Labuntsovite-Fe, an Fe-dominant member of the labuntsovite subgroup, was first discovered in the Khibiny alkaline massif on Mt Kukisvumchorr [Khomyakov
et al. (2001).
Zap. Vseross. Mineral. Oba, 130, 36–45]. However, no data are published about the crystal structure of this mineral. Labuntsovite-Fe from a peralkaline pegmatite located on Mt Nyorkpakhk, in the Khibiny alkaline complex, Kola Peninsula, Russia, has been investigated by means of electron microprobe analyses, single-crystal X-ray structure refinement, and IR and Raman spectroscopies. Monoclinic unit-cell parameters of labuntsovite-Fe are:
a = 14.2584 (4),
b = 13.7541 (6),
c = 7.7770 (2) Å, β = 116.893 (3)°;
V = 1360.22 (9) Å
3; space group
C2/
m. The structure was refined to final
R1 = 0.0467,
wR2 = 0.0715 for 3202 reflections [
I > 3σ(
I)]. The refined crystal chemical formula is (
Z = 2): Na
2K
2Ba
0.7[(Fe
0.5Ti
0.1Mg
0.05)(H
2O)
1.3]{[Ti
2(Ti
1.9Nb
0.1)(O,OH)
4][Si
4O
12]
2}·4H
2O. The high-pressure
in situ single-crystal X-ray diffraction study of the labuntsovite-Fe has been carried out in a diamond anvil cell. The labuntsovite-type structure is stable up to 23 GPa and phase transitions are not observed. Calculations using the BM3 equation of state resulted in the bulk modulus
K = 72 (2) GPa,
K′
0 = 3.7 (2) and
V0 = 1363 (2) Å
3. Compressing of the heteropolyhedral zeolite-like framework leads to the deformation of main structural units. Octahedral rods show the gradual increase of distortion and the wave-like character of rods becomes more distinct. Rod deformations result in the distortion of the silicon–oxygen ring which is not equal in different directions. Structural channels are characterized by a different ellipticity–pressure relationship: the cross-section of the largest channel I and channel II demonstrates the stability of the geometrical characteristics which practically do not depend on pressure:
channel I ≃ 0.85 (4) (cross-section is rather regular) and
channel II ≃ 0.52 (2) within the whole pressure range. However, channel III is characterized by the increasing of ellipticity with pressure (
= 0.40 → 0.10).
Supporting information
CCDC references: 1541219; 1541220; 1541221; 1541222; 1541223; 1541224; 1541225; 1541226; 1541227
Data collection: CrysAlis PRO, Agilent Technologies, Version 1.171.34.49 (release 20-01-2011 CrysAlis171 .NET) (compiled Jan 20 2011,15:58:25) for (I). Cell refinement: CrysAlis PRO, Agilent Technologies, Version 1.171.34.49 (release 20-01-2011 CrysAlis171 .NET) (compiled Jan 20 2011,15:58:25) for (I). Data reduction: CrysAlis PRO, Agilent Technologies, Version 1.171.34.49 (release 20-01-2011 CrysAlis171 .NET) (compiled Jan 20 2011,15:58:25) for (I).
Crystal data top
Ba0.7Fe0.5K2.1Mg0.05Na2Nb0.1O33Si8Ti4 | Z = 2 |
Mr = 1206.8 | F(000) = 1167 |
Monoclinic, C2/m | Dx = 2.946 Mg m−3 |
Hall symbol: -C 2y | Mo Kα radiation, λ = 0.7107 Å |
a = 14.2584 (4) Å | Cell parameters from 11867 reflections |
b = 13.7541 (6) Å | θ = 4.2–56.1° |
c = 7.7770 (2) Å | µ = 3.27 mm−1 |
β = 116.893 (3)° | T = 293 K |
V = 1360.22 (9) Å3 | Anhedral grain |
Data collection top
Xcalibur, Sapphire3 with high theta cut diffractometer | 3751 independent reflections |
Radiation source: Enhance (Mo) X-ray Source | 3202 reflections with I > 3σ(I) |
Graphite monochromator | Rint = 0.051 |
Detector resolution: 16.0628 pixels mm-1 | θmax = 40.6°, θmin = 4.2° |
ω scans | h = −33→33 |
Absorption correction: multi-scan CrysAlisPro, Agilent Technologies,
Version 1.171.34.49 (release 20-01-2011 CrysAlis171 .NET)
(compiled Jan 20 2011,15:58:25)
Empirical absorption correction using spherical harmonics,
implemented in SCALE3 ABSPACK scaling algorithm. | k = −30→19 |
Tmin = 0.763, Tmax = 1 | l = −18→18 |
37871 measured reflections | |
Refinement top
Refinement on F | 0 restraints |
R[F2 > 2σ(F2)] = 0.047 | 20 constraints |
wR(F2) = 0.072 | Weighting scheme based on measured s.u.'s w = 1/(σ2(F) + 0.003025F2) |
S = 1.03 | (Δ/σ)max = 0.047 |
3751 reflections | Δρmax = 1.38 e Å−3 |
131 parameters | Δρmin = −1.17 e Å−3 |
Fractional atomic coordinates and isotropic or equivalent isotropic displacement parameters (Å2) top | x | y | z | Uiso*/Ueq | Occ. (<1) |
Na_a | 0.41379 (18) | 0.26252 (18) | 0.0121 (4) | 0.0275 (7) | 0.5 |
K_b | 0.41956 (7) | 0 | 0.70218 (11) | 0.0357 (3) | |
Ti_m1(1) | 0.25 | 0.25 | 0.5 | 0.01529 (13) | 0.95 |
Ti_m1(2) | 0 | 0.22729 (3) | 0.5 | 0.01615 (12) | |
Fe_m2 | 0 | 0 | 0.5 | 0.0210 (3) | 0.5 |
Si1 | 0.31974 (3) | 0.11129 (3) | 0.25001 (5) | 0.00679 (12) | |
Si2 | 0.20825 (3) | 0.10994 (3) | 0.80309 (5) | 0.00632 (12) | |
O1 | 0.08208 (9) | 0.11546 (9) | 0.67278 (17) | 0.0112 (3) | |
O2 | 0.27382 (9) | 0.18333 (9) | 0.73861 (15) | 0.0097 (3) | |
O3 | 0.26504 (9) | 0.12547 (9) | 0.38878 (16) | 0.0098 (3) | |
O4 | 0.36441 (13) | 0 | 0.2714 (2) | 0.0105 (4) | |
O5 | 0.24755 (14) | 0 | 0.7865 (3) | 0.0118 (4) | |
O6 | 0.41951 (10) | 0.18040 (10) | 0.30303 (18) | 0.0123 (3) | |
O7 | 0.23225 (9) | 0.12801 (10) | 0.02623 (15) | 0.0117 (3) | |
Oh | 0.10017 (9) | 0.22422 (10) | 0.39672 (16) | 0.0108 (3) | |
Ba | 0.08549 (3) | 0 | 0.34374 (5) | 0.01770 (12) | 0.35 |
W1 | 0.5 | 0.1455 (4) | 0 | 0.130 (4) | |
W2 | 0 | 0.1123 (4) | 0 | 0.093 (4) | |
W_c | 0.08549 (3) | 0 | 0.34374 (5) | 0.01770 (12) | 0.65 |
Nb_m1(1) | 0.25 | 0.25 | 0.5 | 0.01529 (13) | 0.05 |
Ti_m2 | 0 | 0 | 0.5 | 0.0210 (3) | 0.1 |
Mg_m2 | 0 | 0 | 0.5 | 0.0210 (3) | 0.05 |
Atomic displacement parameters (Å2) top | U11 | U22 | U33 | U12 | U13 | U23 |
Na_a | 0.0212 (8) | 0.0241 (10) | 0.0416 (11) | −0.0014 (7) | 0.0181 (8) | −0.0032 (8) |
K_b | 0.0268 (3) | 0.0596 (6) | 0.0199 (3) | 0 | 0.0100 (2) | 0 |
Ti_m1(1) | 0.0331 (2) | 0.00652 (17) | 0.01275 (14) | 0.00572 (13) | 0.01613 (14) | 0.00263 (10) |
Ti_m1(2) | 0.01421 (17) | 0.00453 (17) | 0.01478 (16) | 0 | −0.00656 (12) | 0 |
Fe_m2 | 0.0180 (4) | 0.0141 (4) | 0.0236 (4) | 0 | 0.0029 (3) | 0 |
Si1 | 0.00819 (16) | 0.00526 (18) | 0.00655 (15) | −0.00074 (10) | 0.00302 (12) | −0.00081 (10) |
Si2 | 0.00678 (16) | 0.00518 (18) | 0.00613 (15) | 0.00005 (10) | 0.00217 (12) | 0.00055 (10) |
O1 | 0.0070 (4) | 0.0110 (5) | 0.0115 (4) | 0.0003 (3) | 0.0005 (3) | 0.0032 (3) |
O2 | 0.0110 (4) | 0.0091 (5) | 0.0097 (3) | −0.0020 (3) | 0.0052 (3) | 0.0018 (3) |
O3 | 0.0124 (4) | 0.0089 (4) | 0.0117 (4) | −0.0005 (3) | 0.0087 (3) | −0.0012 (3) |
O4 | 0.0116 (5) | 0.0056 (6) | 0.0155 (6) | 0 | 0.0071 (5) | 0 |
O5 | 0.0141 (6) | 0.0053 (6) | 0.0174 (6) | 0 | 0.0084 (5) | 0 |
O6 | 0.0128 (4) | 0.0110 (5) | 0.0145 (4) | −0.0058 (3) | 0.0075 (3) | −0.0047 (3) |
O7 | 0.0128 (4) | 0.0146 (5) | 0.0063 (3) | 0.0018 (3) | 0.0030 (3) | 0.0006 (3) |
Oh | 0.0073 (4) | 0.0144 (5) | 0.0101 (4) | −0.0001 (3) | 0.0033 (3) | 0.0001 (3) |
Ba | 0.01926 (16) | 0.01662 (18) | 0.01658 (15) | 0 | 0.00755 (12) | 0 |
W1 | 0.234 (10) | 0.027 (2) | 0.0261 (15) | 0 | −0.031 (3) | 0 |
W2 | 0.200 (8) | 0.038 (2) | 0.0250 (14) | 0 | 0.037 (3) | 0 |
W_c | 0.01926 (16) | 0.01662 (18) | 0.01658 (15) | 0 | 0.00755 (12) | 0 |
Nb_m1(1) | 0.0331 (2) | 0.00652 (17) | 0.01275 (14) | 0.00572 (13) | 0.01613 (14) | 0.00263 (10) |
Ti_m2 | 0.0180 (4) | 0.0141 (4) | 0.0236 (4) | 0 | 0.0029 (3) | 0 |
Mg_m2 | 0.0180 (4) | 0.0141 (4) | 0.0236 (4) | 0 | 0.0029 (3) | 0 |
Geometric parameters (Å, º) top
Na_a—Na_ai | 2.549 (4) | Fe_m2—O1 | 2.0674 (12) |
Na_a—K_bii | 4.363 (3) | Fe_m2—O1xii | 2.0674 (12) |
Na_a—K_biii | 4.341 (2) | Fe_m2—O1xiv | 2.0674 (12) |
Na_a—Ti_m1(2)iv | 3.422 (3) | Fe_m2—O1ix | 2.0674 (12) |
Na_a—Si2iv | 3.230 (3) | Fe_m2—Ba | 2.0742 (5) |
Na_a—O2ii | 2.419 (2) | Fe_m2—Baxii | 2.0742 (5) |
Na_a—Bav | 4.196 (2) | Fe_m2—W_c | 2.0742 (5) |
Na_a—Bavi | 4.284 (3) | Fe_m2—W_cxii | 2.0742 (5) |
Na_a—W1 | 2.053 (5) | Fe_m2—Ti_m2 | 0 |
Na_a—W2vii | 2.142 (5) | Fe_m2—Mg_m2 | 0 |
K_b—K_biii | 4.6559 (15) | Si1—O3 | 1.6039 (16) |
K_b—K_bviii | 4.1361 (11) | Si1—O4 | 1.6373 (8) |
K_b—Si1 | 3.4939 (8) | Si1—O6 | 1.6020 (14) |
K_b—Si1ix | 3.4939 (8) | Si1—O7 | 1.6352 (10) |
K_b—O5 | 2.811 (3) | Si2—O1 | 1.6186 (11) |
K_b—Ba | 4.2951 (9) | Si2—O2 | 1.6026 (14) |
K_b—W1x | 2.878 (4) | Si2—O5 | 1.6378 (10) |
K_b—W1xi | 2.878 (4) | Si2—O7x | 1.6289 (13) |
Ti_m1(1)—O2 | 1.9570 (12) | Si2—Ba | 3.5292 (5) |
Ti_m1(1)—O2iv | 1.9570 (12) | O1—Baxii | 2.8229 (14) |
Ti_m1(1)—O3 | 1.9737 (13) | O1—Ti_m2 | 2.0674 (12) |
Ti_m1(1)—O3iv | 1.9737 (13) | O1—Mg_m2 | 2.0674 (12) |
Ti_m1(1)—Oh | 1.9449 (12) | O2—Nb_m1(1) | 1.9570 (12) |
Ti_m1(1)—Ohiv | 1.9449 (12) | O3—Nb_m1(1) | 1.9737 (13) |
Ti_m1(1)—Nb_m1(1) | 0 | Oh—Nb_m1(1) | 1.9449 (12) |
Ti_m1(2)—O1 | 2.0294 (12) | Ba—Baxii | 4.1484 (8) |
Ti_m1(2)—O1xii | 2.0294 (12) | Ba—W2 | 2.841 (3) |
Ti_m1(2)—O6iv | 1.9197 (12) | Ba—W2xv | 2.841 (3) |
Ti_m1(2)—O6xiii | 1.9197 (12) | Ba—W_c | 0 |
Ti_m1(2)—Oh | 1.9299 (15) | Ba—Ti_m2 | 2.0742 (5) |
Ti_m1(2)—Ohxii | 1.9299 (15) | Ba—Mg_m2 | 2.0742 (5) |
Ti_m1(2)—Ba | 3.7517 (5) | W_c—Ti_m2 | 2.0742 (5) |
Ti_m1(2)—Baxii | 3.7517 (5) | W_c—Mg_m2 | 2.0742 (5) |
Ti_m1(2)—Mg_m2 | 3.1262 (5) | Ti_m2—Mg_m2 | 0 |
| | | |
Na_ai—Na_a—K_bii | 72.51 (9) | Na_axvii—Ba—Si2 | 147.16 (4) |
Na_ai—Na_a—K_biii | 73.43 (8) | Na_axvii—Ba—Si2ix | 99.96 (4) |
Na_ai—Na_a—Ti_m1(2)iv | 101.95 (9) | Na_axvii—Ba—O1xii | 99.41 (4) |
Na_ai—Na_a—Si2iv | 139.86 (11) | Na_axvii—Ba—O1xiv | 44.57 (5) |
Na_ai—Na_a—O2ii | 112.01 (14) | Na_axvii—Ba—Baxii | 91.49 (5) |
Na_ai—Na_a—Bav | 74.41 (8) | Na_axvii—Ba—W2 | 87.83 (10) |
Na_ai—Na_a—Bavi | 70.62 (9) | Na_axvii—Ba—W2xv | 27.81 (8) |
Na_ai—Na_a—W1 | 51.63 (12) | Na_axvii—Ba—W_c | 0 |
Na_ai—Na_a—W2vii | 53.49 (12) | Na_axvii—Ba—Ti_m2 | 91.49 (5) |
K_bii—Na_a—K_biii | 56.75 (3) | Na_axvii—Ba—Mg_m2 | 91.49 (5) |
K_bii—Na_a—Ti_m1(2)iv | 124.02 (7) | Na_axviii—Ba—Na_avii | 99.36 (6) |
K_bii—Na_a—Si2iv | 147.55 (8) | Na_axviii—Ba—Na_axiii | 111.57 (5) |
K_bii—Na_a—O2ii | 49.90 (6) | Na_axviii—Ba—K_b | 95.35 (3) |
K_bii—Na_a—Bav | 146.35 (7) | Na_axviii—Ba—Ti_m1(2) | 160.15 (3) |
K_bii—Na_a—Bavi | 105.54 (7) | Na_axviii—Ba—Ti_m1(2)xiv | 70.73 (4) |
K_bii—Na_a—W1 | 33.34 (6) | Na_axviii—Ba—Fe_m2 | 123.52 (4) |
K_bii—Na_a—W2vii | 119.10 (14) | Na_axviii—Ba—Si2 | 146.67 (3) |
K_biii—Na_a—Ti_m1(2)iv | 68.13 (4) | Na_axviii—Ba—Si2ix | 100.50 (3) |
K_biii—Na_a—Si2iv | 120.28 (8) | Na_axviii—Ba—O1xii | 130.45 (4) |
K_biii—Na_a—O2ii | 96.80 (8) | Na_axviii—Ba—O1xiv | 77.94 (5) |
K_biii—Na_a—Bav | 107.50 (5) | Na_axviii—Ba—Baxii | 123.52 (4) |
K_biii—Na_a—Bavi | 143.52 (8) | Na_axviii—Ba—W2 | 86.10 (10) |
K_biii—Na_a—W1 | 34.00 (7) | Na_axviii—Ba—W2xv | 26.23 (7) |
K_biii—Na_a—W2vii | 119.93 (11) | Na_axviii—Ba—W_c | 0 |
Ti_m1(2)iv—Na_a—Si2iv | 58.67 (5) | Na_axviii—Ba—Ti_m2 | 123.52 (4) |
Ti_m1(2)iv—Na_a—O2ii | 137.14 (12) | Na_axviii—Ba—Mg_m2 | 123.52 (4) |
Ti_m1(2)iv—Na_a—Bav | 57.95 (4) | Na_avii—Ba—Na_axiii | 34.97 (6) |
Ti_m1(2)iv—Na_a—Bavi | 125.48 (7) | Na_avii—Ba—K_b | 95.35 (3) |
Ti_m1(2)iv—Na_a—W1 | 99.25 (8) | Na_avii—Ba—Ti_m1(2) | 70.73 (4) |
Ti_m1(2)iv—Na_a—W2vii | 95.18 (8) | Na_avii—Ba—Ti_m1(2)xiv | 160.15 (3) |
Si2iv—Na_a—O2ii | 103.86 (9) | Na_avii—Ba—Fe_m2 | 123.52 (4) |
Si2iv—Na_a—Bav | 65.52 (5) | Na_avii—Ba—Si2 | 100.50 (3) |
Si2iv—Na_a—Bavi | 91.87 (6) | Na_avii—Ba—Si2ix | 146.67 (3) |
Si2iv—Na_a—W1 | 154.21 (14) | Na_avii—Ba—O1xii | 77.94 (5) |
Si2iv—Na_a—W2vii | 91.05 (12) | Na_avii—Ba—O1xiv | 130.45 (4) |
O2ii—Na_a—Bav | 155.63 (9) | Na_avii—Ba—Baxii | 123.52 (4) |
O2ii—Na_a—Bavi | 91.00 (8) | Na_avii—Ba—W2 | 26.23 (7) |
O2ii—Na_a—W1 | 83.09 (11) | Na_avii—Ba—W2xv | 86.10 (10) |
O2ii—Na_a—W2vii | 125.79 (13) | Na_avii—Ba—W_c | 0 |
Bav—Na_a—Bavi | 68.43 (4) | Na_avii—Ba—Ti_m2 | 123.52 (4) |
Bav—Na_a—W1 | 116.33 (10) | Na_avii—Ba—Mg_m2 | 123.52 (4) |
Bav—Na_a—W2vii | 38.22 (6) | Na_axiii—Ba—K_b | 124.50 (3) |
Bavi—Na_a—W1 | 113.06 (14) | Na_axiii—Ba—Ti_m1(2) | 50.63 (4) |
Bavi—Na_a—W2vii | 35.88 (5) | Na_axiii—Ba—Ti_m1(2)xiv | 131.54 (4) |
W1—Na_a—W2vii | 105.11 (18) | Na_axiii—Ba—Fe_m2 | 91.49 (5) |
Na_ax—K_b—Na_aiii | 34.06 (5) | Na_axiii—Ba—Si2 | 99.96 (4) |
Na_ax—K_b—Na_axi | 123.26 (5) | Na_axiii—Ba—Si2ix | 147.16 (4) |
Na_ax—K_b—Na_axvi | 111.72 (6) | Na_axiii—Ba—O1xii | 44.57 (5) |
Na_ax—K_b—K_biii | 120.75 (4) | Na_axiii—Ba—O1xiv | 99.41 (4) |
Na_ax—K_b—K_bviii | 61.36 (3) | Na_axiii—Ba—Baxii | 91.49 (5) |
Na_ax—K_b—Si1 | 95.31 (4) | Na_axiii—Ba—W2 | 27.81 (8) |
Na_ax—K_b—Si1ix | 144.86 (3) | Na_axiii—Ba—W2xv | 87.83 (10) |
Na_ax—K_b—O5 | 68.57 (4) | Na_axiii—Ba—W_c | 0 |
Na_ax—K_b—Ba | 93.79 (3) | Na_axiii—Ba—Ti_m2 | 91.49 (5) |
Na_ax—K_b—W1x | 23.08 (6) | Na_axiii—Ba—Mg_m2 | 91.49 (5) |
Na_ax—K_b—W1xi | 103.36 (8) | K_b—Ba—Ti_m1(2) | 102.544 (9) |
Na_aiii—K_b—Na_axi | 112.56 (4) | K_b—Ba—Ti_m1(2)xiv | 102.544 (9) |
Na_aiii—K_b—Na_axvi | 123.26 (5) | K_b—Ba—Fe_m2 | 113.132 (18) |
Na_aiii—K_b—K_biii | 91.31 (5) | K_b—Ba—Si2 | 56.384 (15) |
Na_aiii—K_b—K_bviii | 61.89 (4) | K_b—Ba—Si2ix | 56.384 (15) |
Na_aiii—K_b—Si1 | 91.73 (4) | K_b—Ba—O1xii | 134.18 (2) |
Na_aiii—K_b—Si1ix | 139.38 (5) | K_b—Ba—O1xiv | 134.18 (2) |
Na_aiii—K_b—O5 | 102.35 (5) | K_b—Ba—Baxii | 113.132 (17) |
Na_aiii—K_b—Ba | 121.45 (3) | K_b—Ba—W2 | 119.25 (4) |
Na_aiii—K_b—W1x | 23.51 (7) | K_b—Ba—W2xv | 119.25 (4) |
Na_aiii—K_b—W1xi | 103.88 (8) | K_b—Ba—W_c | 0 |
Na_axi—K_b—Na_axvi | 34.06 (5) | K_b—Ba—Ti_m2 | 113.132 (18) |
Na_axi—K_b—K_biii | 91.31 (5) | K_b—Ba—Mg_m2 | 113.132 (18) |
Na_axi—K_b—K_bviii | 61.89 (4) | Ti_m1(2)—Ba—Ti_m1(2)xiv | 112.872 (15) |
Na_axi—K_b—Si1 | 139.38 (5) | Ti_m1(2)—Ba—Fe_m2 | 56.436 (8) |
Na_axi—K_b—Si1ix | 91.73 (4) | Ti_m1(2)—Ba—Si2 | 53.142 (8) |
Na_axi—K_b—O5 | 102.35 (5) | Ti_m1(2)—Ba—Si2ix | 96.559 (13) |
Na_axi—K_b—Ba | 121.45 (3) | Ti_m1(2)—Ba—O1xii | 32.19 (2) |
Na_axi—K_b—W1x | 103.88 (8) | Ti_m1(2)—Ba—O1xiv | 95.23 (3) |
Na_axi—K_b—W1xi | 23.51 (7) | Ti_m1(2)—Ba—Baxii | 56.436 (8) |
Na_axvi—K_b—K_biii | 120.75 (4) | Ti_m1(2)—Ba—W2 | 77.75 (8) |
Na_axvi—K_b—K_bviii | 61.36 (3) | Ti_m1(2)—Ba—W2xv | 133.94 (7) |
Na_axvi—K_b—Si1 | 144.86 (3) | Ti_m1(2)—Ba—W_c | 0 |
Na_axvi—K_b—Si1ix | 95.31 (4) | Ti_m1(2)—Ba—Ti_m2 | 56.436 (8) |
Na_axvi—K_b—O5 | 68.57 (4) | Ti_m1(2)—Ba—Mg_m2 | 56.436 (8) |
Na_axvi—K_b—Ba | 93.79 (3) | Ti_m1(2)xiv—Ba—Fe_m2 | 56.436 (8) |
Na_axvi—K_b—W1x | 103.36 (8) | Ti_m1(2)xiv—Ba—Si2 | 96.559 (13) |
