Supporting information
Crystallographic Information File (CIF) https://doi.org/10.1107/S1600536807016169/at2253sup1.cif | |
Structure factor file (CIF format) https://doi.org/10.1107/S1600536807016169/at2253Isup2.hkl |
CCDC reference: 646703
Key indicators
- Single-crystal X-ray study
- T = 100 K
- Mean (C-C) = 0.018 Å
- R factor = 0.047
- wR factor = 0.108
- Data-to-parameter ratio = 18.1
checkCIF/PLATON results
No syntax errors found
Alert level C PLAT029_ALERT_3_C _diffrn_measured_fraction_theta_full Low ....... 0.97 PLAT241_ALERT_2_C Check High Ueq as Compared to Neighbors for C7A PLAT342_ALERT_3_C Low Bond Precision on C-C bonds (x 1000) Ang ... 18 PLAT720_ALERT_4_C Number of Unusual/Non-Standard Label(s) ........ 16
Alert level G ABSTM02_ALERT_3_G The ratio of expected to reported Tmax/Tmin(RR) is > 2.00 Tmin and Tmax reported: 0.035 0.630 Tmin and Tmax expected: 0.000 0.601 RR = 105.357 Please check that your absorption correction is appropriate.
0 ALERT level A = In general: serious problem 0 ALERT level B = Potentially serious problem 4 ALERT level C = Check and explain 1 ALERT level G = General alerts; check 0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 1 ALERT type 2 Indicator that the structure model may be wrong or deficient 3 ALERT type 3 Indicator that the structure quality may be low 1 ALERT type 4 Improvement, methodology, query or suggestion 0 ALERT type 5 Informative message, check
Data collection: APEX2 (Bruker, 2005); cell refinement: SAINT-Plus (Bruker, 2001); data reduction: SAINT-Plus; program(s) used to solve structure: SHELXTL-NT (Sheldrick, 2001); program(s) used to refine structure: SHELXTL-NT; molecular graphics: SHELXTL-NT; software used to prepare material for publication: SHELXTL-NT.
[FeHgCl(C5H4)(C5H5)] | F(000) = 1536 |
Mr = 421.06 | Dx = 2.792 Mg m−3 |
Monoclinic, P21/c | Mo Kα radiation, λ = 0.71073 Å |
Hall symbol: -P 2ybc | Cell parameters from 5313 reflections |
a = 24.618 (11) Å | θ = 2.9–30.6° |
b = 5.997 (3) Å | µ = 16.97 mm−1 |
c = 14.136 (7) Å | T = 100 K |
β = 106.288 (6)° | Plate, orange |
V = 2003.2 (16) Å3 | 0.60 × 0.50 × 0.03 mm |
Z = 8 |
Bruker SMART APEXII CCD area-detector diffractometer | 4251 independent reflections |
Radiation source: fine-focus sealed tube | 3739 reflections with I > 2σ(I) |
Graphite monochromator | Rint = 0.056 |
φ and ω scans | θmax = 27.0°, θmin = 3.4° |
Absorption correction: multi-scan (SADABS; Sheldrick, 2003) | h = −31→31 |
Tmin = 0.035, Tmax = 0.630 | k = −7→7 |
21721 measured reflections | l = −18→18 |
Refinement on F2 | Primary atom site location: structure-invariant direct methods |
Least-squares matrix: full | Secondary atom site location: difference Fourier map |
R[F2 > 2σ(F2)] = 0.047 | Hydrogen site location: inferred from neighbouring sites |
wR(F2) = 0.108 | H-atom parameters constrained |
S = 1.00 | w = 1/[σ2(Fo2) + (0.01P)2 + 4P] where P = (Fo2 + 2Fc2)/3 |
4251 reflections | (Δ/σ)max = 0.001 |
235 parameters | Δρmax = 1.86 e Å−3 |
0 restraints | Δρmin = −1.16 e Å−3 |
Geometry. All e.s.d.'s (except the e.s.d. in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell e.s.d.'s are taken into account individually in the estimation of e.s.d.'s in distances, angles and torsion angles; correlations between e.s.d.'s in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell e.s.d.'s is used for estimating e.s.d.'s involving l.s. planes. |
