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In the title compound, C42H38N4, the two independent mol­ecules are each located on an inversion centre. The central C=N-N=C linkage is therefore planar.

Supporting information

cif

Crystallographic Information File (CIF) https://doi.org/10.1107/S1600536806047155/bh2059sup1.cif
Contains datablocks global, I

hkl

Structure factor file (CIF format) https://doi.org/10.1107/S1600536806047155/bh2059Isup2.hkl
Contains datablock I

CCDC reference: 629430

Key indicators

  • Single-crystal X-ray study
  • T = 294 K
  • Mean [sigma](C-C) = 0.004 Å
  • R factor = 0.050
  • wR factor = 0.124
  • Data-to-parameter ratio = 14.3

checkCIF/PLATON results

No syntax errors found



Alert level C PLAT066_ALERT_1_C Predicted and Reported Transmissions Identical . ? PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for C11
0 ALERT level A = In general: serious problem 0 ALERT level B = Potentially serious problem 2 ALERT level C = Check and explain 0 ALERT level G = General alerts; check 1 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 1 ALERT type 2 Indicator that the structure model may be wrong or deficient 0 ALERT type 3 Indicator that the structure quality may be low 0 ALERT type 4 Improvement, methodology, query or suggestion 0 ALERT type 5 Informative message, check

Computing details top

Data collection: SMART (Bruker, 1997); cell refinement: SAINT (Bruker, 1997); data reduction: SAINT; program(s) used to solve structure: SHELXS97 (Sheldrick, 1997); program(s) used to refine structure: SHELXL97 (Sheldrick, 1997); molecular graphics: SHELXTL (Bruker, 1997); software used to prepare material for publication: SHELXTL.