Na_axvi—K_b—W1xi | 23.08 (6) | Ti_m1(2)xiv—Ba—Si2ix | 53.142 (8) |
K_biii—K_b—K_bviii | 124.29 (3) | Ti_m1(2)xiv—Ba—O1xii | 95.23 (3) |
K_biii—K_b—Si1 | 54.623 (18) | Ti_m1(2)xiv—Ba—O1xiv | 32.19 (2) |
K_biii—K_b—Si1ix | 54.623 (18) | Ti_m1(2)xiv—Ba—Baxii | 56.436 (8) |
K_biii—K_b—O5 | 154.97 (4) | Ti_m1(2)xiv—Ba—W2 | 133.94 (7) |
K_biii—K_b—Ba | 107.592 (19) | Ti_m1(2)xiv—Ba—W2xv | 77.75 (8) |
K_biii—K_b—W1x | 113.88 (4) | Ti_m1(2)xiv—Ba—W_c | 0 |
K_biii—K_b—W1xi | 113.88 (4) | Ti_m1(2)xiv—Ba—Ti_m2 | 56.436 (8) |
K_bviii—K_b—Si1 | 153.418 (10) | Ti_m1(2)xiv—Ba—Mg_m2 | 56.436 (8) |
K_bviii—K_b—Si1ix | 153.418 (10) | Fe_m2—Ba—Si2 | 63.949 (13) |
K_bviii—K_b—O5 | 80.74 (4) | Fe_m2—Ba—Si2ix | 63.949 (13) |
K_bviii—K_b—Ba | 128.12 (3) | Fe_m2—Ba—O1xii | 46.93 (3) |
K_bviii—K_b—W1x | 44.06 (7) | Fe_m2—Ba—O1xiv | 46.93 (3) |
K_bviii—K_b—W1xi | 44.06 (7) | Fe_m2—Ba—Baxii | 0.0 (5) |
Si1—K_b—Si1ix | 51.969 (15) | Fe_m2—Ba—W2 | 115.82 (3) |
Si1—K_b—O5 | 103.51 (4) | Fe_m2—Ba—W2xv | 115.82 (3) |
Si1—K_b—Ba | 61.282 (14) | Fe_m2—Ba—W_c | 0 |
Si1—K_b—W1x | 109.76 (7) | Fe_m2—Ba—Ti_m2 | 0.0 (5) |
Si1—K_b—W1xi | 161.32 (7) | Fe_m2—Ba—Mg_m2 | 0.0 (5) |
Si1ix—K_b—O5 | 103.51 (4) | Si2—Ba—Si2ix | 50.741 (11) |
Si1ix—K_b—Ba | 61.282 (14) | Si2—Ba—O1xii | 80.04 (2) |
Si1ix—K_b—W1x | 161.32 (7) | Si2—Ba—O1xiv | 108.01 (3) |
Si1ix—K_b—W1xi | 109.76 (7) | Si2—Ba—Baxii | 63.949 (12) |
O5—K_b—Ba | 47.38 (4) | Si2—Ba—W2 | 121.66 (9) |
O5—K_b—W1x | 83.36 (3) | Si2—Ba—W2xv | 172.20 (9) |
O5—K_b—W1xi | 83.36 (3) | Si2—Ba—W_c | 0 |
Ba—K_b—W1x | 116.34 (4) | Si2—Ba—Ti_m2 | 63.949 (13) |
Ba—K_b—W1xi | 116.34 (4) | Si2—Ba—Mg_m2 | 63.949 (13) |
W1x—K_b—W1xi | 88.12 (10) | Si2ix—Ba—O1xii | 108.01 (3) |
O2—Ti_m1(1)—O2iv | 180.0 (5) | Si2ix—Ba—O1xiv | 80.04 (2) |
O2—Ti_m1(1)—O3 | 90.13 (5) | Si2ix—Ba—Baxii | 63.949 (12) |
O2—Ti_m1(1)—O3iv | 89.87 (5) | Si2ix—Ba—W2 | 172.20 (9) |
O2—Ti_m1(1)—Oh | 89.61 (5) | Si2ix—Ba—W2xv | 121.66 (9) |
O2—Ti_m1(1)—Ohiv | 90.39 (5) | Si2ix—Ba—W_c | 0 |
O2—Ti_m1(1)—Nb_m1(1) | 0 | Si2ix—Ba—Ti_m2 | 63.949 (13) |
O2iv—Ti_m1(1)—O3 | 89.87 (5) | Si2ix—Ba—Mg_m2 | 63.949 (13) |
O2iv—Ti_m1(1)—O3iv | 90.13 (5) | O1xii—Ba—O1xiv | 68.46 (4) |
O2iv—Ti_m1(1)—Oh | 90.39 (5) | O1xii—Ba—Baxii | 46.93 (3) |
O2iv—Ti_m1(1)—Ohiv | 89.61 (5) | O1xii—Ba—W2 | 69.96 (5) |
O2iv—Ti_m1(1)—Nb_m1(1) | 0 | O1xii—Ba—W2xv | 105.60 (5) |
O3—Ti_m1(1)—O3iv | 180.0 (5) | O1xii—Ba—W_c | 0 |
O3—Ti_m1(1)—Oh | 88.71 (5) | O1xii—Ba—Ti_m2 | 46.93 (3) |
O3—Ti_m1(1)—Ohiv | 91.29 (5) | O1xii—Ba—Mg_m2 | 46.93 (3) |
O3—Ti_m1(1)—Nb_m1(1) | 0 | O1xiv—Ba—Baxii | 46.93 (3) |
O3iv—Ti_m1(1)—Oh | 91.29 (5) | O1xiv—Ba—W2 | 105.60 (5) |
O3iv—Ti_m1(1)—Ohiv | 88.71 (5) | O1xiv—Ba—W2xv | 69.96 (5) |
O3iv—Ti_m1(1)—Nb_m1(1) | 0 | O1xiv—Ba—W_c | 0 |
Oh—Ti_m1(1)—Ohiv | 180.0 (5) | O1xiv—Ba—Ti_m2 | 46.93 (3) |
Oh—Ti_m1(1)—Nb_m1(1) | 0 | O1xiv—Ba—Mg_m2 | 46.93 (3) |
Ohiv—Ti_m1(1)—Nb_m1(1) | 0 | Baxii—Ba—W2 | 115.82 (3) |
Na_aiv—Ti_m1(2)—Na_axiii | 175.31 (6) | Baxii—Ba—W2xv | 115.82 (3) |
Na_aiv—Ti_m1(2)—O1 | 59.10 (6) | Baxii—Ba—W_c | 0 |
Na_aiv—Ti_m1(2)—O1xii | 125.14 (6) | Baxii—Ba—Ti_m2 | 0.0 (5) |
Na_aiv—Ti_m1(2)—O6iv | 45.80 (6) | Baxii—Ba—Mg_m2 | 0.0 (5) |
Na_aiv—Ti_m1(2)—O6xiii | 130.02 (6) | W2—Ba—W2xv | 65.87 (13) |
Na_aiv—Ti_m1(2)—Oh | 120.01 (5) | W2—Ba—W_c | 0 |
Na_aiv—Ti_m1(2)—Ohxii | 60.11 (5) | W2—Ba—Ti_m2 | 115.82 (3) |
Na_aiv—Ti_m1(2)—Ba | 112.76 (4) | W2—Ba—Mg_m2 | 115.82 (3) |
Na_aiv—Ti_m1(2)—Baxii | 71.42 (4) | W2xv—Ba—W_c | 0 |
Na_aiv—Ti_m1(2)—Mg_m2 | 92.35 (4) | W2xv—Ba—Ti_m2 | 115.82 (3) |
Na_axiii—Ti_m1(2)—O1 | 125.14 (6) | W2xv—Ba—Mg_m2 | 115.82 (3) |
Na_axiii—Ti_m1(2)—O1xii | 59.10 (6) | W_c—Ba—Ti_m2 | 0 |
Na_axiii—Ti_m1(2)—O6iv | 130.02 (6) | W_c—Ba—Mg_m2 | 0 |
Na_axiii—Ti_m1(2)—O6xiii | 45.80 (6) | Ti_m2—Ba—Mg_m2 | 0.0 (5) |
Na_axiii—Ti_m1(2)—Oh | 60.11 (5) | Na_a—W1—Na_ai | 76.7 (2) |
Na_axiii—Ti_m1(2)—Ohxii | 120.01 (5) | Na_a—W1—K_bii | 123.58 (6) |
Na_axiii—Ti_m1(2)—Ba | 71.42 (4) | Na_a—W1—K_biii | 122.49 (9) |
Na_axiii—Ti_m1(2)—Baxii | 112.76 (4) | Na_ai—W1—K_bii | 122.49 (9) |
Na_axiii—Ti_m1(2)—Mg_m2 | 92.35 (4) | Na_ai—W1—K_biii | 123.58 (6) |
O1—Ti_m1(2)—O1xii | 81.43 (5) | K_bii—W1—K_biii | 91.88 (15) |
O1—Ti_m1(2)—O6iv | 90.88 (5) | Na_avii—W2—Na_axiii | 73.0 (2) |
O1—Ti_m1(2)—O6xiii | 170.82 (6) | Na_avii—W2—Ba | 117.89 (7) |
O1—Ti_m1(2)—Oh | 86.86 (6) | Na_avii—W2—Baxix | 113.96 (9) |
O1—Ti_m1(2)—Ohxii | 91.23 (6) | Na_axiii—W2—Ba | 113.96 (9) |
O1—Ti_m1(2)—Ba | 53.73 (4) | Na_axiii—W2—Baxix | 117.89 (7) |
O1—Ti_m1(2)—Baxii | 47.82 (4) | Ba—W2—Baxix | 114.13 (18) |
O1—Ti_m1(2)—Mg_m2 | 40.72 (3) | Fe_m2—W_c—Ba | 0 |
O1xii—Ti_m1(2)—O6iv | 170.82 (6) | Fe_m2—W_c—Ti_m2 | 0.0 (5) |
O1xii—Ti_m1(2)—O6xiii | 90.88 (5) | Fe_m2—W_c—Mg_m2 | 0.0 (5) |
O1xii—Ti_m1(2)—Oh | 91.23 (6) | Ba—W_c—Ti_m2 | 0 |
O1xii—Ti_m1(2)—Ohxii | 86.86 (6) | Ba—W_c—Mg_m2 | 0 |
O1xii—Ti_m1(2)—Ba | 47.82 (4) | Ti_m2—W_c—Mg_m2 | 0.0 (5) |
O1xii—Ti_m1(2)—Baxii | 53.73 (4) | Ti_m1(1)—Nb_m1(1)—O2 | 0 |
O1xii—Ti_m1(2)—Mg_m2 | 40.72 (3) | Ti_m1(1)—Nb_m1(1)—O2iv | 0 |
O6iv—Ti_m1(2)—O6xiii | 97.19 (5) | Ti_m1(1)—Nb_m1(1)—O3 | 0 |
O6iv—Ti_m1(2)—Oh | 93.37 (6) | Ti_m1(1)—Nb_m1(1)—O3iv | 0 |
O6iv—Ti_m1(2)—Ohxii | 88.29 (6) | Ti_m1(1)—Nb_m1(1)—Oh | 0 |
O6iv—Ti_m1(2)—Ba | 130.17 (4) | Ti_m1(1)—Nb_m1(1)—Ohiv | 0 |
O6iv—Ti_m1(2)—Baxii | 117.21 (4) | O2—Nb_m1(1)—O2iv | 180.0 (5) |
O6iv—Ti_m1(2)—Mg_m2 | 131.40 (4) | O2—Nb_m1(1)—O3 | 90.13 (5) |
O6xiii—Ti_m1(2)—Oh | 88.29 (6) | O2—Nb_m1(1)—O3iv | 89.87 (5) |
O6xiii—Ti_m1(2)—Ohxii | 93.37 (6) | O2—Nb_m1(1)—Oh | 89.61 (5) |
O6xiii—Ti_m1(2)—Ba | 117.21 (4) | O2—Nb_m1(1)—Ohiv | 90.39 (5) |
O6xiii—Ti_m1(2)—Baxii | 130.17 (4) | O2iv—Nb_m1(1)—O3 | 89.87 (5) |
O6xiii—Ti_m1(2)—Mg_m2 | 131.40 (4) | O2iv—Nb_m1(1)—O3iv | 90.13 (5) |
Oh—Ti_m1(2)—Ohxii | 177.49 (6) | O2iv—Nb_m1(1)—Oh | 90.39 (5) |
Oh—Ti_m1(2)—Ba | 55.73 (4) | O2iv—Nb_m1(1)—Ohiv | 89.61 (5) |
Oh—Ti_m1(2)—Baxii | 121.77 (4) | O3—Nb_m1(1)—O3iv | 180.0 (5) |
Oh—Ti_m1(2)—Mg_m2 | 88.74 (4) | O3—Nb_m1(1)—Oh | 88.71 (5) |
Ohxii—Ti_m1(2)—Ba | 121.77 (4) | O3—Nb_m1(1)—Ohiv | 91.29 (5) |
Ohxii—Ti_m1(2)—Baxii | 55.73 (4) | O3iv—Nb_m1(1)—Oh | 91.29 (5) |
Ohxii—Ti_m1(2)—Mg_m2 | 88.74 (4) | O3iv—Nb_m1(1)—Ohiv | 88.71 (5) |
Ba—Ti_m1(2)—Baxii | 67.128 (12) | Oh—Nb_m1(1)—Ohiv | 180.0 (5) |
Ba—Ti_m1(2)—Mg_m2 | 33.564 (8) | Fe_m2—Ti_m2—O1 | 0 |
Baxii—Ti_m1(2)—Mg_m2 | 33.564 (8) | Fe_m2—Ti_m2—O1xii | 0 |
O1—Fe_m2—O1xii | 79.63 (4) | Fe_m2—Ti_m2—O1xiv | 0 |
O1—Fe_m2—O1xiv | 180.0 (5) | Fe_m2—Ti_m2—O1ix | 0 |
O1—Fe_m2—O1ix | 100.37 (4) | Fe_m2—Ti_m2—Ba | 0 |
O1—Fe_m2—Ba | 94.06 (4) | Fe_m2—Ti_m2—Baxii | 0 |
O1—Fe_m2—Baxii | 85.94 (4) | Fe_m2—Ti_m2—W_c | 0 |
O1—Fe_m2—W_c | 94.06 (4) | Fe_m2—Ti_m2—W_cxii | 0 |
O1—Fe_m2—W_cxii | 85.94 (4) | Fe_m2—Ti_m2—Mg_m2 | 0 |
O1—Fe_m2—Ti_m2 | 0 | O1—Ti_m2—O1xii | 79.63 (4) |
O1—Fe_m2—Mg_m2 | 0 | O1—Ti_m2—O1xiv | 180.0 (5) |
O1xii—Fe_m2—O1xiv | 100.37 (4) | O1—Ti_m2—O1ix | 100.37 (4) |
O1xii—Fe_m2—O1ix | 180.0 (5) | O1—Ti_m2—Ba | 94.06 (4) |
O1xii—Fe_m2—Ba | 85.94 (4) | O1—Ti_m2—Baxii | 85.94 (4) |
O1xii—Fe_m2—Baxii | 94.06 (4) | O1—Ti_m2—W_c | 94.06 (4) |
O1xii—Fe_m2—W_c | 85.94 (4) | O1—Ti_m2—W_cxii | 85.94 (4) |
O1xii—Fe_m2—W_cxii | 94.06 (4) | O1—Ti_m2—Mg_m2 | 0 |
O1xii—Fe_m2—Ti_m2 | 0 | O1xii—Ti_m2—O1xiv | 100.37 (4) |
O1xii—Fe_m2—Mg_m2 | 0 | O1xii—Ti_m2—O1ix | 180.0 (5) |
O1xiv—Fe_m2—O1ix | 79.63 (4) | O1xii—Ti_m2—Ba | 85.94 (4) |
O1xiv—Fe_m2—Ba | 85.94 (4) | O1xii—Ti_m2—Baxii | 94.06 (4) |
O1xiv—Fe_m2—Baxii | 94.06 (4) | O1xii—Ti_m2—W_c | 85.94 (4) |
O1xiv—Fe_m2—W_c | 85.94 (4) | O1xii—Ti_m2—W_cxii | 94.06 (4) |
O1xiv—Fe_m2—W_cxii | 94.06 (4) | O1xii—Ti_m2—Mg_m2 | 0 |
O1xiv—Fe_m2—Ti_m2 | 0 | O1xiv—Ti_m2—O1ix | 79.63 (4) |
O1xiv—Fe_m2—Mg_m2 | 0 | O1xiv—Ti_m2—Ba | 85.94 (4) |
O1ix—Fe_m2—Ba | 94.06 (4) | O1xiv—Ti_m2—Baxii | 94.06 (4) |
O1ix—Fe_m2—Baxii | 85.94 (4) | O1xiv—Ti_m2—W_c | 85.94 (4) |
O1ix—Fe_m2—W_c | 94.06 (4) | O1xiv—Ti_m2—W_cxii | 94.06 (4) |
O1ix—Fe_m2—W_cxii | 85.94 (4) | O1xiv—Ti_m2—Mg_m2 | 0 |
O1ix—Fe_m2—Ti_m2 | 0 | O1ix—Ti_m2—Ba | 94.06 (4) |
O1ix—Fe_m2—Mg_m2 | 0 | O1ix—Ti_m2—Baxii | 85.94 (4) |
Ba—Fe_m2—Baxii | 180.0 (5) | O1ix—Ti_m2—W_c | 94.06 (4) |
Ba—Fe_m2—W_c | 0.0 (5) | O1ix—Ti_m2—W_cxii | 85.94 (4) |
Ba—Fe_m2—W_cxii | 180.0 (5) | O1ix—Ti_m2—Mg_m2 | 0 |
Ba—Fe_m2—Ti_m2 | 0 | Ba—Ti_m2—Baxii | 180.0 (5) |
Ba—Fe_m2—Mg_m2 | 0 | Ba—Ti_m2—W_c | 0.0 (5) |
Baxii—Fe_m2—W_c | 180.0 (5) | Ba—Ti_m2—W_cxii | 180.0 (5) |
Baxii—Fe_m2—W_cxii | 0.0 (5) | Ba—Ti_m2—Mg_m2 | 0 |
Baxii—Fe_m2—Ti_m2 | 0 | Baxii—Ti_m2—W_c | 180.0 (5) |
Baxii—Fe_m2—Mg_m2 | 0 | Baxii—Ti_m2—W_cxii | 0.0 (5) |
W_c—Fe_m2—W_cxii | 180.0 (5) | Baxii—Ti_m2—Mg_m2 | 0 |
W_c—Fe_m2—Ti_m2 | 0 | W_c—Ti_m2—W_cxii | 180.0 (5) |
W_c—Fe_m2—Mg_m2 | 0 | W_c—Ti_m2—Mg_m2 | 0 |
W_cxii—Fe_m2—Ti_m2 | 0 | W_cxii—Ti_m2—Mg_m2 | 0 |
W_cxii—Fe_m2—Mg_m2 | 0 | Ti_m1(2)—Mg_m2—Ti_m1(2)xiv | 180.0 (5) |
Ti_m2—Fe_m2—Mg_m2 | 0 | Ti_m1(2)—Mg_m2—Fe_m2 | 0 |
K_b—Si1—O3 | 58.45 (4) | Ti_m1(2)—Mg_m2—O1 | 39.82 (3) |
K_b—Si1—O4 | 61.66 (7) | Ti_m1(2)—Mg_m2—O1xii | 39.82 (3) |
K_b—Si1—O6 | 95.21 (5) | Ti_m1(2)—Mg_m2—O1xiv | 140.18 (3) |
K_b—Si1—O7 | 154.18 (6) | Ti_m1(2)—Mg_m2—O1ix | 140.18 (3) |
O3—Si1—O4 | 109.29 (9) | Ti_m1(2)—Mg_m2—Ba | 90 |
O3—Si1—O6 | 113.59 (7) | Ti_m1(2)—Mg_m2—Baxii | 90 |
O3—Si1—O7 | 109.27 (7) | Ti_m1(2)—Mg_m2—W_c | 90 |
O4—Si1—O6 | 105.62 (8) | Ti_m1(2)—Mg_m2—W_cxii | 90 |
O4—Si1—O7 | 108.31 (8) | Ti_m1(2)—Mg_m2—Ti_m2 | 0 |
O6—Si1—O7 | 110.59 (7) | Ti_m1(2)xiv—Mg_m2—Fe_m2 | 0 |
Na_aiv—Si2—O1 | 65.37 (6) | Ti_m1(2)xiv—Mg_m2—O1 | 140.18 (3) |
Na_aiv—Si2—O2 | 107.76 (7) | Ti_m1(2)xiv—Mg_m2—O1xii | 140.18 (3) |
Na_aiv—Si2—O5 | 143.97 (10) | Ti_m1(2)xiv—Mg_m2—O1xiv | 39.82 (3) |
Na_aiv—Si2—O7x | 48.62 (6) | Ti_m1(2)xiv—Mg_m2—O1ix | 39.82 (3) |
Na_aiv—Si2—Ba | 124.25 (4) | Ti_m1(2)xiv—Mg_m2—Ba | 90 |
O1—Si2—O2 | 114.52 (6) | Ti_m1(2)xiv—Mg_m2—Baxii | 90 |
O1—Si2—O5 | 108.48 (7) | Ti_m1(2)xiv—Mg_m2—W_c | 90 |
O1—Si2—O7x | 107.36 (7) | Ti_m1(2)xiv—Mg_m2—W_cxii | 90 |
O1—Si2—Ba | 58.96 (5) | Ti_m1(2)xiv—Mg_m2—Ti_m2 | 0 |
O2—Si2—O5 | 106.75 (9) | Fe_m2—Mg_m2—O1 | 0 |
O2—Si2—O7x | 111.47 (7) | Fe_m2—Mg_m2—O1xii | 0 |
O2—Si2—Ba | 92.61 (4) | Fe_m2—Mg_m2—O1xiv | 0 |
O5—Si2—O7x | 108.07 (8) | Fe_m2—Mg_m2—O1ix | 0 |
O5—Si2—Ba | 63.61 (6) | Fe_m2—Mg_m2—Ba | 0 |
O7x—Si2—Ba | 155.89 (5) | Fe_m2—Mg_m2—Baxii | 0 |
Ti_m1(2)—O1—Fe_m2 | 99.47 (4) | Fe_m2—Mg_m2—W_c | 0 |
Ti_m1(2)—O1—Si2 | 126.50 (8) | Fe_m2—Mg_m2—W_cxii | 0 |
Ti_m1(2)—O1—Baxii | 99.99 (4) | Fe_m2—Mg_m2—Ti_m2 | 0 |
Ti_m1(2)—O1—Ti_m2 | 99.47 (4) | O1—Mg_m2—O1xii | 79.63 (4) |
Ti_m1(2)—O1—Mg_m2 | 99.47 (4) | O1—Mg_m2—O1xiv | 180.0 (5) |
Fe_m2—O1—Si2 | 120.87 (7) | O1—Mg_m2—O1ix | 100.37 (4) |
Fe_m2—O1—Baxii | 47.13 (3) | O1—Mg_m2—Ba | 94.06 (4) |
Fe_m2—O1—Ti_m2 | 0.0 (5) | O1—Mg_m2—Baxii | 85.94 (4) |
Fe_m2—O1—Mg_m2 | 0.0 (5) | O1—Mg_m2—W_c | 94.06 (4) |
Si2—O1—Baxii | 132.86 (7) | O1—Mg_m2—W_cxii | 85.94 (4) |
Si2—O1—Ti_m2 | 120.87 (7) | O1—Mg_m2—Ti_m2 | 0 |
Si2—O1—Mg_m2 | 120.87 (7) | O1xii—Mg_m2—O1xiv | 100.37 (4) |
Baxii—O1—Ti_m2 | 47.13 (3) | O1xii—Mg_m2—O1ix | 180.0 (5) |
Baxii—O1—Mg_m2 | 47.13 (3) | O1xii—Mg_m2—Ba | 85.94 (4) |
Ti_m2—O1—Mg_m2 | 0.0 (5) | O1xii—Mg_m2—Baxii | 94.06 (4) |
Na_ax—O2—Ti_m1(1) | 110.06 (9) | O1xii—Mg_m2—W_c | 85.94 (4) |
Na_ax—O2—Si2 | 111.99 (10) | O1xii—Mg_m2—W_cxii | 94.06 (4) |
Na_ax—O2—Nb_m1(1) | 110.06 (9) | O1xii—Mg_m2—Ti_m2 | 0 |
Ti_m1(1)—O2—Si2 | 135.74 (6) | O1xiv—Mg_m2—O1ix | 79.63 (4) |
Ti_m1(1)—O2—Nb_m1(1) | 0.0 (5) | O1xiv—Mg_m2—Ba | 85.94 (4) |
Si2—O2—Nb_m1(1) | 135.74 (6) | O1xiv—Mg_m2—Baxii | 94.06 (4) |
Ti_m1(1)—O3—Si1 | 125.64 (8) | O1xiv—Mg_m2—W_c | 85.94 (4) |
Ti_m1(1)—O3—Nb_m1(1) | 0.0 (5) | O1xiv—Mg_m2—W_cxii | 94.06 (4) |
Si1—O3—Nb_m1(1) | 125.64 (8) | O1xiv—Mg_m2—Ti_m2 | 0 |
Si1—O4—Si1ix | 138.44 (12) | O1ix—Mg_m2—Ba | 94.06 (4) |
K_b—O5—Si2 | 112.58 (8) | O1ix—Mg_m2—Baxii | 85.94 (4) |
K_b—O5—Si2ix | 112.58 (8) | O1ix—Mg_m2—W_c | 94.06 (4) |
Si2—O5—Si2ix | 134.82 (15) | O1ix—Mg_m2—W_cxii | 85.94 (4) |
Ti_m1(2)iv—O6—Si1 | 137.60 (10) | O1ix—Mg_m2—Ti_m2 | 0 |
Si1—O7—Si2ii | 143.51 (10) | Ba—Mg_m2—Baxii | 180.0 (5) |
Ti_m1(1)—Oh—Ti_m1(2) | 134.87 (6) | Ba—Mg_m2—W_c | 0.0 (5) |
Ti_m1(1)—Oh—Nb_m1(1) | 0.0 (5) | Ba—Mg_m2—W_cxii | 180.0 (5) |
Ti_m1(2)—Oh—Nb_m1(1) | 134.87 (6) | Ba—Mg_m2—Ti_m2 | 0 |
Na_axvii—Ba—Na_axviii | 34.97 (6) | Baxii—Mg_m2—W_c | 180.0 (5) |
Na_axvii—Ba—Na_avii | 111.57 (5) | Baxii—Mg_m2—W_cxii | 0.0 (5) |
Na_axvii—Ba—Na_axiii | 102.25 (4) | Baxii—Mg_m2—Ti_m2 | 0 |
Na_axvii—Ba—K_b | 124.50 (3) | W_c—Mg_m2—W_cxii | 180.0 (5) |
Na_axvii—Ba—Ti_m1(2) | 131.54 (4) | W_c—Mg_m2—Ti_m2 | 0 |
Na_axvii—Ba—Ti_m1(2)xiv | 50.63 (4) | W_cxii—Mg_m2—Ti_m2 | 0 |
Na_axvii—Ba—Fe_m2 | 91.49 (5) | | |
Symmetry codes: (i) −x+1, y, −z; (ii) x, y, z−1; (iii) −x+1, y, −z+1; (iv) −x+1/2, −y+1/2, −z+1; (v) x+1/2, y+1/2, z; (vi) −x+1/2, y+1/2, −z; (vii) −x+1/2, −y+1/2, −z; (viii) −x+1, y, −z+2; (ix) x, −y, z; (x) x, y, z+1; (xi) −x+1, −y, −z+1; (xii) −x, y, −z+1; (xiii) x−1/2, −y+1/2, z; (xiv) −x, −y, −z+1; (xv) −x, −y, −z; (xvi) x, −y, z+1; (xvii) x−1/2, y−1/2, z; (xviii) −x+1/2, y−1/2, −z; (xix) −x, y, −z. |
Crystal data top
Ba0.7Fe0.5K2.1Mg0.05Na2Nb0.1O33Si8Ti4 | Z = 2 |
Mr = 1206.8 | F(000) = 1167 |
Monoclinic, C2/m | Dx = 3.058 Mg m−3 |
Hall symbol: -C 2y | Synchrotron radiation, λ = 0.414 Å |
a = 14.081 (13) Å | Cell parameters from 3042 reflections |
b = 13.5962 (10) Å | θ = 1.7–18.9° |
c = 7.663 (3) Å | µ = 0.81 mm−1 |
β = 116.74 (6)° | T = 293 K |
V = 1310.3 (15) Å3 | Anhedral grain |
Data collection top
ESRF ID 09 diffractometer | θmax = 18.9°, θmin = 1.7° |
3042 measured reflections | h = −8→8 |
936 independent reflections | k = −21→20 |
760 reflections with I > 2σ(I) | l = −11→10 |
Rint = 0.072 | |
Refinement top
Refinement on F | 0 restraints |
R[F2 > 2σ(F2)] = 0.074 | 6 constraints |
wR(F2) = 0.134 | Weighting scheme based on measured s.u.'s w = 1/(σ2(F) + 0.0120999999F2) |
S = 1.06 | (Δ/σ)max = 0.049 |
936 reflections | Δρmax = 0.83 e Å−3 |
66 parameters | Δρmin = −1.03 e Å−3 |
Fractional atomic coordinates and isotropic or equivalent isotropic displacement parameters (Å2) top | x | y | z | Uiso*/Ueq | Occ. (<1) |
Na_a | 0.4156 (14) | 0.2641 (5) | 0.0131 (11) | 0.0253 (16)* | 0.5 |
