x+1/2, y+1/2, z+1; (v) x+1/2, y+1/2, z; (vi) x+1/2, y+1/2, z; (vii) x+1/2, y+1/2, z; (viii) x+1, y, z+2; (ix) x+1, y, z+1; (x) x, y, z; (xi) x, y, z+1; (xii) x+1/2, y+1/2, z+1; (xiii) x, y, z+1; (xiv) x1/2, y+1/2, z; (xv) x, y, z+1; (xvi) x, y, z; (xvii) x, y, z; (xviii) x+1/2, y1/2, z+1; (xix) x, y, z+1; (xx) x1/2, y1/2, z; (xxi) x+1/2, y1/2, z.
(labu-Fe_22.53) top
Crystal data top
Ba0.7Fe0.5K2.1Mg0.05Na2Nb0.1O33Si8Ti4Z = 2
Mr = 1206.8F(000) = 1167
Monoclinic, C2/mDx = 3.632 Mg m3
Hall symbol: -C 2ySynchrotron radiation, λ = 0.414 Å
a = 13.342 (6) ÅCell parameters from 1825 reflections
b = 13.0162 (6) Åθ = 1.9–18.9°
c = 7.0497 (13) ŵ = 0.96 mm1
β = 115.68 (3)°T = 293 K
V = 1103.3 (6) Å3Anhedral grain
Data collection top
ESRF ID 09
diffractometer
θmax = 18.9°, θmin = 1.9°
1825 measured reflectionsh = 88
666 independent reflectionsk = 2020
293 reflections with I > 2σ(I)l = 910
Rint = 0.053
Refinement top
Refinement on F0 restraints
R[F2 > 2σ(F2)] = 0.0986 constraints
wR(F2) = 0.168Weighting scheme based on measured s.u.'s w = 1/(σ2(F) + 0.0100000007F2)
S = 1.01(Δ/σ)max = 0.049
666 reflectionsΔρmax = 0.96 e Å3
57 parametersΔρmin = 0.96 e Å3
Fractional atomic coordinates and isotropic or equivalent isotropic displacement parameters (Å2) top
xyzUiso*/UeqOcc. (<1)
Na_a0.414 (3)0.2741 (13)0.018 (3)0.053 (5)*0.5
K_b0.4385 (16)00.7443 (13)0.067 (3)*
Ti_m1(1)0.250.250.50.0368 (13)*0.95
Ti_m1(2)00.2162 (3)0.50.0311 (12)*
Fe_m2000.50.050 (3)*0.5
Si10.3318 (9)0.1098 (3)0.2777 (6)0.0220 (11)*
Si20.2130 (8)0.1087 (3)0.8217 (6)0.0207 (10)*
O10.0758 (19)0.1041 (7)0.6874 (16)0.022 (2)*
O20.270 (2)0.2019 (8)0.7708 (16)0.027 (3)*
O30.299 (2)0.1145 (8)0.4537 (16)0.026 (3)*
O40.389 (3)00.298 (2)0.030 (4)*
O50.271 (3)00.796 (2)0.025 (4)*
O60.416 (2)0.1904 (10)0.2853 (19)0.040 (4)*
O70.221 (2)0.1117 (7)0.0592 (15)0.021 (2)*
Oh0.0988 (19)0.2075 (7)0.3788 (14)0.017 (2)*
Ba0.0988 (7)00.3345 (6)0.0287 (10)*0.35
W10.50.146 (2)00.075 (8)*
W200.1056 (13)00.038 (5)*
W_c0.0988 (7)00.3345 (6)0.0287 (10)*0.65
Nb_m1(1)0.250.250.50.0368 (13)*0.05
Ti_m2000.50.050 (3)*0.1
Mg_m2000.50.050 (3)*0.05
Atomic displacement parameters (Å2) top
U11U22U33U12U13U23
???????
Geometric parameters (Å, º) top
Na_a—Na_ai2.41 (6)Ti_m1(2)—Ohxiii1.86 (2)
Na_a—K_bii4.14 (2)Ti_m1(2)—Ba3.515 (6)
Na_a—K_biii4.07 (2)Ti_m1(2)—Baxiii3.515 (6)
Na_a—Ti_m1(1)ii3.364 (17)Ti_m1(2)—Ti_m22.815 (4)
Na_a—Ti_m1(2)iv3.080 (18)Ti_m1(2)—Mg_m22.815 (4)
Na_a—Si2iv2.85 (4)Fe_m2—O11.856 (11)
Na_a—O2ii2.17 (3)Fe_m2—O1xiii1.856 (11)
Na_a—O62.16 (3)Fe_m2—O1xv1.856 (11)
Na_a—O7v2.22 (4)Fe_m2—O1x1.856 (11)
Na_a—Bavi3.86 (2)Fe_m2—Ba2.105 (9)
Na_a—Bavii3.81 (2)Fe_m2—Baxiii2.105 (9)
Na_a—W12.06 (4)Fe_m2—W_c2.105 (9)
Na_a—W2v1.98 (3)Fe_m2—W_cxiii2.105 (9)
Na_a—Nb_m1(1)ii3.364 (17)Fe_m2—Ti_m20
K_b—K_biii4.41 (3)Fe_m2—Mg_m20
K_b—K_bviii3.250 (11)Si1—O31.48 (2)
K_b—Si13.291 (8)Si1—O41.60 (2)
K_b—Si1iii3.44 (2)Si1—O61.52 (3)
K_b—Si1ix3.44 (2)Si1—O71.607 (16)
K_b—Si1x3.291 (8)Si2—O11.66 (2)
K_b—Si23.57 (2)Si2—O21.56 (2)
K_b—Si2x3.57 (2)Si2—O51.66 (2)
K_b—O32.563 (17)Si2—O7xi1.631 (16)
K_b—O3x2.563 (17)Si2—Ba3.404 (5)
K_b—O4iii2.44 (5)O1—Baxiii2.64 (2)
K_b—O52.42 (5)O1—Ti_m21.856 (11)
K_b—Ba4.19 (2)O1—Mg_m21.856 (11)
K_b—W1xi2.50 (2)O2—Nb_m1(1)1.913 (14)
K_b—W1ix2.50 (2)O3—Ba2.85 (3)
Ti_m1(1)—O21.913 (14)O3—Nb_m1(1)1.958 (15)
Ti_m1(1)—O2iv1.913 (14)Oh—Ba2.718 (9)
Ti_m1(1)—O31.958 (15)Oh—Nb_m1(1)1.90 (2)
Ti_m1(1)—O3iv1.958 (15)Ba—Baxvi4.291 (6)
Ti_m1(1)—Oh1.90 (2)Ba—Baxiii4.210 (13)
Ti_m1(1)—Ohiv1.90 (2)Ba—W22.548 (10)
Ti_m1(1)—Ba3.739 (4)Ba—W2xvii2.548 (10)
Ti_m1(1)—Baxii3.739 (4)Ba—W_c0
Ti_m1(1)—Nb_m1(1)0Ba—Nb_m1(1)3.739 (4)
Ti_m1(2)—Fe_m22.815 (4)Ba—Nb_m1(1)xviii3.739 (4)
Ti_m1(2)—O11.934 (11)Ba—Ti_m22.105 (9)
Ti_m1(2)—O1xiii1.934 (11)Ba—Mg_m22.105 (9)
Ti_m1(2)—O6iv1.884 (14)W_c—Ti_m22.105 (9)
Ti_m1(2)—O6xiv1.884 (14)W_c—Mg_m22.105 (9)
Ti_m1(2)—Oh1.86 (2)Ti_m2—Mg_m20