Refinement. Refinement of F2 against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F2, conventional R-factors R are based on F, with F set to zero for negative F2. The threshold expression of F2 > σ(F2) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F2 are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger. |
x | y | z | Uiso*/Ueq | ||
Hg1A | 0.060744 (17) | 0.48445 (7) | 0.26780 (3) | 0.04197 (13) | |
Hg1B | 0.489733 (18) | 0.69185 (7) | 0.64542 (3) | 0.04753 (14) | |
Cl1A | −0.02395 (12) | 0.4903 (4) | 0.3126 (2) | 0.0474 (6) | |
Cl1B | 0.54847 (13) | 0.7119 (5) | 0.8071 (2) | 0.0556 (7) | |
Fe1A | 0.14441 (6) | 0.4464 (3) | 0.09187 (10) | 0.0430 (3) | |
Fe1B | 0.35517 (7) | 0.7474 (3) | 0.45616 (11) | 0.0462 (4) | |
C1A | 0.1342 (5) | 0.5051 (19) | 0.2287 (8) | 0.047 (2) | |
C2A | 0.1757 (5) | 0.327 (2) | 0.2334 (7) | 0.049 (3) | |
H2AA | 0.1732 | 0.1701 | 0.2558 | 0.059* | |
C3A | 0.2194 (5) | 0.419 (2) | 0.1980 (8) | 0.054 (3) | |
H3AA | 0.2533 | 0.3353 | 0.1909 | 0.065* | |
C4A | 0.2074 (5) | 0.647 (2) | 0.1733 (8) | 0.054 (3) | |
H4AA | 0.2312 | 0.7517 | 0.1467 | 0.064* | |
C5A | 0.1555 (5) | 0.701 (2) | 0.1935 (8) | 0.052 (3) | |
H5AA | 0.1361 | 0.8492 | 0.1820 | 0.062* | |
C6A | 0.0701 (5) | 0.330 (2) | 0.0006 (8) | 0.055 (3) | |
H6AA | 0.0355 | 0.2914 | 0.0209 | 0.066* | |
C7A | 0.1153 (7) | 0.181 (2) | 0.0008 (8) | 0.072 (4) | |
H7AA | 0.1178 | 0.0204 | 0.0207 | 0.086* | |
C8A | 0.1559 (6) | 0.301 (2) | −0.0316 (8) | 0.060 (3) | |
H8AA | 0.1923 | 0.2400 | −0.0389 | 0.072* | |
C9A | 0.1357 (5) | 0.523 (2) | −0.0532 (8) | 0.056 (3) | |
H9AA | 0.1554 | 0.6459 | −0.0780 | 0.068* | |
C10A | 0.0820 (5) | 0.538 (2) | −0.0334 (8) | 0.053 (3) | |
H10A | 0.0576 | 0.6740 | −0.0411 | 0.064* | |
C1B | 0.4392 (4) | 0.6817 (19) | 0.5013 (8) | 0.045 (2) | |
C2B | 0.4100 (4) | 0.4923 (19) | 0.4539 (9) | 0.048 (2) | |
H2BA | 0.4098 | 0.3417 | 0.4842 | 0.058* | |
C3B | 0.3799 (5) | 0.554 (2) | 0.3554 (8) | 0.055 (3) | |
H3BA | 0.3551 | 0.4547 | 0.3042 | 0.066* | |
C4B | 0.3927 (6) | 0.782 (3) | 0.3438 (9) | 0.063 (3) | |
H4BA | 0.3773 | 0.8727 | 0.2827 | 0.076* | |
C5B | 0.4295 (5) | 0.863 (2) | 0.4338 (8) | 0.051 (3) | |
H5BA | 0.4453 | 1.0176 | 0.4470 | 0.061* | |
C6B | 0.3299 (5) | 0.860 (2) | 0.5742 (10) | 0.060 (3) | |
H6BA | 0.3554 | 0.8980 | 0.6408 | 0.072* | |
C7B | 0.3055 (5) | 0.646 (2) | 0.5436 (9) | 0.060 (3) | |
H7BA | 0.3104 | 0.5075 | 0.5846 | 0.072* | |
C8B | 0.2719 (5) | 0.670 (2) | 0.4422 (10) | 0.062 (3) | |
H8BA | 0.2500 | 0.5480 | 0.4002 | 0.075* | |
C9B | 0.2759 (5) | 0.892 (3) | 0.4114 (10) | 0.065 (3) | |
H9BA | 0.2572 | 0.9549 | 0.3446 | 0.077* | |
C10B | 0.3119 (7) | 1.011 (2) | 0.4929 (11) | 0.068 (4) | |
H10C | 0.3227 | 1.1719 | 0.4929 | 0.082* |
U11 | U22 | U33 | U12 | U13 | U23 | |
Hg1A | 0.0449 (2) | 0.0419 (2) | 0.0415 (2) | −0.00141 (16) | 0.01607 (17) | −0.00125 (15) |
Hg1B | 0.0459 (2) | 0.0470 (2) | 0.0500 (2) | 0.00122 (17) | 0.01383 (18) | −0.00050 (17) |
Cl1A | 0.0491 (15) | 0.0458 (14) | 0.0526 (14) | 0.0004 (11) | 0.0227 (12) | 0.0005 (11) |
Cl1B | 0.0557 (17) | 0.0537 (16) | 0.0550 (15) | 0.0062 (13) | 0.0112 (13) | −0.0041 (12) |
Fe1A | 0.0425 (8) | 0.0489 (8) | 0.0387 (7) | −0.0032 (6) | 0.0132 (6) | −0.0027 (6) |
Fe1B | 0.0421 (8) | 0.0516 (9) | 0.0466 (8) | 0.0005 (7) | 0.0150 (7) | −0.0055 (7) |
C1A | 0.043 (6) | 0.059 (7) | 0.045 (5) | −0.001 (5) | 0.024 (5) | 0.000 (5) |
C2A | 0.054 (7) | 0.055 (6) | 0.036 (5) | 0.001 (5) | 0.010 (5) | −0.007 (5) |
C3A | 0.034 (5) | 0.077 (8) | 0.049 (6) | 0.002 (5) | 0.008 (5) | −0.005 (6) |