K_b | 0.4244 (6) | 0 | 0.7085 (4) | 0.024 (4) | |
Ti_m1(1) | 0.25 | 0.25 | 0.5 | 0.0109 (5)* | 0.95 |
Ti_m1(2) | 0 | 0.22420 (12) | 0.5 | 0.0084 (5)* | |
Fe_m2 | 0 | 0 | 0.5 | 0.0243 (11)* | 0.5 |
Si1 | 0.3213 (4) | 0.11100 (12) | 0.2553 (2) | 0.0053 (5)* | |
Si2 | 0.2094 (3) | 0.10955 (12) | 0.8066 (2) | 0.0051 (5)* | |
O1 | 0.0827 (9) | 0.1121 (3) | 0.6759 (7) | 0.0086 (10)* | |
O2 | 0.2749 (8) | 0.1875 (3) | 0.7462 (6) | 0.0074 (10)* | |
O3 | 0.2715 (9) | 0.1222 (3) | 0.4026 (6) | 0.0072 (10)* | |
O4 | 0.3735 (14) | 0 | 0.2759 (10) | 0.0098 (14)* | |
O5 | 0.2550 (13) | 0 | 0.7915 (10) | 0.0094 (14)* | |
O6 | 0.4174 (9) | 0.1837 (3) | 0.2980 (7) | 0.0126 (11)* | |
O7 | 0.2314 (9) | 0.1262 (3) | 0.0296 (7) | 0.0106 (11)* | |
Oh | 0.1010 (9) | 0.2201 (3) | 0.3935 (7) | 0.0089 (10)* | |
Ba | 0.0874 (3) | 0 | 0.3422 (2) | 0.0125 (5)* | 0.35 |
W1 | 0.5 | 0.1457 (7) | 0 | 0.097 (17) | |
W2 | 0 | 0.1134 (7) | 0 | 0.08 (2) | |
W_c | 0.0874 (3) | 0 | 0.3422 (2) | 0.0125 (5)* | 0.65 |
Nb_m1(1) | 0.25 | 0.25 | 0.5 | 0.0109 (5)* | 0.05 |
Ti_m2 | 0 | 0 | 0.5 | 0.0243 (11)* | 0.1 |
Mg_m2 | 0 | 0 | 0.5 | 0.0243 (11)* | 0.05 |
Atomic displacement parameters (Å2) top | U11 | U22 | U33 | U12 | U13 | U23 |
K_b | 0.019 (8) | 0.0411 (15) | 0.0140 (11) | 0 | 0.0091 (19) | 0 |
W1 | 0.19 (4) | 0.025 (5) | 0.019 (4) | 0 | −0.007 (8) | 0 |
W2 | 0.15 (5) | 0.035 (6) | 0.026 (5) | 0 | 0.020 (10) | 0 |
Geometric parameters (Å, º) top
Na_a—Na_ai | 2.47 (3) | Si2—Si2vi | 2.979 (2) |
Na_a—Ti_m1(2)ii | 3.372 (9) | Si2—O1 | 1.605 (12) |
Na_a—Si1 | 3.429 (15) | Si2—O1vi | 3.414 (7) |
Na_a—Si1iii | 3.475 (16) | Si2—O2 | 1.604 (10) |
Na_a—Si2iv | 3.349 (15) | Si2—O5 | 1.647 (9) |
Na_a—Si2ii | 3.186 (17) | Si2—O6ii | 3.232 (8) |
Na_a—O1ii | 2.909 (13) | Si2—O7ix | 1.609 (7) |
Na_a—O2iv | 2.356 (13) | Si2—Oh | 3.204 (6) |
Na_a—O3iii | 3.454 (12) | Si2—Nb_m1(1) | 3.272 (3) |
Na_a—O6 | 2.432 (14) | Si2—Ti_m2 | 3.194 (7) |
Na_a—O7 | 3.25 (2) | Si2—Mg_m2 | 3.194 (7) |
Na_a—O7iii | 2.45 (2) | O1—O1xi | 2.655 (11) |
Na_a—Ohiii | 3.026 (14) | O1—O1vi | 3.048 (6) |
Na_a—Ohv | 2.917 (13) | O1—O2 | 2.711 (17) |
Na_a—W1 | 2.029 (15) | O1—O5 | 2.657 (18) |
Na_a—W2iii | 2.075 (15) | O1—O6ii | 2.784 (6) |
K_b—Si1 | 3.451 (5) | O1—O7ix | 2.580 (10) |
K_b—Si1vi | 3.451 (5) | O1—Oh | 2.722 (11) |
K_b—O2 | 3.400 (10) | O1—Ohxi | 2.809 (16) |
K_b—O2vi | 3.400 (10) | O1—Ba | 3.004 (8) |
K_b—O3 | 2.890 (8) | O1—Baxi | 2.790 (13) |
K_b—O3vi | 2.890 (8) | O1—W2ix | 3.183 (11) |
K_b—O4 | 3.061 (10) | O1—W_c | 3.004 (8) |
K_b—O4vii | 2.79 (2) | O1—W_cxi | 2.790 (13) |
K_b—O5 | 2.73 (2) | O1—Ti_m2 | 2.021 (5) |
K_b—O6vii | 3.361 (11) | O1—Mg_m2 | 2.021 (5) |
K_b—O6viii | 3.361 (11) | O2—O3 | 2.759 (10) |
K_b—W1ix | 2.812 (7) | O2—O3ii | 2.785 (6) |
K_b—W1viii | 2.812 (7) | O2—O5 | 2.605 (6) |
Ti_m1(1)—Si1 | 3.129 (4) | O2—O6ii | 3.113 (16) |
Ti_m1(1)—Si1ii | 3.129 (4) | O2—O7ix | 2.642 (13) |
Ti_m1(1)—Si2 | 3.272 (3) | O2—O7ii | 3.084 (8) |
Ti_m1(1)—Si2ii | 3.272 (3) | O2—Oh | 2.746 (11) |
Ti_m1(1)—O2 | 1.952 (6) | O2—Ohii | 2.732 (15) |
Ti_m1(1)—O2ii | 1.952 (6) | O2—W1ix | 2.933 (12) |
Ti_m1(1)—O3 | 1.968 (6) | O2—Nb_m1(1) | 1.952 (6) |
Ti_m1(1)—O3ii | 1.968 (6) | O3—O3vi | 3.322 (6) |
Ti_m1(1)—O6 | 3.471 (13) | O3—O4 | 2.649 (18) |
Ti_m1(1)—O6ii | 3.471 (13) | O3—O6 | 2.653 (18) |
Ti_m1(1)—Oh | 1.922 (12) | O3—O7 | 2.653 (9) |
Ti_m1(1)—Ohii | 1.922 (12) | O3—Oh | 2.720 (17) |
Ti_m1(1)—Nb_m1(1) | 0 | O3—Ohii | 2.782 (9) |
Ti_m1(2)—Fe_m2 | 3.0483 (17) | O3—Ba | 2.935 (12) |
Ti_m1(2)—Si1ii | 3.259 (5) | O3—W_c | 2.935 (12) |
Ti_m1(2)—Si1x | 3.259 (5) | O3—Nb_m1(1) | 1.968 (6) |
Ti_m1(2)—Si2 | 3.227 (7) | O4—O5iv | 3.315 (10) |
Ti_m1(2)—Si2xi | 3.227 (7) | O4—O6 | 2.559 (7) |
Ti_m1(2)—O1 | 2.021 (6) | O4—O6vi | 2.559 (7) |
Ti_m1(2)—O1xi | 2.021 (6) | O4—O7 | 2.668 (12) |
Ti_m1(2)—O2 | 3.496 (13) | O4—O7vi | 2.668 (12) |
Ti_m1(2)—O2xi | 3.496 (13) | O5—O7ix | 2.633 (13) |
Ti_m1(2)—O6ii | 1.923 (6) | O5—O7xiii | 2.633 (13) |
Ti_m1(2)—O6x | 1.923 (6) | O5—Ba | 3.180 (9) |
Ti_m1(2)—Oh | 1.933 (12) | O5—W_c | 3.180 (9) |
Ti_m1(2)—Ohxi | 1.933 (12) | O5—Ti_m2 | 3.266 (17) |
Ti_m1(2)—Ti_m2 | 3.0483 (17) | O5—Mg_m2 | 3.266 (17) |
Ti_m1(2)—Mg_m2 | 3.0483 (17) | O6—O6vii | 2.919 (10) |
Fe_m2—Si2 | 3.194 (7) | O6—O7 | 2.618 (14) |
Fe_m2—Si2xi | 3.194 (7) | O6—Ohii | 2.814 (11) |
Fe_m2—Si2xii | 3.194 (7) | O6—Ohv | 2.689 (16) |
Fe_m2—Si2vi | 3.194 (7) | O6—W1 | 3.037 (11) |
Fe_m2—O1 | 2.021 (5) | O6—Nb_m1(1) | 3.471 (13) |
Fe_m2—O1xi | 2.021 (5) | O7—O7iii | 3.467 (8) |
Fe_m2—O1xii | 2.021 (5) | O7—O7vi | 3.433 (7) |
Fe_m2—O1vi | 2.021 (5) | O7—W2 | 3.167 (15) |
Fe_m2—O5 | 3.266 (17) | Oh—Ba | 3.013 (4) |
Fe_m2—O5xi | 3.266 (17) | Oh—W1iii | 3.253 (8) |
Fe_m2—Ba | 2.078 (4) | Oh—W2 | 3.060 (7) |
Fe_m2—Baxi | 2.078 (4) | Oh—W_c | 3.013 (4) |
Fe_m2—W_c | 2.078 (4) | Oh—Nb_m1(1) | 1.922 (12) |
Fe_m2—W_cxi | 2.078 (4) | Ba—W2 | 2.804 (6) |
Fe_m2—Ti_m2 | 0 | Ba—W2xiv | 2.804 (6) |
Fe_m2—Mg_m2 | 0 | Ba—W_c | 0 |
Si1—Si1vi | 3.018 (2) | Ba—Ti_m2 | 2.078 (4) |
Si1—Si2iv | 3.071 (5) | Ba—Mg_m2 | 2.078 (4) |
Si1—O2ii | 3.054 (7) | W1—W2iii | 3.275 (14) |
Si1—O3 | 1.581 (12) | W2—W2xiv | 3.084 (14) |
Si1—O4 | 1.655 (8) | W2—W_c | 2.804 (6) |
Si1—O6 | 1.586 (11) | W2—W_cxv | 2.804 (6) |
Si1—O7 | 1.633 (7) | W_c—Ti_m2 | 2.078 (4) |
Si1—Ohii | 3.326 (5) | W_c—Mg_m2 | 2.078 (4) |
Si1—Nb_m1(1) | 3.129 (4) | Ti_m2—Mg_m2 | 0 |
| | | |
Na_ai—Na_a—Ti_m1(2)ii | 102.5 (4) | Si1vi—O4—O6 | 168.4 (11) |
Na_ai—Na_a—Si1 | 131.6 (4) | Si1vi—O4—O6vi | 36.9 (4) |
Na_ai—Na_a—Si1iii | 130.8 (4) | Si1vi—O4—O7 | 111.1 (7) |
Na_ai—Na_a—Si2iv | 128.5 (4) | Si1vi—O4—O7vi | 35.5 (2) |
Na_ai—Na_a—Si2ii | 140.7 (4) | O3—O4—O3vi | 77.7 (6) |
Na_ai—Na_a—O1ii | 114.4 (5) | O3—O4—O5iv | 109.1 (5) |
Na_ai—Na_a—O2iv | 113.2 (6) | O3—O4—O6 | 61.2 (4) |
Na_ai—Na_a—O3iii | 106.7 (5) | O3—O4—O6vi | 137.9 (7) |
Na_ai—Na_a—O6 | 116.8 (6) | O3—O4—O7 | 59.9 (4) |
Na_ai—Na_a—O7 | 144.7 (4) | O3—O4—O7vi | 107.7 (7) |
Na_ai—Na_a—O7iii | 140.7 (5) | O3vi—O4—O5iv | 109.1 (5) |
Na_ai—Na_a—Ohiii | 63.1 (5) | O3vi—O4—O6 | 137.9 (7) |
Na_ai—Na_a—Ohv | 67.7 (5) | O3vi—O4—O6vi | 61.2 (4) |
Na_ai—Na_a—W1 | 52.5 (5) | O3vi—O4—O7 | 107.7 (7) |
Na_ai—Na_a—W2iii | 53.4 (5) | O3vi—O4—O7vi | 59.9 (4) |
Ti_m1(2)ii—Na_a—Si1 | 57.3 (2) | O5iv—O4—O6 | 93.4 (2) |
Ti_m1(2)ii—Na_a—Si1iii | 113.5 (5) | O5iv—O4—O6vi | 93.4 (2) |
Ti_m1(2)ii—Na_a—Si2iv | 110.6 (4) | O5iv—O4—O7 | 50.8 (3) |
Ti_m1(2)ii—Na_a—Si2ii | 58.9 (2) | O5iv—O4—O7vi | 50.8 (3) |
Ti_m1(2)ii—Na_a—O1ii | 36.61 (15) | O6—O4—O6vi | 154.6 (9) |
Ti_m1(2)ii—Na_a—O2iv | 136.2 (7) | O6—O4—O7 | 60.1 (3) |
Ti_m1(2)ii—Na_a—O3iii | 137.9 (5) | O6—O4—O7vi | 139.2 (4) |
Ti_m1(2)ii—Na_a—O6 | 34.07 (18) | O6vi—O4—O7 | 139.2 (4) |
Ti_m1(2)ii—Na_a—O7 | 82.8 (4) | O6vi—O4—O7vi | 60.1 (3) |
Ti_m1(2)ii—Na_a—O7iii | 88.6 (4) | O7—O4—O7vi | 80.1 (4) |
Ti_m1(2)ii—Na_a—Ohiii | 164.1 (7) | K_b—O5—Fe_m2 | 130.3 (3) |
Ti_m1(2)ii—Na_a—Ohv | 34.9 (3) | K_b—O5—Si2 | 115.2 (6) |
Ti_m1(2)ii—Na_a—W1 | 99.8 (3) | K_b—O5—Si2vi | 115.2 (6) |
Ti_m1(2)ii—Na_a—W2iii | 95.2 (3) | K_b—O5—O1 | 133.2 (4) |
Si1—Na_a—Si1iii | 96.6 (5) | K_b—O5—O1vi | 133.2 (4) |
Si1—Na_a—Si2iv | 53.9 (2) | K_b—O5—O2 | 79.1 (5) |
Si1—Na_a—Si2ii | 70.6 (4) | K_b—O5—O2vi | 79.1 (5) |
Si1—Na_a—O1ii | 76.7 (4) | K_b—O5—O4ix | 102.0 (5) |
Si1—Na_a—O2iv | 79.8 (5) | K_b—O5—O7ix | 123.9 (5) |
Si1—Na_a—O3iii | 116.8 (6) | K_b—O5—O7xiii | 123.9 (5) |
Si1—Na_a—O6 | 24.6 (3) | K_b—O5—Ba | 92.8 (3) |
Si1—Na_a—O7 | 28.15 (17) | K_b—O5—W_c | 92.8 (3) |
Si1—Na_a—O7iii | 86.1 (6) | K_b—O5—Ti_m2 | 130.3 (3) |
Si1—Na_a—Ohiii | 137.0 (3) | K_b—O5—Mg_m2 | 130.3 (3) |
Si1—Na_a—Ohv | 83.9 (3) | Fe_m2—O5—Si2 | 72.8 (5) |
Si1—Na_a—W1 | 85.6 (3) | Fe_m2—O5—Si2vi | 72.8 (5) |
Si1—Na_a—W2iii | 152.0 (4) | Fe_m2—O5—O1 | 38.2 (2) |
Si1iii—Na_a—Si2iv | 68.2 (3) | Fe_m2—O5—O1vi | 38.2 (2) |
Si1iii—Na_a—Si2ii | 54.7 (3) | Fe_m2—O5—O2 | 93.4 (4) |
Si1iii—Na_a—O1ii | 81.6 (4) | Fe_m2—O5—O2vi | 93.4 (4) |
Si1iii—Na_a—O2iv | 59.6 (4) | Fe_m2—O5—O4ix | 127.6 (7) |
Si1iii—Na_a—O3iii | 26.4 (2) | Fe_m2—O5—O7ix | 91.8 (5) |
Si1iii—Na_a—O6 | 111.7 (7) | Fe_m2—O5—O7xiii | 91.8 (5) |
Si1iii—Na_a—O7 | 74.6 (4) | Fe_m2—O5—Ba | 37.58 (17) |
Si1iii—Na_a—O7iii | 25.19 (17) | Fe_m2—O5—W_c | 37.58 (17) |
Si1iii—Na_a—Ohiii | 75.3 (3) | Fe_m2—O5—Ti_m2 | 0.0 (5) |
Si1iii—Na_a—Ohv | 138.1 (4) | Fe_m2—O5—Mg_m2 | 0.0 (5) |
Si1iii—Na_a—W1 | 141.8 (3) | Si2—O5—Si2vi | 129.5 (12) |
Si1iii—Na_a—W2iii | 89.8 (3) | Si2—O5—O1 | 34.7 (4) |
Si2iv—Na_a—Si2ii | 90.7 (5) | Si2—O5—O1vi | 102.5 (9) |
Si2iv—Na_a—O1ii | 115.8 (7) | Si2—O5—O2 | 36.2 (4) |
Si2iv—Na_a—O2iv | 25.9 (3) | Si2—O5—O2vi | 164.5 (10) |
Si2iv—Na_a—O3iii | 72.9 (3) | Si2—O5—O4ix | 86.4 (3) |
Si2iv—Na_a—O6 | 78.4 (4) | Si2—O5—O7ix | 35.6 (2) |
Si2iv—Na_a—O7 | 28.18 (17) | Si2—O5—O7xiii | 111.5 (8) |
Si2iv—Na_a—O7iii | 79.5 (5) | Si2—O5—Ba | 87.3 (3) |
Si2iv—Na_a—Ohiii | 84.8 (3) | Si2—O5—W_c | 87.3 (3) |
Si2iv—Na_a—Ohv | 135.6 (4) | Si2—O5—Ti_m2 | 72.8 (5) |
Si2iv—Na_a—W1 | 83.2 (3) | Si2—O5—Mg_m2 | 72.8 (5) |
Si2iv—Na_a—W2iii | 151.0 (3) | Si2vi—O5—O1 | 102.5 (9) |
Si2ii—Na_a—O1ii | 30.1 (3) | Si2vi—O5—O1vi | 34.7 (4) |
Si2ii—Na_a—O2iv | 101.6 (7) | Si2vi—O5—O2 | 164.5 (10) |
Si2ii—Na_a—O3iii | 79.5 (4) | Si2vi—O5—O2vi | 36.2 (4) |
Si2ii—Na_a—O6 | 68.7 (5) | Si2vi—O5—O4ix | 86.4 (3) |
Si2ii—Na_a—O7 | 71.8 (4) | Si2vi—O5—O7ix | 111.5 (8) |
Si2ii—Na_a—O7iii | 29.7 (2) | Si2vi—O5—O7xiii | 35.6 (2) |
Si2ii—Na_a—Ohiii | 127.3 (4) | Si2vi—O5—Ba | 87.3 (3) |
Si2ii—Na_a—Ohv | 87.0 (3) | Si2vi—O5—W_c | 87.3 (3) |
Si2ii—Na_a—W1 | 154.1 (5) | Si2vi—O5—Ti_m2 | 72.8 (5) |
Si2ii—Na_a—W2iii | 91.6 (3) | Si2vi—O5—Mg_m2 | 72.8 (5) |
O1ii—Na_a—O2iv | 131.3 (9) | O1—O5—O1vi | 70.0 (5) |
O1ii—Na_a—O3iii | 102.6 (4) | O1—O5—O2 | 62.0 (3) |
O1ii—Na_a—O6 | 62.1 (3) | O1—O5—O2vi | 130.8 (6) |
O1ii—Na_a—O7 | 90.8 (6) | O1—O5—O4ix | 107.3 (5) |
O1ii—Na_a—O7iii | 56.8 (4) | O1—O5—O7ix | 58.4 (4) |
O1ii—Na_a—Ohiii | 140.4 (3) | O1—O5—O7xiii | 103.0 (7) |
O1ii—Na_a—Ohv | 57.7 (3) | O1—O5—Ba | 61.2 (3) |
O1ii—Na_a—W1 | 135.3 (4) | O1—O5—W_c | 61.2 (3) |
O1ii—Na_a—W2iii | 77.4 (3) | O1—O5—Ti_m2 | 38.2 (2) |
O2iv—Na_a—O3iii | 53.3 (2) | O1—O5—Mg_m2 | 38.2 (2) |
O2iv—Na_a—O6 | 104.2 (6) | O1vi—O5—O2 | 130.8 (6) |
O2iv—Na_a—O7 | 53.4 (4) | O1vi—O5—O2vi | 62.0 (3) |
O2iv—Na_a—O7iii | 79.8 (6) | O1vi—O5—O4ix | 107.3 (5) |
O2iv—Na_a—Ohiii | 59.5 (4) | O1vi—O5—O7ix | 103.0 (7) |
O2iv—Na_a—Ohv | 157.7 (3) | O1vi—O5—O7xiii | 58.4 (4) |
O2iv—Na_a—W1 | 83.6 (3) | O1vi—O5—Ba | 61.2 (3) |
O2iv—Na_a—W2iii | 126.1 (4) | O1vi—O5—W_c | 61.2 (3) |
O3iii—Na_a—O6 | 136.4 (8) | O1vi—O5—Ti_m2 | 38.2 (2) |
O3iii—Na_a—O7 | 90.2 (4) | O1vi—O5—Mg_m2 | 38.2 (2) |
O3iii—Na_a—O7iii | 49.9 (3) | O2—O5—O2vi | 156.3 (8) |
O3iii—Na_a—Ohiii | 49.1 (3) | O2—O5—O4ix | 96.84 (18) |
O3iii—Na_a—Ohv | 149.0 (3) | O2—O5—O7ix | 60.6 (3) |
O3iii—Na_a—W1 | 122.0 (4) | O2—O5—O7xiii | 141.7 (5) |
O3iii—Na_a—W2iii | 79.1 (3) | O2—O5—Ba | 85.84 (18) |
O6—Na_a—O7 | 52.5 (4) | O2—O5—W_c | 85.84 (18) |
O6—Na_a—O7iii | 93.4 (7) | O2—O5—Ti_m2 | 93.4 (4) |
O6—Na_a—Ohiii | 157.1 (3) | O2—O5—Mg_m2 | 93.4 (4) |
O6—Na_a—Ohv | 59.5 (3) | O2vi—O5—O4ix | 96.84 (18) |
O6—Na_a—W1 | 85.3 (3) | O2vi—O5—O7ix | 141.7 (5) |
O6—Na_a—W2iii | 129.0 (4) | O2vi—O5—O7xiii | 60.6 (3) |
O7—Na_a—O7iii | 73.4 (6) | O2vi—O5—Ba | 85.84 (18) |
O7—Na_a—Ohiii | 112.8 (4) | O2vi—O5—W_c | 85.84 (18) |
O7—Na_a—Ohv | 112.0 (4) | O2vi—O5—Ti_m2 | 93.4 (4) |
O7—Na_a—W1 | 92.3 (4) | O2vi—O5—Mg_m2 | 93.4 (4) |
O7—Na_a—W2iii | 161.8 (7) | O4ix—O5—O7ix | 51.8 (3) |
O7iii—Na_a—Ohiii | 98.6 (3) | O4ix—O5—O7xiii | 51.8 (3) |
O7iii—Na_a—Ohv | 114.2 (4) | O4ix—O5—Ba | 165.2 (8) |
O7iii—Na_a—W1 | 162.6 (7) | O4ix—O5—W_c | 165.2 (8) |
O7iii—Na_a—W2iii | 88.4 (4) | O4ix—O5—Ti_m2 | 127.6 (7) |
Ohiii—Na_a—Ohv | 130.1 (8) | O4ix—O5—Mg_m2 | 127.6 (7) |
Ohiii—Na_a—W1 | 77.4 (5) | O7ix—O5—O7xiii | 81.4 (4) |
Ohiii—Na_a—W2iii | 71.0 (4) | O7ix—O5—Ba | 119.1 (5) |
Ohv—Na_a—W1 | 80.1 (5) | O7ix—O5—W_c | 119.1 (5) |
Ohv—Na_a—W2iii | 73.4 (4) | O7ix—O5—Ti_m2 | 91.8 (5) |
W1—Na_a—W2iii | 105.9 (9) | O7ix—O5—Mg_m2 | 91.8 (5) |
Si1—K_b—Si1vi | 51.86 (6) | O7xiii—O5—Ba | 119.1 (5) |
Si1—K_b—O2 | 76.19 (13) | O7xiii—O5—W_c | 119.1 (5) |
Si1—K_b—O2vi | 114.64 (18) | O7xiii—O5—Ti_m2 | 91.8 (5) |
Si1—K_b—O3 | 27.1 (2) | O7xiii—O5—Mg_m2 | 91.8 (5) |
Si1—K_b—O3vi | 67.18 (13) | Ba—O5—W_c | 0.0 (5) |
Si1—K_b—O4 | 28.65 (15) | Ba—O5—Ti_m2 | 37.58 (17) |
Si1—K_b—O4vii | 90.1 (2) | Ba—O5—Mg_m2 | 37.58 (17) |
Si1—K_b—O5 | 102.6 (2) | W_c—O5—Ti_m2 | 37.58 (17) |
Si1—K_b—O6vii | 69.01 (15) | W_c—O5—Mg_m2 | 37.58 (17) |
Si1—K_b—O6viii | 106.9 (2) | Ti_m2—O5—Mg_m2 | 0.0 (5) |
Si1—K_b—W1ix | 109.19 (15) | Na_a—O6—K_bvii | 93.4 (5) |
Si1—K_b—W1viii | 160.89 (16) | Na_a—O6—Ti_m1(1) | 123.3 (5) |
Si1vi—K_b—O2 | 114.64 (18) | Na_a—O6—Ti_m1(2)ii | 100.8 (4) |
Si1vi—K_b—O2vi | 76.19 (13) | Na_a—O6—Si1 | 115.6 (4) |
Si1vi—K_b—O3 | 67.18 (13) | Na_a—O6—Si2ii | 66.7 (4) |
Si1vi—K_b—O3vi | 27.1 (2) | Na_a—O6—O1ii | 67.4 (3) |
Si1vi—K_b—O4 | 28.65 (15) | Na_a—O6—O2ii | 89.6 (5) |
Si1vi—K_b—O4vii | 90.1 (2) | Na_a—O6—O3 | 135.8 (6) |
Si1vi—K_b—O5 | 102.6 (2) | Na_a—O6—O4 | 118.3 (4) |
Si1vi—K_b—O6vii | 106.9 (2) | Na_a—O6—O6vii | 129.3 (6) |
Si1vi—K_b—O6viii | 69.01 (15) | Na_a—O6—O7 | 80.0 (4) |
Si1vi—K_b—W1ix | 160.89 (16) | Na_a—O6—Ohii | 125.3 (3) |
Si1vi—K_b—W1viii | 109.19 (15) | Na_a—O6—Ohv | 69.2 (5) |
O2—K_b—O2vi | 97.1 (3) | Na_a—O6—W1 | 41.7 (4) |
O2—K_b—O3 | 51.3 (2) | Na_a—O6—Nb_m1(1) | 123.3 (5) |
O2—K_b—O3vi | 103.6 (3) | K_bvii—O6—Ti_m1(1) | 141.9 (2) |
O2—K_b—O4 | 103.9 (3) | K_bvii—O6—Ti_m1(2)ii | 109.3 (4) |
O2—K_b—O4vii | 130.85 (19) | K_bvii—O6—Si1 | 92.5 (3) |
O2—K_b—O5 | 48.78 (19) | K_bvii—O6—Si2ii | 159.7 (4) |
O2—K_b—O6vii | 83.4 (2) | K_bvii—O6—O1ii | 139.8 (5) |
O2—K_b—O6viii | 176.33 (15) | K_bvii—O6—O2ii | 165.1 (3) |
O2—K_b—W1ix | 55.38 (17) | K_bvii—O6—O3 | 112.2 (2) |
O2—K_b—W1viii | 119.2 (2) | K_bvii—O6—O4 | 54.3 (5) |
O2vi—K_b—O3 | 103.6 (3) | K_bvii—O6—O6vii | 78.4 (3) |
O2vi—K_b—O3vi | 51.3 (2) | K_bvii—O6—O7 | 101.7 (3) |
O2vi—K_b—O4 | 103.9 (3) | K_bvii—O6—Ohii | 132.1 (2) |
O2vi—K_b—O4vii | 130.85 (19) | K_bvii—O6—Ohv | 78.6 (4) |
O2vi—K_b—O5 | 48.78 (19) | K_bvii—O6—W1 | 51.8 (2) |
O2vi—K_b—O6vii | 176.33 (15) | K_bvii—O6—Nb_m1(1) | 141.9 (2) |