Na_ai—Na_a—K_bii71.3 (8)Na_axx—Ba—Ti_m1(1)xviii68.9 (4)
Na_ai—Na_a—K_biii74.5 (8)Na_axx—Ba—Ti_m1(2)124.3 (6)
Na_ai—Na_a—Ti_m1(1)ii94.9 (9)Na_axx—Ba—Ti_m1(2)xv49.1 (4)
Na_ai—Na_a—Ti_m1(2)iv101.7 (10)Na_axx—Ba—Fe_m285.6 (6)
Na_ai—Na_a—Si2iv142.9 (9)Na_axx—Ba—Si2142.5 (5)
Na_ai—Na_a—O2ii117.6 (14)Na_axx—Ba—Si2x99.2 (3)
Na_ai—Na_a—O6116.0 (15)Na_axx—Ba—O1xiii91.8 (7)
Na_ai—Na_a—O7v133.1 (12)Na_axx—Ba—O1xv41.4 (7)
Na_ai—Na_a—Bavi70.4 (8)Na_axx—Ba—O3148.2 (8)
Na_ai—Na_a—Bavii72.9 (8)Na_axx—Ba—O3x93.1 (6)
Na_ai—Na_a—W154.1 (11)Na_axx—Ba—Oh142.3 (6)
Na_ai—Na_a—W2v52.4 (11)Na_axx—Ba—Ohx43.8 (4)
Na_ai—Na_a—Nb_m1(1)ii94.9 (9)Na_axx—Ba—Baxvi55.4 (3)
K_bii—Na_a—K_biii46.7 (3)Na_axx—Ba—Baxiii85.6 (6)
K_bii—Na_a—Ti_m1(1)ii63.8 (3)Na_axx—Ba—W286.1 (4)
K_bii—Na_a—Ti_m1(2)iv118.9 (5)Na_axx—Ba—W2xvii27.2 (5)
K_bii—Na_a—Si2iv145.7 (12)Na_axx—Ba—W_c0
K_bii—Na_a—O2ii58.1 (8)Na_axx—Ba—Nb_m1(1)164.9 (3)
K_bii—Na_a—O689.9 (7)Na_axx—Ba—Nb_m1(1)xviii68.9 (4)
K_bii—Na_a—O7v133.1 (9)Na_axx—Ba—Ti_m285.6 (6)
K_bii—Na_a—Bavi140.1 (12)Na_axx—Ba—Mg_m285.6 (6)
K_bii—Na_a—Bavii110.6 (7)Na_axxi—Ba—Na_av101.1 (5)
K_bii—Na_a—W127.5 (4)Na_axxi—Ba—Na_axiv111.9 (4)
K_bii—Na_a—W2v119.2 (15)Na_axxi—Ba—K_b100.4 (6)
K_bii—Na_a—Nb_m1(1)ii63.8 (3)Na_axxi—Ba—Ti_m1(1)137.9 (6)
K_biii—Na_a—Ti_m1(1)ii109.6 (5)Na_axxi—Ba—Ti_m1(1)xviii52.9 (3)
K_biii—Na_a—Ti_m1(2)iv72.5 (4)Na_axxi—Ba—Ti_m1(2)156.6 (5)
K_biii—Na_a—Si2iv124.8 (8)Na_axxi—Ba—Ti_m1(2)xv71.4 (5)
K_biii—Na_a—O2ii93.0 (6)Na_axxi—Ba—Fe_m2120.0 (6)
K_biii—Na_a—O651.6 (8)Na_axxi—Ba—Si2148.7 (4)
K_biii—Na_a—O7v152.4 (16)Na_axxi—Ba—Si2x102.3 (3)
K_biii—Na_a—Bavi110.9 (7)Na_axxi—Ba—O1xiii124.7 (6)
K_biii—Na_a—Bavii145.4 (12)Na_axxi—Ba—O1xv77.1 (7)
K_biii—Na_a—W129.8 (5)Na_axxi—Ba—O3111.6 (8)
K_biii—Na_a—W2v122.1 (15)Na_axxi—Ba—O3x63.9 (6)
K_biii—Na_a—Nb_m1(1)ii109.6 (5)Na_axxi—Ba—Oh147.1 (5)
Ti_m1(1)ii—Na_a—Ti_m1(2)iv163.2 (15)Na_axxi—Ba—Ohx46.0 (4)
Ti_m1(1)ii—Na_a—Si2iv105.1 (10)Na_axxi—Ba—Baxvi56.6 (3)
Ti_m1(1)ii—Na_a—O2ii32.1 (5)Na_axxi—Ba—Baxiii120.0 (6)
Ti_m1(1)ii—Na_a—O6130.9 (13)Na_axxi—Ba—W287.3 (4)
Ti_m1(1)ii—Na_a—O7v73.6 (6)Na_axxi—Ba—W2xvii28.3 (5)
Ti_m1(1)ii—Na_a—Bavi130.6 (6)Na_axxi—Ba—W_c0
Ti_m1(1)ii—Na_a—Bavii62.5 (3)Na_axxi—Ba—Nb_m1(1)137.9 (6)
Ti_m1(1)ii—Na_a—W188.5 (6)Na_axxi—Ba—Nb_m1(1)xviii52.9 (3)
Ti_m1(1)ii—Na_a—W2v97.2 (7)Na_axxi—Ba—Ti_m2120.0 (6)
Ti_m1(1)ii—Na_a—Nb_m1(1)ii0.0 (5)Na_axxi—Ba—Mg_m2120.0 (6)
Ti_m1(2)iv—Na_a—Si2iv62.8 (6)Na_av—Ba—Na_axiv36.7 (9)
Ti_m1(2)iv—Na_a—O2ii132.9 (16)Na_av—Ba—K_b100.4 (6)
Ti_m1(2)iv—Na_a—O637.2 (5)Na_av—Ba—Ti_m1(1)52.9 (3)
Ti_m1(2)iv—Na_a—O7v96.8 (10)Na_av—Ba—Ti_m1(1)xviii137.9 (6)
Ti_m1(2)iv—Na_a—Bavi59.6 (3)Na_av—Ba—Ti_m1(2)71.4 (5)
Ti_m1(2)iv—Na_a—Bavii125.4 (5)Na_av—Ba—Ti_m1(2)xv156.6 (5)
Ti_m1(2)iv—Na_a—W198.7 (7)Na_av—Ba—Fe_m2120.0 (6)
Ti_m1(2)iv—Na_a—W2v95.2 (7)Na_av—Ba—Si2102.3 (3)
Ti_m1(2)iv—Na_a—Nb_m1(1)ii163.2 (15)Na_av—Ba—Si2x148.7 (4)
Si2iv—Na_a—O2ii94.5 (16)Na_av—Ba—O1xiii77.1 (7)
Si2iv—Na_a—O673.2 (12)Na_av—Ba—O1xv124.7 (6)
Si2iv—Na_a—O7v34.7 (6)Na_av—Ba—O363.9 (6)
Si2iv—Na_a—Bavi72.8 (4)Na_av—Ba—O3x111.6 (8)
Si2iv—Na_a—Bavii88.8 (5)Na_av—Ba—Oh46.0 (4)
Si2iv—Na_a—W1154.2 (12)Na_av—Ba—Ohx147.1 (5)
Si2iv—Na_a—W2v93.6 (8)Na_av—Ba—Baxvi56.6 (3)
Si2iv—Na_a—Nb_m1(1)ii105.1 (10)Na_av—Ba—Baxiii120.0 (6)
O2ii—Na_a—O698.9 (15)Na_av—Ba—W228.3 (5)
O2ii—Na_a—O7v75.5 (12)Na_av—Ba—W2xvii87.3 (4)
O2ii—Na_a—Bavi156.1 (9)Na_av—Ba—W_c0
O2ii—Na_a—Bavii92.0 (6)Na_av—Ba—Nb_m1(1)52.9 (3)
O2ii—Na_a—W185.4 (8)Na_av—Ba—Nb_m1(1)xviii137.9 (6)
O2ii—Na_a—W2v128.7 (9)Na_av—Ba—Ti_m2120.0 (6)
O2ii—Na_a—Nb_m1(1)ii32.1 (5)Na_av—Ba—Mg_m2120.0 (6)
O6—Na_a—O7v104.7 (19)Na_axiv—Ba—K_b128.8 (5)
O6—Na_a—Bavi96.7 (7)Na_axiv—Ba—Ti_m1(1)68.9 (4)
O6—Na_a—Bavii159.6 (10)Na_axiv—Ba—Ti_m1(1)xviii164.9 (3)
O6—Na_a—W181.3 (9)Na_axiv—Ba—Ti_m1(2)49.1 (4)
O6—Na_a—W2v131.8 (11)Na_axiv—Ba—Ti_m1(2)xv124.3 (6)
O6—Na_a—Nb_m1(1)ii130.9 (13)Na_axiv—Ba—Fe_m285.6 (6)
O7v—Na_a—Bavi83.1 (6)Na_axiv—Ba—Si299.2 (3)