1,4-Bis[4-(di-p-tolylamino)benzyl]-2,3-diaza-1,3-butadiene top
Crystal data top
C42H38N4Z = 2
Mr = 598.76F(000) = 636
Triclinic, P1Dx = 1.161 Mg m3
Hall symbol: -P 1Melting point: 498 K
a = 11.142 (4) ÅMo Kα radiation, λ = 0.71073 Å
b = 12.562 (5) ÅCell parameters from 1730 reflections
c = 13.848 (5) Åθ = 2.7–22.1°
α = 72.191 (6)°µ = 0.07 mm1
β = 84.891 (7)°T = 294 K
γ = 68.143 (7)°Block, colourless
V = 1712.1 (10) Å30.32 × 0.20 × 0.12 mm
Data collection top
Bruker SMART CCD area-detector
diffractometer
6005 independent reflections
Radiation source: fine-focus sealed tube3032 reflections with I > 2σ(I)
Graphite monochromatorRint = 0.027
φ and ω scansθmax = 25.0°, θmin = 1.6°
Absorption correction: multi-scan
(SADABS; Sheldrick, 1996)
h = 138
Tmin = 0.979, Tmax = 0.992k = 1410
8794 measured reflectionsl = 1615
Refinement top
Refinement on F2Primary atom site location: structure-invariant direct methods
Least-squares matrix: fullSecondary atom site location: difference Fourier map
R[F2 > 2σ(F2)] = 0.050Hydrogen site location: inferred from neighbouring sites
wR(F2) = 0.124H-atom parameters constrained
S = 1.03 w = 1/[σ2(Fo2) + (0.0442P)2]
where P = (Fo2 + 2Fc2)/3
6005 reflections(Δ/σ)max = 0.002
419 parametersΔρmax = 0.15 e Å3
0 restraintsΔρmin = 0.16 e Å3
Fractional atomic coordinates and isotropic or equivalent isotropic displacement parameters (Å2) top
xyzUiso*/Ueq
N10.0943 (2)0.85304 (18)0.27873 (15)0.0624 (6)
N20.0085 (2)0.53336 (19)0.03447 (14)0.0673 (6)
N30.6145 (2)0.81483 (17)0.30673 (14)0.0598 (6)
N40.52487 (18)0.51356 (17)0.03813 (12)0.0521 (5)
C10.1452 (2)0.9463 (2)0.24908 (19)0.0574 (7)
C20.2256 (2)0.9553 (2)0.31406 (19)0.0626 (7)
H20.24750.89960.37800.075*
C30.2739 (3)1.0473 (3)0.2841 (2)0.0737 (8)
H30.32621.05280.32970.088*
C40.2474 (3)1.1305 (3)0.1900 (2)0.0728 (8)
C50.1674 (3)1.1198 (2)0.1264 (2)0.0782 (8)
H50.14751.17460.06200.094*
C60.1152 (3)1.0310 (2)0.1541 (2)0.0742 (8)
H60.06001.02800.10930.089*
C70.3024 (3)1.2292 (3)0.1589 (2)0.1127 (12)
H7A0.26551.28330.19910.169*
H7B0.28191.27230.08850.169*
H7C0.39461.19460.16950.169*
C80.0762 (2)0.8029 (2)0.38441 (18)0.0563 (7)
C90.1367 (3)0.6823 (3)0.4324 (2)0.0807 (9)
H90.19060.63280.39580.097*
C100.1186 (3)0.6340 (3)0.5335 (2)0.0818 (9)
H100.15890.55190.56360.098*
C110.0424 (2)0.7040 (3)0.59100 (19)0.0605 (7)
C120.0170 (3)0.8238 (2)0.5429 (2)0.0694 (8)
H120.06900.87340.58020.083*
C130.0023 (2)0.8739 (2)0.4407 (2)0.0655 (7)
H130.04540.95550.41020.079*
C140.0247 (3)0.6492 (3)0.70253 (18)0.0837 (9)
H14A0.02460.59890.70950.126*
H14B0.02030.71200.73290.126*
H14C0.10780.60200.73580.126*
C150.0870 (2)0.7910 (2)0.21166 (17)0.0539 (6)
C160.0052 (2)0.7374 (2)0.22579 (18)0.0598 (7)
H160.06300.74560.27820.072*
C170.0121 (2)0.6727 (2)0.16383 (17)0.0597 (7)