C4A | 0.049 (6) | 0.065 (7) | 0.052 (6) | −0.017 (6) | 0.023 (5) | −0.011 (5) |
C5A | 0.060 (7) | 0.047 (6) | 0.049 (6) | −0.010 (5) | 0.016 (5) | −0.011 (5) |
C6A | 0.039 (6) | 0.080 (9) | 0.042 (5) | −0.016 (6) | 0.004 (5) | −0.003 (6) |
C7A | 0.118 (13) | 0.054 (7) | 0.035 (6) | −0.004 (8) | 0.008 (7) | −0.002 (5) |
C8A | 0.062 (8) | 0.078 (9) | 0.038 (5) | 0.011 (7) | 0.013 (5) | −0.007 (6) |
C9A | 0.051 (7) | 0.072 (8) | 0.048 (6) | −0.003 (6) | 0.017 (5) | 0.009 (6) |
C10A | 0.043 (6) | 0.066 (7) | 0.049 (6) | 0.002 (5) | 0.011 (5) | −0.001 (5) |
C1B | 0.036 (5) | 0.052 (6) | 0.053 (6) | −0.001 (5) | 0.019 (5) | −0.001 (5) |
C2B | 0.032 (5) | 0.053 (6) | 0.061 (6) | 0.004 (4) | 0.015 (5) | −0.004 (5) |
C3B | 0.062 (7) | 0.058 (7) | 0.048 (6) | 0.006 (6) | 0.019 (5) | −0.008 (5) |
C4B | 0.065 (8) | 0.087 (10) | 0.045 (6) | 0.007 (7) | 0.028 (6) | 0.008 (6) |
C5B | 0.046 (6) | 0.053 (6) | 0.056 (6) | −0.001 (5) | 0.018 (5) | 0.002 (5) |
C6B | 0.051 (7) | 0.073 (8) | 0.061 (7) | −0.007 (6) | 0.023 (6) | −0.019 (6) |
C7B | 0.055 (7) | 0.071 (8) | 0.062 (7) | −0.006 (6) | 0.030 (6) | −0.005 (6) |
C8B | 0.050 (7) | 0.067 (8) | 0.074 (8) | −0.010 (6) | 0.025 (6) | −0.022 (7) |
C9B | 0.043 (6) | 0.083 (9) | 0.069 (8) | 0.014 (6) | 0.016 (6) | 0.011 (7) |
C10B | 0.080 (10) | 0.051 (7) | 0.086 (10) | −0.003 (6) | 0.042 (8) | −0.016 (7) |
Hg1A—C1A | 2.038 (10) | C4A—H4AA | 1.0000 |
Hg1A—Cl1A | 2.343 (3) | C5A—H5AA | 1.0000 |
Hg1B—C1B | 2.068 (11) | C6A—C10A | 1.397 (18) |
Hg1B—Cl1B | 2.340 (3) | C6A—C7A | 1.43 (2) |
Fe1A—C3A | 2.033 (11) | C6A—H6AA | 1.0000 |
Fe1A—C8A | 2.041 (11) | C7A—C8A | 1.41 (2) |
Fe1A—C6A | 2.043 (11) | C7A—H7AA | 1.0000 |
Fe1A—C4A | 2.045 (11) | C8A—C9A | 1.426 (18) |
Fe1A—C7A | 2.046 (13) | C8A—H8AA | 1.0000 |
Fe1A—C1A | 2.049 (10) | C9A—C10A | 1.428 (16) |
Fe1A—C9A | 2.053 (11) | C9A—H9AA | 1.0000 |
Fe1A—C2A | 2.060 (11) | C10A—H10A | 1.0000 |
Fe1A—C5A | 2.061 (11) | C1B—C2B | 1.410 (15) |
Fe1A—C10A | 2.067 (12) | C1B—C5B | 1.424 (16) |
Fe1B—C1B | 2.026 (11) | C2B—C3B | 1.430 (17) |
Fe1B—C2B | 2.046 (11) | C2B—H2BA | 1.0000 |
Fe1B—C6B | 2.053 (12) | C3B—C4B | 1.427 (19) |
Fe1B—C10B | 2.054 (13) | C3B—H3BA | 1.0000 |
Fe1B—C8B | 2.057 (13) | C4B—C5B | 1.424 (18) |
Fe1B—C3B | 2.058 (11) | C4B—H4BA | 1.0000 |
Fe1B—C4B | 2.059 (11) | C5B—H5BA | 1.0000 |
Fe1B—C7B | 2.059 (12) | C6B—C10B | 1.43 (2) |
Fe1B—C5B | 2.062 (11) | C6B—C7B | 1.434 (19) |
Fe1B—C9B | 2.068 (13) | C6B—H6BA | 1.0000 |
C1A—C5A | 1.431 (15) | C7B—C8B | 1.447 (19) |
C1A—C2A | 1.467 (16) | C7B—H7BA | 1.0000 |
C2A—C3A | 1.419 (16) | C8B—C9B | 1.42 (2) |
C2A—H2AA | 1.0000 | C8B—H8BA | 1.0000 |
C3A—C4A | 1.427 (18) | C9B—C10B | 1.43 (2) |
C3A—H3AA | 1.0000 | C9B—H9BA | 1.0000 |
C4A—C5A | 1.422 (16) | C10B—H10C | 1.0000 |
C1A—Hg1A—Cl1A | 175.7 (3) | C4A—C3A—Fe1A | 70.0 (7) |
C1B—Hg1B—Cl1B | 178.3 (3) | C2A—C3A—H3AA | 125.3 |
C3A—Fe1A—C8A | 106.3 (5) | C4A—C3A—H3AA | 125.3 |
C3A—Fe1A—C6A | 154.8 (6) | Fe1A—C3A—H3AA | 125.3 |
C8A—Fe1A—C6A | 68.2 (5) | C5A—C4A—C3A | 107.7 (10) |
C3A—Fe1A—C4A | 41.0 (5) | C5A—C4A—Fe1A | 70.3 (6) |
C8A—Fe1A—C4A | 118.0 (5) | C3A—C4A—Fe1A | 69.1 (6) |
C6A—Fe1A—C4A | 163.8 (6) | C5A—C4A—H4AA | 126.1 |
C3A—Fe1A—C7A | 119.0 (6) | C3A—C4A—H4AA | 126.1 |
C8A—Fe1A—C7A | 40.3 (6) | Fe1A—C4A—H4AA | 126.1 |
C6A—Fe1A—C7A | 40.8 (6) | C4A—C5A—C1A | 108.8 (11) |
C4A—Fe1A—C7A | 152.8 (6) | C4A—C5A—Fe1A | 69.1 (6) |
C3A—Fe1A—C1A | 69.2 (4) | C1A—C5A—Fe1A | 69.2 (6) |