O2vi—K_b—O6viii | 83.4 (2) | Ti_m1(1)—O6—Ti_m1(2)ii | 76.0 (3) |
O2vi—K_b—W1ix | 119.2 (2) | Ti_m1(1)—O6—Si1 | 64.3 (4) |
O2vi—K_b—W1viii | 55.38 (17) | Ti_m1(1)—O6—Si2ii | 58.3 (2) |
O3—K_b—O3vi | 70.17 (18) | Ti_m1(1)—O6—O1ii | 71.7 (3) |
O3—K_b—O4 | 52.8 (3) | Ti_m1(1)—O6—O2ii | 33.94 (18) |
O3—K_b—O4vii | 114.0 (3) | Ti_m1(1)—O6—O3 | 34.31 (18) |
O3—K_b—O5 | 77.2 (3) | Ti_m1(1)—O6—O4 | 95.2 (5) |
O3—K_b—O6vii | 79.5 (3) | Ti_m1(1)—O6—O6vii | 84.5 (3) |
O3—K_b—O6viii | 132.2 (2) | Ti_m1(1)—O6—O7 | 77.8 (4) |
O3—K_b—W1ix | 96.72 (18) | Ti_m1(1)—O6—Ohii | 33.6 (3) |
O3—K_b—W1viii | 158.0 (4) | Ti_m1(1)—O6—Ohv | 121.0 (2) |
O3vi—K_b—O4 | 52.8 (3) | Ti_m1(1)—O6—W1 | 161.1 (3) |
O3vi—K_b—O4vii | 114.0 (3) | Ti_m1(1)—O6—Nb_m1(1) | 0.0 (5) |
O3vi—K_b—O5 | 77.2 (3) | Ti_m1(2)ii—O6—Si1 | 136.3 (6) |
O3vi—K_b—O6vii | 132.2 (2) | Ti_m1(2)ii—O6—Si2ii | 72.5 (2) |
O3vi—K_b—O6viii | 79.5 (3) | Ti_m1(2)ii—O6—O1ii | 46.54 (17) |
O3vi—K_b—W1ix | 158.0 (4) | Ti_m1(2)ii—O6—O2ii | 84.4 (3) |
O3vi—K_b—W1viii | 96.72 (18) | Ti_m1(2)ii—O6—O3 | 103.4 (4) |
O4—K_b—O4vii | 77.5 (4) | Ti_m1(2)ii—O6—O4 | 136.8 (3) |
O4—K_b—O5 | 116.7 (4) | Ti_m1(2)ii—O6—O6vii | 40.65 (15) |
O4—K_b—O6vii | 79.5 (3) | Ti_m1(2)ii—O6—O7 | 148.8 (6) |
O4—K_b—O6viii | 79.5 (3) | Ti_m1(2)ii—O6—Ohii | 43.3 (3) |
O4—K_b—W1ix | 132.91 (19) | Ti_m1(2)ii—O6—Ohv | 45.9 (3) |
O4—K_b—W1viii | 132.91 (19) | Ti_m1(2)ii—O6—W1 | 114.7 (5) |
O4vii—K_b—O5 | 165.8 (2) | Ti_m1(2)ii—O6—Nb_m1(1) | 76.0 (3) |
O4vii—K_b—O6vii | 48.1 (2) | Si1—O6—Si2ii | 99.6 (5) |
O4vii—K_b—O6viii | 48.1 (2) | Si1—O6—O1ii | 127.5 (7) |
O4vii—K_b—W1ix | 87.2 (2) | Si1—O6—O2ii | 73.1 (5) |
O4vii—K_b—W1viii | 87.2 (2) | Si1—O6—O3 | 33.0 (3) |
O5—K_b—O6vii | 131.1 (2) | Si1—O6—O4 | 38.8 (4) |
O5—K_b—O6viii | 131.1 (2) | Si1—O6—O6vii | 114.7 (4) |
O5—K_b—W1ix | 82.71 (19) | Si1—O6—O7 | 36.2 (2) |
O5—K_b—W1viii | 82.71 (19) | Si1—O6—Ohii | 94.1 (6) |
O6vii—K_b—O6viii | 95.9 (3) | Si1—O6—Ohv | 170.4 (5) |
O6vii—K_b—W1ix | 58.13 (17) | Si1—O6—W1 | 108.6 (3) |
O6vii—K_b—W1viii | 121.3 (2) | Si1—O6—Nb_m1(1) | 64.3 (4) |
O6viii—K_b—W1ix | 121.3 (2) | Si2ii—O6—O1ii | 29.8 (2) |
O6viii—K_b—W1viii | 58.13 (17) | Si2ii—O6—O2ii | 29.21 (18) |
W1ix—K_b—W1viii | 89.6 (2) | Si2ii—O6—O3 | 86.2 (4) |
Si1—Ti_m1(1)—Si1ii | 180.0 (5) | Si2ii—O6—O4 | 137.9 (6) |
Si1—Ti_m1(1)—Si2 | 106.55 (7) | Si2ii—O6—O6vii | 110.5 (2) |
Si1—Ti_m1(1)—Si2ii | 73.45 (7) | Si2ii—O6—O7 | 79.6 (3) |
Si1—Ti_m1(1)—O2 | 110.5 (2) | Si2ii—O6—Ohii | 63.6 (2) |
Si1—Ti_m1(1)—O2ii | 69.5 (2) | Si2ii—O6—Ohv | 90.0 (2) |
Si1—Ti_m1(1)—O3 | 25.0 (3) | Si2ii—O6—W1 | 108.5 (2) |
Si1—Ti_m1(1)—O3ii | 155.0 (3) | Si2ii—O6—Nb_m1(1) | 58.3 (2) |
Si1—Ti_m1(1)—O6 | 27.17 (14) | O1ii—O6—O2ii | 54.4 (3) |
Si1—Ti_m1(1)—O6ii | 152.83 (14) | O1ii—O6—O3 | 105.5 (5) |
Si1—Ti_m1(1)—Oh | 101.6 (2) | O1ii—O6—O4 | 165.9 (8) |
Si1—Ti_m1(1)—Ohii | 78.4 (2) | O1ii—O6—O6vii | 87.1 (2) |
Si1—Ti_m1(1)—Nb_m1(1) | 0 | O1ii—O6—O7 | 108.7 (4) |
Si1ii—Ti_m1(1)—Si2 | 73.45 (7) | O1ii—O6—Ohii | 58.2 (2) |
Si1ii—Ti_m1(1)—Si2ii | 106.55 (7) | O1ii—O6—Ohv | 61.7 (3) |
Si1ii—Ti_m1(1)—O2 | 69.5 (2) | O1ii—O6—W1 | 103.6 (4) |
Si1ii—Ti_m1(1)—O2ii | 110.5 (2) | O1ii—O6—Nb_m1(1) | 71.7 (3) |
Si1ii—Ti_m1(1)—O3 | 155.0 (3) | O2ii—O6—O3 | 57.1 (3) |
Si1ii—Ti_m1(1)—O3ii | 25.0 (3) | O2ii—O6—O4 | 111.7 (6) |
Si1ii—Ti_m1(1)—O6 | 152.83 (14) | O2ii—O6—O6vii | 110.8 (3) |
Si1ii—Ti_m1(1)—O6ii | 27.17 (14) | O2ii—O6—O7 | 64.4 (3) |
Si1ii—Ti_m1(1)—Oh | 78.4 (2) | O2ii—O6—Ohii | 54.9 (3) |
Si1ii—Ti_m1(1)—Ohii | 101.6 (2) | O2ii—O6—Ohv | 116.0 (3) |
Si1ii—Ti_m1(1)—Nb_m1(1) | 0 | O2ii—O6—W1 | 128.5 (2) |
Si2—Ti_m1(1)—Si2ii | 180.0 (5) | O2ii—O6—Nb_m1(1) | 33.94 (18) |
Si2—Ti_m1(1)—O2 | 20.8 (3) | O3—O6—O4 | 61.1 (5) |
Si2—Ti_m1(1)—O2ii | 159.2 (3) | O3—O6—O6vii | 92.0 (4) |
Si2—Ti_m1(1)—O3 | 82.2 (3) | O3—O6—O7 | 60.4 (4) |
Si2—Ti_m1(1)—O3ii | 97.8 (3) | O3—O6—Ohii | 61.1 (3) |
Si2—Ti_m1(1)—O6 | 122.81 (11) | O3—O6—Ohv | 148.3 (3) |
Si2—Ti_m1(1)—O6ii | 57.19 (11) | O3—O6—W1 | 141.6 (3) |
Si2—Ti_m1(1)—Oh | 70.80 (19) | O3—O6—Nb_m1(1) | 34.31 (18) |
Si2—Ti_m1(1)—Ohii | 109.20 (19) | O4—O6—O6vii | 97.1 (3) |
Si2—Ti_m1(1)—Nb_m1(1) | 0 | O4—O6—O7 | 62.0 (3) |
Si2ii—Ti_m1(1)—O2 | 159.2 (3) | O4—O6—Ohii | 113.5 (5) |
Si2ii—Ti_m1(1)—O2ii | 20.8 (3) | O4—O6—Ohv | 131.8 (6) |
Si2ii—Ti_m1(1)—O3 | 97.8 (3) | O4—O6—W1 | 87.0 (4) |
Si2ii—Ti_m1(1)—O3ii | 82.2 (3) | O4—O6—Nb_m1(1) | 95.2 (5) |
Si2ii—Ti_m1(1)—O6 | 57.19 (11) | O6vii—O6—O7 | 150.7 (5) |
Si2ii—Ti_m1(1)—O6ii | 122.81 (11) | O6vii—O6—Ohii | 55.9 (3) |
Si2ii—Ti_m1(1)—Oh | 109.20 (19) | O6vii—O6—Ohv | 60.1 (3) |
Si2ii—Ti_m1(1)—Ohii | 70.80 (19) | O6vii—O6—W1 | 113.9 (5) |
Si2ii—Ti_m1(1)—Nb_m1(1) | 0 | O6vii—O6—Nb_m1(1) | 84.5 (3) |
O2—Ti_m1(1)—O2ii | 180.0 (5) | O7—O6—Ohii | 111.2 (6) |
O2—Ti_m1(1)—O3 | 89.5 (2) | O7—O6—Ohv | 149.2 (4) |
O2—Ti_m1(1)—O3ii | 90.5 (2) | O7—O6—W1 | 86.8 (3) |
O2—Ti_m1(1)—O6 | 117.1 (3) | O7—O6—Nb_m1(1) | 77.8 (4) |
O2—Ti_m1(1)—O6ii | 62.9 (3) | Ohii—O6—Ohv | 89.2 (3) |
O2—Ti_m1(1)—Oh | 90.3 (4) | Ohii—O6—W1 | 157.2 (4) |
O2—Ti_m1(1)—Ohii | 89.7 (4) | Ohii—O6—Nb_m1(1) | 33.6 (3) |
O2—Ti_m1(1)—Nb_m1(1) | 0 | Ohv—O6—W1 | 68.9 (4) |
O2ii—Ti_m1(1)—O3 | 90.5 (2) | Ohv—O6—Nb_m1(1) | 121.0 (2) |
O2ii—Ti_m1(1)—O3ii | 89.5 (2) | W1—O6—Nb_m1(1) | 161.1 (3) |
O2ii—Ti_m1(1)—O6 | 62.9 (3) | Na_a—O7—Na_aiii | 106.6 (4) |
O2ii—Ti_m1(1)—O6ii | 117.1 (3) | Na_a—O7—Si1 | 82.1 (5) |
O2ii—Ti_m1(1)—Oh | 89.7 (4) | Na_a—O7—Si2iv | 79.4 (5) |
O2ii—Ti_m1(1)—Ohii | 90.3 (4) | Na_a—O7—O1iv | 106.7 (4) |
O2ii—Ti_m1(1)—Nb_m1(1) | 0 | Na_a—O7—O2iv | 45.7 (3) |
O3—Ti_m1(1)—O3ii | 180.0 (5) | Na_a—O7—O2ii | 76.8 (3) |
O3—Ti_m1(1)—O6 | 49.5 (4) | Na_a—O7—O3 | 105.5 (4) |
O3—Ti_m1(1)—O6ii | 130.5 (4) | Na_a—O7—O4 | 92.3 (5) |
O3—Ti_m1(1)—Oh | 88.7 (4) | Na_a—O7—O5iv | 89.8 (5) |
O3—Ti_m1(1)—Ohii | 91.3 (4) | Na_a—O7—O6 | 47.5 (3) |
O3—Ti_m1(1)—Nb_m1(1) | 0 | Na_a—O7—O7iii | 42.7 (3) |
O3ii—Ti_m1(1)—O6 | 130.5 (4) | Na_a—O7—O7vi | 125.2 (5) |
O3ii—Ti_m1(1)—O6ii | 49.5 (4) | Na_a—O7—W2 | 147.4 (4) |
O3ii—Ti_m1(1)—Oh | 91.3 (4) | Na_aiii—O7—Si1 | 115.1 (5) |
O3ii—Ti_m1(1)—Ohii | 88.7 (4) | Na_aiii—O7—Si2iv | 101.3 (4) |
O3ii—Ti_m1(1)—Nb_m1(1) | 0 | Na_aiii—O7—O1iv | 70.6 (4) |
O6—Ti_m1(1)—O6ii | 180.0 (5) | Na_aiii—O7—O2iv | 101.1 (4) |
O6—Ti_m1(1)—Oh | 125.9 (3) | Na_aiii—O7—O2ii | 48.7 (3) |
O6—Ti_m1(1)—Ohii | 54.1 (3) | Na_aiii—O7—O3 | 85.1 (4) |
O6—Ti_m1(1)—Nb_m1(1) | 0 | Na_aiii—O7—O4 | 143.7 (6) |
O6ii—Ti_m1(1)—Oh | 54.1 (3) | Na_aiii—O7—O5iv | 131.8 (4) |
O6ii—Ti_m1(1)—Ohii | 125.9 (3) | Na_aiii—O7—O6 | 114.2 (3) |
O6ii—Ti_m1(1)—Nb_m1(1) | 0 | Na_aiii—O7—O7iii | 63.9 (4) |
Oh—Ti_m1(1)—Ohii | 180.0 (5) | Na_aiii—O7—O7vi | 127.5 (6) |
Oh—Ti_m1(1)—Nb_m1(1) | 0 | Na_aiii—O7—W2 | 40.9 (4) |
Ohii—Ti_m1(1)—Nb_m1(1) | 0 | Si1—O7—Si2iv | 142.5 (9) |
Na_aii—Ti_m1(2)—Na_ax | 174.58 (17) | Si1—O7—O1iv | 168.2 (3) |
Na_aii—Ti_m1(2)—Fe_m2 | 92.71 (12) | Si1—O7—O2iv | 123.7 (7) |
Na_aii—Ti_m1(2)—Si1ii | 62.3 (2) | Si1—O7—O2ii | 73.6 (2) |
Na_aii—Ti_m1(2)—Si1x | 113.6 (2) | Si1—O7—O3 | 33.7 (4) |
Na_aii—Ti_m1(2)—Si2 | 57.7 (3) | Si1—O7—O4 | 36.1 (2) |
Na_aii—Ti_m1(2)—Si2xi | 125.5 (3) | Si1—O7—O5iv | 111.8 (5) |
Na_aii—Ti_m1(2)—O1 | 59.1 (3) | Si1—O7—O6 | 35.0 (3) |
Na_aii—Ti_m1(2)—O1xi | 125.7 (3) | Si1—O7—O7iii | 99.8 (3) |
Na_aii—Ti_m1(2)—O2 | 69.9 (4) | Si1—O7—O7vi | 82.7 (2) |
Na_aii—Ti_m1(2)—O2xi | 110.9 (4) | Si1—O7—W2 | 110.6 (5) |
Na_aii—Ti_m1(2)—O6ii | 45.1 (3) | Si2iv—O7—O1iv | 36.6 (4) |
Na_aii—Ti_m1(2)—O6x | 130.1 (3) | Si2iv—O7—O2iv | 34.6 (3) |
Na_aii—Ti_m1(2)—Oh | 120.6 (4) | Si2iv—O7—O2ii | 131.9 (3) |
Na_aii—Ti_m1(2)—Ohxi | 59.6 (4) | Si2iv—O7—O3 | 170.6 (3) |
Na_aii—Ti_m1(2)—Ti_m2 | 92.71 (12) | Si2iv—O7—O4 | 112.6 (5) |
Na_aii—Ti_m1(2)—Mg_m2 | 92.71 (12) | Si2iv—O7—O5iv | 36.5 (2) |
Na_ax—Ti_m1(2)—Fe_m2 | 92.71 (12) | Si2iv—O7—O6 | 121.5 (7) |
Na_ax—Ti_m1(2)—Si1ii | 113.6 (2) | Si2iv—O7—O7iii | 88.1 (3) |
Na_ax—Ti_m1(2)—Si1x | 62.3 (2) | Si2iv—O7—O7vi | 81.9 (2) |
Na_ax—Ti_m1(2)—Si2 | 125.5 (3) | Si2iv—O7—W2 | 102.5 (5) |
Na_ax—Ti_m1(2)—Si2xi | 57.7 (3) | O1iv—O7—O2iv | 62.5 (4) |
Na_ax—Ti_m1(2)—O1 | 125.7 (3) | O1iv—O7—O2ii | 115.7 (4) |
Na_ax—Ti_m1(2)—O1xi | 59.1 (3) | O1iv—O7—O3 | 144.0 (7) |
Na_ax—Ti_m1(2)—O2 | 110.9 (4) | O1iv—O7—O4 | 133.7 (3) |
Na_ax—Ti_m1(2)—O2xi | 69.9 (4) | O1iv—O7—O5iv | 61.3 (4) |
Na_ax—Ti_m1(2)—O6ii | 130.1 (3) | O1iv—O7—O6 | 154.1 (5) |
Na_ax—Ti_m1(2)—O6x | 45.1 (3) | O1iv—O7—O7iii | 91.95 (19) |
Na_ax—Ti_m1(2)—Oh | 59.6 (4) | O1iv—O7—O7vi | 85.73 (19) |
Na_ax—Ti_m1(2)—Ohxi | 120.6 (4) | O1iv—O7—W2 | 66.3 (4) |
Na_ax—Ti_m1(2)—Ti_m2 | 92.71 (12) | O2iv—O7—O2ii | 105.9 (3) |
Na_ax—Ti_m1(2)—Mg_m2 | 92.71 (12) | O2iv—O7—O3 | 151.2 (5) |
Fe_m2—Ti_m1(2)—Si1ii | 133.43 (6) | O2iv—O7—O4 | 114.0 (6) |
Fe_m2—Ti_m1(2)—Si1x | 133.43 (6) | O2iv—O7—O5iv | 59.2 (3) |
Fe_m2—Ti_m1(2)—Si2 | 61.11 (5) | O2iv—O7—O6 | 91.8 (5) |
Fe_m2—Ti_m1(2)—Si2xi | 61.11 (5) | O2iv—O7—O7iii | 58.8 (2) |
Fe_m2—Ti_m1(2)—O1 | 41.05 (16) | O2iv—O7—O7vi | 108.4 (3) |
Fe_m2—Ti_m1(2)—O1xi | 41.05 (16) | O2iv—O7—W2 | 124.8 (3) |
Fe_m2—Ti_m1(2)—O2 | 81.79 (8) | O2ii—O7—O3 | 57.49 (18) |
Fe_m2—Ti_m1(2)—O2xi | 81.79 (8) | O2ii—O7—O4 | 109.6 (2) |
Fe_m2—Ti_m1(2)—O6ii | 130.65 (16) | O2ii—O7—O5iv | 165.0 (5) |
Fe_m2—Ti_m1(2)—O6x | 130.65 (16) | O2ii—O7—O6 | 65.6 (3) |
Fe_m2—Ti_m1(2)—Oh | 88.35 (14) | O2ii—O7—O7iii | 47.1 (2) |
Fe_m2—Ti_m1(2)—Ohxi | 88.35 (14) | O2ii—O7—O7vi | 145.2 (3) |
Fe_m2—Ti_m1(2)—Ti_m2 | 0.0 (5) | O2ii—O7—W2 | 78.4 (4) |
Fe_m2—Ti_m1(2)—Mg_m2 | 0.0 (5) | O3—O7—O4 | 59.7 (4) |
Si1ii—Ti_m1(2)—Si1x | 93.14 (11) | O3—O7—O5iv | 134.5 (3) |
Si1ii—Ti_m1(2)—Si2 | 72.37 (9) | O3—O7—O6 | 60.4 (4) |
Si1ii—Ti_m1(2)—Si2xi | 165.27 (7) | O3—O7—O7iii | 100.9 (2) |
Si1ii—Ti_m1(2)—O1 | 94.0 (2) | O3—O7—O7vi | 88.8 (2) |
Si1ii—Ti_m1(2)—O1xi | 165.1 (4) | O3—O7—W2 | 77.9 (4) |
Si1ii—Ti_m1(2)—O2 | 53.62 (11) | O4—O7—O5iv | 77.4 (3) |
Si1ii—Ti_m1(2)—O2xi | 142.14 (12) | O4—O7—O6 | 57.9 (3) |
Si1ii—Ti_m1(2)—O6ii | 19.6 (4) | O4—O7—O7iii | 127.4 (4) |
Si1ii—Ti_m1(2)—O6x | 92.6 (2) | O4—O7—O7vi | 49.9 (2) |
Si1ii—Ti_m1(2)—Oh | 74.84 (18) | O4—O7—W2 | 115.8 (5) |
Si1ii—Ti_m1(2)—Ohxi | 107.53 (18) | O5iv—O7—O6 | 110.2 (6) |
Si1ii—Ti_m1(2)—Ti_m2 | 133.43 (6) | O5iv—O7—O7iii | 117.9 (4) |
Si1ii—Ti_m1(2)—Mg_m2 | 133.43 (6) | O5iv—O7—O7vi | 49.3 (3) |
Si1x—Ti_m1(2)—Si2 | 165.27 (7) | O5iv—O7—W2 | 111.2 (5) |
Si1x—Ti_m1(2)—Si2xi | 72.37 (9) | O6—O7—O7iii | 69.9 (2) |
Si1x—Ti_m1(2)—O1 | 165.1 (4) | O6—O7—O7vi | 107.3 (3) |
Si1x—Ti_m1(2)—O1xi | 94.0 (2) | O6—O7—W2 | 134.9 (4) |
Si1x—Ti_m1(2)—O2 | 142.14 (12) | O7iii—O7—O7vi | 166.1 (5) |
Si1x—Ti_m1(2)—O2xi | 53.62 (11) | O7iii—O7—W2 | 104.8 (4) |
Si1x—Ti_m1(2)—O6ii | 92.6 (2) | O7vi—O7—W2 | 86.8 (4) |
Si1x—Ti_m1(2)—O6x | 19.6 (4) | Na_aiii—Oh—Na_ax | 49.1 (5) |
Si1x—Ti_m1(2)—Oh | 107.53 (18) | Na_aiii—Oh—Ti_m1(1) | 89.2 (5) |
Si1x—Ti_m1(2)—Ohxi | 74.84 (18) | Na_aiii—Oh—Ti_m1(2) | 134.6 (5) |
Si1x—Ti_m1(2)—Ti_m2 | 133.43 (6) | Na_aiii—Oh—Si1ii | 129.0 (3) |
Si1x—Ti_m1(2)—Mg_m2 | 133.43 (6) | Na_aiii—Oh—Si2 | 146.4 (4) |
Si2—Ti_m1(2)—Si2xi | 122.22 (9) | Na_aiii—Oh—O1 | 150.0 (2) |
Si2—Ti_m1(2)—O1 | 24.0 (3) | Na_aiii—Oh—O1xi | 101.8 (4) |
Si2—Ti_m1(2)—O1xi | 100.7 (2) | Na_aiii—Oh—O2 | 130.3 (6) |
Si2—Ti_m1(2)—O2 | 27.23 (13) | Na_aiii—Oh—O2ii | 48.0 (3) |
Si2—Ti_m1(2)—O2xi | 138.69 (12) | Na_aiii—Oh—O3 | 73.7 (4) |
Si2—Ti_m1(2)—O6ii | 72.8 (2) | Na_aiii—Oh—O3ii | 104.8 (4) |
Si2—Ti_m1(2)—O6x | 157.6 (4) | Na_aiii—Oh—O6ii | 147.0 (3) |
Si2—Ti_m1(2)—Oh | 71.86 (19) | Na_aiii—Oh—O6x | 93.8 (4) |
Si2—Ti_m1(2)—Ohxi | 106.5 (2) | Na_aiii—Oh—Ba | 88.0 (2) |
Si2—Ti_m1(2)—Ti_m2 | 61.11 (5) | Na_aiii—Oh—W1iii | 37.5 (3) |
Si2—Ti_m1(2)—Mg_m2 | 61.11 (5) | Na_aiii—Oh—W2 | 39.9 (3) |
Si2xi—Ti_m1(2)—O1 | 100.7 (2) | Na_aiii—Oh—W_c | 88.0 (2) |
Si2xi—Ti_m1(2)—O1xi | 24.0 (3) | Na_aiii—Oh—Nb_m1(1) | 89.2 (5) |
Si2xi—Ti_m1(2)—O2 | 138.69 (12) | Na_ax—Oh—Ti_m1(1) | 136.4 (5) |
Si2xi—Ti_m1(2)—O2xi | 27.23 (13) | Na_ax—Oh—Ti_m1(2) | 85.6 (5) |
Si2xi—Ti_m1(2)—O6ii | 157.6 (4) | Na_ax—Oh—Si1ii | 125.3 (3) |
Si2xi—Ti_m1(2)—O6x | 72.8 (2) | Na_ax—Oh—Si2 | 146.8 (4) |
Si2xi—Ti_m1(2)—Oh | 106.5 (2) | Na_ax—Oh—O1 | 118.2 (5) |
Si2xi—Ti_m1(2)—Ohxi | 71.86 (19) | Na_ax—Oh—O1xi | 61.0 (4) |
Si2xi—Ti_m1(2)—Ti_m2 | 61.11 (5) | Na_ax—Oh—O2 | 174.9 (2) |
Si2xi—Ti_m1(2)—Mg_m2 | 61.11 (5) | Na_ax—Oh—O2ii | 91.0 (4) |
O1—Ti_m1(2)—O1xi | 82.1 (2) | Na_ax—Oh—O3 | 116.4 (4) |
O1—Ti_m1(2)—O2 | 50.7 (4) | Na_ax—Oh—O3ii | 124.4 (2) |
O1—Ti_m1(2)—O2xi | 114.7 (3) | Na_ax—Oh—O6ii | 115.2 (5) |
O1—Ti_m1(2)—O6ii | 89.8 (2) | Na_ax—Oh—O6x | 51.2 (4) |
O1—Ti_m1(2)—O6x | 170.6 (2) | Na_ax—Oh—Ba | 88.1 (2) |
O1—Ti_m1(2)—Oh | 87.0 (4) | Na_ax—Oh—W1iii | 37.9 (3) |
O1—Ti_m1(2)—Ohxi | 90.5 (4) | Na_ax—Oh—W2 | 40.5 (3) |
O1—Ti_m1(2)—Ti_m2 | 41.05 (16) | Na_ax—Oh—W_c | 88.1 (2) |
O1—Ti_m1(2)—Mg_m2 | 41.05 (16) | Na_ax—Oh—Nb_m1(1) | 136.4 (5) |
O1xi—Ti_m1(2)—O2 | 114.7 (3) | Ti_m1(1)—Oh—Ti_m1(2) | 133.2 (3) |
O1xi—Ti_m1(2)—O2xi | 50.7 (4) | Ti_m1(1)—Oh—Si1ii | 67.15 (16) |
O1xi—Ti_m1(2)—O6ii | 170.6 (2) | Ti_m1(1)—Oh—Si2 | 74.7 (2) |
O1xi—Ti_m1(2)—O6x | 89.8 (2) | Ti_m1(1)—Oh—O1 | 104.6 (3) |
O1xi—Ti_m1(2)—Oh | 90.5 (4) | Ti_m1(1)—Oh—O1xi | 158.0 (3) |
O1xi—Ti_m1(2)—Ohxi | 87.0 (4) | Ti_m1(1)—Oh—O2 | 45.3 (3) |
O1xi—Ti_m1(2)—Ti_m2 | 41.05 (16) | Ti_m1(1)—Oh—O2ii | 45.6 (3) |
O1xi—Ti_m1(2)—Mg_m2 | 41.05 (16) | Ti_m1(1)—Oh—O3 | 46.4 (3) |
O2—Ti_m1(2)—O2xi | 163.58 (12) | Ti_m1(1)—Oh—O3ii | 45.0 (3) |
O2—Ti_m1(2)—O6ii | 62.4 (4) | Ti_m1(1)—Oh—O6ii | 92.3 (3) |
O2—Ti_m1(2)—O6x | 130.5 (4) | Ti_m1(1)—Oh—O6x | 138.2 (3) |
O2—Ti_m1(2)—Oh | 51.5 (2) | Ti_m1(1)—Oh—Ba | 105.0 (3) |
O2—Ti_m1(2)—Ohxi | 127.9 (2) | Ti_m1(1)—Oh—W1iii | 102.3 (3) |
O2—Ti_m1(2)—Ti_m2 | 81.79 (8) | Ti_m1(1)—Oh—W2 | 116.9 (4) |
O2—Ti_m1(2)—Mg_m2 | 81.79 (8) | Ti_m1(1)—Oh—W_c | 105.0 (3) |
O2xi—Ti_m1(2)—O6ii | 130.5 (4) | Ti_m1(1)—Oh—Nb_m1(1) | 0.0 (5) |
O2xi—Ti_m1(2)—O6x | 62.4 (4) | Ti_m1(2)—Oh—Si1ii | 71.0 (2) |
O2xi—Ti_m1(2)—Oh | 127.9 (2) | Ti_m1(2)—Oh—Si2 | 73.2 (2) |
O2xi—Ti_m1(2)—Ohxi | 51.5 (2) | Ti_m1(2)—Oh—O1 | 47.9 (3) |
O2xi—Ti_m1(2)—Ti_m2 | 81.79 (8) | Ti_m1(2)—Oh—O1xi | 46.0 (3) |
O2xi—Ti_m1(2)—Mg_m2 | 81.79 (8) | Ti_m1(2)—Oh—O2 | 95.1 (3) |
O6ii—Ti_m1(2)—O6x | 98.7 (2) | Ti_m1(2)—Oh—O2ii | 151.0 (3) |