O7v—Na_a—Bavii61.3 (7)Na_axiv—Ba—Si2x142.5 (5)
O7v—Na_a—W1160.6 (11)Na_axiv—Ba—O1xiii41.4 (7)
O7v—Na_a—W2v83.4 (9)Na_axiv—Ba—O1xv91.8 (7)
O7v—Na_a—Nb_m1(1)ii73.6 (6)Na_axiv—Ba—O393.1 (6)
Bavi—Na_a—Bavii68.1 (4)Na_axiv—Ba—O3x148.2 (8)
Bavi—Na_a—W1114.9 (14)Na_axiv—Ba—Oh43.8 (4)
Bavi—Na_a—W2v36.1 (3)Na_axiv—Ba—Ohx142.3 (6)
Bavi—Na_a—Nb_m1(1)ii130.6 (6)Na_axiv—Ba—Baxvi55.4 (3)
Bavii—Na_a—W1117.0 (14)Na_axiv—Ba—Baxiii85.6 (6)
Bavii—Na_a—W2v37.7 (4)Na_axiv—Ba—W227.2 (5)
Bavii—Na_a—Nb_m1(1)ii62.5 (3)Na_axiv—Ba—W2xvii86.1 (4)
W1—Na_a—W2v107 (2)Na_axiv—Ba—W_c0
W1—Na_a—Nb_m1(1)ii88.5 (6)Na_axiv—Ba—Nb_m1(1)68.9 (4)
W2v—Na_a—Nb_m1(1)ii97.2 (7)Na_axiv—Ba—Nb_m1(1)xviii164.9 (3)
Na_axi—K_b—Na_aiii34.2 (8)Na_axiv—Ba—Ti_m285.6 (6)
Na_axi—K_b—Na_aix133.3 (4)Na_axiv—Ba—Mg_m285.6 (6)
Na_axi—K_b—Na_axix119.2 (6)K_b—Ba—Ti_m1(1)60.55 (10)
Na_axi—K_b—K_biii119.7 (5)K_b—Ba—Ti_m1(1)xviii60.55 (10)
Na_axi—K_b—K_bviii65.5 (3)K_b—Ba—Ti_m1(2)102.73 (15)
Na_axi—K_b—Si190.3 (3)K_b—Ba—Ti_m1(2)xv102.73 (15)
Na_axi—K_b—Si1iii85.1 (6)K_b—Ba—Fe_m2111.6 (3)
Na_axi—K_b—Si1ix129.1 (7)K_b—Ba—Si255.0 (3)
Na_axi—K_b—Si1x138.9 (4)K_b—Ba—Si2x55.0 (3)
Na_axi—K_b—Si249.1 (6)K_b—Ba—O1xiii134.7 (3)
Na_axi—K_b—Si2x91.6 (7)K_b—Ba—O1xv134.7 (3)
Na_axi—K_b—O372.3 (4)K_b—Ba—O336.9 (3)
Na_axi—K_b—O3x134.3 (9)K_b—Ba—O3x36.9 (3)
Na_axi—K_b—O4iii109.0 (7)K_b—Ba—Oh88.5 (5)
Na_axi—K_b—O570.4 (7)K_b—Ba—Ohx88.5 (5)
Na_axi—K_b—Ba92.4 (6)K_b—Ba—Baxvi136.4 (3)
Na_axi—K_b—W1xi22.4 (5)K_b—Ba—Baxiii111.6 (2)
Na_axi—K_b—W1ix112.7 (6)K_b—Ba—W2127.5 (3)
Na_aiii—K_b—Na_aix122.6 (6)K_b—Ba—W2xvii127.5 (3)
Na_aiii—K_b—Na_axix133.3 (4)K_b—Ba—W_c0
Na_aiii—K_b—K_biii92.5 (6)K_b—Ba—Nb_m1(1)60.55 (10)
Na_aiii—K_b—K_bviii67.8 (3)K_b—Ba—Nb_m1(1)xviii60.55 (10)
Na_aiii—K_b—Si187.3 (3)K_b—Ba—Ti_m2111.6 (3)
Na_aiii—K_b—Si1iii51.2 (6)K_b—Ba—Mg_m2111.6 (3)
Na_aiii—K_b—Si1ix95.8 (7)Ti_m1(1)—Ba—Ti_m1(1)xviii121.0 (2)
Na_aiii—K_b—Si1x135.6 (5)Ti_m1(1)—Ba—Ti_m1(2)55.16 (4)
Na_aiii—K_b—Si283.0 (6)Ti_m1(1)—Ba—Ti_m1(2)xv145.34 (13)
Na_aiii—K_b—Si2x125.0 (7)Ti_m1(1)—Ba—Fe_m2102.11 (10)
Na_aiii—K_b—O382.6 (4)Ti_m1(1)—Ba—Si251.56 (12)
Na_aiii—K_b—O3x153.2 (4)Ti_m1(1)—Ba—Si2x95.83 (13)
Na_aiii—K_b—O4iii74.8 (7)Ti_m1(1)—Ba—O1xiii85.1 (3)
Na_aiii—K_b—O5104.6 (7)Ti_m1(1)—Ba—O1xv143.9 (4)
Na_aiii—K_b—Ba118.0 (5)Ti_m1(1)—Ba—O331.0 (4)
Na_aiii—K_b—W1xi24.2 (6)Ti_m1(1)—Ba—O3x93.0 (4)
Na_aiii—K_b—W1ix114.9 (5)Ti_m1(1)—Ba—Oh29.1 (5)
Na_aix—K_b—Na_axix34.2 (8)Ti_m1(1)—Ba—Ohx148.8 (4)
Na_aix—K_b—K_biii92.5 (6)Ti_m1(1)—Ba—Baxvi109.53 (10)
Na_aix—K_b—K_bviii67.8 (3)Ti_m1(1)—Ba—Baxiii102.11 (12)
Na_aix—K_b—Si1135.6 (5)Ti_m1(1)—Ba—W279.2 (3)
Na_aix—K_b—Si1iii95.8 (7)Ti_m1(1)—Ba—W2xvii138.7 (3)
Na_aix—K_b—Si1ix51.2 (6)Ti_m1(1)—Ba—W_c0
Na_aix—K_b—Si1x87.3 (3)Ti_m1(1)—Ba—Nb_m1(1)0.0 (5)
Na_aix—K_b—Si2125.0 (7)Ti_m1(1)—Ba—Nb_m1(1)xviii121.0 (2)
Na_aix—K_b—Si2x83.0 (6)Ti_m1(1)—Ba—Ti_m2102.11 (10)
Na_aix—K_b—O3153.2 (4)Ti_m1(1)—Ba—Mg_m2102.11 (10)
Na_aix—K_b—O3x82.6 (4)Ti_m1(1)xviii—Ba—Ti_m1(2)145.34 (13)
Na_aix—K_b—O4iii74.8 (7)Ti_m1(1)xviii—Ba—Ti_m1(2)xv55.16 (4)
Na_aix—K_b—O5104.6 (7)Ti_m1(1)xviii—Ba—Fe_m2102.11 (10)
Na_aix—K_b—Ba118.0 (5)Ti_m1(1)xviii—Ba—Si295.83 (13)
Na_aix—K_b—W1xi114.9 (5)Ti_m1(1)xviii—Ba—Si2x51.56 (12)
Na_aix—K_b—W1ix24.2 (6)Ti_m1(1)xviii—Ba—O1xiii143.9 (4)
Na_axix—K_b—K_biii119.7 (5)Ti_m1(1)xviii—Ba—O1xv85.1 (3)
Na_axix—K_b—K_bviii65.5 (3)Ti_m1(1)xviii—Ba—O393.0 (4)
Na_axix—K_b—Si1138.9 (4)Ti_m1(1)xviii—Ba—O3x31.0 (4)
Na_axix—K_b—Si1iii129.1 (7)Ti_m1(1)xviii—Ba—Oh148.8 (4)
Na_axix—K_b—Si1ix85.1 (6)Ti_m1(1)xviii—Ba—Ohx29.1 (5)
Na_axix—K_b—Si1x90.3 (3)Ti_m1(1)xviii—Ba—Baxvi109.53 (10)
Na_axix—K_b—Si291.6 (7)Ti_m1(1)xviii—Ba—Baxiii102.11 (12)
Na_axix—K_b—Si2x49.1 (6)Ti_m1(1)xviii—Ba—W2138.7 (3)
Na_axix—K_b—O3134.3 (9)Ti_m1(1)xviii—Ba—W2xvii79.2 (3)
Na_axix—K_b—O3x72.3 (4)Ti_m1(1)xviii—Ba—W_c0
Na_axix—K_b—O4iii109.0 (7)Ti_m1(1)xviii—Ba—Nb_m1(1)121.0 (2)