C8A—Fe1A—C1A | 164.5 (5) | C4A—C5A—H5AA | 125.6 |
C6A—Fe1A—C1A | 109.3 (5) | C1A—C5A—H5AA | 125.6 |
C4A—Fe1A—C1A | 69.0 (4) | Fe1A—C5A—H5AA | 125.6 |
C7A—Fe1A—C1A | 127.8 (5) | C10A—C6A—C7A | 108.8 (11) |
C3A—Fe1A—C9A | 125.1 (5) | C10A—C6A—Fe1A | 71.0 (7) |
C8A—Fe1A—C9A | 40.8 (5) | C7A—C6A—Fe1A | 69.7 (7) |
C6A—Fe1A—C9A | 67.7 (5) | C10A—C6A—H6AA | 125.6 |
C4A—Fe1A—C9A | 106.3 (5) | C7A—C6A—H6AA | 125.6 |
C7A—Fe1A—C9A | 68.0 (5) | Fe1A—C6A—H6AA | 125.6 |
C1A—Fe1A—C9A | 153.9 (5) | C8A—C7A—C6A | 107.7 (12) |
C3A—Fe1A—C2A | 40.6 (5) | C8A—C7A—Fe1A | 69.7 (8) |
C8A—Fe1A—C2A | 125.3 (5) | C6A—C7A—Fe1A | 69.5 (7) |
C6A—Fe1A—C2A | 121.3 (5) | C8A—C7A—H7AA | 126.1 |
C4A—Fe1A—C2A | 68.9 (5) | C6A—C7A—H7AA | 126.1 |
C7A—Fe1A—C2A | 108.0 (5) | Fe1A—C7A—H7AA | 126.1 |
C1A—Fe1A—C2A | 41.8 (4) | C7A—C8A—C9A | 108.0 (12) |
C9A—Fe1A—C2A | 162.5 (5) | C7A—C8A—Fe1A | 70.0 (7) |
C3A—Fe1A—C5A | 68.4 (5) | C9A—C8A—Fe1A | 70.1 (7) |
C8A—Fe1A—C5A | 152.9 (5) | C7A—C8A—H8AA | 126.0 |
C6A—Fe1A—C5A | 127.8 (5) | C9A—C8A—H8AA | 126.0 |
C4A—Fe1A—C5A | 40.5 (5) | Fe1A—C8A—H8AA | 126.0 |
C7A—Fe1A—C5A | 165.7 (6) | C8A—C9A—C10A | 107.7 (11) |
C1A—Fe1A—C5A | 40.7 (4) | C8A—C9A—Fe1A | 69.2 (6) |
C9A—Fe1A—C5A | 119.1 (5) | C10A—C9A—Fe1A | 70.2 (6) |
C2A—Fe1A—C5A | 68.9 (5) | C8A—C9A—H9AA | 126.1 |
C3A—Fe1A—C10A | 163.1 (5) | C10A—C9A—H9AA | 126.1 |
C8A—Fe1A—C10A | 68.3 (5) | Fe1A—C9A—H9AA | 126.1 |
C6A—Fe1A—C10A | 39.7 (5) | C6A—C10A—C9A | 107.8 (11) |
C4A—Fe1A—C10A | 126.1 (5) | C6A—C10A—Fe1A | 69.2 (7) |
C7A—Fe1A—C10A | 67.9 (5) | C9A—C10A—Fe1A | 69.2 (7) |
C1A—Fe1A—C10A | 120.3 (5) | C6A—C10A—H10A | 126.1 |
C9A—Fe1A—C10A | 40.6 (5) | C9A—C10A—H10A | 126.1 |
C2A—Fe1A—C10A | 155.5 (5) | Fe1A—C10A—H10A | 126.1 |
C5A—Fe1A—C10A | 108.7 (5) | C2B—C1B—C5B | 109.3 (10) |
C1B—Fe1B—C2B | 40.5 (4) | C2B—C1B—Fe1B | 70.5 (6) |
C1B—Fe1B—C6B | 108.9 (5) | C5B—C1B—Fe1B | 71.0 (6) |
C2B—Fe1B—C6B | 127.7 (5) | C2B—C1B—Hg1B | 125.3 (8) |
C1B—Fe1B—C10B | 128.8 (5) | C5B—C1B—Hg1B | 125.4 (8) |
C2B—Fe1B—C10B | 166.2 (6) | Fe1B—C1B—Hg1B | 125.7 (5) |
C6B—Fe1B—C10B | 40.8 (6) | C1B—C2B—C3B | 108.2 (11) |
C1B—Fe1B—C8B | 152.7 (5) | C1B—C2B—Fe1B | 69.0 (6) |
C2B—Fe1B—C8B | 118.3 (5) | C3B—C2B—Fe1B | 70.1 (6) |
C6B—Fe1B—C8B | 68.3 (5) | C1B—C2B—H2BA | 125.9 |
C10B—Fe1B—C8B | 67.9 (6) | C3B—C2B—H2BA | 125.9 |
C1B—Fe1B—C3B | 68.5 (5) | Fe1B—C2B—H2BA | 125.9 |
C2B—Fe1B—C3B | 40.8 (5) | C4B—C3B—C2B | 106.7 (11) |
C6B—Fe1B—C3B | 164.8 (6) | C4B—C3B—Fe1B | 69.8 (7) |
C10B—Fe1B—C3B | 152.2 (6) | C2B—C3B—Fe1B | 69.2 (6) |
C8B—Fe1B—C3B | 106.7 (5) | C4B—C3B—H3BA | 126.6 |
C1B—Fe1B—C4B | 67.9 (5) | C2B—C3B—H3BA | 126.6 |
C2B—Fe1B—C4B | 67.9 (5) | Fe1B—C3B—H3BA | 126.6 |
C6B—Fe1B—C4B | 153.8 (6) | C5B—C4B—C3B | 109.4 (11) |
C10B—Fe1B—C4B | 119.6 (6) | C5B—C4B—Fe1B | 69.9 (6) |
C8B—Fe1B—C4B | 126.9 (6) | C3B—C4B—Fe1B | 69.7 (6) |
C3B—Fe1B—C4B | 40.5 (5) | C5B—C4B—H4BA | 125.3 |
C1B—Fe1B—C7B | 118.6 (5) | C3B—C4B—H4BA | 125.3 |
C2B—Fe1B—C7B | 107.1 (5) | Fe1B—C4B—H4BA | 125.3 |
C6B—Fe1B—C7B | 40.8 (5) | C4B—C5B—C1B | 106.4 (11) |
C10B—Fe1B—C7B | 68.8 (6) | C4B—C5B—Fe1B | 69.7 (7) |
C8B—Fe1B—C7B | 41.2 (5) | C1B—C5B—Fe1B | 68.2 (6) |
C3B—Fe1B—C7B | 126.1 (5) | C4B—C5B—H5BA | 126.8 |
C4B—Fe1B—C7B | 164.4 (6) | C1B—C5B—H5BA | 126.8 |
C1B—Fe1B—C5B | 40.8 (4) | Fe1B—C5B—H5BA | 126.8 |
C2B—Fe1B—C5B | 68.5 (5) | C10B—C6B—C7B | 108.4 (12) |
C6B—Fe1B—C5B | 119.8 (5) | C10B—C6B—Fe1B | 69.6 (7) |
C10B—Fe1B—C5B | 108.9 (5) | C7B—C6B—Fe1B | 69.8 (7) |
C8B—Fe1B—C5B | 164.7 (5) | C10B—C6B—H6BA | 125.8 |