H170.07500.63860.17430.072*
C180.0744 (2)0.6579 (2)0.08533 (17)0.0527 (6)
C190.1641 (2)0.7129 (2)0.07096 (18)0.0625 (7)
H190.22160.70530.01830.075*
C200.1710 (2)0.7786 (2)0.13227 (18)0.0627 (7)
H200.23220.81480.12040.075*
C210.0724 (3)0.5850 (2)0.02217 (17)0.0603 (7)
H210.13230.57610.02880.072*
C220.6387 (2)0.9230 (2)0.28520 (17)0.0514 (6)
C230.6051 (2)0.9891 (2)0.35349 (19)0.0650 (7)
H230.56020.96580.41100.078*
C240.6372 (3)1.0890 (2)0.3377 (2)0.0708 (8)
H240.61391.13150.38520.085*
C250.7031 (3)1.1276 (2)0.2531 (2)0.0657 (7)
C260.7325 (2)1.0631 (2)0.18431 (19)0.0640 (7)
H260.77491.08810.12580.077*
C270.7015 (2)0.9625 (2)0.19887 (18)0.0562 (6)
H270.72300.92140.15050.067*
C280.7443 (3)1.2336 (3)0.2388 (2)0.1005 (11)
H28A0.83241.21360.21780.151*
H28B0.73721.25250.30170.151*
H28C0.68951.30180.18790.151*
C290.6196 (2)0.7434 (2)0.41003 (17)0.0521 (6)
C300.5241 (2)0.6978 (2)0.44663 (18)0.0599 (7)
H300.45610.71330.40370.072*
C310.5282 (3)0.6291 (2)0.54650 (19)0.0658 (7)
H310.46370.59790.56950.079*
C320.6269 (3)0.6060 (2)0.61299 (18)0.0599 (7)
C330.7219 (3)0.6511 (2)0.57467 (18)0.0676 (8)
H330.79000.63570.61750.081*
C340.7197 (2)0.7181 (2)0.47507 (18)0.0622 (7)
H340.78620.74660.45160.075*
C350.6297 (3)0.5339 (3)0.72280 (18)0.0907 (9)
H35A0.57150.58420.76010.136*
H35B0.71590.50370.75090.136*
H35C0.60350.46790.72730.136*
C360.5931 (2)0.7709 (2)0.22997 (16)0.0486 (6)
C370.5202 (2)0.8458 (2)0.14249 (16)0.0521 (6)
H370.48760.92850.13100.062*
C380.4959 (2)0.7977 (2)0.07229 (16)0.0505 (6)
H380.44790.84910.01350.061*
C390.5414 (2)0.6746 (2)0.08733 (16)0.0448 (6)
C400.6182 (2)0.6009 (2)0.17336 (17)0.0540 (6)
H400.65300.51840.18400.065*
C410.6436 (2)0.6480 (2)0.24279 (17)0.0578 (7)
H410.69560.59680.29970.069*
C420.5036 (2)0.6257 (2)0.01712 (16)0.0491 (6)
H420.46310.67740.04450.059*
Atomic displacement parameters (Å2) top
U11U22U33U12U13U23
N10.0852 (16)0.0568 (14)0.0542 (14)0.0328 (12)0.0041 (11)0.0206 (12)
N20.0872 (17)0.0707 (16)0.0602 (15)0.0396 (14)0.0089 (12)0.0302 (11)
N30.1003 (17)0.0507 (13)0.0420 (12)0.0416 (12)0.0061 (10)0.0127 (11)
N40.0698 (14)0.0549 (14)0.0428 (12)0.0310 (11)0.0020 (10)0.0185 (10)
C10.0595 (18)0.0519 (17)0.0599 (17)0.0168 (13)0.0035 (13)0.0204 (14)
C20.0577 (18)0.0662 (19)0.0619 (17)0.0198 (14)0.0036 (14)0.0202 (14)
C30.0644 (19)0.091 (2)0.084 (2)0.0379 (17)0.0164 (16)0.0419 (19)
C40.071 (2)0.067 (2)0.092 (2)0.0300 (16)0.0252 (17)0.0382 (19)
C50.090 (2)0.0545 (19)0.079 (2)0.0235 (17)0.0061 (17)0.0086 (16)
C60.087 (2)0.0601 (19)0.071 (2)0.0245 (16)0.0165 (15)0.0107 (16)
C70.122 (3)0.104 (3)0.143 (3)0.073 (2)0.053 (2)0.052 (2)
C80.0666 (18)0.0507 (17)0.0542 (16)0.0200 (14)0.0022 (13)0.0210 (14)
C90.099 (2)0.061 (2)0.0598 (19)0.0009 (16)0.0001 (16)0.0237 (16)
C100.103 (2)0.0576 (19)0.063 (2)0.0058 (16)0.0101 (16)0.0142 (16)