Na_axix—K_b—O570.4 (7)Ti_m1(1)xviii—Ba—Nb_m1(1)xviii0.0 (5)
Na_axix—K_b—Ba92.4 (6)Ti_m1(1)xviii—Ba—Ti_m2102.11 (10)
Na_axix—K_b—W1xi112.7 (6)Ti_m1(1)xviii—Ba—Mg_m2102.11 (10)
Na_axix—K_b—W1ix22.4 (5)Ti_m1(2)—Ba—Ti_m1(2)xv106.4 (2)
K_biii—K_b—K_bviii133.3 (7)Ti_m1(2)—Ba—Fe_m253.21 (13)
K_biii—K_b—Si150.6 (3)Ti_m1(2)—Ba—Si253.17 (14)
K_biii—K_b—Si1iii47.6 (3)Ti_m1(2)—Ba—Si2x93.79 (17)
K_biii—K_b—Si1ix47.6 (3)Ti_m1(2)—Ba—O1xiii32.9 (3)
K_biii—K_b—Si1x50.6 (3)Ti_m1(2)—Ba—O1xv89.0 (4)
K_biii—K_b—Si2137.9 (3)Ti_m1(2)—Ba—O385.5 (4)
K_biii—K_b—Si2x137.9 (3)Ti_m1(2)—Ba—O3x139.4 (3)
K_biii—K_b—O376.2 (7)Ti_m1(2)—Ba—Oh31.5 (5)
K_biii—K_b—O3x76.2 (7)Ti_m1(2)—Ba—Ohx137.6 (6)
K_biii—K_b—O4iii38.4 (5)Ti_m1(2)—Ba—Baxvi102.99 (14)
K_biii—K_b—O5143.1 (5)Ti_m1(2)—Ba—Baxiii53.21 (13)
K_biii—K_b—Ba96.8 (3)Ti_m1(2)—Ba—W275.9 (3)
K_biii—K_b—W1xi116.5 (6)Ti_m1(2)—Ba—W2xvii128.4 (3)
K_biii—K_b—W1ix116.5 (6)Ti_m1(2)—Ba—W_c0
K_bviii—K_b—Si1154.23 (10)Ti_m1(2)—Ba—Nb_m1(1)55.16 (4)
K_bviii—K_b—Si1iii91.1 (5)Ti_m1(2)—Ba—Nb_m1(1)xviii145.34 (13)
K_bviii—K_b—Si1ix91.1 (5)Ti_m1(2)—Ba—Ti_m253.21 (13)
K_bviii—K_b—Si1x154.23 (10)Ti_m1(2)—Ba—Mg_m253.21 (13)
K_bviii—K_b—Si283.4 (5)Ti_m1(2)xv—Ba—Fe_m253.21 (13)
K_bviii—K_b—Si2x83.4 (5)Ti_m1(2)xv—Ba—Si293.79 (17)
K_bviii—K_b—O3136.8 (6)Ti_m1(2)xv—Ba—Si2x53.17 (14)
K_bviii—K_b—O3x136.8 (6)Ti_m1(2)xv—Ba—O1xiii89.0 (4)
K_bviii—K_b—O4iii95.0 (7)Ti_m1(2)xv—Ba—O1xv32.9 (3)
K_bviii—K_b—O583.6 (7)Ti_m1(2)xv—Ba—O3139.4 (3)
K_bviii—K_b—Ba129.8 (7)Ti_m1(2)xv—Ba—O3x85.5 (4)
K_bviii—K_b—W1xi49.5 (4)Ti_m1(2)xv—Ba—Oh137.6 (6)
K_bviii—K_b—W1ix49.5 (4)Ti_m1(2)xv—Ba—Ohx31.5 (5)
Si1—K_b—Si1iii77.4 (4)Ti_m1(2)xv—Ba—Baxvi102.99 (14)
Si1—K_b—Si1ix98.2 (5)Ti_m1(2)xv—Ba—Baxiii53.21 (13)
Si1—K_b—Si1x51.47 (16)Ti_m1(2)xv—Ba—W2128.4 (3)
Si1—K_b—Si287.3 (4)Ti_m1(2)xv—Ba—W2xvii75.9 (3)
Si1—K_b—Si2x107.2 (5)Ti_m1(2)xv—Ba—W_c0
Si1—K_b—O325.7 (6)Ti_m1(2)xv—Ba—Nb_m1(1)145.34 (13)
Si1—K_b—O3x66.7 (3)Ti_m1(2)xv—Ba—Nb_m1(1)xviii55.16 (4)
Si1—K_b—O4iii84.2 (5)Ti_m1(2)xv—Ba—Ti_m253.21 (13)
Si1—K_b—O597.1 (6)Ti_m1(2)xv—Ba—Mg_m253.21 (13)
Si1—K_b—Ba56.0 (3)Fe_m2—Ba—Si263.6 (2)
Si1—K_b—W1xi104.8 (4)Fe_m2—Ba—Si2x63.6 (2)
Si1—K_b—W1ix156.2 (5)Fe_m2—Ba—O1xiii44.3 (3)
Si1iii—K_b—Si1ix49.0 (3)Fe_m2—Ba—O1xv44.3 (3)
Si1iii—K_b—Si1x98.2 (5)Fe_m2—Ba—O3124.7 (4)
Si1iii—K_b—Si2131.81 (14)Fe_m2—Ba—O3x124.7 (4)
Si1iii—K_b—Si2x174.3 (3)Fe_m2—Ba—Oh84.6 (5)
Si1iii—K_b—O394.2 (7)Fe_m2—Ba—Ohx84.6 (5)
Si1iii—K_b—O3x123.7 (8)Fe_m2—Ba—Baxvi112.0 (3)
Si1iii—K_b—O4iii24.79 (19)Fe_m2—Ba—Baxiii0.0 (5)
Si1iii—K_b—O5155.0 (2)Fe_m2—Ba—W2108.4 (3)
Si1iii—K_b—Ba133.4 (2)Fe_m2—Ba—W2xvii108.4 (3)
Si1iii—K_b—W1xi72.4 (4)Fe_m2—Ba—W_c0
Si1iii—K_b—W1ix109.1 (6)Fe_m2—Ba—Nb_m1(1)102.11 (10)
Si1ix—K_b—Si1x77.4 (4)Fe_m2—Ba—Nb_m1(1)xviii102.11 (10)
Si1ix—K_b—Si2174.3 (3)Fe_m2—Ba—Ti_m20.0 (5)
Si1ix—K_b—Si2x131.81 (14)Fe_m2—Ba—Mg_m20.0 (5)
Si1ix—K_b—O3123.7 (8)Si2—Ba—Si2x49.11 (10)
Si1ix—K_b—O3x94.2 (7)Si2—Ba—O1xiii81.0 (3)
Si1ix—K_b—O4iii24.79 (19)Si2—Ba—O1xv105.7 (4)
Si1ix—K_b—O5155.0 (2)Si2—Ba—O362.1 (4)
Si1ix—K_b—Ba133.4 (2)Si2—Ba—O3x88.1 (3)
Si1ix—K_b—W1xi109.1 (6)Si2—Ba—Oh59.6 (2)
Si1ix—K_b—W1ix72.4 (4)Si2—Ba—Ohx108.6 (2)
Si1x—K_b—Si2107.2 (5)Si2—Ba—Baxvi154.46 (12)
Si1x—K_b—Si2x87.3 (4)Si2—Ba—Baxiii63.6 (2)
Si1x—K_b—O366.7 (3)Si2—Ba—W2122.4 (3)
Si1x—K_b—O3x25.7 (6)Si2—Ba—W2xvii169.7 (4)
Si1x—K_b—O4iii84.2 (5)Si2—Ba—W_c0
Si1x—K_b—O597.1 (6)Si2—Ba—Nb_m1(1)51.56 (12)
Si1x—K_b—Ba56.0 (3)Si2—Ba—Nb_m1(1)xviii95.83 (13)
Si1x—K_b—W1xi156.2 (5)Si2—Ba—Ti_m263.6 (2)
Si1x—K_b—W1ix104.8 (4)Si2—Ba—Mg_m263.6 (2)
Si2—K_b—Si2x46.6 (3)Si2x—Ba—O1xiii105.7 (4)
Si2—K_b—O361.7 (7)Si2x—Ba—O1xv81.0 (3)
Si2—K_b—O3x89.2 (8)Si2x—Ba—O388.1 (3)
Si2—K_b—O4iii156.58 (18)Si2x—Ba—O3x62.1 (4)
Si2—K_b—O523.33 (17)Si2x—Ba—Oh108.6 (2)
Si2—K_b—Ba51.3 (3)Si2x—Ba—Ohx59.6 (2)
Si2—K_b—W1xi67.9 (4)Si2x—Ba—Baxvi154.46 (12)
Si2—K_b—W1ix103.0 (6)Si2x—Ba—Baxiii63.6 (2)
Si2x—K_b—O389.2 (8)Si2x—Ba—W2169.7 (4)