O6ii—Ti_m1(2)—Oh | 93.7 (4) | Ti_m1(2)—Oh—O3 | 144.3 (3) |
O6ii—Ti_m1(2)—Ohxi | 88.4 (4) | Ti_m1(2)—Oh—O3ii | 98.7 (3) |
O6ii—Ti_m1(2)—Ti_m2 | 130.65 (16) | Ti_m1(2)—Oh—O6ii | 43.0 (3) |
O6ii—Ti_m1(2)—Mg_m2 | 130.65 (16) | Ti_m1(2)—Oh—O6x | 45.6 (3) |
O6x—Ti_m1(2)—Oh | 88.4 (4) | Ti_m1(2)—Oh—Ba | 93.9 (3) |
O6x—Ti_m1(2)—Ohxi | 93.7 (4) | Ti_m1(2)—Oh—W1iii | 106.1 (3) |
O6x—Ti_m1(2)—Ti_m2 | 130.65 (16) | Ti_m1(2)—Oh—W2 | 109.0 (4) |
O6x—Ti_m1(2)—Mg_m2 | 130.65 (16) | Ti_m1(2)—Oh—W_c | 93.9 (3) |
Oh—Ti_m1(2)—Ohxi | 176.7 (2) | Ti_m1(2)—Oh—Nb_m1(1) | 133.2 (3) |
Oh—Ti_m1(2)—Ti_m2 | 88.35 (14) | Si1ii—Oh—Si2 | 71.78 (11) |
Oh—Ti_m1(2)—Mg_m2 | 88.35 (14) | Si1ii—Oh—O1 | 80.99 (19) |
Ohxi—Ti_m1(2)—Ti_m2 | 88.35 (14) | Si1ii—Oh—O1xi | 117.0 (4) |
Ohxi—Ti_m1(2)—Mg_m2 | 88.35 (14) | Si1ii—Oh—O2 | 59.48 (16) |
Ti_m2—Ti_m1(2)—Mg_m2 | 0.0 (5) | Si1ii—Oh—O2ii | 87.9 (2) |
Ti_m1(2)—Fe_m2—Ti_m1(2)xii | 180.0 (5) | Si1ii—Oh—O3 | 110.6 (3) |
Ti_m1(2)—Fe_m2—Si2 | 62.20 (5) | Si1ii—Oh—O3ii | 28.2 (3) |
Ti_m1(2)—Fe_m2—Si2xi | 62.20 (5) | Si1ii—Oh—O6ii | 28.4 (2) |
Ti_m1(2)—Fe_m2—Si2xii | 117.80 (5) | Si1ii—Oh—O6x | 79.1 (2) |
Ti_m1(2)—Fe_m2—Si2vi | 117.80 (5) | Si1ii—Oh—Ba | 140.34 (17) |
Ti_m1(2)—Fe_m2—O1 | 41.05 (16) | Si1ii—Oh—W1iii | 102.15 (19) |
Ti_m1(2)—Fe_m2—O1xi | 41.05 (16) | Si1ii—Oh—W2 | 164.3 (2) |
Ti_m1(2)—Fe_m2—O1xii | 138.95 (16) | Si1ii—Oh—W_c | 140.34 (17) |
Ti_m1(2)—Fe_m2—O1vi | 138.95 (16) | Si1ii—Oh—Nb_m1(1) | 67.15 (16) |
Ti_m1(2)—Fe_m2—O5 | 90 | Si2—Oh—O1 | 30.1 (3) |
Ti_m1(2)—Fe_m2—O5xi | 90 | Si2—Oh—O1xi | 86.0 (2) |
Ti_m1(2)—Fe_m2—Ba | 90 | Si2—Oh—O2 | 30.0 (2) |
Ti_m1(2)—Fe_m2—Baxi | 90 | Si2—Oh—O2ii | 119.9 (4) |
Ti_m1(2)—Fe_m2—W_c | 90 | Si2—Oh—O3 | 73.9 (2) |
Ti_m1(2)—Fe_m2—W_cxi | 90 | Si2—Oh—O3ii | 84.63 (17) |
Ti_m1(2)—Fe_m2—Ti_m2 | 0 | Si2—Oh—O6ii | 64.59 (17) |
Ti_m1(2)—Fe_m2—Mg_m2 | 0 | Si2—Oh—O6x | 118.0 (4) |
Ti_m1(2)xii—Fe_m2—Si2 | 117.80 (5) | Si2—Oh—Ba | 68.72 (10) |
Ti_m1(2)xii—Fe_m2—Si2xi | 117.80 (5) | Si2—Oh—W1iii | 173.9 (2) |
Ti_m1(2)xii—Fe_m2—Si2xii | 62.20 (5) | Si2—Oh—W2 | 123.7 (2) |
Ti_m1(2)xii—Fe_m2—Si2vi | 62.20 (5) | Si2—Oh—W_c | 68.72 (10) |
Ti_m1(2)xii—Fe_m2—O1 | 138.95 (16) | Si2—Oh—Nb_m1(1) | 74.7 (2) |
Ti_m1(2)xii—Fe_m2—O1xi | 138.95 (16) | O1—Oh—O1xi | 57.3 (3) |
Ti_m1(2)xii—Fe_m2—O1xii | 41.05 (16) | O1—Oh—O2 | 59.4 (3) |
Ti_m1(2)xii—Fe_m2—O1vi | 41.05 (16) | O1—Oh—O2ii | 150.0 (5) |
Ti_m1(2)xii—Fe_m2—O5 | 90 | O1—Oh—O3 | 96.5 (3) |
Ti_m1(2)xii—Fe_m2—O5xi | 90 | O1—Oh—O3ii | 103.7 (2) |
Ti_m1(2)xii—Fe_m2—Ba | 90 | O1—Oh—O6ii | 60.4 (2) |
Ti_m1(2)xii—Fe_m2—Baxi | 90 | O1—Oh—O6x | 93.2 (5) |
Ti_m1(2)xii—Fe_m2—W_c | 90 | O1—Oh—Ba | 62.93 (17) |
Ti_m1(2)xii—Fe_m2—W_cxi | 90 | O1—Oh—W1iii | 151.8 (5) |
Ti_m1(2)xii—Fe_m2—Ti_m2 | 0 | O1—Oh—W2 | 111.1 (3) |
Ti_m1(2)xii—Fe_m2—Mg_m2 | 0 | O1—Oh—W_c | 62.93 (17) |
Si2—Fe_m2—Si2xi | 124.40 (8) | O1—Oh—Nb_m1(1) | 104.6 (3) |
Si2—Fe_m2—Si2xii | 180.0 (5) | O1xi—Oh—O2 | 116.1 (3) |
Si2—Fe_m2—Si2vi | 55.60 (8) | O1xi—Oh—O2ii | 149.7 (2) |
Si2—Fe_m2—O1 | 24.9 (3) | O1xi—Oh—O3 | 118.4 (3) |
Si2—Fe_m2—O1xi | 101.7 (2) | O1xi—Oh—O3ii | 144.7 (5) |
Si2—Fe_m2—O1xii | 155.1 (3) | O1xi—Oh—O6ii | 88.7 (4) |
Si2—Fe_m2—O1vi | 78.3 (2) | O1xi—Oh—O6x | 60.8 (3) |
Si2—Fe_m2—O5 | 29.51 (10) | O1xi—Oh—Ba | 57.1 (2) |
Si2—Fe_m2—O5xi | 150.49 (10) | O1xi—Oh—W1iii | 97.8 (3) |
Si2—Fe_m2—Ba | 80.55 (12) | O1xi—Oh—W2 | 65.5 (2) |
Si2—Fe_m2—Baxi | 99.45 (12) | O1xi—Oh—W_c | 57.1 (2) |
Si2—Fe_m2—W_c | 80.55 (12) | O1xi—Oh—Nb_m1(1) | 158.0 (3) |
Si2—Fe_m2—W_cxi | 99.45 (12) | O2—Oh—O2ii | 90.9 (4) |
Si2—Fe_m2—Ti_m2 | 0 | O2—Oh—O3 | 60.6 (3) |
Si2—Fe_m2—Mg_m2 | 0 | O2—Oh—O3ii | 60.5 (2) |
Si2xi—Fe_m2—Si2xii | 55.60 (8) | O2—Oh—O6ii | 68.1 (3) |
Si2xi—Fe_m2—Si2vi | 180.0 (5) | O2—Oh—O6x | 132.0 (4) |
Si2xi—Fe_m2—O1 | 101.7 (2) | O2—Oh—Ba | 86.80 (17) |
Si2xi—Fe_m2—O1xi | 24.9 (3) | O2—Oh—W1iii | 145.8 (4) |
Si2xi—Fe_m2—O1xii | 78.3 (2) | O2—Oh—W2 | 135.0 (3) |
Si2xi—Fe_m2—O1vi | 155.1 (3) | O2—Oh—W_c | 86.80 (17) |
Si2xi—Fe_m2—O5 | 150.49 (10) | O2—Oh—Nb_m1(1) | 45.3 (3) |
Si2xi—Fe_m2—O5xi | 29.51 (10) | O2ii—Oh—O3 | 61.4 (3) |
Si2xi—Fe_m2—Ba | 99.45 (12) | O2ii—Oh—O3ii | 60.0 (3) |
Si2xi—Fe_m2—Baxi | 80.55 (12) | O2ii—Oh—O6ii | 115.6 (3) |
Si2xi—Fe_m2—W_c | 99.45 (12) | O2ii—Oh—O6x | 112.1 (3) |
Si2xi—Fe_m2—W_cxi | 80.55 (12) | O2ii—Oh—Ba | 114.8 (4) |
Si2xi—Fe_m2—Ti_m2 | 0 | O2ii—Oh—W1iii | 57.9 (2) |
Si2xi—Fe_m2—Mg_m2 | 0 | O2ii—Oh—W2 | 85.8 (3) |
Si2xii—Fe_m2—Si2vi | 124.40 (8) | O2ii—Oh—W_c | 114.8 (4) |
Si2xii—Fe_m2—O1 | 155.1 (3) | O2ii—Oh—Nb_m1(1) | 45.6 (3) |
Si2xii—Fe_m2—O1xi | 78.3 (2) | O3—Oh—O3ii | 91.4 (4) |
Si2xii—Fe_m2—O1xii | 24.9 (3) | O3—Oh—O6ii | 128.3 (3) |
Si2xii—Fe_m2—O1vi | 101.7 (2) | O3—Oh—O6x | 167.2 (3) |
Si2xii—Fe_m2—O5 | 150.49 (10) | O3—Oh—Ba | 61.3 (2) |
Si2xii—Fe_m2—O5xi | 29.51 (10) | O3—Oh—W1iii | 108.1 (3) |
Si2xii—Fe_m2—Ba | 99.45 (12) | O3—Oh—W2 | 78.8 (2) |
Si2xii—Fe_m2—Baxi | 80.55 (12) | O3—Oh—W_c | 61.3 (2) |
Si2xii—Fe_m2—W_c | 99.45 (12) | O3—Oh—Nb_m1(1) | 46.4 (3) |
Si2xii—Fe_m2—W_cxi | 80.55 (12) | O3ii—Oh—O6ii | 56.6 (3) |
Si2xii—Fe_m2—Ti_m2 | 0 | O3ii—Oh—O6x | 94.4 (3) |
Si2xii—Fe_m2—Mg_m2 | 0 | O3ii—Oh—Ba | 145.7 (4) |
Si2vi—Fe_m2—O1 | 78.3 (2) | O3ii—Oh—W1iii | 89.5 (2) |
Si2vi—Fe_m2—O1xi | 155.1 (3) | O3ii—Oh—W2 | 144.6 (4) |
Si2vi—Fe_m2—O1xii | 101.7 (2) | O3ii—Oh—W_c | 145.7 (4) |
Si2vi—Fe_m2—O1vi | 24.9 (3) | O3ii—Oh—Nb_m1(1) | 45.0 (3) |
Si2vi—Fe_m2—O5 | 29.51 (10) | O6ii—Oh—O6x | 64.0 (3) |
Si2vi—Fe_m2—O5xi | 150.49 (10) | O6ii—Oh—Ba | 123.2 (3) |
Si2vi—Fe_m2—Ba | 80.55 (12) | O6ii—Oh—W1iii | 110.5 (3) |
Si2vi—Fe_m2—Baxi | 99.45 (12) | O6ii—Oh—W2 | 150.6 (5) |
Si2vi—Fe_m2—W_c | 80.55 (12) | O6ii—Oh—W_c | 123.2 (3) |
Si2vi—Fe_m2—W_cxi | 99.45 (12) | O6ii—Oh—Nb_m1(1) | 92.3 (3) |
Si2vi—Fe_m2—Ti_m2 | 0 | O6x—Oh—Ba | 116.8 (4) |
Si2vi—Fe_m2—Mg_m2 | 0 | O6x—Oh—W1iii | 60.6 (2) |
O1—Fe_m2—O1xi | 82.1 (2) | O6x—Oh—W2 | 89.9 (3) |
O1—Fe_m2—O1xii | 180.0 (5) | O6x—Oh—W_c | 116.8 (4) |
O1—Fe_m2—O1vi | 97.9 (2) | O6x—Oh—Nb_m1(1) | 138.2 (3) |
O1—Fe_m2—O5 | 54.4 (3) | Ba—Oh—W1iii | 117.4 (2) |
O1—Fe_m2—O5xi | 125.6 (3) | Ba—Oh—W2 | 54.99 (18) |
O1—Fe_m2—Ba | 94.2 (4) | Ba—Oh—W_c | 0.0 (5) |
O1—Fe_m2—Baxi | 85.8 (4) | Ba—Oh—Nb_m1(1) | 105.0 (3) |
O1—Fe_m2—W_c | 94.2 (4) | W1iii—Oh—W2 | 62.4 (2) |
O1—Fe_m2—W_cxi | 85.8 (4) | W1iii—Oh—W_c | 117.4 (2) |
O1—Fe_m2—Ti_m2 | 0 | W1iii—Oh—Nb_m1(1) | 102.3 (3) |
O1—Fe_m2—Mg_m2 | 0 | W2—Oh—W_c | 54.99 (18) |
O1xi—Fe_m2—O1xii | 97.9 (2) | W2—Oh—Nb_m1(1) | 116.9 (4) |
O1xi—Fe_m2—O1vi | 180.0 (5) | W_c—Oh—Nb_m1(1) | 105.0 (3) |
O1xi—Fe_m2—O5 | 125.6 (3) | Fe_m2—Ba—O1 | 42.1 (2) |
O1xi—Fe_m2—O5xi | 54.4 (3) | Fe_m2—Ba—O1xi | 46.26 (17) |
O1xi—Fe_m2—Ba | 85.8 (4) | Fe_m2—Ba—O1xii | 46.26 (17) |
O1xi—Fe_m2—Baxi | 94.2 (4) | Fe_m2—Ba—O1vi | 42.1 (2) |
O1xi—Fe_m2—W_c | 85.8 (4) | Fe_m2—Ba—O3 | 128.37 (16) |
O1xi—Fe_m2—W_cxi | 94.2 (4) | Fe_m2—Ba—O3vi | 128.37 (16) |
O1xi—Fe_m2—Ti_m2 | 0 | Fe_m2—Ba—O5 | 73.4 (4) |
O1xi—Fe_m2—Mg_m2 | 0 | Fe_m2—Ba—Oh | 86.8 (2) |
O1xii—Fe_m2—O1vi | 82.1 (2) | Fe_m2—Ba—Ohvi | 86.8 (2) |
O1xii—Fe_m2—O5 | 125.6 (3) | Fe_m2—Ba—W2 | 114.75 (16) |
O1xii—Fe_m2—O5xi | 54.4 (3) | Fe_m2—Ba—W2xiv | 114.75 (16) |
O1xii—Fe_m2—Ba | 85.8 (4) | Fe_m2—Ba—W_c | 0 |
O1xii—Fe_m2—Baxi | 94.2 (4) | Fe_m2—Ba—Ti_m2 | 0.0 (5) |
O1xii—Fe_m2—W_c | 85.8 (4) | Fe_m2—Ba—Mg_m2 | 0.0 (5) |
O1xii—Fe_m2—W_cxi | 94.2 (4) | O1—Ba—O1xi | 54.4 (2) |
O1xii—Fe_m2—Ti_m2 | 0 | O1—Ba—O1xii | 88.4 (3) |
O1xii—Fe_m2—Mg_m2 | 0 | O1—Ba—O1vi | 60.99 (15) |
O1vi—Fe_m2—O5 | 54.4 (3) | O1—Ba—O3 | 86.3 (3) |
O1vi—Fe_m2—O5xi | 125.6 (3) | O1—Ba—O3vi | 120.6 (2) |
O1vi—Fe_m2—Ba | 94.2 (4) | O1—Ba—O5 | 50.8 (3) |
O1vi—Fe_m2—Baxi | 85.8 (4) | O1—Ba—Oh | 53.78 (19) |
O1vi—Fe_m2—W_c | 94.2 (4) | O1—Ba—Ohvi | 114.65 (19) |
O1vi—Fe_m2—W_cxi | 85.8 (4) | O1—Ba—W2 | 110.41 (18) |
O1vi—Fe_m2—Ti_m2 | 0 | O1—Ba—W2xiv | 155.1 (3) |
O1vi—Fe_m2—Mg_m2 | 0 | O1—Ba—W_c | 0 |
O5—Fe_m2—O5xi | 180.0 (5) | O1—Ba—Ti_m2 | 42.1 (2) |
O5—Fe_m2—Ba | 69.0 (3) | O1—Ba—Mg_m2 | 42.1 (2) |
O5—Fe_m2—Baxi | 111.0 (3) | O1xi—Ba—O1xii | 66.2 (3) |
O5—Fe_m2—W_c | 69.0 (3) | O1xi—Ba—O1vi | 88.4 (3) |
O5—Fe_m2—W_cxi | 111.0 (3) | O1xi—Ba—O3 | 112.1 (2) |
O5—Fe_m2—Ti_m2 | 0 | O1xi—Ba—O3vi | 174.20 (18) |
O5—Fe_m2—Mg_m2 | 0 | O1xi—Ba—O5 | 104.8 (3) |
O5xi—Fe_m2—Ba | 111.0 (3) | O1xi—Ba—Oh | 57.8 (3) |
O5xi—Fe_m2—Baxi | 69.0 (3) | O1xi—Ba—Ohvi | 123.5 (3) |
O5xi—Fe_m2—W_c | 111.0 (3) | O1xi—Ba—W2 | 69.35 (17) |
O5xi—Fe_m2—W_cxi | 69.0 (3) | O1xi—Ba—W2xiv | 104.36 (18) |
O5xi—Fe_m2—Ti_m2 | 0 | O1xi—Ba—W_c | 0 |
O5xi—Fe_m2—Mg_m2 | 0 | O1xi—Ba—Ti_m2 | 46.26 (17) |
Ba—Fe_m2—Baxi | 180.0 (5) | O1xi—Ba—Mg_m2 | 46.26 (17) |
Ba—Fe_m2—W_c | 0.0 (5) | O1xii—Ba—O1vi | 54.4 (2) |
Ba—Fe_m2—W_cxi | 180.0 (5) | O1xii—Ba—O3 | 174.20 (18) |
Ba—Fe_m2—Ti_m2 | 0 | O1xii—Ba—O3vi | 112.1 (2) |
Ba—Fe_m2—Mg_m2 | 0 | O1xii—Ba—O5 | 104.8 (3) |
Baxi—Fe_m2—W_c | 180.0 (5) | O1xii—Ba—Oh | 123.5 (3) |
Baxi—Fe_m2—W_cxi | 0.0 (5) | O1xii—Ba—Ohvi | 57.8 (3) |
Baxi—Fe_m2—Ti_m2 | 0 | O1xii—Ba—W2 | 104.36 (18) |
Baxi—Fe_m2—Mg_m2 | 0 | O1xii—Ba—W2xiv | 69.35 (17) |
W_c—Fe_m2—W_cxi | 180.0 (5) | O1xii—Ba—W_c | 0 |
W_c—Fe_m2—Ti_m2 | 0 | O1xii—Ba—Ti_m2 | 46.26 (17) |
W_c—Fe_m2—Mg_m2 | 0 | O1xii—Ba—Mg_m2 | 46.26 (17) |
W_cxi—Fe_m2—Ti_m2 | 0 | O1vi—Ba—O3 | 120.6 (2) |
W_cxi—Fe_m2—Mg_m2 | 0 | O1vi—Ba—O3vi | 86.3 (3) |
Ti_m2—Fe_m2—Mg_m2 | 0 | O1vi—Ba—O5 | 50.8 (3) |
Na_a—Si1—Na_aiii | 83.4 (4) | O1vi—Ba—Oh | 114.65 (19) |
Na_a—Si1—K_b | 136.1 (3) | O1vi—Ba—Ohvi | 53.78 (19) |
Na_a—Si1—Ti_m1(1) | 105.35 (19) | O1vi—Ba—W2 | 155.1 (3) |
Na_a—Si1—Ti_m1(2)ii | 60.49 (15) | O1vi—Ba—W2xiv | 110.41 (18) |
Na_a—Si1—Si1vi | 127.4 (2) | O1vi—Ba—W_c | 0 |
Na_a—Si1—Si2iv | 61.74 (18) | O1vi—Ba—Ti_m2 | 42.1 (2) |
Na_a—Si1—O2ii | 74.5 (3) | O1vi—Ba—Mg_m2 | 42.1 (2) |
Na_a—Si1—O3 | 137.1 (3) | O3—Ba—O3vi | 68.9 (2) |
Na_a—Si1—O4 | 110.0 (7) | O3—Ba—O5 | 69.9 (3) |
Na_a—Si1—O6 | 39.8 (3) | O3—Ba—Oh | 54.4 (3) |
Na_a—Si1—O7 | 69.8 (4) | O3—Ba—Ohvi | 122.8 (3) |
Na_a—Si1—Ohii | 87.3 (2) | O3—Ba—W2 | 79.70 (16) |
Na_a—Si1—Nb_m1(1) | 105.35 (19) | O3—Ba—W2xiv | 116.3 (2) |
Na_aiii—Si1—K_b | 131.8 (3) | O3—Ba—W_c | 0 |
Na_aiii—Si1—Ti_m1(1) | 65.04 (19) | O3—Ba—Ti_m2 | 128.37 (16) |
Na_aiii—Si1—Ti_m1(2)ii | 106.96 (17) | O3—Ba—Mg_m2 | 128.37 (16) |
Na_aiii—Si1—Si1vi | 119.3 (2) | O3vi—Ba—O5 | 69.9 (3) |
Na_aiii—Si1—Si2iv | 57.9 (2) | O3vi—Ba—Oh | 122.8 (3) |
Na_aiii—Si1—O2ii | 41.68 (18) | O3vi—Ba—Ohvi | 54.4 (3) |
Na_aiii—Si1—O3 | 76.1 (4) | O3vi—Ba—W2 | 116.3 (2) |
Na_aiii—Si1—O4 | 140.3 (5) | O3vi—Ba—W2xiv | 79.70 (16) |
Na_aiii—Si1—O6 | 108.7 (4) | O3vi—Ba—W_c | 0 |
Na_aiii—Si1—O7 | 39.7 (4) | O3vi—Ba—Ti_m2 | 128.37 (16) |
Na_aiii—Si1—Ohii | 91.2 (2) | O3vi—Ba—Mg_m2 | 128.37 (16) |
Na_aiii—Si1—Nb_m1(1) | 65.04 (19) | O5—Ba—Oh | 83.45 (10) |
K_b—Si1—Ti_m1(1) | 76.36 (11) | O5—Ba—Ohvi | 83.45 (10) |
K_b—Si1—Ti_m1(2)ii | 81.68 (10) | O5—Ba—W2 | 144.3 (2) |
K_b—Si1—Si1vi | 64.07 (5) | O5—Ba—W2xiv | 144.3 (2) |
K_b—Si1—Si2iv | 153.58 (7) | O5—Ba—W_c | 0 |
K_b—Si1—O2ii | 112.41 (15) | O5—Ba—Ti_m2 | 73.4 (4) |
K_b—Si1—O3 | 56.3 (3) | O5—Ba—Mg_m2 | 73.4 (4) |
K_b—Si1—O4 | 62.5 (3) | Oh—Ba—Ohvi | 166.59 (14) |
K_b—Si1—O6 | 97.5 (2) | Oh—Ba—W2 | 63.35 (19) |
K_b—Si1—O7 | 153.6 (4) | Oh—Ba—W2xiv | 130.1 (2) |
K_b—Si1—Ohii | 69.60 (9) | Oh—Ba—W_c | 0 |
K_b—Si1—Nb_m1(1) | 76.36 (11) | Oh—Ba—Ti_m2 | 86.8 (2) |
Ti_m1(1)—Si1—Ti_m1(2)ii | 67.22 (6) | Oh—Ba—Mg_m2 | 86.8 (2) |
Ti_m1(1)—Si1—Si1vi | 127.16 (15) | Ohvi—Ba—W2 | 130.1 (2) |
Ti_m1(1)—Si1—Si2iv | 122.24 (14) | Ohvi—Ba—W2xiv | 63.35 (19) |
Ti_m1(1)—Si1—O2ii | 36.78 (13) | Ohvi—Ba—W_c | 0 |
Ti_m1(1)—Si1—O3 | 31.72 (16) | Ohvi—Ba—Ti_m2 | 86.8 (2) |
Ti_m1(1)—Si1—O4 | 137.9 (4) | Ohvi—Ba—Mg_m2 | 86.8 (2) |
Ti_m1(1)—Si1—O6 | 88.5 (4) | W2—Ba—W2xiv | 66.7 (2) |
Ti_m1(1)—Si1—O7 | 104.7 (4) | W2—Ba—W_c | 0 |
Ti_m1(1)—Si1—Ohii | 34.5 (2) | W2—Ba—Ti_m2 | 114.75 (16) |
Ti_m1(1)—Si1—Nb_m1(1) | 0.0 (5) | W2—Ba—Mg_m2 | 114.75 (16) |
Ti_m1(2)ii—Si1—Si1vi | 133.43 (14) | W2xiv—Ba—W_c | 0 |
Ti_m1(2)ii—Si1—Si2iv | 121.54 (13) | W2xiv—Ba—Ti_m2 | 114.75 (16) |
Ti_m1(2)ii—Si1—O2ii | 67.16 (18) | W2xiv—Ba—Mg_m2 | 114.75 (16) |
Ti_m1(2)ii—Si1—O3 | 89.9 (3) | W_c—Ba—Ti_m2 | 0 |
Ti_m1(2)ii—Si1—O4 | 112.2 (5) | W_c—Ba—Mg_m2 | 0 |
Ti_m1(2)ii—Si1—O6 | 24.1 (3) | Ti_m2—Ba—Mg_m2 | 0.0 (5) |
Ti_m1(2)ii—Si1—O7 | 123.5 (3) | Na_a—W1—Na_ai | 75.1 (7) |
Ti_m1(2)ii—Si1—Ohii | 34.1 (2) | Na_a—W1—K_biv | 125.3 (3) |
Ti_m1(2)ii—Si1—Nb_m1(1) | 67.22 (6) | Na_a—W1—K_bvii | 122.7 (3) |
Si1vi—Si1—Si2iv | 89.63 (6) | Na_a—W1—O2iv | 52.9 (3) |
Si1vi—Si1—O2ii | 153.8 (3) | Na_a—W1—O2vii | 107.2 (5) |
Si1vi—Si1—O3 | 95.5 (2) | Na_a—W1—O6 | 52.9 (4) |
Si1vi—Si1—O4 | 24.2 (6) | Na_a—W1—O6i | 109.5 (5) |
Si1vi—Si1—O6 | 128.5 (4) | Na_a—W1—Ohiii | 65.2 (4) |
Si1vi—Si1—O7 | 97.29 (19) | Na_a—W1—Ohv | 62.0 (3) |
Si1vi—Si1—Ohii | 133.66 (10) | Na_a—W1—W2iii | 37.5 (5) |
Si1vi—Si1—Nb_m1(1) | 127.16 (15) | Na_ai—W1—K_biv | 122.7 (3) |
Si2iv—Si1—O2ii | 89.90 (12) | Na_ai—W1—K_bvii | 125.3 (3) |
Si2iv—Si1—O3 | 129.1 (4) | Na_ai—W1—O2iv | 107.2 (5) |
Si2iv—Si1—O4 | 94.8 (3) | Na_ai—W1—O2vii | 52.9 (3) |
Si2iv—Si1—O6 | 101.3 (3) | Na_ai—W1—O6 | 109.5 (5) |
Si2iv—Si1—O7 | 18.6 (4) | Na_ai—W1—O6i | 52.9 (4) |
Si2iv—Si1—Ohii | 136.61 (10) | Na_ai—W1—Ohiii | 62.0 (3) |
Si2iv—Si1—Nb_m1(1) | 122.24 (14) | Na_ai—W1—Ohv | 65.2 (4) |
O2ii—Si1—O3 | 65.1 (3) | Na_ai—W1—W2iii | 37.5 (5) |
O2ii—Si1—O4 | 174.7 (4) | K_biv—W1—K_bvii | 90.4 (3) |
O2ii—Si1—O6 | 77.2 (4) | K_biv—W1—O2iv | 72.54 (19) |
O2ii—Si1—O7 | 75.6 (3) | K_biv—W1—O2vii | 124.9 (3) |
O2ii—Si1—Ohii | 50.77 (17) | K_biv—W1—O6 | 125.5 (3) |
O2ii—Si1—Nb_m1(1) | 36.78 (13) | K_biv—W1—O6i | 70.03 (19) |
O3—Si1—O4 | 109.9 (5) | K_biv—W1—Ohiii | 78.90 (9) |
O3—Si1—O6 | 113.8 (4) | K_biv—W1—Ohv | 169.3 (3) |
O3—Si1—O7 | 111.2 (6) | K_biv—W1—W2iii | 134.80 (14) |
O3—Si1—Ohii | 56.4 (3) | K_bvii—W1—O2iv | 124.9 (3) |
O3—Si1—Nb_m1(1) | 31.72 (16) | K_bvii—W1—O2vii | 72.54 (19) |
O4—Si1—O6 | 104.3 (7) | K_bvii—W1—O6 | 70.03 (19) |
O4—Si1—O7 | 108.4 (3) | K_bvii—W1—O6i | 125.5 (3) |
O4—Si1—Ohii | 125.6 (3) | K_bvii—W1—Ohiii | 169.3 (3) |
O4—Si1—Nb_m1(1) | 137.9 (4) | K_bvii—W1—Ohv | 78.90 (9) |
O6—Si1—O7 | 108.8 (4) | K_bvii—W1—W2iii | 134.80 (14) |
O6—Si1—Ohii | 57.6 (4) | O2iv—W1—O2vii | 157.7 (4) |