C3B—Fe1B—C5B | 68.7 (5) | C7B—C6B—H6BA | 125.8 |
C4B—Fe1B—C5B | 40.4 (5) | Fe1B—C6B—H6BA | 125.8 |
C7B—Fe1B—C5B | 153.2 (5) | C6B—C7B—C8B | 106.5 (12) |
C1B—Fe1B—C9B | 166.3 (5) | C6B—C7B—Fe1B | 69.4 (7) |
C2B—Fe1B—C9B | 151.6 (6) | C8B—C7B—Fe1B | 69.3 (7) |
C6B—Fe1B—C9B | 68.5 (6) | C6B—C7B—H7BA | 126.8 |
C10B—Fe1B—C9B | 40.6 (6) | C8B—C7B—H7BA | 126.8 |
C8B—Fe1B—C9B | 40.1 (6) | Fe1B—C7B—H7BA | 126.8 |
C3B—Fe1B—C9B | 117.6 (5) | C9B—C8B—C7B | 109.2 (12) |
C4B—Fe1B—C9B | 108.1 (5) | C9B—C8B—Fe1B | 70.3 (7) |
C7B—Fe1B—C9B | 68.9 (6) | C7B—C8B—Fe1B | 69.5 (7) |
C5B—Fe1B—C9B | 127.8 (5) | C9B—C8B—H8BA | 125.4 |
C5A—C1A—C2A | 107.2 (9) | C7B—C8B—H8BA | 125.4 |
C5A—C1A—Hg1A | 125.7 (8) | Fe1B—C8B—H8BA | 125.4 |
C2A—C1A—Hg1A | 127.1 (8) | C8B—C9B—C10B | 107.6 (12) |
C5A—C1A—Fe1A | 70.1 (6) | C8B—C9B—Fe1B | 69.5 (7) |
C2A—C1A—Fe1A | 69.5 (6) | C10B—C9B—Fe1B | 69.2 (8) |
Hg1A—C1A—Fe1A | 126.8 (6) | C8B—C9B—H9BA | 126.2 |
C3A—C2A—C1A | 106.8 (10) | C10B—C9B—H9BA | 126.2 |
C3A—C2A—Fe1A | 68.7 (6) | Fe1B—C9B—H9BA | 126.2 |
C1A—C2A—Fe1A | 68.7 (6) | C9B—C10B—C6B | 108.3 (12) |
C3A—C2A—H2AA | 126.6 | C9B—C10B—Fe1B | 70.2 (7) |
C1A—C2A—H2AA | 126.6 | C6B—C10B—Fe1B | 69.6 (7) |
Fe1A—C2A—H2AA | 126.6 | C9B—C10B—H10C | 125.8 |
C2A—C3A—C4A | 109.4 (10) | C6B—C10B—H10C | 125.8 |
C2A—C3A—Fe1A | 70.7 (6) | Fe1B—C10B—H10C | 125.8 |
C3A—Fe1A—C1A—C5A | 80.7 (8) | C1A—Fe1A—C10A—C9A | 156.5 (7) |
C8A—Fe1A—C1A—C5A | 156.3 (18) | C2A—Fe1A—C10A—C9A | −166.6 (11) |
C6A—Fe1A—C1A—C5A | −126.1 (8) | C5A—Fe1A—C10A—C9A | 113.2 (8) |
C4A—Fe1A—C1A—C5A | 36.7 (7) | C6B—Fe1B—C1B—C2B | 126.5 (7) |
C7A—Fe1A—C1A—C5A | −168.1 (8) | C10B—Fe1B—C1B—C2B | 167.7 (8) |
C9A—Fe1A—C1A—C5A | −47.6 (14) | C8B—Fe1B—C1B—C2B | 47.3 (13) |
C2A—Fe1A—C1A—C5A | 118.1 (10) | C3B—Fe1B—C1B—C2B | −37.6 (7) |
C10A—Fe1A—C1A—C5A | −83.8 (8) | C4B—Fe1B—C1B—C2B | −81.4 (8) |
C3A—Fe1A—C1A—C2A | −37.5 (7) | C7B—Fe1B—C1B—C2B | 82.9 (8) |
C6A—Fe1A—C1A—C2A | 115.7 (7) | C5B—Fe1B—C1B—C2B | −119.5 (9) |
C4A—Fe1A—C1A—C2A | −81.5 (7) | C9B—Fe1B—C1B—C2B | −157 (2) |
C7A—Fe1A—C1A—C2A | 73.7 (9) | C2B—Fe1B—C1B—C5B | 119.5 (9) |
C9A—Fe1A—C1A—C2A | −165.8 (10) | C6B—Fe1B—C1B—C5B | −114.1 (7) |
C5A—Fe1A—C1A—C2A | −118.1 (10) | C10B—Fe1B—C1B—C5B | −72.8 (9) |
C10A—Fe1A—C1A—C2A | 158.0 (7) | C8B—Fe1B—C1B—C5B | 166.7 (10) |
C3A—Fe1A—C1A—Hg1A | −159.1 (9) | C3B—Fe1B—C1B—C5B | 81.9 (7) |
C6A—Fe1A—C1A—Hg1A | −5.9 (9) | C4B—Fe1B—C1B—C5B | 38.1 (7) |
C4A—Fe1A—C1A—Hg1A | 156.9 (9) | C7B—Fe1B—C1B—C5B | −157.6 (7) |
C7A—Fe1A—C1A—Hg1A | −47.9 (10) | C9B—Fe1B—C1B—C5B | −37 (2) |
C9A—Fe1A—C1A—Hg1A | 72.6 (13) | C2B—Fe1B—C1B—Hg1B | −120.1 (10) |
C2A—Fe1A—C1A—Hg1A | −121.6 (10) | C6B—Fe1B—C1B—Hg1B | 6.4 (8) |
C5A—Fe1A—C1A—Hg1A | 120.2 (10) | C10B—Fe1B—C1B—Hg1B | 47.7 (10) |
C10A—Fe1A—C1A—Hg1A | 36.4 (9) | C8B—Fe1B—C1B—Hg1B | −72.8 (13) |
C5A—C1A—C2A—C3A | −1.9 (12) | C3B—Fe1B—C1B—Hg1B | −157.6 (8) |
Hg1A—C1A—C2A—C3A | 179.5 (8) | C4B—Fe1B—C1B—Hg1B | 158.6 (9) |
Fe1A—C1A—C2A—C3A | 58.3 (7) | C7B—Fe1B—C1B—Hg1B | −37.2 (9) |
C5A—C1A—C2A—Fe1A | −60.2 (7) | C5B—Fe1B—C1B—Hg1B | 120.5 (10) |
Hg1A—C1A—C2A—Fe1A | 121.2 (9) | C9B—Fe1B—C1B—Hg1B | 83 (2) |
C8A—Fe1A—C2A—C3A | 72.7 (9) | C5B—C1B—C2B—C3B | −1.4 (12) |
C6A—Fe1A—C2A—C3A | 156.7 (8) | Fe1B—C1B—C2B—C3B | 59.3 (8) |
C4A—Fe1A—C2A—C3A | −37.4 (7) | Hg1B—C1B—C2B—C3B | 179.8 (7) |
C7A—Fe1A—C2A—C3A | 113.8 (8) | C5B—C1B—C2B—Fe1B | −60.7 (8) |
C1A—Fe1A—C2A—C3A | −119.0 (10) | Hg1B—C1B—C2B—Fe1B | 120.5 (7) |
C9A—Fe1A—C2A—C3A | 39.9 (19) | C6B—Fe1B—C2B—C1B | −74.1 (8) |