C110.0657 (18)0.0653 (19)0.0578 (17)0.0313 (15)0.0001 (14)0.0187 (16)
C120.079 (2)0.066 (2)0.073 (2)0.0302 (16)0.0215 (15)0.0357 (17)
C130.0754 (19)0.0456 (16)0.0737 (19)0.0207 (14)0.0121 (15)0.0197 (15)
C140.094 (2)0.105 (2)0.0655 (19)0.0550 (19)0.0041 (15)0.0215 (17)
C150.0602 (17)0.0526 (16)0.0516 (16)0.0214 (13)0.0020 (13)0.0178 (13)
C160.0656 (19)0.0612 (18)0.0570 (16)0.0259 (14)0.0117 (13)0.0227 (14)
C170.0617 (18)0.0628 (18)0.0603 (17)0.0285 (14)0.0073 (13)0.0202 (14)
C180.0601 (17)0.0530 (16)0.0451 (15)0.0207 (13)0.0018 (12)0.0145 (12)
C190.0667 (18)0.0745 (19)0.0527 (16)0.0320 (15)0.0120 (13)0.0228 (15)
C200.0637 (18)0.0746 (19)0.0643 (17)0.0373 (14)0.0105 (14)0.0280 (15)
C210.073 (2)0.0610 (18)0.0504 (16)0.0273 (15)0.0092 (13)0.0204 (14)
C220.0677 (18)0.0414 (15)0.0498 (15)0.0236 (13)0.0072 (13)0.0129 (13)
C230.084 (2)0.0588 (18)0.0651 (17)0.0333 (15)0.0041 (14)0.0271 (15)
C240.093 (2)0.0499 (17)0.081 (2)0.0274 (15)0.0111 (17)0.0283 (16)
C250.079 (2)0.0457 (17)0.077 (2)0.0287 (14)0.0262 (16)0.0093 (15)
C260.0745 (19)0.0544 (18)0.0639 (17)0.0317 (15)0.0123 (14)0.0042 (15)
C270.0674 (18)0.0499 (16)0.0538 (16)0.0218 (13)0.0055 (13)0.0160 (13)
C280.133 (3)0.070 (2)0.115 (3)0.059 (2)0.031 (2)0.0149 (19)
C290.0722 (18)0.0494 (15)0.0442 (15)0.0306 (13)0.0018 (13)0.0157 (12)
C300.0650 (18)0.0608 (17)0.0600 (17)0.0281 (14)0.0076 (13)0.0169 (14)
C310.072 (2)0.0659 (19)0.0653 (19)0.0356 (15)0.0129 (15)0.0180 (15)
C320.074 (2)0.0565 (17)0.0470 (16)0.0235 (15)0.0035 (14)0.0125 (13)
C330.075 (2)0.083 (2)0.0514 (17)0.0380 (16)0.0082 (14)0.0150 (15)
C340.075 (2)0.0741 (19)0.0492 (16)0.0431 (15)0.0004 (14)0.0141 (14)
C350.115 (3)0.092 (2)0.0563 (18)0.0435 (19)0.0102 (16)0.0051 (17)
C360.0644 (17)0.0454 (16)0.0438 (14)0.0260 (13)0.0034 (12)0.0150 (12)
C370.0678 (17)0.0412 (15)0.0503 (15)0.0214 (12)0.0041 (12)0.0143 (13)
C380.0625 (17)0.0491 (16)0.0414 (14)0.0230 (13)0.0069 (11)0.0098 (12)
C390.0525 (15)0.0483 (15)0.0409 (14)0.0240 (12)0.0008 (11)0.0158 (12)
C400.0668 (17)0.0398 (15)0.0588 (16)0.0200 (12)0.0073 (13)0.0160 (13)
C410.0764 (18)0.0454 (16)0.0526 (15)0.0192 (13)0.0192 (12)0.0137 (13)
C420.0587 (16)0.0514 (16)0.0431 (14)0.0260 (13)0.0025 (11)0.0151 (12)
Geometric parameters (Å, º) top
N1—C151.408 (3)C18—C211.453 (3)
N1—C11.422 (3)C19—C201.377 (3)
N1—C81.434 (3)C19—H190.9300
N2—C211.266 (3)C20—H200.9300
N2—N2i1.410 (3)C21—H210.9300
N3—C361.412 (3)C22—C231.381 (3)
N3—C221.421 (3)C22—C271.383 (3)
N3—C291.431 (3)C23—C241.380 (3)
N4—C421.281 (3)C23—H230.9300
N4—N4ii1.415 (3)C24—C251.382 (3)
C1—C21.380 (3)C24—H240.9300
C1—C61.389 (3)C25—C261.375 (3)
C2—C31.389 (3)C25—C281.517 (3)
C2—H20.9300C26—C271.383 (3)
C3—C41.373 (4)C26—H260.9300
C3—H30.9300C27—H270.9300
C4—C51.375 (3)C28—H28A0.9600
C4—C71.513 (4)C28—H28B0.9600