O6—Si1—Nb_m1(1) | 88.5 (4) | O2iv—W1—O6 | 78.5 (2) |
O7—Si1—Ohii | 125.8 (3) | O2iv—W1—O6i | 97.7 (3) |
O7—Si1—Nb_m1(1) | 104.7 (4) | O2iv—W1—Ohiii | 52.1 (3) |
Ohii—Si1—Nb_m1(1) | 34.5 (2) | O2iv—W1—Ohv | 113.4 (3) |
Na_aix—Si2—Na_aii | 89.3 (4) | O2iv—W1—W2iii | 78.8 (2) |
Na_aix—Si2—Ti_m1(1) | 65.08 (18) | O2vii—W1—O6 | 97.7 (3) |
Na_aix—Si2—Ti_m1(2) | 110.80 (18) | O2vii—W1—O6i | 78.5 (2) |
Na_aix—Si2—Fe_m2 | 163.23 (16) | O2vii—W1—Ohiii | 113.4 (3) |
Na_aix—Si2—Si1ix | 64.4 (2) | O2vii—W1—Ohv | 52.1 (3) |
Na_aix—Si2—Si2vi | 128.8 (3) | O2vii—W1—W2iii | 78.8 (2) |
Na_aix—Si2—O1 | 139.9 (3) | O6—W1—O6i | 160.5 (4) |
Na_aix—Si2—O1vi | 156.9 (3) | O6—W1—Ohiii | 116.5 (3) |
Na_aix—Si2—O2 | 39.9 (2) | O6—W1—Ohv | 50.5 (3) |
Na_aix—Si2—O5 | 108.5 (6) | O6—W1—W2iii | 80.2 (2) |
Na_aix—Si2—O6ii | 80.6 (3) | O6i—W1—Ohiii | 50.5 (3) |
Na_aix—Si2—O7ix | 72.4 (5) | O6i—W1—Ohv | 116.5 (3) |
Na_aix—Si2—Oh | 95.7 (2) | O6i—W1—W2iii | 80.2 (2) |
Na_aix—Si2—Nb_m1(1) | 65.08 (18) | Ohiii—W1—Ohv | 111.8 (3) |
Na_aix—Si2—Ti_m2 | 163.23 (16) | Ohiii—W1—W2iii | 55.90 (16) |
Na_aix—Si2—Mg_m2 | 163.23 (16) | Ohv—W1—W2iii | 55.90 (16) |
Na_aii—Si2—Ti_m1(1) | 107.81 (18) | Na_aiii—W2—Na_ax | 73.2 (7) |
Na_aii—Si2—Ti_m1(2) | 63.45 (17) | Na_aiii—W2—O1iv | 63.1 (4) |
Na_aii—Si2—Fe_m2 | 93.6 (3) | Na_aiii—W2—O1xi | 117.4 (5) |
Na_aii—Si2—Si1ix | 67.4 (2) | Na_aiii—W2—O7 | 50.7 (5) |
Na_aii—Si2—Si2vi | 122.6 (3) | Na_aiii—W2—O7xv | 123.0 (6) |
Na_aii—Si2—O1 | 65.4 (4) | Na_aiii—W2—Oh | 69.2 (4) |
Na_aii—Si2—O1vi | 106.6 (3) | Na_aiii—W2—Ohxv | 66.0 (3) |
Na_aii—Si2—O2 | 105.7 (4) | Na_aiii—W2—Ba | 117.8 (3) |
Na_aii—Si2—O5 | 145.8 (6) | Na_aiii—W2—Baxv | 114.6 (3) |
Na_aii—Si2—O6ii | 44.5 (2) | Na_aiii—W2—W1iii | 36.6 (5) |
Na_aii—Si2—O7ix | 49.0 (4) | Na_aiii—W2—W2xiv | 143.4 (5) |
Na_aii—Si2—Oh | 93.7 (2) | Na_aiii—W2—W_c | 117.8 (3) |
Na_aii—Si2—Nb_m1(1) | 107.81 (18) | Na_aiii—W2—W_cxv | 114.6 (3) |
Na_aii—Si2—Ti_m2 | 93.6 (3) | Na_ax—W2—O1iv | 117.4 (5) |
Na_aii—Si2—Mg_m2 | 93.6 (3) | Na_ax—W2—O1xi | 63.1 (4) |
Ti_m1(1)—Si2—Ti_m1(2) | 65.96 (7) | Na_ax—W2—O7 | 123.0 (6) |
Ti_m1(1)—Si2—Fe_m2 | 98.37 (7) | Na_ax—W2—O7xv | 50.7 (5) |
Ti_m1(1)—Si2—Si1ix | 129.27 (13) | Na_ax—W2—Oh | 66.0 (3) |
Ti_m1(1)—Si2—Si2vi | 125.71 (13) | Na_ax—W2—Ohxv | 69.2 (4) |
Ti_m1(1)—Si2—O1 | 92.5 (3) | Na_ax—W2—Ba | 114.6 (3) |
Ti_m1(1)—Si2—O1vi | 122.78 (13) | Na_ax—W2—Baxv | 117.8 (3) |
Ti_m1(1)—Si2—O2 | 25.57 (19) | Na_ax—W2—W1iii | 36.6 (5) |
Ti_m1(1)—Si2—O5 | 106.1 (5) | Na_ax—W2—W2xiv | 143.4 (5) |
Ti_m1(1)—Si2—O6ii | 64.5 (2) | Na_ax—W2—W_c | 114.6 (3) |
Ti_m1(1)—Si2—O7ix | 131.9 (3) | Na_ax—W2—W_cxv | 117.8 (3) |
Ti_m1(1)—Si2—Oh | 34.5 (2) | O1iv—W2—O1xi | 179.4 (4) |
Ti_m1(1)—Si2—Nb_m1(1) | 0.0 (5) | O1iv—W2—O7 | 47.9 (2) |
Ti_m1(1)—Si2—Ti_m2 | 98.37 (7) | O1iv—W2—O7xv | 132.1 (2) |
Ti_m1(1)—Si2—Mg_m2 | 98.37 (7) | O1iv—W2—Oh | 126.9 (3) |
Ti_m1(2)—Si2—Fe_m2 | 56.69 (9) | O1iv—W2—Ohxv | 53.5 (3) |
Ti_m1(2)—Si2—Si1ix | 130.75 (16) | O1iv—W2—Ba | 124.5 (3) |
Ti_m1(2)—Si2—Si2vi | 118.89 (12) | O1iv—W2—Baxv | 55.11 (17) |
Ti_m1(2)—Si2—O1 | 30.8 (2) | O1iv—W2—W1iii | 90.32 (19) |
Ti_m1(2)—Si2—O1vi | 91.56 (18) | O1iv—W2—W2xiv | 89.68 (19) |
Ti_m1(2)—Si2—O2 | 85.8 (3) | O1iv—W2—W_c | 124.5 (3) |
Ti_m1(2)—Si2—O5 | 130.0 (3) | O1iv—W2—W_cxv | 55.11 (17) |
Ti_m1(2)—Si2—O6ii | 34.65 (12) | O1xi—W2—O7 | 132.1 (2) |
Ti_m1(2)—Si2—O7ix | 112.4 (4) | O1xi—W2—O7xv | 47.9 (2) |
Ti_m1(2)—Si2—Oh | 35.0 (2) | O1xi—W2—Oh | 53.5 (3) |
Ti_m1(2)—Si2—Nb_m1(1) | 65.96 (7) | O1xi—W2—Ohxv | 126.9 (3) |
Ti_m1(2)—Si2—Ti_m2 | 56.69 (9) | O1xi—W2—Ba | 55.11 (17) |
Ti_m1(2)—Si2—Mg_m2 | 56.69 (9) | O1xi—W2—Baxv | 124.5 (3) |
Fe_m2—Si2—Si1ix | 131.73 (16) | O1xi—W2—W1iii | 90.32 (19) |
Fe_m2—Si2—Si2vi | 62.20 (8) | O1xi—W2—W2xiv | 89.68 (19) |
Fe_m2—Si2—O1 | 32.05 (19) | O1xi—W2—W_c | 55.11 (17) |
Fe_m2—Si2—O1vi | 35.42 (12) | O1xi—W2—W_cxv | 124.5 (3) |
Fe_m2—Si2—O2 | 123.79 (19) | O7—W2—O7xv | 173.7 (4) |
Fe_m2—Si2—O5 | 77.7 (5) | O7—W2—Oh | 84.1 (3) |
Fe_m2—Si2—O6ii | 89.96 (18) | O7—W2—Ohxv | 92.9 (3) |
Fe_m2—Si2—O7ix | 121.3 (5) | O7—W2—Ba | 87.64 (17) |
Fe_m2—Si2—Oh | 67.67 (17) | O7—W2—Baxv | 95.84 (18) |
Fe_m2—Si2—Nb_m1(1) | 98.37 (7) | O7—W2—W1iii | 86.8 (2) |
Fe_m2—Si2—Ti_m2 | 0.0 (5) | O7—W2—W2xiv | 93.2 (2) |
Fe_m2—Si2—Mg_m2 | 0.0 (5) | O7—W2—W_c | 87.64 (17) |
Si1ix—Si2—Si2vi | 90.37 (6) | O7—W2—W_cxv | 95.84 (18) |
Si1ix—Si2—O1 | 124.4 (4) | O7xv—W2—Oh | 92.9 (3) |
Si1ix—Si2—O1vi | 105.74 (12) | O7xv—W2—Ohxv | 84.1 (3) |
Si1ix—Si2—O2 | 104.3 (2) | O7xv—W2—Ba | 95.84 (18) |
Si1ix—Si2—O5 | 93.7 (2) | O7xv—W2—Baxv | 87.64 (17) |
Si1ix—Si2—O6ii | 102.72 (13) | O7xv—W2—W1iii | 86.8 (2) |
Si1ix—Si2—O7ix | 18.9 (4) | O7xv—W2—W2xiv | 93.2 (2) |
Si1ix—Si2—Oh | 151.61 (10) | O7xv—W2—W_c | 95.84 (18) |
Si1ix—Si2—Nb_m1(1) | 129.27 (13) | O7xv—W2—W_cxv | 87.64 (17) |
Si1ix—Si2—Ti_m2 | 131.73 (16) | Oh—W2—Ohxv | 123.4 (3) |
Si1ix—Si2—Mg_m2 | 131.73 (16) | Oh—W2—Ba | 61.66 (9) |
Si2vi—Si2—O1 | 91.24 (19) | Oh—W2—Baxv | 174.9 (3) |
Si2vi—Si2—O1vi | 28.04 (19) | Oh—W2—W1iii | 61.70 (18) |
Si2vi—Si2—O2 | 131.3 (4) | Oh—W2—W2xiv | 118.30 (18) |
Si2vi—Si2—O5 | 25.2 (6) | Oh—W2—W_c | 61.66 (9) |
Si2vi—Si2—O6ii | 150.4 (3) | Oh—W2—W_cxv | 174.9 (3) |
Si2vi—Si2—O7ix | 98.11 (19) | Ohxv—W2—Ba | 174.9 (3) |
Si2vi—Si2—Oh | 117.98 (10) | Ohxv—W2—Baxv | 61.66 (9) |
Si2vi—Si2—Nb_m1(1) | 125.71 (13) | Ohxv—W2—W1iii | 61.70 (18) |
Si2vi—Si2—Ti_m2 | 62.20 (8) | Ohxv—W2—W2xiv | 118.30 (18) |
Si2vi—Si2—Mg_m2 | 62.20 (8) | Ohxv—W2—W_c | 174.9 (3) |
O1—Si2—O1vi | 63.2 (2) | Ohxv—W2—W_cxv | 61.66 (9) |
O1—Si2—O2 | 115.3 (4) | Ba—W2—Baxv | 113.3 (3) |
O1—Si2—O5 | 109.5 (5) | Ba—W2—W1iii | 123.35 (17) |
O1—Si2—O6ii | 59.5 (2) | Ba—W2—W2xiv | 56.65 (17) |
O1—Si2—O7ix | 106.8 (6) | Ba—W2—W_c | 0.0 (5) |
O1—Si2—Oh | 58.1 (4) | Ba—W2—W_cxv | 113.3 (3) |
O1—Si2—Nb_m1(1) | 92.5 (3) | Baxv—W2—W1iii | 123.35 (17) |
O1—Si2—Ti_m2 | 32.05 (19) | Baxv—W2—W2xiv | 56.65 (17) |
O1—Si2—Mg_m2 | 32.05 (19) | Baxv—W2—W_c | 113.3 (3) |
O1vi—Si2—O2 | 142.3 (3) | Baxv—W2—W_cxv | 0.0 (5) |
O1vi—Si2—O5 | 49.4 (6) | W1iii—W2—W2xiv | 180.0 (5) |
O1vi—Si2—O6ii | 122.5 (3) | W1iii—W2—W_c | 123.35 (17) |
O1vi—Si2—O7ix | 105.2 (3) | W1iii—W2—W_cxv | 123.35 (17) |
O1vi—Si2—Oh | 99.82 (15) | W2xiv—W2—W_c | 56.65 (17) |
O1vi—Si2—Nb_m1(1) | 122.78 (13) | W2xiv—W2—W_cxv | 56.65 (17) |
O1vi—Si2—Ti_m2 | 35.42 (12) | W_c—W2—W_cxv | 113.3 (3) |
O1vi—Si2—Mg_m2 | 35.42 (12) | Fe_m2—W_c—O1 | 42.1 (2) |
O2—Si2—O5 | 106.5 (7) | Fe_m2—W_c—O1xi | 46.26 (17) |
O2—Si2—O6ii | 71.3 (4) | Fe_m2—W_c—O1xii | 46.26 (17) |
O2—Si2—O7ix | 110.6 (4) | Fe_m2—W_c—O1vi | 42.1 (2) |
O2—Si2—Oh | 59.0 (3) | Fe_m2—W_c—O3 | 128.37 (16) |
O2—Si2—Nb_m1(1) | 25.57 (19) | Fe_m2—W_c—O3vi | 128.37 (16) |
O2—Si2—Ti_m2 | 123.79 (19) | Fe_m2—W_c—O5 | 73.4 (4) |
O2—Si2—Mg_m2 | 123.79 (19) | Fe_m2—W_c—Oh | 86.8 (2) |
O5—Si2—O6ii | 163.5 (3) | Fe_m2—W_c—Ohvi | 86.8 (2) |
O5—Si2—O7ix | 107.9 (4) | Fe_m2—W_c—Ba | 0 |
O5—Si2—Oh | 112.5 (3) | Fe_m2—W_c—W2 | 114.75 (16) |
O5—Si2—Nb_m1(1) | 106.1 (5) | Fe_m2—W_c—W2xiv | 114.75 (16) |
O5—Si2—Ti_m2 | 77.7 (5) | Fe_m2—W_c—Ti_m2 | 0.0 (5) |
O5—Si2—Mg_m2 | 77.7 (5) | Fe_m2—W_c—Mg_m2 | 0.0 (5) |
O6ii—Si2—O7ix | 87.8 (3) | O1—W_c—O1xi | 54.4 (2) |
O6ii—Si2—Oh | 51.85 (19) | O1—W_c—O1xii | 88.4 (3) |
O6ii—Si2—Nb_m1(1) | 64.5 (2) | O1—W_c—O1vi | 60.99 (15) |
O6ii—Si2—Ti_m2 | 89.96 (18) | O1—W_c—O3 | 86.3 (3) |
O6ii—Si2—Mg_m2 | 89.96 (18) | O1—W_c—O3vi | 120.6 (2) |
O7ix—Si2—Oh | 139.6 (3) | O1—W_c—O5 | 50.8 (3) |
O7ix—Si2—Nb_m1(1) | 131.9 (3) | O1—W_c—Oh | 53.78 (19) |
O7ix—Si2—Ti_m2 | 121.3 (5) | O1—W_c—Ohvi | 114.65 (19) |
O7ix—Si2—Mg_m2 | 121.3 (5) | O1—W_c—Ba | 0 |
Oh—Si2—Nb_m1(1) | 34.5 (2) | O1—W_c—W2 | 110.41 (18) |
Oh—Si2—Ti_m2 | 67.67 (17) | O1—W_c—W2xiv | 155.1 (3) |
Oh—Si2—Mg_m2 | 67.67 (17) | O1—W_c—Ti_m2 | 42.1 (2) |
Nb_m1(1)—Si2—Ti_m2 | 98.37 (7) | O1—W_c—Mg_m2 | 42.1 (2) |
Nb_m1(1)—Si2—Mg_m2 | 98.37 (7) | O1xi—W_c—O1xii | 66.2 (3) |
Ti_m2—Si2—Mg_m2 | 0.0 (5) | O1xi—W_c—O1vi | 88.4 (3) |
Na_aii—O1—Ti_m1(2) | 84.2 (3) | O1xi—W_c—O3 | 112.1 (2) |
Na_aii—O1—Fe_m2 | 140.6 (7) | O1xi—W_c—O3vi | 174.20 (18) |
Na_aii—O1—Si2 | 84.5 (4) | O1xi—W_c—O5 | 104.8 (3) |
Na_aii—O1—Si2vi | 117.4 (2) | O1xi—W_c—Oh | 57.8 (3) |
Na_aii—O1—O1xi | 120.8 (5) | O1xi—W_c—Ohvi | 123.5 (3) |
Na_aii—O1—O1vi | 125.4 (3) | O1xi—W_c—Ba | 0 |
Na_aii—O1—O2 | 88.8 (4) | O1xi—W_c—W2 | 69.35 (17) |
Na_aii—O1—O5 | 112.9 (4) | O1xi—W_c—W2xiv | 104.36 (18) |
Na_aii—O1—O6ii | 50.5 (3) | O1xi—W_c—Ti_m2 | 46.26 (17) |
Na_aii—O1—O7ix | 52.6 (4) | O1xi—W_c—Mg_m2 | 46.26 (17) |
Na_aii—O1—Oh | 111.7 (3) | O1xii—W_c—O1vi | 54.4 (2) |
Na_aii—O1—Ohxi | 61.3 (4) | O1xii—W_c—O3 | 174.20 (18) |
Na_aii—O1—Ba | 174.9 (4) | O1xii—W_c—O3vi | 112.1 (2) |
Na_aii—O1—Baxi | 92.7 (5) | O1xii—W_c—O5 | 104.8 (3) |
Na_aii—O1—W2ix | 39.5 (4) | O1xii—W_c—Oh | 123.5 (3) |
Na_aii—O1—W_c | 174.9 (4) | O1xii—W_c—Ohvi | 57.8 (3) |
Na_aii—O1—W_cxi | 92.7 (5) | O1xii—W_c—Ba | 0 |
Na_aii—O1—Ti_m2 | 140.6 (7) | O1xii—W_c—W2 | 104.36 (18) |
Na_aii—O1—Mg_m2 | 140.6 (7) | O1xii—W_c—W2xiv | 69.35 (17) |
Ti_m1(2)—O1—Fe_m2 | 97.9 (3) | O1xii—W_c—Ti_m2 | 46.26 (17) |
Ti_m1(2)—O1—Si2 | 125.3 (5) | O1xii—W_c—Mg_m2 | 46.26 (17) |
Ti_m1(2)—O1—Si2vi | 158.4 (3) | O1vi—W_c—O3 | 120.6 (2) |
Ti_m1(2)—O1—O1xi | 48.95 (17) | O1vi—W_c—O3vi | 86.3 (3) |
Ti_m1(2)—O1—O1vi | 138.9 (3) | O1vi—W_c—O5 | 50.8 (3) |
Ti_m1(2)—O1—O2 | 94.1 (3) | O1vi—W_c—Oh | 114.65 (19) |
Ti_m1(2)—O1—O5 | 145.2 (6) | O1vi—W_c—Ohvi | 53.78 (19) |
Ti_m1(2)—O1—O6ii | 43.69 (15) | O1vi—W_c—Ba | 0 |
Ti_m1(2)—O1—O7ix | 126.6 (2) | O1vi—W_c—W2 | 155.1 (3) |
Ti_m1(2)—O1—Oh | 45.2 (3) | O1vi—W_c—W2xiv | 110.41 (18) |
Ti_m1(2)—O1—Ohxi | 43.5 (3) | O1vi—W_c—Ti_m2 | 42.1 (2) |
Ti_m1(2)—O1—Ba | 92.4 (2) | O1vi—W_c—Mg_m2 | 42.1 (2) |
Ti_m1(2)—O1—Baxi | 98.9 (5) | O3—W_c—O3vi | 68.9 (2) |
Ti_m1(2)—O1—W2ix | 102.3 (4) | O3—W_c—O5 | 69.9 (3) |
Ti_m1(2)—O1—W_c | 92.4 (2) | O3—W_c—Oh | 54.4 (3) |
Ti_m1(2)—O1—W_cxi | 98.9 (5) | O3—W_c—Ohvi | 122.8 (3) |
Ti_m1(2)—O1—Ti_m2 | 97.9 (3) | O3—W_c—Ba | 0 |
Ti_m1(2)—O1—Mg_m2 | 97.9 (3) | O3—W_c—W2 | 79.70 (16) |
Fe_m2—O1—Si2 | 123.0 (5) | O3—W_c—W2xiv | 116.3 (2) |
Fe_m2—O1—Si2vi | 66.31 (16) | O3—W_c—Ti_m2 | 128.37 (16) |
Fe_m2—O1—O1xi | 48.95 (16) | O3—W_c—Mg_m2 | 128.37 (16) |
Fe_m2—O1—O1vi | 41.05 (15) | O3vi—W_c—O5 | 69.9 (3) |
Fe_m2—O1—O2 | 129.9 (5) | O3vi—W_c—Oh | 122.8 (3) |
Fe_m2—O1—O5 | 87.5 (3) | O3vi—W_c—Ohvi | 54.4 (3) |
Fe_m2—O1—O6ii | 141.4 (3) | O3vi—W_c—Ba | 0 |
Fe_m2—O1—O7ix | 135.1 (2) | O3vi—W_c—W2 | 116.3 (2) |
Fe_m2—O1—Oh | 96.2 (2) | O3vi—W_c—W2xiv | 79.70 (16) |
Fe_m2—O1—Ohxi | 93.6 (4) | O3vi—W_c—Ti_m2 | 128.37 (16) |
Fe_m2—O1—Ba | 43.62 (17) | O3vi—W_c—Mg_m2 | 128.37 (16) |
Fe_m2—O1—Baxi | 48.0 (2) | O5—W_c—Oh | 83.45 (10) |
Fe_m2—O1—W2ix | 102.8 (5) | O5—W_c—Ohvi | 83.45 (10) |
Fe_m2—O1—W_c | 43.62 (17) | O5—W_c—Ba | 0 |
Fe_m2—O1—W_cxi | 48.0 (2) | O5—W_c—W2 | 144.3 (2) |
Fe_m2—O1—Ti_m2 | 0.0 (5) | O5—W_c—W2xiv | 144.3 (2) |
Fe_m2—O1—Mg_m2 | 0.0 (5) | O5—W_c—Ti_m2 | 73.4 (4) |
Si2—O1—Si2vi | 60.7 (2) | O5—W_c—Mg_m2 | 73.4 (4) |
Si2—O1—O1xi | 148.7 (7) | Oh—W_c—Ohvi | 166.59 (14) |
Si2—O1—O1vi | 88.8 (3) | Oh—W_c—Ba | 0 |
Si2—O1—O2 | 32.3 (3) | Oh—W_c—W2 | 63.35 (19) |
Si2—O1—O5 | 35.7 (3) | Oh—W_c—W2xiv | 130.1 (2) |
Si2—O1—O6ii | 90.8 (3) | Oh—W_c—Ti_m2 | 86.8 (2) |
Si2—O1—O7ix | 36.7 (3) | Oh—W_c—Mg_m2 | 86.8 (2) |
Si2—O1—Oh | 91.8 (6) | Ohvi—W_c—Ba | 0 |
Si2—O1—Ohxi | 143.1 (3) | Ohvi—W_c—W2 | 130.1 (2) |
Si2—O1—Ba | 94.4 (5) | Ohvi—W_c—W2xiv | 63.35 (19) |
Si2—O1—Baxi | 135.0 (3) | Ohvi—W_c—Ti_m2 | 86.8 (2) |
Si2—O1—W2ix | 102.0 (3) | Ohvi—W_c—Mg_m2 | 86.8 (2) |
Si2—O1—W_c | 94.4 (5) | Ba—W_c—W2 | 0 |
Si2—O1—W_cxi | 135.0 (3) | Ba—W_c—W2xiv | 0 |
Si2—O1—Ti_m2 | 123.0 (5) | Ba—W_c—Ti_m2 | 0 |
Si2—O1—Mg_m2 | 123.0 (5) | Ba—W_c—Mg_m2 | 0 |
Si2vi—O1—O1xi | 113.69 (18) | W2—W_c—W2xiv | 66.7 (2) |
Si2vi—O1—O1vi | 28.0 (2) | W2—W_c—Ti_m2 | 114.75 (16) |
Si2vi—O1—O2 | 86.1 (3) | W2—W_c—Mg_m2 | 114.75 (16) |
Si2vi—O1—O5 | 28.1 (3) | W2xiv—W_c—Ti_m2 | 114.75 (16) |
Si2vi—O1—O6ii | 151.2 (4) | W2xiv—W_c—Mg_m2 | 114.75 (16) |
Si2vi—O1—O7ix | 71.8 (2) | Ti_m2—W_c—Mg_m2 | 0.0 (5) |
Si2vi—O1—Oh | 119.1 (4) | Ti_m1(1)—Nb_m1(1)—Si1 | 0 |
Si2vi—O1—Ohxi | 146.3 (4) | Ti_m1(1)—Nb_m1(1)—Si1ii | 0 |
Si2vi—O1—Ba | 66.00 (16) | Ti_m1(1)—Nb_m1(1)—Si2 | 0 |
Si2vi—O1—Baxi | 81.71 (16) | Ti_m1(1)—Nb_m1(1)—Si2ii | 0 |
Si2vi—O1—W2ix | 95.9 (2) | Ti_m1(1)—Nb_m1(1)—O2 | 0 |
Si2vi—O1—W_c | 66.00 (16) | Ti_m1(1)—Nb_m1(1)—O2ii | 0 |
Si2vi—O1—W_cxi | 81.71 (16) | Ti_m1(1)—Nb_m1(1)—O3 | 0 |
Si2vi—O1—Ti_m2 | 66.31 (16) | Ti_m1(1)—Nb_m1(1)—O3ii | 0 |
Si2vi—O1—Mg_m2 | 66.31 (16) | Ti_m1(1)—Nb_m1(1)—O6 | 0 |
O1xi—O1—O1vi | 90.0 (2) | Ti_m1(1)—Nb_m1(1)—O6ii | 0 |
O1xi—O1—O2 | 122.9 (4) | Ti_m1(1)—Nb_m1(1)—Oh | 0 |
O1xi—O1—O5 | 126.2 (4) | Ti_m1(1)—Nb_m1(1)—Ohii | 0 |
O1xi—O1—O6ii | 92.5 (2) | Si1—Nb_m1(1)—Si1ii | 180.0 (5) |
O1xi—O1—O7ix | 173.4 (5) | Si1—Nb_m1(1)—Si2 | 106.55 (7) |
O1xi—O1—Oh | 63.0 (3) | Si1—Nb_m1(1)—Si2ii | 73.45 (7) |
O1xi—O1—Ohxi | 59.7 (3) | Si1—Nb_m1(1)—O2 | 110.5 (2) |
O1xi—O1—Ba | 58.7 (3) | Si1—Nb_m1(1)—O2ii | 69.5 (2) |
O1xi—O1—Baxi | 66.9 (3) | Si1—Nb_m1(1)—O3 | 25.0 (3) |
O1xi—O1—W2ix | 109.3 (5) | Si1—Nb_m1(1)—O3ii | 155.0 (3) |
O1xi—O1—W_c | 58.7 (3) | Si1—Nb_m1(1)—O6 | 27.17 (14) |
O1xi—O1—W_cxi | 66.9 (3) | Si1—Nb_m1(1)—O6ii | 152.83 (14) |
O1xi—O1—Ti_m2 | 48.95 (16) | Si1—Nb_m1(1)—Oh | 101.6 (2) |
O1xi—O1—Mg_m2 | 48.95 (16) | Si1—Nb_m1(1)—Ohii | 78.4 (2) |
O1vi—O1—O2 | 112.2 (5) | Si1ii—Nb_m1(1)—Si2 | 73.45 (7) |
O1vi—O1—O5 | 55.0 (3) | Si1ii—Nb_m1(1)—Si2ii | 106.55 (7) |
O1vi—O1—O6ii | 175.9 (4) | Si1ii—Nb_m1(1)—O2 | 69.5 (2) |
O1vi—O1—O7ix | 94.3 (2) | Si1ii—Nb_m1(1)—O2ii | 110.5 (2) |
O1vi—O1—Oh | 122.7 (3) | Si1ii—Nb_m1(1)—O3 | 155.0 (3) |
O1vi—O1—Ohxi | 121.5 (5) | Si1ii—Nb_m1(1)—O3ii | 25.0 (3) |
O1vi—O1—Ba | 59.51 (18) | Si1ii—Nb_m1(1)—O6 | 152.83 (14) |
O1vi—O1—Baxi | 56.9 (3) | Si1ii—Nb_m1(1)—O6ii | 27.17 (14) |
O1vi—O1—W2ix | 90.3 (3) | Si1ii—Nb_m1(1)—Oh | 78.4 (2) |
O1vi—O1—W_c | 59.51 (18) | Si1ii—Nb_m1(1)—Ohii | 101.6 (2) |
O1vi—O1—W_cxi | 56.9 (3) | Si2—Nb_m1(1)—Si2ii | 180.0 (5) |
O1vi—O1—Ti_m2 | 41.05 (15) | Si2—Nb_m1(1)—O2 | 20.8 (3) |
O1vi—O1—Mg_m2 | 41.05 (15) | Si2—Nb_m1(1)—O2ii | 159.2 (3) |