C5A—Fe1A—C2A—C3A | −81.0 (8) | C10B—Fe1B—C2B—C1B | −44 (2) |
C10A—Fe1A—C2A—C3A | −170.1 (11) | C8B—Fe1B—C2B—C1B | −157.5 (7) |
C3A—Fe1A—C2A—C1A | 119.0 (10) | C3B—Fe1B—C2B—C1B | 119.7 (10) |
C8A—Fe1A—C2A—C1A | −168.3 (7) | C4B—Fe1B—C2B—C1B | 81.4 (7) |
C6A—Fe1A—C2A—C1A | −84.3 (8) | C7B—Fe1B—C2B—C1B | −114.3 (7) |
C4A—Fe1A—C2A—C1A | 81.6 (7) | C5B—Fe1B—C2B—C1B | 37.7 (6) |
C7A—Fe1A—C2A—C1A | −127.1 (8) | C9B—Fe1B—C2B—C1B | 168.7 (10) |
C9A—Fe1A—C2A—C1A | 159.0 (15) | C1B—Fe1B—C2B—C3B | −119.7 (10) |
C5A—Fe1A—C2A—C1A | 38.1 (7) | C6B—Fe1B—C2B—C3B | 166.2 (8) |
C10A—Fe1A—C2A—C1A | −51.1 (14) | C8B—Fe1B—C2B—C3B | 82.8 (8) |
C1A—C2A—C3A—C4A | 1.1 (12) | C4B—Fe1B—C2B—C3B | −38.3 (8) |
Fe1A—C2A—C3A—C4A | 59.5 (8) | C7B—Fe1B—C2B—C3B | 126.0 (8) |
C1A—C2A—C3A—Fe1A | −58.3 (7) | C5B—Fe1B—C2B—C3B | −82.0 (8) |
C8A—Fe1A—C3A—C2A | −125.7 (7) | C9B—Fe1B—C2B—C3B | 49.0 (14) |
C6A—Fe1A—C3A—C2A | −52.5 (14) | C1B—C2B—C3B—C4B | 1.3 (12) |
C4A—Fe1A—C3A—C2A | 120.2 (10) | Fe1B—C2B—C3B—C4B | 59.9 (8) |
C7A—Fe1A—C3A—C2A | −84.0 (8) | C1B—C2B—C3B—Fe1B | −58.6 (7) |
C1A—Fe1A—C3A—C2A | 38.6 (7) | C1B—Fe1B—C3B—C4B | −80.6 (8) |
C9A—Fe1A—C3A—C2A | −166.4 (7) | C2B—Fe1B—C3B—C4B | −117.9 (11) |
C5A—Fe1A—C3A—C2A | 82.4 (7) | C6B—Fe1B—C3B—C4B | −163.8 (18) |
C10A—Fe1A—C3A—C2A | 165.8 (15) | C10B—Fe1B—C3B—C4B | 53.8 (15) |
C8A—Fe1A—C3A—C4A | 114.1 (7) | C8B—Fe1B—C3B—C4B | 127.8 (8) |
C6A—Fe1A—C3A—C4A | −172.7 (10) | C7B—Fe1B—C3B—C4B | 168.9 (8) |
C7A—Fe1A—C3A—C4A | 155.8 (7) | C5B—Fe1B—C3B—C4B | −36.7 (8) |
C1A—Fe1A—C3A—C4A | −81.6 (7) | C9B—Fe1B—C3B—C4B | 85.9 (9) |
C9A—Fe1A—C3A—C4A | 73.5 (8) | C1B—Fe1B—C3B—C2B | 37.3 (7) |
C2A—Fe1A—C3A—C4A | −120.2 (10) | C10B—Fe1B—C3B—C2B | 171.7 (11) |
C5A—Fe1A—C3A—C4A | −37.7 (6) | C8B—Fe1B—C3B—C2B | −114.2 (8) |
C10A—Fe1A—C3A—C4A | 45.6 (19) | C4B—Fe1B—C3B—C2B | 117.9 (11) |
C2A—C3A—C4A—C5A | 0.1 (13) | C7B—Fe1B—C3B—C2B | −73.2 (9) |
Fe1A—C3A—C4A—C5A | 60.0 (8) | C5B—Fe1B—C3B—C2B | 81.2 (7) |
C2A—C3A—C4A—Fe1A | −59.9 (8) | C9B—Fe1B—C3B—C2B | −156.1 (7) |
C3A—Fe1A—C4A—C5A | −118.9 (10) | C2B—C3B—C4B—C5B | −0.8 (13) |
C8A—Fe1A—C4A—C5A | 158.4 (7) | Fe1B—C3B—C4B—C5B | 58.7 (8) |
C6A—Fe1A—C4A—C5A | 50.0 (18) | C2B—C3B—C4B—Fe1B | −59.5 (8) |
C7A—Fe1A—C4A—C5A | −170.5 (10) | C1B—Fe1B—C4B—C5B | −38.4 (7) |
C1A—Fe1A—C4A—C5A | −36.9 (7) | C2B—Fe1B—C4B—C5B | −82.3 (8) |
C9A—Fe1A—C4A—C5A | 116.0 (7) | C6B—Fe1B—C4B—C5B | 49.7 (16) |
C2A—Fe1A—C4A—C5A | −81.8 (7) | C10B—Fe1B—C4B—C5B | 84.8 (9) |
C10A—Fe1A—C4A—C5A | 76.0 (8) | C8B—Fe1B—C4B—C5B | 168.2 (7) |
C8A—Fe1A—C4A—C3A | −82.7 (8) | C3B—Fe1B—C4B—C5B | −120.8 (11) |
C6A—Fe1A—C4A—C3A | 168.9 (14) | C7B—Fe1B—C4B—C5B | −156.2 (19) |
C7A—Fe1A—C4A—C3A | −51.6 (13) | C9B—Fe1B—C4B—C5B | 127.6 (8) |
C1A—Fe1A—C4A—C3A | 82.0 (7) | C1B—Fe1B—C4B—C3B | 82.4 (8) |
C9A—Fe1A—C4A—C3A | −125.1 (7) | C2B—Fe1B—C4B—C3B | 38.5 (7) |
C2A—Fe1A—C4A—C3A | 37.0 (6) | C6B—Fe1B—C4B—C3B | 170.5 (11) |
C5A—Fe1A—C4A—C3A | 118.9 (10) | C10B—Fe1B—C4B—C3B | −154.4 (8) |
C10A—Fe1A—C4A—C3A | −165.1 (6) | C8B—Fe1B—C4B—C3B | −71.0 (10) |
C3A—C4A—C5A—C1A | −1.3 (13) | C7B—Fe1B—C4B—C3B | −35 (2) |
Fe1A—C4A—C5A—C1A | 57.9 (8) | C5B—Fe1B—C4B—C3B | 120.8 (11) |
C3A—C4A—C5A—Fe1A | −59.2 (8) | C9B—Fe1B—C4B—C3B | −111.5 (8) |
C2A—C1A—C5A—C4A | 1.9 (12) | C3B—C4B—C5B—C1B | 0.0 (13) |
Hg1A—C1A—C5A—C4A | −179.4 (8) | Fe1B—C4B—C5B—C1B | 58.6 (7) |
Fe1A—C1A—C5A—C4A | −57.9 (8) | C3B—C4B—C5B—Fe1B | −58.6 (8) |
C2A—C1A—C5A—Fe1A | 59.8 (7) | C2B—C1B—C5B—C4B | 0.9 (12) |