Si2x—K_b—O3x61.7 (7)Si2x—Ba—W2xvii122.4 (3)
Si2x—K_b—O4iii156.58 (18)Si2x—Ba—W_c0
Si2x—K_b—O523.33 (17)Si2x—Ba—Nb_m1(1)95.83 (13)
Si2x—K_b—Ba51.3 (3)Si2x—Ba—Nb_m1(1)xviii51.56 (12)
Si2x—K_b—W1xi103.0 (6)Si2x—Ba—Ti_m263.6 (2)
Si2x—K_b—W1ix67.9 (4)Si2x—Ba—Mg_m263.6 (2)
O3—K_b—O3x71.1 (5)O1xiii—Ba—O1xv61.7 (5)
O3—K_b—O4iii107.2 (8)O1xiii—Ba—O3116.1 (5)
O3—K_b—O573.9 (8)O1xiii—Ba—O3x167.5 (4)
O3—K_b—Ba41.9 (6)O1xiii—Ba—Oh56.9 (6)
O3—K_b—W1xi91.8 (5)O1xiii—Ba—Ohx118.2 (7)
O3—K_b—W1ix156.4 (10)O1xiii—Ba—Baxvi80.2 (3)
O3x—K_b—O4iii107.2 (8)O1xiii—Ba—Baxiii44.3 (3)
O3x—K_b—O573.9 (8)O1xiii—Ba—W265.2 (3)
O3x—K_b—Ba41.9 (6)O1xiii—Ba—W2xvii97.7 (4)
O3x—K_b—W1xi156.4 (10)O1xiii—Ba—W_c0
O3x—K_b—W1ix91.8 (5)O1xiii—Ba—Nb_m1(1)85.1 (3)
O4iii—K_b—O5178.6 (6)O1xiii—Ba—Nb_m1(1)xviii143.9 (4)
O4iii—K_b—Ba135.2 (5)O1xiii—Ba—Ti_m244.3 (3)
O4iii—K_b—W1xi93.2 (6)O1xiii—Ba—Mg_m244.3 (3)
O4iii—K_b—W1ix93.2 (6)O1xv—Ba—O3167.5 (4)
O5—K_b—Ba46.2 (4)O1xv—Ba—O3x116.1 (5)
O5—K_b—W1xi85.8 (6)O1xv—Ba—Oh118.2 (7)
O5—K_b—W1ix85.8 (6)O1xv—Ba—Ohx56.9 (6)
Ba—K_b—W1xi114.6 (6)O1xv—Ba—Baxvi80.2 (3)
Ba—K_b—W1ix114.6 (6)O1xv—Ba—Baxiii44.3 (3)
W1xi—K_b—W1ix98.9 (6)O1xv—Ba—W297.7 (4)
Na_axi—Ti_m1(1)—Na_av180.0 (5)O1xv—Ba—W2xvii65.2 (3)
Na_axi—Ti_m1(1)—O237.1 (8)O1xv—Ba—W_c0
Na_axi—Ti_m1(1)—O2iv142.9 (8)O1xv—Ba—Nb_m1(1)143.9 (4)
Na_axi—Ti_m1(1)—O399.1 (5)O1xv—Ba—Nb_m1(1)xviii85.1 (3)
Na_axi—Ti_m1(1)—O3iv80.9 (5)O1xv—Ba—Ti_m244.3 (3)
Na_axi—Ti_m1(1)—Oh125.5 (8)O1xv—Ba—Mg_m244.3 (3)
Na_axi—Ti_m1(1)—Ohiv54.5 (8)O3—Ba—O3x63.0 (5)
Na_axi—Ti_m1(1)—Ba115.5 (4)O3—Ba—Oh59.6 (6)
Na_axi—Ti_m1(1)—Baxii64.5 (4)O3—Ba—Ohx122.1 (6)
Na_axi—Ti_m1(1)—Nb_m1(1)0O3—Ba—Baxvi112.0 (3)
Na_av—Ti_m1(1)—O2142.9 (8)O3—Ba—Baxiii124.7 (4)
Na_av—Ti_m1(1)—O2iv37.1 (8)O3—Ba—W291.9 (3)
Na_av—Ti_m1(1)—O380.9 (5)O3—Ba—W2xvii126.7 (5)
Na_av—Ti_m1(1)—O3iv99.1 (5)O3—Ba—W_c0
Na_av—Ti_m1(1)—Oh54.5 (8)O3—Ba—Nb_m1(1)31.0 (4)
Na_av—Ti_m1(1)—Ohiv125.5 (8)O3—Ba—Nb_m1(1)xviii93.0 (4)
Na_av—Ti_m1(1)—Ba64.5 (4)O3—Ba—Ti_m2124.7 (4)
Na_av—Ti_m1(1)—Baxii115.5 (4)O3—Ba—Mg_m2124.7 (4)
Na_av—Ti_m1(1)—Nb_m1(1)0O3x—Ba—Oh122.1 (6)
O2—Ti_m1(1)—O2iv180.0 (5)O3x—Ba—Ohx59.6 (6)
O2—Ti_m1(1)—O387.7 (6)O3x—Ba—Baxvi112.0 (3)
O2—Ti_m1(1)—O3iv92.3 (6)O3x—Ba—Baxiii124.7 (4)
O2—Ti_m1(1)—Oh91.0 (8)O3x—Ba—W2126.7 (5)
O2—Ti_m1(1)—Ohiv89.0 (8)O3x—Ba—W2xvii91.9 (3)
O2—Ti_m1(1)—Ba81.4 (4)O3x—Ba—W_c0
O2—Ti_m1(1)—Baxii98.6 (4)O3x—Ba—Nb_m1(1)93.0 (4)
O2—Ti_m1(1)—Nb_m1(1)0O3x—Ba—Nb_m1(1)xviii31.0 (4)
O2iv—Ti_m1(1)—O392.3 (6)O3x—Ba—Ti_m2124.7 (4)
O2iv—Ti_m1(1)—O3iv87.7 (6)O3x—Ba—Mg_m2124.7 (4)
O2iv—Ti_m1(1)—Oh89.0 (8)Oh—Ba—Ohx166.8 (5)
O2iv—Ti_m1(1)—Ohiv91.0 (8)Oh—Ba—Baxvi95.5 (2)
O2iv—Ti_m1(1)—Ba98.6 (4)Oh—Ba—Baxiii84.6 (5)
O2iv—Ti_m1(1)—Baxii81.4 (4)Oh—Ba—W262.9 (4)
O2iv—Ti_m1(1)—Nb_m1(1)0Oh—Ba—W2xvii128.1 (4)
O3—Ti_m1(1)—O3iv180.0 (5)Oh—Ba—W_c0
O3—Ti_m1(1)—Oh91.8 (8)Oh—Ba—Nb_m1(1)29.1 (5)
O3—Ti_m1(1)—Ohiv88.2 (8)Oh—Ba—Nb_m1(1)xviii148.8 (4)
O3—Ti_m1(1)—Ba48.6 (8)Oh—Ba—Ti_m284.6 (5)
O3—Ti_m1(1)—Baxii131.4 (8)Oh—Ba—Mg_m284.6 (5)
O3—Ti_m1(1)—Nb_m1(1)0Ohx—Ba—Baxvi95.5 (2)
O3iv—Ti_m1(1)—Oh88.2 (8)Ohx—Ba—Baxiii84.6 (5)
O3iv—Ti_m1(1)—Ohiv91.8 (8)Ohx—Ba—W2128.1 (4)
O3iv—Ti_m1(1)—Ba131.4 (8)Ohx—Ba—W2xvii62.9 (4)
O3iv—Ti_m1(1)—Baxii48.6 (8)Ohx—Ba—W_c0
O3iv—Ti_m1(1)—Nb_m1(1)0Ohx—Ba—Nb_m1(1)148.8 (4)
Oh—Ti_m1(1)—Ohiv180.0 (5)Ohx—Ba—Nb_m1(1)xviii29.1 (5)
Oh—Ti_m1(1)—Ba44.1 (4)Ohx—Ba—Ti_m284.6 (5)
Oh—Ti_m1(1)—Baxii135.9 (4)Ohx—Ba—Mg_m284.6 (5)
Oh—Ti_m1(1)—Nb_m1(1)0Baxvi—Ba—Baxiii112.0 (2)
Ohiv—Ti_m1(1)—Ba135.9 (4)Baxvi—Ba—W232.7 (3)
Ohiv—Ti_m1(1)—Baxii44.1 (4)Baxvi—Ba—W2xvii32.7 (3)
Ohiv—Ti_m1(1)—Nb_m1(1)0Baxvi—Ba—W_c0
Ba—Ti_m1(1)—Baxii180.0 (5)Baxvi—Ba—Nb_m1(1)109.53 (10)
Ba—Ti_m1(1)—Nb_m1(1)0Baxvi—Ba—Nb_m1(1)xviii109.53 (10)
Baxii—Ti_m1(1)—Nb_m1(1)0Baxvi—Ba—Ti_m2112.0 (3)
Na_aiv—Ti_m1(2)—Na_axiv175.3 (5)Baxvi—Ba—Mg_m2112.0 (3)
Na_aiv—Ti_m1(2)—Fe_m292.3 (3)Baxiii—Ba—W2108.4 (3)
Na_aiv—Ti_m1(2)—O156.2 (5)Baxiii—Ba—W2xvii108.4 (3)