O2—O1—O5 | 58.0 (4) | Si2—Nb_m1(1)—O3 | 82.2 (3) |
O2—O1—O6ii | 69.0 (3) | Si2—Nb_m1(1)—O3ii | 97.8 (3) |
O2—O1—O7ix | 59.9 (4) | Si2—Nb_m1(1)—O6 | 122.81 (11) |
O2—O1—Oh | 60.7 (3) | Si2—Nb_m1(1)—O6ii | 57.19 (11) |
O2—O1—Ohxi | 126.3 (3) | Si2—Nb_m1(1)—Oh | 70.80 (19) |
O2—O1—Ba | 87.6 (4) | Si2—Nb_m1(1)—Ohii | 109.20 (19) |
O2—O1—Baxi | 167.0 (3) | Si2ii—Nb_m1(1)—O2 | 159.2 (3) |
O2—O1—W2ix | 121.7 (2) | Si2ii—Nb_m1(1)—O2ii | 20.8 (3) |
O2—O1—W_c | 87.6 (4) | Si2ii—Nb_m1(1)—O3 | 97.8 (3) |
O2—O1—W_cxi | 167.0 (3) | Si2ii—Nb_m1(1)—O3ii | 82.2 (3) |
O2—O1—Ti_m2 | 129.9 (5) | Si2ii—Nb_m1(1)—O6 | 57.19 (11) |
O2—O1—Mg_m2 | 129.9 (5) | Si2ii—Nb_m1(1)—O6ii | 122.81 (11) |
O5—O1—O6ii | 125.3 (5) | Si2ii—Nb_m1(1)—Oh | 109.20 (19) |
O5—O1—O7ix | 60.3 (3) | Si2ii—Nb_m1(1)—Ohii | 70.80 (19) |
O5—O1—Oh | 100.1 (6) | O2—Nb_m1(1)—O2ii | 180.0 (5) |
O5—O1—Ohxi | 171.0 (4) | O2—Nb_m1(1)—O3 | 89.5 (2) |
O5—O1—Ba | 68.1 (3) | O2—Nb_m1(1)—O3ii | 90.5 (2) |
O5—O1—Baxi | 109.7 (3) | O2—Nb_m1(1)—O6 | 117.1 (3) |
O5—O1—W2ix | 110.0 (3) | O2—Nb_m1(1)—O6ii | 62.9 (3) |
O5—O1—W_c | 68.1 (3) | O2—Nb_m1(1)—Oh | 90.3 (4) |
O5—O1—W_cxi | 109.7 (3) | O2—Nb_m1(1)—Ohii | 89.7 (4) |
O5—O1—Ti_m2 | 87.5 (3) | O2ii—Nb_m1(1)—O3 | 90.5 (2) |
O5—O1—Mg_m2 | 87.5 (3) | O2ii—Nb_m1(1)—O3ii | 89.5 (2) |
O6ii—O1—O7ix | 82.9 (2) | O2ii—Nb_m1(1)—O6 | 62.9 (3) |
O6ii—O1—Oh | 61.5 (2) | O2ii—Nb_m1(1)—O6ii | 117.1 (3) |
O6ii—O1—Ohxi | 57.5 (3) | O2ii—Nb_m1(1)—Oh | 89.7 (4) |
O6ii—O1—Ba | 124.6 (3) | O2ii—Nb_m1(1)—Ohii | 90.3 (4) |
O6ii—O1—Baxi | 121.4 (5) | O3—Nb_m1(1)—O3ii | 180.0 (5) |
O6ii—O1—W2ix | 85.8 (4) | O3—Nb_m1(1)—O6 | 49.5 (4) |
O6ii—O1—W_c | 124.6 (3) | O3—Nb_m1(1)—O6ii | 130.5 (4) |
O6ii—O1—W_cxi | 121.4 (5) | O3—Nb_m1(1)—Oh | 88.7 (4) |
O6ii—O1—Ti_m2 | 141.4 (3) | O3—Nb_m1(1)—Ohii | 91.3 (4) |
O6ii—O1—Mg_m2 | 141.4 (3) | O3ii—Nb_m1(1)—O6 | 130.5 (4) |
O7ix—O1—Oh | 118.2 (5) | O3ii—Nb_m1(1)—O6ii | 49.5 (4) |
O7ix—O1—Ohxi | 113.7 (4) | O3ii—Nb_m1(1)—Oh | 91.3 (4) |
O7ix—O1—Ba | 127.9 (5) | O3ii—Nb_m1(1)—Ohii | 88.7 (4) |
O7ix—O1—Baxi | 111.4 (4) | O6—Nb_m1(1)—O6ii | 180.0 (5) |
O7ix—O1—W2ix | 65.7 (3) | O6—Nb_m1(1)—Oh | 125.9 (3) |
O7ix—O1—W_c | 127.9 (5) | O6—Nb_m1(1)—Ohii | 54.1 (3) |
O7ix—O1—W_cxi | 111.4 (4) | O6ii—Nb_m1(1)—Oh | 54.1 (3) |
O7ix—O1—Ti_m2 | 135.1 (2) | O6ii—Nb_m1(1)—Ohii | 125.9 (3) |
O7ix—O1—Mg_m2 | 135.1 (2) | Oh—Nb_m1(1)—Ohii | 180.0 (5) |
Oh—O1—Ohxi | 88.6 (3) | Ti_m1(2)—Ti_m2—Ti_m1(2)xii | 180.0 (5) |
Oh—O1—Ba | 63.3 (2) | Ti_m1(2)—Ti_m2—Fe_m2 | 0 |
Oh—O1—Baxi | 129.9 (3) | Ti_m1(2)—Ti_m2—Si2 | 62.20 (5) |
Oh—O1—W2ix | 144.7 (4) | Ti_m1(2)—Ti_m2—Si2xi | 62.20 (5) |
Oh—O1—W_c | 63.3 (2) | Ti_m1(2)—Ti_m2—Si2xii | 117.80 (5) |
Oh—O1—W_cxi | 129.9 (3) | Ti_m1(2)—Ti_m2—Si2vi | 117.80 (5) |
Oh—O1—Ti_m2 | 96.2 (2) | Ti_m1(2)—Ti_m2—O1 | 41.05 (16) |
Oh—O1—Mg_m2 | 96.2 (2) | Ti_m1(2)—Ti_m2—O1xi | 41.05 (16) |
Ohxi—O1—Ba | 118.4 (2) | Ti_m1(2)—Ti_m2—O1xii | 138.95 (16) |
Ohxi—O1—Baxi | 65.1 (3) | Ti_m1(2)—Ti_m2—O1vi | 138.95 (16) |
Ohxi—O1—W2ix | 61.0 (3) | Ti_m1(2)—Ti_m2—O5 | 90 |
Ohxi—O1—W_c | 118.4 (2) | Ti_m1(2)—Ti_m2—O5xi | 90 |
Ohxi—O1—W_cxi | 65.1 (3) | Ti_m1(2)—Ti_m2—Ba | 90 |
Ohxi—O1—Ti_m2 | 93.6 (4) | Ti_m1(2)—Ti_m2—Baxi | 90 |
Ohxi—O1—Mg_m2 | 93.6 (4) | Ti_m1(2)—Ti_m2—W_c | 90 |
Ba—O1—Baxi | 91.59 (17) | Ti_m1(2)—Ti_m2—W_cxi | 90 |
Ba—O1—W2ix | 145.4 (3) | Ti_m1(2)—Ti_m2—Mg_m2 | 0 |
Ba—O1—W_c | 0.0 (5) | Ti_m1(2)xii—Ti_m2—Fe_m2 | 0 |
Ba—O1—W_cxi | 91.59 (17) | Ti_m1(2)xii—Ti_m2—Si2 | 117.80 (5) |
Ba—O1—Ti_m2 | 43.62 (17) | Ti_m1(2)xii—Ti_m2—Si2xi | 117.80 (5) |
Ba—O1—Mg_m2 | 43.62 (17) | Ti_m1(2)xii—Ti_m2—Si2xii | 62.20 (5) |
Baxi—O1—W2ix | 55.5 (3) | Ti_m1(2)xii—Ti_m2—Si2vi | 62.20 (5) |
Baxi—O1—W_c | 91.59 (17) | Ti_m1(2)xii—Ti_m2—O1 | 138.95 (16) |
Baxi—O1—W_cxi | 0.0 (5) | Ti_m1(2)xii—Ti_m2—O1xi | 138.95 (16) |
Baxi—O1—Ti_m2 | 48.0 (2) | Ti_m1(2)xii—Ti_m2—O1xii | 41.05 (16) |
Baxi—O1—Mg_m2 | 48.0 (2) | Ti_m1(2)xii—Ti_m2—O1vi | 41.05 (16) |
W2ix—O1—W_c | 145.4 (3) | Ti_m1(2)xii—Ti_m2—O5 | 90 |
W2ix—O1—W_cxi | 55.5 (3) | Ti_m1(2)xii—Ti_m2—O5xi | 90 |
W2ix—O1—Ti_m2 | 102.8 (5) | Ti_m1(2)xii—Ti_m2—Ba | 90 |
W2ix—O1—Mg_m2 | 102.8 (5) | Ti_m1(2)xii—Ti_m2—Baxi | 90 |
W_c—O1—W_cxi | 91.59 (17) | Ti_m1(2)xii—Ti_m2—W_c | 90 |
W_c—O1—Ti_m2 | 43.62 (17) | Ti_m1(2)xii—Ti_m2—W_cxi | 90 |
W_c—O1—Mg_m2 | 43.62 (17) | Ti_m1(2)xii—Ti_m2—Mg_m2 | 0 |
W_cxi—O1—Ti_m2 | 48.0 (2) | Fe_m2—Ti_m2—Si2 | 0 |
W_cxi—O1—Mg_m2 | 48.0 (2) | Fe_m2—Ti_m2—Si2xi | 0 |
Ti_m2—O1—Mg_m2 | 0.0 (5) | Fe_m2—Ti_m2—Si2xii | 0 |
Na_aix—O2—K_b | 95.4 (5) | Fe_m2—Ti_m2—Si2vi | 0 |
Na_aix—O2—Ti_m1(1) | 111.2 (5) | Fe_m2—Ti_m2—O1 | 0 |
Na_aix—O2—Ti_m1(2) | 134.4 (5) | Fe_m2—Ti_m2—O1xi | 0 |
Na_aix—O2—Si1ii | 78.8 (3) | Fe_m2—Ti_m2—O1xii | 0 |
Na_aix—O2—Si2 | 114.2 (4) | Fe_m2—Ti_m2—O1vi | 0 |
Na_aix—O2—O1 | 135.6 (6) | Fe_m2—Ti_m2—O5 | 0 |
Na_aix—O2—O3 | 128.1 (7) | Fe_m2—Ti_m2—O5xi | 0 |
Na_aix—O2—O3ii | 84.0 (3) | Fe_m2—Ti_m2—Ba | 0 |
Na_aix—O2—O5 | 114.6 (3) | Fe_m2—Ti_m2—Baxi | 0 |
Na_aix—O2—O6ii | 101.3 (5) | Fe_m2—Ti_m2—W_c | 0 |
Na_aix—O2—O7ix | 80.9 (4) | Fe_m2—Ti_m2—W_cxi | 0 |
Na_aix—O2—O7ii | 51.5 (4) | Fe_m2—Ti_m2—Mg_m2 | 0 |
Na_aix—O2—Oh | 144.3 (3) | Si2—Ti_m2—Si2xi | 124.40 (8) |
Na_aix—O2—Ohii | 72.6 (5) | Si2—Ti_m2—Si2xii | 180.0 (5) |
Na_aix—O2—W1ix | 43.4 (4) | Si2—Ti_m2—Si2vi | 55.60 (8) |
Na_aix—O2—Nb_m1(1) | 111.2 (5) | Si2—Ti_m2—O1 | 24.9 (3) |
K_b—O2—Ti_m1(1) | 95.3 (3) | Si2—Ti_m2—O1xi | 101.7 (2) |
K_b—O2—Ti_m1(2) | 129.71 (17) | Si2—Ti_m2—O1xii | 155.1 (3) |
K_b—O2—Si1ii | 164.3 (4) | Si2—Ti_m2—O1vi | 78.3 (2) |
K_b—O2—Si2 | 89.3 (3) | Si2—Ti_m2—O5 | 29.51 (10) |
K_b—O2—O1 | 107.5 (2) | Si2—Ti_m2—O5xi | 150.49 (10) |
K_b—O2—O3 | 54.8 (2) | Si2—Ti_m2—Ba | 80.55 (12) |
K_b—O2—O3ii | 134.6 (4) | Si2—Ti_m2—Baxi | 99.45 (12) |
K_b—O2—O5 | 52.1 (4) | Si2—Ti_m2—W_c | 80.55 (12) |
K_b—O2—O6ii | 162.6 (3) | Si2—Ti_m2—W_cxi | 99.45 (12) |
K_b—O2—O7ix | 102.4 (2) | Si2—Ti_m2—Mg_m2 | 0 |
K_b—O2—O7ii | 146.8 (3) | Si2xi—Ti_m2—Si2xii | 55.60 (8) |
K_b—O2—Oh | 110.5 (2) | Si2xi—Ti_m2—Si2vi | 180.0 (5) |
K_b—O2—Ohii | 77.4 (3) | Si2xi—Ti_m2—O1 | 101.7 (2) |
K_b—O2—W1ix | 52.1 (2) | Si2xi—Ti_m2—O1xi | 24.9 (3) |
K_b—O2—Nb_m1(1) | 95.3 (3) | Si2xi—Ti_m2—O1xii | 78.3 (2) |
Ti_m1(1)—O2—Ti_m1(2) | 75.1 (3) | Si2xi—Ti_m2—O1vi | 155.1 (3) |
Ti_m1(1)—O2—Si1ii | 73.69 (16) | Si2xi—Ti_m2—O5 | 150.49 (10) |
Ti_m1(1)—O2—Si2 | 133.7 (4) | Si2xi—Ti_m2—O5xi | 29.51 (10) |
Ti_m1(1)—O2—O1 | 104.1 (3) | Si2xi—Ti_m2—Ba | 99.45 (12) |
Ti_m1(1)—O2—O3 | 45.50 (17) | Si2xi—Ti_m2—Baxi | 80.55 (12) |
Ti_m1(1)—O2—O3ii | 44.98 (17) | Si2xi—Ti_m2—W_c | 99.45 (12) |
Ti_m1(1)—O2—O5 | 124.9 (3) | Si2xi—Ti_m2—W_cxi | 80.55 (12) |
Ti_m1(1)—O2—O6ii | 83.1 (3) | Si2xi—Ti_m2—Mg_m2 | 0 |
Ti_m1(1)—O2—O7ix | 157.6 (6) | Si2xii—Ti_m2—Si2vi | 124.40 (8) |
Ti_m1(1)—O2—O7ii | 98.24 (19) | Si2xii—Ti_m2—O1 | 155.1 (3) |
Ti_m1(1)—O2—Oh | 44.4 (3) | Si2xii—Ti_m2—O1xi | 78.3 (2) |
Ti_m1(1)—O2—Ohii | 44.7 (3) | Si2xii—Ti_m2—O1xii | 24.9 (3) |
Ti_m1(1)—O2—W1ix | 113.3 (5) | Si2xii—Ti_m2—O1vi | 101.7 (2) |
Ti_m1(1)—O2—Nb_m1(1) | 0.0 (5) | Si2xii—Ti_m2—O5 | 150.49 (10) |
Ti_m1(2)—O2—Si1ii | 59.22 (19) | Si2xii—Ti_m2—O5xi | 29.51 (10) |
Ti_m1(2)—O2—Si2 | 67.0 (4) | Si2xii—Ti_m2—Ba | 99.45 (12) |
Ti_m1(2)—O2—O1 | 35.21 (17) | Si2xii—Ti_m2—Baxi | 80.55 (12) |
Ti_m1(2)—O2—O3 | 89.5 (3) | Si2xii—Ti_m2—W_c | 99.45 (12) |
Ti_m1(2)—O2—O3ii | 69.3 (3) | Si2xii—Ti_m2—W_cxi | 80.55 (12) |
Ti_m1(2)—O2—O5 | 93.0 (5) | Si2xii—Ti_m2—Mg_m2 | 0 |
Ti_m1(2)—O2—O6ii | 33.20 (16) | Si2vi—Ti_m2—O1 | 78.3 (2) |
Ti_m1(2)—O2—O7ix | 83.0 (4) | Si2vi—Ti_m2—O1xi | 155.1 (3) |
Ti_m1(2)—O2—O7ii | 83.2 (3) | Si2vi—Ti_m2—O1xii | 101.7 (2) |
Ti_m1(2)—O2—Oh | 33.4 (3) | Si2vi—Ti_m2—O1vi | 24.9 (3) |
Ti_m1(2)—O2—Ohii | 118.1 (2) | Si2vi—Ti_m2—O5 | 29.51 (10) |
Ti_m1(2)—O2—W1ix | 171.6 (3) | Si2vi—Ti_m2—O5xi | 150.49 (10) |
Ti_m1(2)—O2—Nb_m1(1) | 75.1 (3) | Si2vi—Ti_m2—Ba | 80.55 (12) |
Si1ii—O2—Si2 | 106.4 (5) | Si2vi—Ti_m2—Baxi | 99.45 (12) |
Si1ii—O2—O1 | 86.4 (3) | Si2vi—Ti_m2—W_c | 80.55 (12) |
Si1ii—O2—O3 | 117.90 (19) | Si2vi—Ti_m2—W_cxi | 99.45 (12) |
Si1ii—O2—O3ii | 31.0 (2) | Si2vi—Ti_m2—Mg_m2 | 0 |
Si1ii—O2—O5 | 143.5 (6) | O1—Ti_m2—O1xi | 82.1 (2) |
Si1ii—O2—O6ii | 29.78 (19) | O1—Ti_m2—O1xii | 180.0 (5) |
Si1ii—O2—O7ix | 91.1 (3) | O1—Ti_m2—O1vi | 97.9 (2) |
Si1ii—O2—O7ii | 30.86 (14) | O1—Ti_m2—O5 | 54.4 (3) |
Si1ii—O2—Oh | 69.7 (2) | O1—Ti_m2—O5xi | 125.6 (3) |
Si1ii—O2—Ohii | 87.0 (2) | O1—Ti_m2—Ba | 94.2 (4) |
Si1ii—O2—W1ix | 121.4 (3) | O1—Ti_m2—Baxi | 85.8 (4) |
Si1ii—O2—Nb_m1(1) | 73.69 (16) | O1—Ti_m2—W_c | 94.2 (4) |
Si2—O2—O1 | 32.4 (3) | O1—Ti_m2—W_cxi | 85.8 (4) |
Si2—O2—O3 | 107.3 (3) | O1—Ti_m2—Mg_m2 | 0 |
Si2—O2—O3ii | 132.3 (6) | O1xi—Ti_m2—O1xii | 97.9 (2) |
Si2—O2—O5 | 37.3 (4) | O1xi—Ti_m2—O1vi | 180.0 (5) |
Si2—O2—O6ii | 79.5 (5) | O1xi—Ti_m2—O5 | 125.6 (3) |
Si2—O2—O7ix | 34.7 (2) | O1xi—Ti_m2—O5xi | 54.4 (3) |
Si2—O2—O7ii | 102.5 (5) | O1xi—Ti_m2—Ba | 85.8 (4) |
Si2—O2—Oh | 91.0 (4) | O1xi—Ti_m2—Baxi | 94.2 (4) |
Si2—O2—Ohii | 165.8 (4) | O1xi—Ti_m2—W_c | 85.8 (4) |
Si2—O2—W1ix | 105.7 (3) | O1xi—Ti_m2—W_cxi | 94.2 (4) |
Si2—O2—Nb_m1(1) | 133.7 (4) | O1xi—Ti_m2—Mg_m2 | 0 |
O1—O2—O3 | 95.8 (3) | O1xii—Ti_m2—O1vi | 82.1 (2) |
O1—O2—O3ii | 103.9 (4) | O1xii—Ti_m2—O5 | 125.6 (3) |
O1—O2—O5 | 59.9 (5) | O1xii—Ti_m2—O5xi | 54.4 (3) |
O1—O2—O6ii | 56.6 (3) | O1xii—Ti_m2—Ba | 85.8 (4) |
O1—O2—O7ix | 57.6 (3) | O1xii—Ti_m2—Baxi | 94.2 (4) |
O1—O2—O7ii | 98.3 (4) | O1xii—Ti_m2—W_c | 85.8 (4) |
O1—O2—Oh | 59.8 (3) | O1xii—Ti_m2—W_cxi | 94.2 (4) |
O1—O2—Ohii | 148.6 (2) | O1xii—Ti_m2—Mg_m2 | 0 |
O1—O2—W1ix | 138.0 (3) | O1vi—Ti_m2—O5 | 54.4 (3) |
O1—O2—Nb_m1(1) | 104.1 (3) | O1vi—Ti_m2—O5xi | 125.6 (3) |
O3—O2—O3ii | 90.5 (2) | O1vi—Ti_m2—Ba | 94.2 (4) |
O3—O2—O5 | 81.7 (3) | O1vi—Ti_m2—Baxi | 85.8 (4) |
O3—O2—O6ii | 115.9 (3) | O1vi—Ti_m2—W_c | 94.2 (4) |
O3—O2—O7ix | 140.6 (3) | O1vi—Ti_m2—W_cxi | 85.8 (4) |
O3—O2—O7ii | 143.5 (2) | O1vi—Ti_m2—Mg_m2 | 0 |
O3—O2—Oh | 59.2 (3) | O5—Ti_m2—O5xi | 180.0 (5) |
O3—O2—Ohii | 60.9 (3) | O5—Ti_m2—Ba | 69.0 (3) |
O3—O2—W1ix | 96.9 (4) | O5—Ti_m2—Baxi | 111.0 (3) |
O3—O2—Nb_m1(1) | 45.50 (17) | O5—Ti_m2—W_c | 69.0 (3) |
O3ii—O2—O5 | 160.8 (5) | O5—Ti_m2—W_cxi | 111.0 (3) |
O3ii—O2—O6ii | 53.1 (3) | O5—Ti_m2—Mg_m2 | 0 |
O3ii—O2—O7ix | 122.1 (4) | O5xi—Ti_m2—Ba | 111.0 (3) |
O3ii—O2—O7ii | 53.46 (18) | O5xi—Ti_m2—Baxi | 69.0 (3) |
O3ii—O2—Oh | 60.4 (2) | O5xi—Ti_m2—W_c | 111.0 (3) |
O3ii—O2—Ohii | 59.1 (3) | O5xi—Ti_m2—W_cxi | 69.0 (3) |
O3ii—O2—W1ix | 115.8 (4) | O5xi—Ti_m2—Mg_m2 | 0 |
O3ii—O2—Nb_m1(1) | 44.98 (17) | Ba—Ti_m2—Baxi | 180.0 (5) |
O5—O2—O6ii | 115.1 (6) | Ba—Ti_m2—W_c | 0.0 (5) |
O5—O2—O7ix | 60.2 (3) | Ba—Ti_m2—W_cxi | 180.0 (5) |
O5—O2—O7ii | 134.2 (4) | Ba—Ti_m2—Mg_m2 | 0 |
O5—O2—Oh | 100.8 (3) | Baxi—Ti_m2—W_c | 180.0 (5) |
O5—O2—Ohii | 128.9 (6) | Baxi—Ti_m2—W_cxi | 0.0 (5) |
O5—O2—W1ix | 82.6 (4) | Baxi—Ti_m2—Mg_m2 | 0 |
O5—O2—Nb_m1(1) | 124.9 (3) | W_c—Ti_m2—W_cxi | 180.0 (5) |
O6ii—O2—O7ix | 75.8 (4) | W_c—Ti_m2—Mg_m2 | 0 |
O6ii—O2—O7ii | 50.0 (3) | W_cxi—Ti_m2—Mg_m2 | 0 |
O6ii—O2—Oh | 57.0 (3) | Ti_m1(2)—Mg_m2—Ti_m1(2)xii | 180.0 (5) |
O6ii—O2—Ohii | 112.1 (3) | Ti_m1(2)—Mg_m2—Fe_m2 | 0 |
O6ii—O2—W1ix | 144.0 (2) | Ti_m1(2)—Mg_m2—Si2 | 62.20 (5) |
O6ii—O2—Nb_m1(1) | 83.1 (3) | Ti_m1(2)—Mg_m2—Si2xi | 62.20 (5) |
O7ix—O2—O7ii | 74.1 (3) | Ti_m1(2)—Mg_m2—Si2xii | 117.80 (5) |
O7ix—O2—Oh | 115.2 (5) | Ti_m1(2)—Mg_m2—Si2vi | 117.80 (5) |
O7ix—O2—Ohii | 153.2 (3) | Ti_m1(2)—Mg_m2—O1 | 41.05 (16) |
O7ix—O2—W1ix | 88.6 (3) | Ti_m1(2)—Mg_m2—O1xi | 41.05 (16) |
O7ix—O2—Nb_m1(1) | 157.6 (6) | Ti_m1(2)—Mg_m2—O1xii | 138.95 (16) |
O7ii—O2—Oh | 100.3 (3) | Ti_m1(2)—Mg_m2—O1vi | 138.95 (16) |
O7ii—O2—Ohii | 91.4 (3) | Ti_m1(2)—Mg_m2—O5 | 90 |
O7ii—O2—W1ix | 94.7 (3) | Ti_m1(2)—Mg_m2—O5xi | 90 |
O7ii—O2—Nb_m1(1) | 98.24 (19) | Ti_m1(2)—Mg_m2—Ba | 90 |
Oh—O2—Ohii | 89.1 (3) | Ti_m1(2)—Mg_m2—Baxi | 90 |
Oh—O2—W1ix | 154.5 (5) | Ti_m1(2)—Mg_m2—W_c | 90 |
Oh—O2—Nb_m1(1) | 44.4 (3) | Ti_m1(2)—Mg_m2—W_cxi | 90 |
Ohii—O2—W1ix | 70.0 (3) | Ti_m1(2)—Mg_m2—Ti_m2 | 0 |
Ohii—O2—Nb_m1(1) | 44.7 (3) | Ti_m1(2)xii—Mg_m2—Fe_m2 | 0 |
W1ix—O2—Nb_m1(1) | 113.3 (5) | Ti_m1(2)xii—Mg_m2—Si2 | 117.80 (5) |
Na_aiii—O3—K_b | 170.6 (2) | Ti_m1(2)xii—Mg_m2—Si2xi | 117.80 (5) |
Na_aiii—O3—Ti_m1(1) | 76.7 (2) | Ti_m1(2)xii—Mg_m2—Si2xii | 62.20 (5) |
Na_aiii—O3—Si1 | 77.5 (4) | Ti_m1(2)xii—Mg_m2—Si2vi | 62.20 (5) |
Na_aiii—O3—O2 | 114.5 (4) | Ti_m1(2)xii—Mg_m2—O1 | 138.95 (16) |
Na_aiii—O3—O2ii | 42.7 (2) | Ti_m1(2)xii—Mg_m2—O1xi | 138.95 (16) |
Na_aiii—O3—O3vi | 116.6 (2) | Ti_m1(2)xii—Mg_m2—O1xii | 41.05 (16) |
Na_aiii—O3—O4 | 104.9 (3) | Ti_m1(2)xii—Mg_m2—O1vi | 41.05 (16) |
Na_aiii—O3—O6 | 87.3 (4) | Ti_m1(2)xii—Mg_m2—O5 | 90 |
Na_aiii—O3—O7 | 45.0 (4) | Ti_m1(2)xii—Mg_m2—O5xi | 90 |
Na_aiii—O3—Oh | 57.2 (3) | Ti_m1(2)xii—Mg_m2—Ba | 90 |
Na_aiii—O3—Ohii | 101.8 (2) | Ti_m1(2)xii—Mg_m2—Baxi | 90 |
Na_aiii—O3—Ba | 81.6 (4) | Ti_m1(2)xii—Mg_m2—W_c | 90 |
Na_aiii—O3—W_c | 81.6 (4) | Ti_m1(2)xii—Mg_m2—W_cxi | 90 |
Na_aiii—O3—Nb_m1(1) | 76.7 (2) | Ti_m1(2)xii—Mg_m2—Ti_m2 | 0 |
K_b—O3—Ti_m1(1) | 112.67 (19) | Fe_m2—Mg_m2—Si2 | 0 |
K_b—O3—Si1 | 96.7 (5) | Fe_m2—Mg_m2—Si2xi | 0 |
K_b—O3—O2 | 74.0 (2) | Fe_m2—Mg_m2—Si2xii | 0 |
K_b—O3—O2ii | 144.9 (3) | Fe_m2—Mg_m2—Si2vi | 0 |
K_b—O3—O3vi | 54.92 (15) | Fe_m2—Mg_m2—O1 | 0 |
K_b—O3—O4 | 66.9 (3) | Fe_m2—Mg_m2—O1xi | 0 |
K_b—O3—O6 | 91.8 (4) | Fe_m2—Mg_m2—O1xii | 0 |
K_b—O3—O7 | 127.3 (4) | Fe_m2—Mg_m2—O1vi | 0 |
K_b—O3—Oh | 129.0 (4) | Fe_m2—Mg_m2—O5 | 0 |
K_b—O3—Ohii | 86.0 (2) | Fe_m2—Mg_m2—O5xi | 0 |
K_b—O3—Ba | 94.9 (2) | Fe_m2—Mg_m2—Ba | 0 |
K_b—O3—W_c | 94.9 (2) | Fe_m2—Mg_m2—Baxi | 0 |
K_b—O3—Nb_m1(1) | 112.67 (19) | Fe_m2—Mg_m2—W_c | 0 |
Ti_m1(1)—O3—Si1 | 123.3 (4) | Fe_m2—Mg_m2—W_cxi | 0 |
Ti_m1(1)—O3—O2 | 45.02 (17) | Fe_m2—Mg_m2—Ti_m2 | 0 |
Ti_m1(1)—O3—O2ii | 44.50 (17) | Si2—Mg_m2—Si2xi | 124.40 (8) |
Ti_m1(1)—O3—O3vi | 152.0 (5) | Si2—Mg_m2—Si2xii | 180.0 (5) |
Ti_m1(1)—O3—O4 | 153.4 (6) | Si2—Mg_m2—Si2vi | 55.60 (8) |
Ti_m1(1)—O3—O6 | 96.2 (3) | Si2—Mg_m2—O1 | 24.9 (3) |
Ti_m1(1)—O3—O7 | 113.3 (2) | Si2—Mg_m2—O1xi | 101.7 (2) |
Ti_m1(1)—O3—Oh | 44.9 (3) | Si2—Mg_m2—O1xii | 155.1 (3) |
Ti_m1(1)—O3—Ohii | 43.7 (3) | Si2—Mg_m2—O1vi | 78.3 (2) |
Ti_m1(1)—O3—Ba | 106.5 (5) | Si2—Mg_m2—O5 | 29.51 (10) |