C5—C61.382 (3)C28—H28C0.9600
C5—H50.9300C29—C341.377 (3)
C6—H60.9300C29—C301.379 (3)
C7—H7A0.9600C30—C311.382 (3)
C7—H7B0.9600C30—H300.9300
C7—H7C0.9600C31—C321.386 (3)
C8—C131.375 (3)C31—H310.9300
C8—C91.376 (3)C32—C331.372 (3)
C9—C101.375 (3)C32—C351.509 (3)
C9—H90.9300C33—C341.376 (3)
C10—C111.371 (3)C33—H330.9300
C10—H100.9300C34—H340.9300
C11—C121.368 (3)C35—H35A0.9600
C11—C141.515 (3)C35—H35B0.9600
C12—C131.384 (3)C35—H35C0.9600
C12—H120.9300C36—C371.386 (3)
C13—H130.9300C36—C411.391 (3)
C14—H14A0.9600C37—C381.382 (3)
C14—H14B0.9600C37—H370.9300
C14—H14C0.9600C38—C391.390 (3)
C15—C201.386 (3)C38—H380.9300
C15—C161.394 (3)C39—C401.388 (3)
C16—C171.374 (3)C39—C421.459 (3)
C16—H160.9300C40—C411.370 (3)
C17—C181.396 (3)C40—H400.9300
C17—H170.9300C41—H410.9300
C18—C191.383 (3)C42—H420.9300
C15—N1—C1121.9 (2)C15—C20—H20119.9
C15—N1—C8117.7 (2)N2—C21—C18122.0 (2)
C1—N1—C8119.0 (2)N2—C21—H21119.0
C21—N2—N2i112.1 (3)C18—C21—H21119.0
C36—N3—C22122.70 (18)C23—C22—C27117.9 (2)
C36—N3—C29118.26 (18)C23—C22—N3120.2 (2)
C22—N3—C29118.92 (18)C27—C22—N3121.8 (2)
C42—N4—N4ii112.4 (2)C24—C23—C22121.0 (2)
C2—C1—C6118.2 (2)C24—C23—H23119.5
C2—C1—N1120.8 (2)C22—C23—H23119.5
C6—C1—N1121.0 (2)C23—C24—C25121.6 (2)
C1—C2—C3120.1 (3)C23—C24—H24119.2
C1—C2—H2119.9C25—C24—H24119.2
C3—C2—H2119.9C26—C25—C24116.7 (2)
C4—C3—C2122.6 (3)C26—C25—C28121.8 (3)
C4—C3—H3118.7C24—C25—C28121.5 (3)
C2—C3—H3118.7C25—C26—C27122.5 (2)
C3—C4—C5116.3 (3)C25—C26—H26118.8
C3—C4—C7121.5 (3)C27—C26—H26118.8
C5—C4—C7122.1 (3)C22—C27—C26120.2 (2)
C4—C5—C6122.8 (3)C22—C27—H27119.9
C4—C5—H5118.6C26—C27—H27119.9
C6—C5—H5118.6C25—C28—H28A109.5
C5—C6—C1119.9 (3)C25—C28—H28B109.5
C5—C6—H6120.0H28A—C28—H28B109.5
C1—C6—H6120.0C25—C28—H28C109.5
C4—C7—H7A109.5H28A—C28—H28C109.5
C4—C7—H7B109.5H28B—C28—H28C109.5
H7A—C7—H7B109.5C34—C29—C30118.4 (2)
C4—C7—H7C109.5C34—C29—N3121.1 (2)
H7A—C7—H7C109.5C30—C29—N3120.4 (2)
H7B—C7—H7C109.5C29—C30—C31120.7 (2)
C13—C8—C9118.1 (2)C29—C30—H30119.7
C13—C8—N1121.0 (2)C31—C30—H30119.7
C9—C8—N1121.0 (2)C30—C31—C32121.1 (2)
C10—C9—C8121.0 (2)C30—C31—H31119.4
C10—C9—H9119.5C32—C31—H31119.4
C8—C9—H9119.5C33—C32—C31117.2 (2)
C11—C10—C9121.5 (3)C33—C32—C35121.6 (3)
C11—C10—H10119.2C31—C32—C35121.2 (3)
C9—C10—H10119.2C32—C33—C34122.2 (2)
C12—C11—C10117.1 (2)C32—C33—H33118.9
C12—C11—C14122.2 (3)C34—C33—H33118.9
C10—C11—C14120.7 (3)C33—C34—C29120.3 (2)
C11—C12—C13122.3 (2)C33—C34—H34119.8
C11—C12—H12118.9C29—C34—H34119.8
C13—C12—H12118.9C32—C35—H35A109.5
C8—C13—C12120.0 (2)C32—C35—H35B109.5
C8—C13—H13120.0H35A—C35—H35B109.5
C12—C13—H13120.0C32—C35—H35C109.5
C11—C14—H14A109.5H35A—C35—H35C109.5
C11—C14—H14B109.5H35B—C35—H35C109.5
H14A—C14—H14B109.5C37—C36—C41118.2 (2)
C11—C14—H14C109.5C37—C36—N3122.3 (2)
H14A—C14—H14C109.5C41—C36—N3119.5 (2)