Na_aiv—Ti_m1(2)—O1xiii128.2 (6)Baxiii—Ba—W_c0
Na_aiv—Ti_m1(2)—O6iv44.0 (7)Baxiii—Ba—Nb_m1(1)102.11 (12)
Na_aiv—Ti_m1(2)—O6xiv131.8 (7)Baxiii—Ba—Nb_m1(1)xviii102.11 (12)
Na_aiv—Ti_m1(2)—Oh120.7 (9)Baxiii—Ba—Ti_m20.0 (5)
Na_aiv—Ti_m1(2)—Ohxiii59.6 (9)Baxiii—Ba—Mg_m20.0 (5)
Na_aiv—Ti_m1(2)—Ba112.6 (5)W2—Ba—W2xvii65.3 (5)
Na_aiv—Ti_m1(2)—Baxiii71.3 (5)W2—Ba—W_c0
Na_aiv—Ti_m1(2)—Ti_m292.3 (3)W2—Ba—Nb_m1(1)79.2 (3)
Na_aiv—Ti_m1(2)—Mg_m292.3 (3)W2—Ba—Nb_m1(1)xviii138.7 (3)
Na_axiv—Ti_m1(2)—Fe_m292.3 (3)W2—Ba—Ti_m2108.4 (3)
Na_axiv—Ti_m1(2)—O1128.2 (6)W2—Ba—Mg_m2108.4 (3)
Na_axiv—Ti_m1(2)—O1xiii56.2 (5)W2xvii—Ba—W_c0
Na_axiv—Ti_m1(2)—O6iv131.8 (7)W2xvii—Ba—Nb_m1(1)138.7 (3)
Na_axiv—Ti_m1(2)—O6xiv44.0 (7)W2xvii—Ba—Nb_m1(1)xviii79.2 (3)
Na_axiv—Ti_m1(2)—Oh59.6 (9)W2xvii—Ba—Ti_m2108.4 (3)
Na_axiv—Ti_m1(2)—Ohxiii120.7 (9)W2xvii—Ba—Mg_m2108.4 (3)
Na_axiv—Ti_m1(2)—Ba71.3 (5)W_c—Ba—Nb_m1(1)0
Na_axiv—Ti_m1(2)—Baxiii112.6 (5)W_c—Ba—Nb_m1(1)xviii0
Na_axiv—Ti_m1(2)—Ti_m292.3 (3)W_c—Ba—Ti_m20
Na_axiv—Ti_m1(2)—Mg_m292.3 (3)W_c—Ba—Mg_m20
Fe_m2—Ti_m1(2)—O141.0 (3)Nb_m1(1)—Ba—Nb_m1(1)xviii121.0 (2)
Fe_m2—Ti_m1(2)—O1xiii41.0 (3)Nb_m1(1)—Ba—Ti_m2102.11 (10)
Fe_m2—Ti_m1(2)—O6iv130.2 (4)Nb_m1(1)—Ba—Mg_m2102.11 (10)
Fe_m2—Ti_m1(2)—O6xiv130.2 (4)Nb_m1(1)xviii—Ba—Ti_m2102.11 (10)
Fe_m2—Ti_m1(2)—Oh86.5 (3)Nb_m1(1)xviii—Ba—Mg_m2102.11 (10)
Fe_m2—Ti_m1(2)—Ohxiii86.5 (3)Ti_m2—Ba—Mg_m20.0 (5)
Fe_m2—Ti_m1(2)—Ba36.79 (13)Na_a—W1—Na_ai71.7 (17)
Fe_m2—Ti_m1(2)—Baxiii36.79 (13)Na_a—W1—K_bii130.1 (8)
Fe_m2—Ti_m1(2)—Ti_m20.0 (5)Na_a—W1—K_biii126.0 (8)
Fe_m2—Ti_m1(2)—Mg_m20.0 (5)Na_ai—W1—K_bii126.0 (8)
O1—Ti_m1(2)—O1xiii82.0 (5)Na_ai—W1—K_biii130.1 (8)
O1—Ti_m1(2)—O6iv89.2 (5)K_bii—W1—K_biii81.1 (8)
O1—Ti_m1(2)—O6xiv171.1 (5)Na_av—W2—Na_axiv75.2 (16)
O1—Ti_m1(2)—Oh90.2 (8)Na_av—W2—Ba114.0 (6)
O1—Ti_m1(2)—Ohxiii84.5 (8)Na_av—W2—Baxvi116.6 (6)
O1—Ti_m1(2)—Ba57.5 (5)Na_axiv—W2—Ba116.6 (6)
O1—Ti_m1(2)—Baxiii47.8 (7)Na_axiv—W2—Baxvi114.0 (6)
O1—Ti_m1(2)—Ti_m241.0 (3)Ba—W2—Baxvi114.7 (6)
O1—Ti_m1(2)—Mg_m241.0 (3)Fe_m2—W_c—Ba0
O1xiii—Ti_m1(2)—O6iv171.1 (5)Fe_m2—W_c—Ti_m20.0 (5)
O1xiii—Ti_m1(2)—O6xiv89.2 (5)Fe_m2—W_c—Mg_m20.0 (5)
O1xiii—Ti_m1(2)—Oh84.5 (8)Ba—W_c—Ti_m20
O1xiii—Ti_m1(2)—Ohxiii90.2 (8)Ba—W_c—Mg_m20
O1xiii—Ti_m1(2)—Ba47.8 (7)Ti_m2—W_c—Mg_m20.0 (5)
O1xiii—Ti_m1(2)—Baxiii57.5 (5)Na_axi—Nb_m1(1)—Na_av180.0 (5)
O1xiii—Ti_m1(2)—Ti_m241.0 (3)Na_axi—Nb_m1(1)—Ti_m1(1)0
O1xiii—Ti_m1(2)—Mg_m241.0 (3)Na_axi—Nb_m1(1)—O237.1 (8)
O6iv—Ti_m1(2)—O6xiv99.7 (6)Na_axi—Nb_m1(1)—O2iv142.9 (8)
O6iv—Ti_m1(2)—Oh96.7 (11)Na_axi—Nb_m1(1)—O399.1 (5)
O6iv—Ti_m1(2)—Ohxiii87.8 (10)Na_axi—Nb_m1(1)—O3iv80.9 (5)
O6iv—Ti_m1(2)—Ba127.3 (9)Na_axi—Nb_m1(1)—Oh125.5 (8)
O6iv—Ti_m1(2)—Baxiii115.3 (6)Na_axi—Nb_m1(1)—Ohiv54.5 (8)
O6iv—Ti_m1(2)—Ti_m2130.2 (4)Na_axi—Nb_m1(1)—Ba115.5 (4)
O6iv—Ti_m1(2)—Mg_m2130.2 (4)Na_axi—Nb_m1(1)—Baxii64.5 (4)
O6xiv—Ti_m1(2)—Oh87.8 (10)Na_av—Nb_m1(1)—Ti_m1(1)0
O6xiv—Ti_m1(2)—Ohxiii96.7 (11)Na_av—Nb_m1(1)—O2142.9 (8)
O6xiv—Ti_m1(2)—Ba115.3 (6)Na_av—Nb_m1(1)—O2iv37.1 (8)
O6xiv—Ti_m1(2)—Baxiii127.3 (9)Na_av—Nb_m1(1)—O380.9 (5)
O6xiv—Ti_m1(2)—Ti_m2130.2 (4)Na_av—Nb_m1(1)—O3iv99.1 (5)
O6xiv—Ti_m1(2)—Mg_m2130.2 (4)Na_av—Nb_m1(1)—Oh54.5 (8)
Oh—Ti_m1(2)—Ohxiii173.0 (5)Na_av—Nb_m1(1)—Ohiv125.5 (8)
Oh—Ti_m1(2)—Ba49.9 (3)Na_av—Nb_m1(1)—Ba64.5 (4)
Oh—Ti_m1(2)—Baxiii123.1 (3)Na_av—Nb_m1(1)—Baxii115.5 (4)
Oh—Ti_m1(2)—Ti_m286.5 (3)Ti_m1(1)—Nb_m1(1)—O20
Oh—Ti_m1(2)—Mg_m286.5 (3)Ti_m1(1)—Nb_m1(1)—O2iv0
Ohxiii—Ti_m1(2)—Ba123.1 (3)Ti_m1(1)—Nb_m1(1)—O30
Ohxiii—Ti_m1(2)—Baxiii49.9 (3)Ti_m1(1)—Nb_m1(1)—O3iv0
Ohxiii—Ti_m1(2)—Ti_m286.5 (3)Ti_m1(1)—Nb_m1(1)—Oh0
Ohxiii—Ti_m1(2)—Mg_m286.5 (3)Ti_m1(1)—Nb_m1(1)—Ohiv0
Ba—Ti_m1(2)—Baxiii73.59 (19)Ti_m1(1)—Nb_m1(1)—Ba0
Ba—Ti_m1(2)—Ti_m236.79 (13)Ti_m1(1)—Nb_m1(1)—Baxii0
Ba—Ti_m1(2)—Mg_m236.79 (13)O2—Nb_m1(1)—O2iv180.0 (5)
Baxiii—Ti_m1(2)—Ti_m236.79 (13)O2—Nb_m1(1)—O387.7 (6)
Baxiii—Ti_m1(2)—Mg_m236.79 (13)O2—Nb_m1(1)—O3iv92.3 (6)