Hg1A—C1A—C5A—Fe1A | −121.6 (9) | Fe1B—C1B—C5B—C4B | −59.5 (8) |
C3A—Fe1A—C5A—C4A | 38.1 (7) | Hg1B—C1B—C5B—C4B | 179.7 (8) |
C8A—Fe1A—C5A—C4A | −45.5 (14) | C2B—C1B—C5B—Fe1B | 60.4 (7) |
C6A—Fe1A—C5A—C4A | −164.3 (7) | Hg1B—C1B—C5B—Fe1B | −120.8 (8) |
C7A—Fe1A—C5A—C4A | 162 (2) | C1B—Fe1B—C5B—C4B | 118.2 (10) |
C1A—Fe1A—C5A—C4A | 120.9 (10) | C2B—Fe1B—C5B—C4B | 80.7 (8) |
C9A—Fe1A—C5A—C4A | −81.0 (8) | C6B—Fe1B—C5B—C4B | −157.2 (8) |
C2A—Fe1A—C5A—C4A | 81.8 (8) | C10B—Fe1B—C5B—C4B | −113.7 (9) |
C10A—Fe1A—C5A—C4A | −124.2 (7) | C3B—Fe1B—C5B—C4B | 36.8 (8) |
C3A—Fe1A—C5A—C1A | −82.7 (7) | C7B—Fe1B—C5B—C4B | 166.1 (11) |
C8A—Fe1A—C5A—C1A | −166.3 (10) | C9B—Fe1B—C5B—C4B | −72.3 (10) |
C6A—Fe1A—C5A—C1A | 74.8 (9) | C2B—Fe1B—C5B—C1B | −37.4 (7) |
C4A—Fe1A—C5A—C1A | −120.9 (10) | C6B—Fe1B—C5B—C1B | 84.7 (8) |
C7A—Fe1A—C5A—C1A | 41 (2) | C10B—Fe1B—C5B—C1B | 128.1 (8) |
C9A—Fe1A—C5A—C1A | 158.1 (7) | C8B—Fe1B—C5B—C1B | −156.6 (17) |
C2A—Fe1A—C5A—C1A | −39.1 (7) | C3B—Fe1B—C5B—C1B | −81.4 (7) |
C10A—Fe1A—C5A—C1A | 115.0 (7) | C4B—Fe1B—C5B—C1B | −118.2 (10) |
C3A—Fe1A—C6A—C10A | −163.7 (10) | C7B—Fe1B—C5B—C1B | 47.9 (14) |
C8A—Fe1A—C6A—C10A | −81.8 (8) | C9B—Fe1B—C5B—C1B | 169.5 (7) |
C4A—Fe1A—C6A—C10A | 33.7 (19) | C1B—Fe1B—C6B—C10B | 128.1 (8) |
C7A—Fe1A—C6A—C10A | −119.3 (10) | C2B—Fe1B—C6B—C10B | 169.4 (8) |
C1A—Fe1A—C6A—C10A | 114.5 (7) | C8B—Fe1B—C6B—C10B | −80.9 (9) |
C9A—Fe1A—C6A—C10A | −37.7 (7) | C3B—Fe1B—C6B—C10B | −154.2 (19) |
C2A—Fe1A—C6A—C10A | 159.2 (7) | C4B—Fe1B—C6B—C10B | 50.0 (16) |
C5A—Fe1A—C6A—C10A | 72.7 (8) | C7B—Fe1B—C6B—C10B | −119.7 (11) |
C3A—Fe1A—C6A—C7A | −44.3 (14) | C5B—Fe1B—C6B—C10B | 84.7 (9) |
C8A—Fe1A—C6A—C7A | 37.5 (7) | C9B—Fe1B—C6B—C10B | −37.6 (8) |
C4A—Fe1A—C6A—C7A | 153.0 (15) | C1B—Fe1B—C6B—C7B | −112.2 (8) |
C1A—Fe1A—C6A—C7A | −126.1 (7) | C2B—Fe1B—C6B—C7B | −70.9 (9) |
C9A—Fe1A—C6A—C7A | 81.6 (8) | C10B—Fe1B—C6B—C7B | 119.7 (11) |
C2A—Fe1A—C6A—C7A | −81.5 (8) | C8B—Fe1B—C6B—C7B | 38.8 (8) |
C5A—Fe1A—C6A—C7A | −168.0 (7) | C4B—Fe1B—C6B—C7B | 169.6 (11) |
C10A—Fe1A—C6A—C7A | 119.3 (10) | C5B—Fe1B—C6B—C7B | −155.6 (8) |
C10A—C6A—C7A—C8A | 1.1 (13) | C9B—Fe1B—C6B—C7B | 82.1 (9) |
Fe1A—C6A—C7A—C8A | −59.4 (9) | C10B—C6B—C7B—C8B | −0.6 (13) |
C10A—C6A—C7A—Fe1A | 60.5 (8) | Fe1B—C6B—C7B—C8B | −59.7 (8) |
C3A—Fe1A—C7A—C8A | −80.9 (9) | C10B—C6B—C7B—Fe1B | 59.1 (9) |
C6A—Fe1A—C7A—C8A | 119.0 (11) | C1B—Fe1B—C7B—C6B | 86.2 (9) |
C4A—Fe1A—C7A—C8A | −44.9 (14) | C2B—Fe1B—C7B—C6B | 128.6 (8) |
C1A—Fe1A—C7A—C8A | −166.0 (7) | C10B—Fe1B—C7B—C6B | −37.5 (8) |
C9A—Fe1A—C7A—C8A | 38.1 (8) | C8B—Fe1B—C7B—C6B | −117.8 (12) |
C2A—Fe1A—C7A—C8A | −123.7 (8) | C3B—Fe1B—C7B—C6B | 169.4 (8) |
C5A—Fe1A—C7A—C8A | 160.9 (19) | C4B—Fe1B—C7B—C6B | −162.8 (19) |
C10A—Fe1A—C7A—C8A | 82.0 (8) | C5B—Fe1B—C7B—C6B | 52.7 (15) |
C3A—Fe1A—C7A—C6A | 160.1 (7) | C9B—Fe1B—C7B—C6B | −81.2 (9) |
C8A—Fe1A—C7A—C6A | −119.0 (11) | C1B—Fe1B—C7B—C8B | −156.1 (7) |
C4A—Fe1A—C7A—C6A | −163.9 (10) | C2B—Fe1B—C7B—C8B | −113.7 (8) |
C1A—Fe1A—C7A—C6A | 74.9 (9) | C6B—Fe1B—C7B—C8B | 117.8 (12) |
C9A—Fe1A—C7A—C6A | −80.9 (8) | C10B—Fe1B—C7B—C8B | 80.3 (9) |
C2A—Fe1A—C7A—C6A | 117.2 (7) | C3B—Fe1B—C7B—C8B | −72.8 (10) |
C5A—Fe1A—C7A—C6A | 42 (2) | C5B—Fe1B—C7B—C8B | 170.4 (10) |
C10A—Fe1A—C7A—C6A | −37.0 (7) | C9B—Fe1B—C7B—C8B | 36.6 (8) |
C6A—C7A—C8A—C9A | −0.7 (13) | C6B—C7B—C8B—C9B | 0.4 (14) |
Fe1A—C7A—C8A—C9A | −60.0 (8) | Fe1B—C7B—C8B—C9B | −59.3 (9) |
C6A—C7A—C8A—Fe1A | 59.3 (8) | C6B—C7B—C8B—Fe1B | 59.7 (8) |