H14B—C14—H14C109.5C38—C37—C36120.1 (2)
C20—C15—C16118.2 (2)C38—C37—H37119.9
C20—C15—N1122.1 (2)C36—C37—H37119.9
C16—C15—N1119.7 (2)C37—C38—C39121.7 (2)
C17—C16—C15121.2 (2)C37—C38—H38119.2
C17—C16—H16119.4C39—C38—H38119.2
C15—C16—H16119.4C40—C39—C38117.6 (2)
C16—C17—C18120.6 (2)C40—C39—C42121.8 (2)
C16—C17—H17119.7C38—C39—C42120.5 (2)
C18—C17—H17119.7C41—C40—C39121.0 (2)
C19—C18—C17117.7 (2)C41—C40—H40119.5
C19—C18—C21121.0 (2)C39—C40—H40119.5
C17—C18—C21121.3 (2)C40—C41—C36121.4 (2)
C20—C19—C18122.0 (2)C40—C41—H41119.3
C20—C19—H19119.0C36—C41—H41119.3
C18—C19—H19119.0N4—C42—C39121.7 (2)
C19—C20—C15120.2 (2)N4—C42—H42119.1
C19—C20—H20119.9C39—C42—H42119.1
C15—N1—C1—C2138.5 (2)C36—N3—C22—C23152.2 (2)
C8—N1—C1—C227.7 (3)C29—N3—C22—C2331.7 (3)
C15—N1—C1—C641.7 (3)C36—N3—C22—C2731.1 (3)
C8—N1—C1—C6152.1 (2)C29—N3—C22—C27145.1 (2)
C6—C1—C2—C30.2 (4)C27—C22—C23—C242.2 (4)
N1—C1—C2—C3179.6 (2)N3—C22—C23—C24174.7 (2)
C1—C2—C3—C41.5 (4)C22—C23—C24—C250.5 (4)
C2—C3—C4—C51.3 (4)C23—C24—C25—C261.4 (4)
C2—C3—C4—C7179.4 (2)C23—C24—C25—C28176.7 (3)
C3—C4—C5—C60.1 (4)C24—C25—C26—C271.6 (4)
C7—C4—C5—C6179.2 (3)C28—C25—C26—C27176.6 (2)
C4—C5—C6—C11.3 (4)C23—C22—C27—C262.0 (4)
C2—C1—C6—C51.1 (4)N3—C22—C27—C26174.9 (2)
N1—C1—C6—C5179.1 (2)C25—C26—C27—C220.1 (4)
C15—N1—C8—C13134.6 (2)C36—N3—C29—C34130.3 (2)
C1—N1—C8—C1358.7 (3)C22—N3—C29—C3446.0 (3)
C15—N1—C8—C945.3 (3)C36—N3—C29—C3049.5 (3)
C1—N1—C8—C9121.4 (3)C22—N3—C29—C30134.2 (2)
C13—C8—C9—C100.4 (4)C34—C29—C30—C310.5 (4)
N1—C8—C9—C10179.5 (2)N3—C29—C30—C31179.7 (2)
C8—C9—C10—C111.6 (4)C29—C30—C31—C321.2 (4)
C9—C10—C11—C121.3 (4)C30—C31—C32—C331.9 (4)
C9—C10—C11—C14179.4 (3)C30—C31—C32—C35178.3 (2)
C10—C11—C12—C130.1 (4)C31—C32—C33—C341.0 (4)
C14—C11—C12—C13179.1 (2)C35—C32—C33—C34179.2 (2)
C9—C8—C13—C121.0 (4)C32—C33—C34—C290.6 (4)
N1—C8—C13—C12179.1 (2)C30—C29—C34—C331.4 (4)
C11—C12—C13—C81.3 (4)N3—C29—C34—C33178.8 (2)
C1—N1—C15—C2026.9 (4)C22—N3—C36—C3739.8 (3)
C8—N1—C15—C20139.4 (2)C29—N3—C36—C37144.1 (2)
C1—N1—C15—C16154.5 (2)C22—N3—C36—C41142.0 (2)
C8—N1—C15—C1639.1 (3)C29—N3—C36—C4134.1 (3)
C20—C15—C16—C170.8 (4)C41—C36—C37—C382.0 (3)
N1—C15—C16—C17177.8 (2)N3—C36—C37—C38176.3 (2)
C15—C16—C17—C180.7 (4)C36—C37—C38—C390.9 (3)
C16—C17—C18—C191.7 (4)C37—C38—C39—C403.2 (3)
C16—C17—C18—C21177.0 (2)C37—C38—C39—C42173.9 (2)
C17—C18—C19—C201.2 (4)C38—C39—C40—C412.6 (3)
C21—C18—C19—C20177.5 (2)C42—C39—C40—C41174.4 (2)
C18—C19—C20—C150.3 (4)C39—C40—C41—C360.2 (4)
C16—C15—C20—C191.3 (4)C37—C36—C41—C402.6 (3)
N1—C15—C20—C19177.3 (2)N3—C36—C41—C40175.7 (2)
N2i—N2—C21—C18179.3 (2)N4ii—N4—C42—C39177.2 (2)
C19—C18—C21—N2179.6 (2)C40—C39—C42—N49.4 (3)
C17—C18—C21—N20.9 (4)C38—C39—C42—N4167.6 (2)
Symmetry codes: (i) x, y+1, z; (ii) x+1, y+1, z.
 

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