Ti_m2—Ti_m1(2)—Mg_m20.0 (5)O2—Nb_m1(1)—Oh91.0 (8)
Ti_m1(2)—Fe_m2—Ti_m1(2)xv180.0 (5)O2—Nb_m1(1)—Ohiv89.0 (8)
Ti_m1(2)—Fe_m2—O143.1 (3)O2—Nb_m1(1)—Ba81.4 (4)
Ti_m1(2)—Fe_m2—O1xiii43.1 (3)O2—Nb_m1(1)—Baxii98.6 (4)
Ti_m1(2)—Fe_m2—O1xv136.9 (3)O2iv—Nb_m1(1)—O392.3 (6)
Ti_m1(2)—Fe_m2—O1x136.9 (3)O2iv—Nb_m1(1)—O3iv87.7 (6)
Ti_m1(2)—Fe_m2—Ba90O2iv—Nb_m1(1)—Oh89.0 (8)
Ti_m1(2)—Fe_m2—Baxiii90O2iv—Nb_m1(1)—Ohiv91.0 (8)
Ti_m1(2)—Fe_m2—W_c90O2iv—Nb_m1(1)—Ba98.6 (4)
Ti_m1(2)—Fe_m2—W_cxiii90O2iv—Nb_m1(1)—Baxii81.4 (4)
Ti_m1(2)—Fe_m2—Ti_m20O3—Nb_m1(1)—O3iv180.0 (5)
Ti_m1(2)—Fe_m2—Mg_m20O3—Nb_m1(1)—Oh91.8 (8)
Ti_m1(2)xv—Fe_m2—O1136.9 (3)O3—Nb_m1(1)—Ohiv88.2 (8)
Ti_m1(2)xv—Fe_m2—O1xiii136.9 (3)O3—Nb_m1(1)—Ba48.6 (8)
Ti_m1(2)xv—Fe_m2—O1xv43.1 (3)O3—Nb_m1(1)—Baxii131.4 (8)
Ti_m1(2)xv—Fe_m2—O1x43.1 (3)O3iv—Nb_m1(1)—Oh88.2 (8)
Ti_m1(2)xv—Fe_m2—Ba90O3iv—Nb_m1(1)—Ohiv91.8 (8)
Ti_m1(2)xv—Fe_m2—Baxiii90O3iv—Nb_m1(1)—Ba131.4 (8)
Ti_m1(2)xv—Fe_m2—W_c90O3iv—Nb_m1(1)—Baxii48.6 (8)
Ti_m1(2)xv—Fe_m2—W_cxiii90Oh—Nb_m1(1)—Ohiv180.0 (5)
Ti_m1(2)xv—Fe_m2—Ti_m20Oh—Nb_m1(1)—Ba44.1 (4)
Ti_m1(2)xv—Fe_m2—Mg_m20Oh—Nb_m1(1)—Baxii135.9 (4)
O1—Fe_m2—O1xiii86.3 (5)Ohiv—Nb_m1(1)—Ba135.9 (4)
O1—Fe_m2—O1xv180.0 (5)Ohiv—Nb_m1(1)—Baxii44.1 (4)
O1—Fe_m2—O1x93.7 (5)Ba—Nb_m1(1)—Baxii180.0 (5)
O1—Fe_m2—Ba96.7 (7)Ti_m1(2)—Ti_m2—Ti_m1(2)xv180.0 (5)
O1—Fe_m2—Baxiii83.3 (7)Ti_m1(2)—Ti_m2—Fe_m20
O1—Fe_m2—W_c96.7 (7)Ti_m1(2)—Ti_m2—O143.1 (3)
O1—Fe_m2—W_cxiii83.3 (7)Ti_m1(2)—Ti_m2—O1xiii43.1 (3)
O1—Fe_m2—Ti_m20Ti_m1(2)—Ti_m2—O1xv136.9 (3)
O1—Fe_m2—Mg_m20Ti_m1(2)—Ti_m2—O1x136.9 (3)
O1xiii—Fe_m2—O1xv93.7 (5)Ti_m1(2)—Ti_m2—Ba90
O1xiii—Fe_m2—O1x180.0 (5)Ti_m1(2)—Ti_m2—Baxiii90
O1xiii—Fe_m2—Ba83.3 (7)Ti_m1(2)—Ti_m2—W_c90
O1xiii—Fe_m2—Baxiii96.7 (7)Ti_m1(2)—Ti_m2—W_cxiii90
O1xiii—Fe_m2—W_c83.3 (7)Ti_m1(2)—Ti_m2—Mg_m20
O1xiii—Fe_m2—W_cxiii96.7 (7)Ti_m1(2)xv—Ti_m2—Fe_m20
O1xiii—Fe_m2—Ti_m20Ti_m1(2)xv—Ti_m2—O1136.9 (3)
O1xiii—Fe_m2—Mg_m20Ti_m1(2)xv—Ti_m2—O1xiii136.9 (3)
O1xv—Fe_m2—O1x86.3 (5)Ti_m1(2)xv—Ti_m2—O1xv43.1 (3)
O1xv—Fe_m2—Ba83.3 (7)Ti_m1(2)xv—Ti_m2—O1x43.1 (3)
O1xv—Fe_m2—Baxiii96.7 (7)Ti_m1(2)xv—Ti_m2—Ba90
O1xv—Fe_m2—W_c83.3 (7)Ti_m1(2)xv—Ti_m2—Baxiii90
O1xv—Fe_m2—W_cxiii96.7 (7)Ti_m1(2)xv—Ti_m2—W_c90
O1xv—Fe_m2—Ti_m20Ti_m1(2)xv—Ti_m2—W_cxiii90
O1xv—Fe_m2—Mg_m20Ti_m1(2)xv—Ti_m2—Mg_m20
O1x—Fe_m2—Ba96.7 (7)Fe_m2—Ti_m2—O10
O1x—Fe_m2—Baxiii83.3 (7)Fe_m2—Ti_m2—O1xiii0
O1x—Fe_m2—W_c96.7 (7)Fe_m2—Ti_m2—O1xv0
O1x—Fe_m2—W_cxiii83.3 (7)Fe_m2—Ti_m2—O1x0
O1x—Fe_m2—Ti_m20Fe_m2—Ti_m2—Ba0
O1x—Fe_m2—Mg_m20Fe_m2—Ti_m2—Baxiii0
Ba—Fe_m2—Baxiii180.0 (5)Fe_m2—Ti_m2—W_c0
Ba—Fe_m2—W_c0.0 (5)Fe_m2—Ti_m2—W_cxiii0
Ba—Fe_m2—W_cxiii180.0 (5)Fe_m2—Ti_m2—Mg_m20
Ba—Fe_m2—Ti_m20O1—Ti_m2—O1xiii86.3 (5)
Ba—Fe_m2—Mg_m20O1—Ti_m2—O1xv180.0 (5)
Baxiii—Fe_m2—W_c180.0 (5)O1—Ti_m2—O1x93.7 (5)
Baxiii—Fe_m2—W_cxiii0.0 (5)O1—Ti_m2—Ba96.7 (7)
Baxiii—Fe_m2—Ti_m20O1—Ti_m2—Baxiii83.3 (7)
Baxiii—Fe_m2—Mg_m20O1—Ti_m2—W_c96.7 (7)
W_c—Fe_m2—W_cxiii180.0 (5)O1—Ti_m2—W_cxiii83.3 (7)
W_c—Fe_m2—Ti_m20O1—Ti_m2—Mg_m20
W_c—Fe_m2—Mg_m20O1xiii—Ti_m2—O1xv93.7 (5)
W_cxiii—Fe_m2—Ti_m20O1xiii—Ti_m2—O1x180.0 (5)
W_cxiii—Fe_m2—Mg_m20O1xiii—Ti_m2—Ba83.3 (7)
Ti_m2—Fe_m2—Mg_m20O1xiii—Ti_m2—Baxiii96.7 (7)
K_b—Si1—K_biii81.8 (4)O1xiii—Ti_m2—W_c83.3 (7)
K_b—Si1—O348.6 (8)O1xiii—Ti_m2—W_cxiii96.7 (7)
K_b—Si1—O462.5 (7)O1xiii—Ti_m2—Mg_m20
K_b—Si1—O6105.7 (6)O1xv—Ti_m2—O1x86.3 (5)
K_b—Si1—O7141.7 (9)O1xv—Ti_m2—Ba83.3 (7)
K_biii—Si1—O3130.1 (8)O1xv—Ti_m2—Baxiii96.7 (7)
K_biii—Si1—O439.8 (15)O1xv—Ti_m2—W_c83.3 (7)
K_biii—Si1—O668.2 (10)O1xv—Ti_m2—W_cxiii96.7 (7)
K_biii—Si1—O7115.4 (9)O1xv—Ti_m2—Mg_m20
O3—Si1—O4105.3 (12)O1x—Ti_m2—Ba96.7 (7)
O3—Si1—O6114.9 (10)O1x—Ti_m2—Baxiii83.3 (7)
O3—Si1—O7108.7 (14)O1x—Ti_m2—W_c96.7 (7)
O4—Si1—O6107.1 (18)O1x—Ti_m2—W_cxiii83.3 (7)
O4—Si1—O7107.9 (9)O1x—Ti_m2—Mg_m20
O6—Si1—O7112.4 (9)Ba—Ti_m2—Baxiii180.0 (5)
Na_aiv—Si2—K_b163.0 (6)Ba—Ti_m2—W_c0.0 (5)
Na_aiv—Si2—O163.0 (8)Ba—Ti_m2—W_cxiii180.0 (5)