C3A—Fe1A—C8A—C7A | 115.9 (9) | C1B—Fe1B—C8B—C9B | 171.4 (10) |
C6A—Fe1A—C8A—C7A | −38.0 (8) | C2B—Fe1B—C8B—C9B | −155.8 (8) |
C4A—Fe1A—C8A—C7A | 158.6 (8) | C6B—Fe1B—C8B—C9B | 82.0 (9) |
C1A—Fe1A—C8A—C7A | 45 (2) | C10B—Fe1B—C8B—C9B | 37.8 (8) |
C9A—Fe1A—C8A—C7A | −118.8 (11) | C3B—Fe1B—C8B—C9B | −113.3 (8) |
C2A—Fe1A—C8A—C7A | 75.6 (10) | C4B—Fe1B—C8B—C9B | −73.3 (10) |
C5A—Fe1A—C8A—C7A | −169.8 (11) | C7B—Fe1B—C8B—C9B | 120.4 (11) |
C10A—Fe1A—C8A—C7A | −81.0 (9) | C1B—Fe1B—C8B—C7B | 51.0 (13) |
C3A—Fe1A—C8A—C9A | −125.3 (8) | C2B—Fe1B—C8B—C7B | 83.8 (9) |
C6A—Fe1A—C8A—C9A | 80.8 (8) | C6B—Fe1B—C8B—C7B | −38.5 (8) |
C4A—Fe1A—C8A—C9A | −82.6 (8) | C10B—Fe1B—C8B—C7B | −82.6 (9) |
C7A—Fe1A—C8A—C9A | 118.8 (11) | C3B—Fe1B—C8B—C7B | 126.3 (8) |
C1A—Fe1A—C8A—C9A | 164.1 (16) | C4B—Fe1B—C8B—C7B | 166.2 (8) |
C2A—Fe1A—C8A—C9A | −165.6 (7) | C5B—Fe1B—C8B—C7B | −163.6 (17) |
C5A—Fe1A—C8A—C9A | −51.0 (14) | C9B—Fe1B—C8B—C7B | −120.4 (11) |
C10A—Fe1A—C8A—C9A | 37.8 (7) | C7B—C8B—C9B—C10B | −0.1 (14) |
C7A—C8A—C9A—C10A | 0.1 (13) | Fe1B—C8B—C9B—C10B | −58.9 (9) |
Fe1A—C8A—C9A—C10A | −59.9 (8) | C7B—C8B—C9B—Fe1B | 58.8 (9) |
C7A—C8A—C9A—Fe1A | 60.0 (8) | C1B—Fe1B—C9B—C8B | −163.2 (18) |
C3A—Fe1A—C9A—C8A | 73.2 (9) | C2B—Fe1B—C9B—C8B | 49.4 (14) |
C6A—Fe1A—C9A—C8A | −81.9 (8) | C6B—Fe1B—C9B—C8B | −81.4 (8) |
C4A—Fe1A—C9A—C8A | 114.1 (8) | C10B—Fe1B—C9B—C8B | −119.2 (11) |
C7A—Fe1A—C9A—C8A | −37.7 (9) | C3B—Fe1B—C9B—C8B | 83.2 (9) |
C1A—Fe1A—C9A—C8A | −170.4 (10) | C4B—Fe1B—C9B—C8B | 126.2 (8) |
C2A—Fe1A—C9A—C8A | 43 (2) | C7B—Fe1B—C9B—C8B | −37.5 (8) |
C5A—Fe1A—C9A—C8A | 156.1 (8) | C5B—Fe1B—C9B—C8B | 166.8 (7) |
C10A—Fe1A—C9A—C8A | −118.8 (11) | C2B—Fe1B—C9B—C10B | 168.6 (10) |
C3A—Fe1A—C9A—C10A | −168.0 (8) | C6B—Fe1B—C9B—C10B | 37.7 (8) |
C8A—Fe1A—C9A—C10A | 118.8 (11) | C8B—Fe1B—C9B—C10B | 119.2 (11) |
C6A—Fe1A—C9A—C10A | 36.9 (8) | C3B—Fe1B—C9B—C10B | −157.6 (8) |
C4A—Fe1A—C9A—C10A | −127.1 (8) | C4B—Fe1B—C9B—C10B | −114.6 (9) |
C7A—Fe1A—C9A—C10A | 81.2 (9) | C7B—Fe1B—C9B—C10B | 81.7 (9) |
C1A—Fe1A—C9A—C10A | −51.6 (14) | C5B—Fe1B—C9B—C10B | −74.1 (10) |
C2A—Fe1A—C9A—C10A | 161.4 (15) | C8B—C9B—C10B—C6B | −0.2 (14) |
C5A—Fe1A—C9A—C10A | −85.1 (8) | Fe1B—C9B—C10B—C6B | −59.4 (9) |
C7A—C6A—C10A—C9A | −1.1 (13) | C8B—C9B—C10B—Fe1B | 59.1 (9) |
Fe1A—C6A—C10A—C9A | 58.6 (8) | C7B—C6B—C10B—C9B | 0.5 (14) |
C7A—C6A—C10A—Fe1A | −59.7 (8) | Fe1B—C6B—C10B—C9B | 59.8 (9) |
C8A—C9A—C10A—C6A | 0.6 (13) | C7B—C6B—C10B—Fe1B | −59.2 (8) |
Fe1A—C9A—C10A—C6A | −58.6 (8) | C1B—Fe1B—C10B—C9B | 167.8 (7) |
C8A—C9A—C10A—Fe1A | 59.3 (8) | C2B—Fe1B—C10B—C9B | −157 (2) |
C3A—Fe1A—C10A—C6A | 155.6 (16) | C6B—Fe1B—C10B—C9B | −119.3 (11) |
C8A—Fe1A—C10A—C6A | 81.6 (8) | C8B—Fe1B—C10B—C9B | −37.4 (8) |
C4A—Fe1A—C10A—C6A | −168.9 (7) | C3B—Fe1B—C10B—C9B | 46.5 (15) |
C7A—Fe1A—C10A—C6A | 38.0 (8) | C4B—Fe1B—C10B—C9B | 83.5 (9) |
C1A—Fe1A—C10A—C6A | −84.0 (8) | C7B—Fe1B—C10B—C9B | −81.8 (9) |
C9A—Fe1A—C10A—C6A | 119.6 (11) | C5B—Fe1B—C10B—C9B | 126.6 (8) |
C2A—Fe1A—C10A—C6A | −47.0 (15) | C1B—Fe1B—C10B—C6B | −72.8 (9) |
C5A—Fe1A—C10A—C6A | −127.2 (7) | C8B—Fe1B—C10B—C6B | 82.0 (8) |
C3A—Fe1A—C10A—C9A | 36 (2) | C3B—Fe1B—C10B—C6B | 165.8 (10) |
C8A—Fe1A—C10A—C9A | −38.0 (8) | C4B—Fe1B—C10B—C6B | −157.1 (8) |
C6A—Fe1A—C10A—C9A | −119.6 (11) | C7B—Fe1B—C10B—C6B | 37.5 (8) |
C4A—Fe1A—C10A—C9A | 71.5 (9) | C5B—Fe1B—C10B—C6B | −114.1 (8) |
C7A—Fe1A—C10A—C9A | −81.6 (9) | C9B—Fe1B—C10B—C6B | 119.3 (11) |
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