Na_aiv—Si2—O296.3 (10)Ba—Ti_m2—Mg_m20
Na_aiv—Si2—O5152.2 (12)Baxiii—Ti_m2—W_c180.0 (5)
Na_aiv—Si2—O7xi50.8 (8)Baxiii—Ti_m2—W_cxiii0.0 (5)
Na_aiv—Si2—Ba122.5 (6)Baxiii—Ti_m2—Mg_m20
K_b—Si2—O1133.9 (6)W_c—Ti_m2—W_cxiii180.0 (5)
K_b—Si2—O275.2 (9)W_c—Ti_m2—Mg_m20
K_b—Si2—O535.2 (12)W_cxiii—Ti_m2—Mg_m20
K_b—Si2—O7xi118.7 (9)Ti_m1(2)—Mg_m2—Ti_m1(2)xv180.0 (5)
K_b—Si2—Ba73.7 (3)Ti_m1(2)—Mg_m2—Fe_m20
O1—Si2—O2115.3 (9)Ti_m1(2)—Mg_m2—O143.1 (3)
O1—Si2—O5111.0 (11)Ti_m1(2)—Mg_m2—O1xiii43.1 (3)
O1—Si2—O7xi98.8 (12)Ti_m1(2)—Mg_m2—O1xv136.9 (3)
O1—Si2—Ba60.5 (6)Ti_m1(2)—Mg_m2—O1x136.9 (3)
O2—Si2—O5109.9 (16)Ti_m1(2)—Mg_m2—Ba90
O2—Si2—O7xi113.4 (7)Ti_m1(2)—Mg_m2—Baxiii90
O2—Si2—Ba98.1 (5)Ti_m1(2)—Mg_m2—W_c90
O5—Si2—O7xi107.8 (8)Ti_m1(2)—Mg_m2—W_cxiii90
O5—Si2—Ba64.0 (6)Ti_m1(2)—Mg_m2—Ti_m20
O7xi—Si2—Ba147.9 (8)Ti_m1(2)xv—Mg_m2—Fe_m20
Ti_m1(2)—O1—Fe_m295.9 (5)Ti_m1(2)xv—Mg_m2—O1136.9 (3)
Ti_m1(2)—O1—Si2118.9 (10)Ti_m1(2)xv—Mg_m2—O1xiii136.9 (3)
Ti_m1(2)—O1—Baxiii99.2 (9)Ti_m1(2)xv—Mg_m2—O1xv43.1 (3)
Ti_m1(2)—O1—Ti_m295.9 (5)Ti_m1(2)xv—Mg_m2—O1x43.1 (3)
Ti_m1(2)—O1—Mg_m295.9 (5)Ti_m1(2)xv—Mg_m2—Ba90
Fe_m2—O1—Si2124.0 (11)Ti_m1(2)xv—Mg_m2—Baxiii90
Fe_m2—O1—Baxiii52.4 (5)Ti_m1(2)xv—Mg_m2—W_c90
Fe_m2—O1—Ti_m20.0 (5)Ti_m1(2)xv—Mg_m2—W_cxiii90
Fe_m2—O1—Mg_m20.0 (5)Ti_m1(2)xv—Mg_m2—Ti_m20
Si2—O1—Baxiii141.2 (6)Fe_m2—Mg_m2—O10
Si2—O1—Ti_m2124.0 (11)Fe_m2—Mg_m2—O1xiii0
Si2—O1—Mg_m2124.0 (11)Fe_m2—Mg_m2—O1xv0
Baxiii—O1—Ti_m252.4 (5)Fe_m2—Mg_m2—O1x0
Baxiii—O1—Mg_m252.4 (5)Fe_m2—Mg_m2—Ba0
Ti_m2—O1—Mg_m20.0 (5)Fe_m2—Mg_m2—Baxiii0
Na_axi—O2—Ti_m1(1)110.7 (13)Fe_m2—Mg_m2—W_c0
Na_axi—O2—Si2120.2 (9)Fe_m2—Mg_m2—W_cxiii0
Na_axi—O2—Nb_m1(1)110.7 (13)Fe_m2—Mg_m2—Ti_m20
Ti_m1(1)—O2—Si2127.8 (7)O1—Mg_m2—O1xiii86.3 (5)
Ti_m1(1)—O2—Nb_m1(1)0.0 (5)O1—Mg_m2—O1xv180.0 (5)
Si2—O2—Nb_m1(1)127.8 (7)O1—Mg_m2—O1x93.7 (5)
K_b—O3—Ti_m1(1)124.7 (5)O1—Mg_m2—Ba96.7 (7)
K_b—O3—Si1105.7 (13)O1—Mg_m2—Baxiii83.3 (7)
K_b—O3—Ba101.2 (6)O1—Mg_m2—W_c96.7 (7)
K_b—O3—Nb_m1(1)124.7 (5)O1—Mg_m2—W_cxiii83.3 (7)
Ti_m1(1)—O3—Si1114.7 (7)O1—Mg_m2—Ti_m20
Ti_m1(1)—O3—Ba100.3 (11)O1xiii—Mg_m2—O1xv93.7 (5)
Ti_m1(1)—O3—Nb_m1(1)0.0 (5)O1xiii—Mg_m2—O1x180.0 (5)
Si1—O3—Ba108.0 (7)O1xiii—Mg_m2—Ba83.3 (7)
Si1—O3—Nb_m1(1)114.7 (7)O1xiii—Mg_m2—Baxiii96.7 (7)
Ba—O3—Nb_m1(1)100.3 (11)O1xiii—Mg_m2—W_c83.3 (7)
K_biii—O4—Si1115.4 (15)O1xiii—Mg_m2—W_cxiii96.7 (7)
K_biii—O4—Si1x115.4 (15)O1xiii—Mg_m2—Ti_m20
Si1—O4—Si1x127 (3)O1xv—Mg_m2—O1x86.3 (5)
K_b—O5—Si2121.5 (12)O1xv—Mg_m2—Ba83.3 (7)
K_b—O5—Si2x121.5 (12)O1xv—Mg_m2—Baxiii96.7 (7)
Si2—O5—Si2x117 (2)O1xv—Mg_m2—W_c83.3 (7)
Na_a—O6—Ti_m1(2)iv98.8 (10)O1xv—Mg_m2—W_cxiii96.7 (7)
Na_a—O6—Si1125.9 (11)O1xv—Mg_m2—Ti_m20
Ti_m1(2)iv—O6—Si1130.1 (14)O1x—Mg_m2—Ba96.7 (7)
Na_av—O7—Si1124.0 (8)O1x—Mg_m2—Baxiii83.3 (7)
Na_av—O7—Si2ii94.5 (8)O1x—Mg_m2—W_c96.7 (7)
Si1—O7—Si2ii127.5 (18)O1x—Mg_m2—W_cxiii83.3 (7)
Ti_m1(1)—Oh—Ti_m1(2)126.9 (5)O1x—Mg_m2—Ti_m20
Ti_m1(1)—Oh—Ba106.8 (8)Ba—Mg_m2—Baxiii180.0 (5)
Ti_m1(1)—Oh—Nb_m1(1)0.0 (5)Ba—Mg_m2—W_c0.0 (5)
Ti_m1(2)—Oh—Ba98.6 (7)Ba—Mg_m2—W_cxiii180.0 (5)
Ti_m1(2)—Oh—Nb_m1(1)126.9 (5)Ba—Mg_m2—Ti_m20
Ba—Oh—Nb_m1(1)106.8 (8)Baxiii—Mg_m2—W_c180.0 (5)
Na_axx—Ba—Na_axxi36.7 (9)Baxiii—Mg_m2—W_cxiii0.0 (5)
Na_axx—Ba—Na_av111.9 (4)Baxiii—Mg_m2—Ti_m20
Na_axx—Ba—Na_axiv99.2 (5)W_c—Mg_m2—W_cxiii180.0 (5)
Na_axx—Ba—K_b128.8 (5)W_c—Mg_m2—Ti_m20
Na_axx—Ba—Ti_m1(1)164.9 (3)W_cxiii—Mg_m2—Ti_m20
Symmetry codes: (i) x+1, y, z; (ii) x, y, z1; (iii) x+1, y, z+1; (iv) x+1/2, y+1/2, z+1; (v) x+1/2, y+1/2, z; (vi) x+1/2, y+1/2, z; (vii) x+1/2, y+1/2, z; (viii) x+1, y, z+2; (ix) x+1, y, z+1; (x) x, y, z; (xi) x, y, z+1; (xii) x+1/2, y+1/2, z+1; (xiii) x, y, z+1; (xiv) x1/2, y+1/2, z; (xv) x, y, z+1; (xvi) x, y, z; (xvii) x, y, z; (xviii) x+1/2, y1/2, z+1; (xix) x, y, z+1; (xx) x1/2, y1/2, z; (xxi) x+1/2, y1/2, z.
 

Follow Acta Cryst. B
Sign up for e-alerts
Follow Acta Cryst. on Twitter
Follow us on facebook
Sign up for RSS feeds