Ti_m1(1)—O3—W_c | 106.5 (5) | Si2—Mg_m2—O5xi | 150.49 (10) |
Ti_m1(1)—O3—Nb_m1(1) | 0.0 (5) | Si2—Mg_m2—Ba | 80.55 (12) |
Si1—O3—O2 | 152.8 (6) | Si2—Mg_m2—Baxi | 99.45 (12) |
Si1—O3—O2ii | 84.0 (3) | Si2—Mg_m2—W_c | 80.55 (12) |
Si1—O3—O3vi | 84.5 (3) | Si2—Mg_m2—W_cxi | 99.45 (12) |
Si1—O3—O4 | 36.0 (3) | Si2—Mg_m2—Ti_m2 | 0 |
Si1—O3—O6 | 33.1 (3) | Si2xi—Mg_m2—Si2xii | 55.60 (8) |
Si1—O3—O7 | 35.0 (3) | Si2xi—Mg_m2—Si2vi | 180.0 (5) |
Si1—O3—Oh | 134.3 (3) | Si2xi—Mg_m2—O1 | 101.7 (2) |
Si1—O3—Ohii | 95.4 (5) | Si2xi—Mg_m2—O1xi | 24.9 (3) |
Si1—O3—Ba | 118.5 (3) | Si2xi—Mg_m2—O1xii | 78.3 (2) |
Si1—O3—W_c | 118.5 (3) | Si2xi—Mg_m2—O1vi | 155.1 (3) |
Si1—O3—Nb_m1(1) | 123.3 (4) | Si2xi—Mg_m2—O5 | 150.49 (10) |
O2—O3—O2ii | 89.5 (2) | Si2xi—Mg_m2—O5xi | 29.51 (10) |
O2—O3—O3vi | 108.8 (3) | Si2xi—Mg_m2—Ba | 99.45 (12) |
O2—O3—O4 | 140.5 (3) | Si2xi—Mg_m2—Baxi | 80.55 (12) |
O2—O3—O6 | 120.2 (3) | Si2xi—Mg_m2—W_c | 99.45 (12) |
O2—O3—O7 | 157.7 (3) | Si2xi—Mg_m2—W_cxi | 80.55 (12) |
O2—O3—Oh | 60.2 (3) | Si2xi—Mg_m2—Ti_m2 | 0 |
O2—O3—Ohii | 59.1 (3) | Si2xii—Mg_m2—Si2vi | 124.40 (8) |
O2—O3—Ba | 88.1 (4) | Si2xii—Mg_m2—O1 | 155.1 (3) |
O2—O3—W_c | 88.1 (4) | Si2xii—Mg_m2—O1xi | 78.3 (2) |
O2—O3—Nb_m1(1) | 45.02 (17) | Si2xii—Mg_m2—O1xii | 24.9 (3) |
O2ii—O3—O3vi | 158.3 (2) | Si2xii—Mg_m2—O1vi | 101.7 (2) |
O2ii—O3—O4 | 119.9 (4) | Si2xii—Mg_m2—O5 | 150.49 (10) |
O2ii—O3—O6 | 69.8 (3) | Si2xii—Mg_m2—O5xi | 29.51 (10) |
O2ii—O3—O7 | 69.1 (2) | Si2xii—Mg_m2—Ba | 99.45 (12) |
O2ii—O3—Oh | 59.5 (3) | Si2xii—Mg_m2—Baxi | 80.55 (12) |
O2ii—O3—Ohii | 59.1 (2) | Si2xii—Mg_m2—W_c | 99.45 (12) |
O2ii—O3—Ba | 115.7 (4) | Si2xii—Mg_m2—W_cxi | 80.55 (12) |
O2ii—O3—W_c | 115.7 (4) | Si2xii—Mg_m2—Ti_m2 | 0 |
O2ii—O3—Nb_m1(1) | 44.50 (17) | Si2vi—Mg_m2—O1 | 78.3 (2) |
O3vi—O3—O4 | 51.2 (3) | Si2vi—Mg_m2—O1xi | 155.1 (3) |
O3vi—O3—O6 | 108.4 (4) | Si2vi—Mg_m2—O1xii | 101.7 (2) |
O3vi—O3—O7 | 91.2 (2) | Si2vi—Mg_m2—O1vi | 24.9 (3) |
O3vi—O3—Oh | 119.3 (5) | Si2vi—Mg_m2—O5 | 29.51 (10) |
O3vi—O3—Ohii | 140.4 (3) | Si2vi—Mg_m2—O5xi | 150.49 (10) |
O3vi—O3—Ba | 55.5 (2) | Si2vi—Mg_m2—Ba | 80.55 (12) |
O3vi—O3—W_c | 55.5 (2) | Si2vi—Mg_m2—Baxi | 99.45 (12) |
O3vi—O3—Nb_m1(1) | 152.0 (5) | Si2vi—Mg_m2—W_c | 80.55 (12) |
O4—O3—O6 | 57.7 (4) | Si2vi—Mg_m2—W_cxi | 99.45 (12) |
O4—O3—O7 | 60.4 (3) | Si2vi—Mg_m2—Ti_m2 | 0 |
O4—O3—Oh | 156.3 (4) | O1—Mg_m2—O1xi | 82.1 (2) |
O4—O3—Ohii | 111.7 (6) | O1—Mg_m2—O1xii | 180.0 (5) |
O4—O3—Ba | 100.0 (3) | O1—Mg_m2—O1vi | 97.9 (2) |
O4—O3—W_c | 100.0 (3) | O1—Mg_m2—O5 | 54.4 (3) |
O4—O3—Nb_m1(1) | 153.4 (6) | O1—Mg_m2—O5xi | 125.6 (3) |
O6—O3—O7 | 59.1 (4) | O1—Mg_m2—Ba | 94.2 (4) |
O6—O3—Oh | 129.2 (3) | O1—Mg_m2—Baxi | 85.8 (4) |
O6—O3—Ohii | 62.3 (3) | O1—Mg_m2—W_c | 94.2 (4) |
O6—O3—Ba | 151.6 (2) | O1—Mg_m2—W_cxi | 85.8 (4) |
O6—O3—W_c | 151.6 (2) | O1—Mg_m2—Ti_m2 | 0 |
O6—O3—Nb_m1(1) | 96.2 (3) | O1xi—Mg_m2—O1xii | 97.9 (2) |
O7—O3—Oh | 101.8 (4) | O1xi—Mg_m2—O1vi | 180.0 (5) |
O7—O3—Ohii | 111.1 (4) | O1xi—Mg_m2—O5 | 125.6 (3) |
O7—O3—Ba | 95.6 (3) | O1xi—Mg_m2—O5xi | 54.4 (3) |
O7—O3—W_c | 95.6 (3) | O1xi—Mg_m2—Ba | 85.8 (4) |
O7—O3—Nb_m1(1) | 113.3 (2) | O1xi—Mg_m2—Baxi | 94.2 (4) |
Oh—O3—Ohii | 88.6 (3) | O1xi—Mg_m2—W_c | 85.8 (4) |
Oh—O3—Ba | 64.3 (3) | O1xi—Mg_m2—W_cxi | 94.2 (4) |
Oh—O3—W_c | 64.3 (3) | O1xi—Mg_m2—Ti_m2 | 0 |
Oh—O3—Nb_m1(1) | 44.9 (3) | O1xii—Mg_m2—O1vi | 82.1 (2) |
Ohii—O3—Ba | 145.7 (5) | O1xii—Mg_m2—O5 | 125.6 (3) |
Ohii—O3—W_c | 145.7 (5) | O1xii—Mg_m2—O5xi | 54.4 (3) |
Ohii—O3—Nb_m1(1) | 43.7 (3) | O1xii—Mg_m2—Ba | 85.8 (4) |
Ba—O3—W_c | 0.0 (5) | O1xii—Mg_m2—Baxi | 94.2 (4) |
Ba—O3—Nb_m1(1) | 106.5 (5) | O1xii—Mg_m2—W_c | 85.8 (4) |
W_c—O3—Nb_m1(1) | 106.5 (5) | O1xii—Mg_m2—W_cxi | 94.2 (4) |
K_b—O4—K_bvii | 102.5 (4) | O1xii—Mg_m2—Ti_m2 | 0 |
K_b—O4—Si1 | 88.9 (4) | O1vi—Mg_m2—O5 | 54.4 (3) |
K_b—O4—Si1vi | 88.9 (4) | O1vi—Mg_m2—O5xi | 125.6 (3) |
K_b—O4—O3 | 60.3 (3) | O1vi—Mg_m2—Ba | 94.2 (4) |
K_b—O4—O3vi | 60.3 (3) | O1vi—Mg_m2—Baxi | 85.8 (4) |
K_b—O4—O5iv | 165.4 (8) | O1vi—Mg_m2—W_c | 94.2 (4) |
K_b—O4—O6 | 89.8 (2) | O1vi—Mg_m2—W_cxi | 85.8 (4) |
K_b—O4—O6vi | 89.8 (2) | O1vi—Mg_m2—Ti_m2 | 0 |
K_b—O4—O7 | 120.1 (5) | O5—Mg_m2—O5xi | 180.0 (5) |
K_b—O4—O7vi | 120.1 (5) | O5—Mg_m2—Ba | 69.0 (3) |
K_bvii—O4—Si1 | 113.8 (6) | O5—Mg_m2—Baxi | 111.0 (3) |
K_bvii—O4—Si1vi | 113.8 (6) | O5—Mg_m2—W_c | 69.0 (3) |
K_bvii—O4—O3 | 133.9 (4) | O5—Mg_m2—W_cxi | 111.0 (3) |
K_bvii—O4—O3vi | 133.9 (4) | O5—Mg_m2—Ti_m2 | 0 |
K_bvii—O4—O5iv | 92.2 (5) | O5xi—Mg_m2—Ba | 111.0 (3) |
K_bvii—O4—O6 | 77.7 (5) | O5xi—Mg_m2—Baxi | 69.0 (3) |
K_bvii—O4—O6vi | 77.7 (5) | O5xi—Mg_m2—W_c | 111.0 (3) |
K_bvii—O4—O7 | 117.1 (5) | O5xi—Mg_m2—W_cxi | 69.0 (3) |
K_bvii—O4—O7vi | 117.1 (5) | O5xi—Mg_m2—Ti_m2 | 0 |
Si1—O4—Si1vi | 131.6 (12) | Ba—Mg_m2—Baxi | 180.0 (5) |
Si1—O4—O3 | 34.1 (4) | Ba—Mg_m2—W_c | 0.0 (5) |
Si1—O4—O3vi | 108.4 (9) | Ba—Mg_m2—W_cxi | 180.0 (5) |
Si1—O4—O5iv | 85.1 (3) | Ba—Mg_m2—Ti_m2 | 0 |
Si1—O4—O6 | 36.9 (4) | Baxi—Mg_m2—W_c | 180.0 (5) |
Si1—O4—O6vi | 168.4 (11) | Baxi—Mg_m2—W_cxi | 0.0 (5) |
Si1—O4—O7 | 35.5 (2) | Baxi—Mg_m2—Ti_m2 | 0 |
Si1—O4—O7vi | 111.1 (7) | W_c—Mg_m2—W_cxi | 180.0 (5) |
Si1vi—O4—O3 | 108.4 (9) | W_c—Mg_m2—Ti_m2 | 0 |
Si1vi—O4—O3vi | 34.1 (4) | W_cxi—Mg_m2—Ti_m2 | 0 |
Si1vi—O4—O5iv | 85.1 (3) | | |
Symmetry codes: (i) −x+1, y, −z; (ii) −x+1/2, −y+1/2, −z+1; (iii) −x+1/2, −y+1/2, −z; (iv) x, y, z−1; (v) x+1/2, −y+1/2, z; (vi) x, −y, z; (vii) −x+1, y, −z+1; (viii) −x+1, −y, −z+1; (ix) x, y, z+1; (x) x−1/2, −y+1/2, z; (xi) −x, y, −z+1; (xii) −x, −y, −z+1; (xiii) x, −y, z+1; (xiv) −x, −y, −z; (xv) −x, y, −z. |
Crystal data top
Ba0.7Fe0.5K2.1Mg0.05Na2Nb0.1O33Si8Ti4 | Z = 2 |
Mr = 1206.8 | F(000) = 1167 |
Monoclinic, C2/m | Dx = 3.137 Mg m−3 |
Hall symbol: -C 2y | Synchrotron radiation, λ = 0.414 Å |
a = 13.958 (7) Å | Cell parameters from 3342 reflections |
b = 13.4952 (8) Å | θ = 1.8–19.1° |
c = 7.5836 (11) Å | µ = 0.83 mm−1 |
β = 116.62 (4)° | T = 293 K |
V = 1277.1 (8) Å3 | Anhedral grain |
Data collection top
ESRF ID 09 diffractometer | θmax = 19.1°, θmin = 1.8° |
3342 measured reflections | h = −7→8 |
980 independent reflections | k = −21→20 |
672 reflections with I > 2σ(I) | l = −11→10 |
Rint = 0.065 | |
Refinement top
Refinement on F | 0 restraints |
R[F2 > 2σ(F2)] = 0.082 | 11 constraints |
wR(F2) = 0.147 | Weighting scheme based on measured s.u.'s w = 1/(σ2(F) + 0.0100000007F2) |
S = 1.17 | (Δ/σ)max = 0.045 |
980 reflections | Δρmax = 0.88 e Å−3 |
89 parameters | Δρmin = −1.13 e Å−3 |
Fractional atomic coordinates and isotropic or equivalent isotropic displacement parameters (Å2) top | x | y | z | Uiso*/Ueq | Occ. (<1) |
Na_a | 0.4181 (18) | 0.2648 (6) | 0.0154 (14) | 0.031 (11) | 0.5 |
K_b | 0.4260 (7) | 0 | 0.7119 (5) | 0.032 (4) | |
Ti_m1(1) | 0.25 | 0.25 | 0.5 | 0.028 (3) | 0.95 |
Ti_m1(2) | 0 | 0.22270 (15) | 0.5 | 0.025 (3) | |
Fe_m2 | 0 | 0 | 0.5 | 0.0300 (13)* | 0.5 |
Si1 | 0.3235 (5) | 0.11099 (15) | 0.2585 (3) | 0.021 (3) | |
Si2 | 0.2104 (5) | 0.10971 (15) | 0.8086 (3) | 0.024 (3) | |
O1 | 0.0837 (12) | 0.1107 (4) | 0.6763 (8) | 0.0144 (13)* | |
O2 | 0.2743 (11) | 0.1901 (4) | 0.7496 (8) | 0.0111 (12)* | |
O3 | 0.2730 (12) | 0.1204 (4) | 0.4090 (8) | 0.0132 (12)* | |
O4 | 0.3757 (16) | 0 | 0.2758 (12) | 0.0136 (17)* | |
O5 | 0.2565 (15) | 0 | 0.7933 (11) | 0.0120 (17)* | |
O6 | 0.4179 (12) | 0.1844 (5) | 0.2979 (9) | 0.0220 (15)* | |
O7 | 0.2285 (12) | 0.1245 (4) | 0.0338 (9) | 0.0167 (14)* | |
Oh | 0.1019 (12) | 0.2185 (4) | 0.3909 (8) | 0.0121 (12)* | |
Ba | 0.0893 (4) | 0 | 0.3418 (3) | 0.0185 (5)* | 0.35 |
W1 | 0.5 | 0.1469 (7) | 0 | 0.049 (15) | |
W2 | 0 | 0.1103 (7) | 0 | 0.11 (2) | |
W_c | 0.0893 (4) | 0 | 0.3418 (3) | 0.0185 (5)* | 0.65 |
Nb_m1(1) | 0.25 | 0.25 | 0.5 | 0.028 (3) | 0.05 |
Ti_m2 | 0 | 0 | 0.5 | 0.0300 (13)* | 0.1 |
Mg_m2 | 0 | 0 | 0.5 | 0.0300 (13)* | 0.05 |
Atomic displacement parameters (Å2) top | U11 | U22 | U33 | U12 | U13 | U23 |
Na_a | 0.03 (2) | 0.028 (4) | 0.035 (4) | −0.005 (6) | 0.013 (7) | −0.003 (3) |
K_b | 0.029 (10) | 0.0424 (18) | 0.0193 (14) | 0 | 0.006 (2) | 0 |
Ti_m1(1) | 0.050 (7) | 0.0121 (9) | 0.0154 (9) | 0.0069 (13) | 0.0095 (16) | 0.0030 (6) |
Ti_m1(2) | 0.026 (7) | 0.0109 (9) | 0.0175 (10) | 0 | −0.0089 (16) | 0 |
Si1 | 0.031 (7) | 0.0100 (9) | 0.0110 (10) | 0.0004 (13) | −0.0010 (16) | −0.0006 (6) |
Si2 | 0.040 (7) | 0.0104 (9) | 0.0089 (10) | 0.0038 (13) | −0.0002 (16) | 0.0005 (6) |
W1 | 0.08 (3) | 0.023 (5) | 0.025 (5) | 0 | 0.009 (8) | 0 |
W2 | 0.22 (5) | 0.021 (5) | 0.020 (5) | 0 | −0.003 (10) | 0 |
Nb_m1(1) | 0.050 (7) | 0.0121 (9) | 0.0154 (9) | 0.0069 (13) | 0.0095 (16) | 0.0030 (6) |
Geometric parameters (Å, º) top
Na_a—Na_ai | 2.40 (4) | Si2—O1 | 1.595 (15) |
Na_a—Ti_m1(2)ii | 3.328 (11) | Si2—O1vi | 3.376 (8) |
Na_a—Si1 | 3.410 (19) | Si2—O2 | 1.591 (12) |
Na_a—Si1iii | 3.496 (19) | Si2—O5 | 1.639 (10) |
Na_a—Si2iv | 3.342 (18) | Si2—O6ii | 3.206 (10) |
Na_a—Si2ii | 3.16 (2) | Si2—O7ix | 1.622 (9) |
Na_a—O1ii | 2.888 (16) | Si2—Oh | 3.191 (6) |
Na_a—O2iv | 2.341 (15) | Si2—Ba | 3.496 (3) |
Na_a—O3iii | 3.491 (14) | Si2—W_c | 3.496 (3) |
Na_a—O6 | 2.402 (17) | Si2—Nb_m1(1) | 3.244 (4) |
Na_a—O7 | 3.31 (3) | Si2—Ti_m2 | 3.183 (5) |
Na_a—O7iii | 2.42 (2) | Si2—Mg_m2 | 3.183 (5) |
Na_a—Ohiii | 2.976 (16) | O1—O1xi | 2.647 (12) |
Na_a—Ohv | 2.863 (15) | O1—O1vi | 2.989 (7) |
Na_a—W1 | 1.992 (18) | O1—O2 | 2.69 (2) |
Na_a—W2iii | 2.070 (18) | O1—O5 | 2.63 (2) |
K_b—Si1 | 3.421 (4) | O1—O6ii | 2.772 (8) |
K_b—Si1vi | 3.421 (4) | O1—O7ix | 2.561 (10) |
K_b—O2 | 3.419 (12) | O1—Oh | 2.712 (13) |
K_b—O2vi | 3.419 (12) | O1—Ohxi | 2.81 (2) |
K_b—O3 | 2.842 (9) | O1—Ba | 2.975 (9) |
K_b—O3vi | 2.842 (9) | O1—Baxi | 2.790 (15) |
K_b—O4 | 3.057 (11) | O1—W2ix | 3.156 (13) |
K_b—O4vii | 2.73 (3) | O1—W_c | 2.975 (9) |
K_b—O5 | 2.70 (2) | O1—W_cxi | 2.790 (15) |
K_b—O6vii | 3.330 (14) | O1—Ti_m2 | 1.996 (7) |
K_b—O6viii | 3.330 (14) | O1—Mg_m2 | 1.996 (7) |
K_b—W1ix | 2.784 (8) | O2—O3 | 2.741 (13) |
K_b—W1viii | 2.784 (8) | O2—O3ii | 2.777 (7) |
Ti_m1(1)—Si1 | 3.100 (5) | O2—O5 | 2.613 (7) |
Ti_m1(1)—Si1ii | 3.100 (5) | O2—O6ii | 3.055 (19) |
Ti_m1(1)—Si2 | 3.244 (4) | O2—O7ix | 2.660 (16) |
Ti_m1(1)—Si2ii | 3.244 (4) | O2—O7ii | 3.004 (10) |
Ti_m1(1)—O2 | 1.943 (7) | O2—Oh | 2.733 (11) |
Ti_m1(1)—O2ii | 1.943 (7) | O2—Ohii | 2.700 (19) |
Ti_m1(1)—O3 | 1.959 (7) | O2—W1ix | 2.917 (13) |
Ti_m1(1)—O3ii | 1.959 (7) | O2—Nb_m1(1) | 1.943 (7) |
Ti_m1(1)—O6 | 3.441 (16) | O3—O3vi | 3.249 (7) |
Ti_m1(1)—O6ii | 3.441 (16) | O3—O4 | 2.65 (2) |
Ti_m1(1)—Oh | 1.899 (15) | O3—O5 | 3.433 (15) |
Ti_m1(1)—Ohii | 1.899 (15) | O3—O6 | 2.66 (2) |
Ti_m1(1)—Nb_m1(1) | 0 | O3—O7 | 2.627 (11) |
Ti_m1(2)—Fe_m2 | 3.005 (2) | O3—Oh | 2.68 (2) |
Ti_m1(2)—Si1ii | 3.227 (5) | O3—Ohii | 2.775 (11) |
Ti_m1(2)—Si1x | 3.227 (5) | O3—Ba | 2.882 (14) |
Ti_m1(2)—Si2 | 3.204 (5) | O3—W_c | 2.882 (14) |
Ti_m1(2)—Si2xi | 3.204 (5) | O3—Nb_m1(1) | 1.959 (7) |
Ti_m1(2)—O1 | 2.009 (7) | O4—O5iv | 3.271 (11) |
Ti_m1(2)—O1xi | 2.009 (7) | O4—O6 | 2.546 (9) |
Ti_m1(2)—O2 | 3.456 (14) | O4—O6vi | 2.546 (9) |
Ti_m1(2)—O2xi | 3.456 (14) | O4—O7 | 2.652 (14) |
Ti_m1(2)—O6ii | 1.913 (7) | O4—O7vi | 2.652 (14) |
Ti_m1(2)—O6x | 1.913 (7) | O5—O7ix | 2.634 (15) |
Ti_m1(2)—Oh | 1.940 (16) | O5—O7xiii | 2.634 (15) |
Ti_m1(2)—Ohxi | 1.940 (16) | O5—Ba | 3.164 (9) |
Ti_m1(2)—Ti_m2 | 3.005 (2) | O5—W_c | 3.164 (9) |
Ti_m1(2)—Mg_m2 | 3.005 (2) | O5—Ti_m2 | 3.261 (18) |
Fe_m2—Si2 | 3.183 (5) | O5—Mg_m2 | 3.261 (18) |
Fe_m2—Si2xi | 3.183 (5) | O6—O6vii | 2.890 (11) |
Fe_m2—Si2xii | 3.183 (5) | O6—O7 | 2.629 (17) |
Fe_m2—Si2vi | 3.183 (5) | O6—Ohii | 2.819 (14) |
Fe_m2—O1 | 1.996 (7) | O6—Ohv | 2.68 (2) |
Fe_m2—O1xi | 1.996 (7) | O6—W1 | 2.999 (14) |
Fe_m2—O1xii | 1.996 (7) | O6—Nb_m1(1) | 3.441 (16) |
Fe_m2—O1vi | 1.996 (7) | O7—O7vi | 3.359 (8) |
Fe_m2—O5 | 3.261 (18) | O7—W2 | 3.089 (17) |
Fe_m2—O5xi | 3.261 (18) | Oh—Ba | 2.967 (5) |
Fe_m2—Ba | 2.081 (5) | Oh—W1iii | 3.214 (8) |
Fe_m2—Baxi | 2.081 (5) | Oh—W2 | 3.028 (7) |
Fe_m2—W_c | 2.081 (5) | Oh—W_c | 2.967 (5) |
Fe_m2—W_cxi | 2.081 (5) | Oh—Nb_m1(1) | 1.899 (15) |
Fe_m2—Ti_m2 | 0 | Ba—W2 | 2.755 (6) |
Fe_m2—Mg_m2 | 0 | Ba—W2xiv | 2.755 (6) |
Si1—Si1vi | 2.996 (3) | Ba—W_c | 0 |
Si1—Si2iv | 3.051 (4) | Ba—Ti_m2 | 2.081 (5) |
Si1—O2ii | 3.000 (9) | Ba—Mg_m2 | 2.081 (5) |
Si1—O3 | 1.593 (15) | W1—W2iii | 3.277 (14) |
Si1—O4 | 1.645 (10) | W2—W2xiv | 2.976 (14) |
Si1—O6 | 1.566 (15) | W2—W_c | 2.755 (6) |
Si1—O7 | 1.635 (8) | W2—W_cxv | 2.755 (6) |
Si1—Ohii | 3.312 (6) | W_c—Ti_m2 | 2.081 (5) |
Si1—Nb_m1(1) | 3.100 (5) | W_c—Mg_m2 | 2.081 (5) |
Si2—Si2vi | 2.961 (3) | Ti_m2—Mg_m2 | 0 |
| | | |
Na_ai—Na_a—Ti_m1(2)ii | 103.7 (5) | O5iv—O4—O6 | 93.5 (3) |
Na_ai—Na_a—Si1 | 132.0 (5) | O5iv—O4—O6vi | 93.5 (3) |
Na_ai—Na_a—Si1iii | 130.5 (5) | O5iv—O4—O7 | 51.5 (3) |
Na_ai—Na_a—Si2iv | 128.2 (5) | O5iv—O4—O7vi | 51.5 (3) |
Na_ai—Na_a—Si2ii | 141.8 (5) | O6—O4—O6vi | 155.7 (11) |
Na_ai—Na_a—O1ii | 115.7 (7) | O6—O4—O7 | 60.7 (3) |
Na_ai—Na_a—O2iv | 113.7 (8) | O6—O4—O7vi | 138.5 (5) |
Na_ai—Na_a—O3iii | 106.1 (6) | O6vi—O4—O7 | 138.5 (5) |
Na_ai—Na_a—O6 | 117.9 (8) | O6vi—O4—O7vi | 60.7 (3) |
Na_ai—Na_a—O7 | 145.0 (5) | O7—O4—O7vi | 78.6 (5) |
Na_ai—Na_a—O7iii | 139.5 (6) | K_b—O5—Fe_m2 | 130.6 (3) |
Na_ai—Na_a—Ohiii | 63.3 (6) | K_b—O5—Si2 | 115.4 (7) |
Na_ai—Na_a—Ohv | 68.2 (6) | K_b—O5—Si2vi | 115.4 (7) |
Na_ai—Na_a—W1 | 53.0 (6) | K_b—O5—O1 | 133.5 (4) |
Na_ai—Na_a—W2iii | 54.6 (6) | K_b—O5—O1vi | 133.5 (4) |
Ti_m1(2)ii—Na_a—Si1 | 57.2 (3) | K_b—O5—O2 | 80.1 (6) |
Ti_m1(2)ii—Na_a—Si1iii | 113.2 (6) | K_b—O5—O2vi | 80.1 (6) |
Ti_m1(2)ii—Na_a—Si2iv | 110.3 (6) | K_b—O5—O3 | 53.6 (4) |
Ti_m1(2)ii—Na_a—Si2ii | 59.1 (3) | K_b—O5—O3vi | 53.6 (4) |
Ti_m1(2)ii—Na_a—O1ii | 36.85 (19) | K_b—O5—O4ix | 101.4 (6) |
Ti_m1(2)ii—Na_a—O2iv | 135.3 (9) | K_b—O5—O7ix | 125.1 (6) |
Ti_m1(2)ii—Na_a—O3iii | 137.6 (6) | K_b—O5—O7xiii | 125.1 (6) |
Ti_m1(2)ii—Na_a—O6 | 34.4 (2) | K_b—O5—Ba | 92.8 (4) |
Ti_m1(2)ii—Na_a—O7 | 82.4 (4) | K_b—O5—W_c | 92.8 (4) |
Ti_m1(2)ii—Na_a—O7iii | 89.3 (5) | K_b—O5—Ti_m2 | 130.6 (3) |
Ti_m1(2)ii—Na_a—Ohiii | 165.0 (8) | K_b—O5—Mg_m2 | 130.6 (3) |
Ti_m1(2)ii—Na_a—Ohv | 35.5 (3) | Fe_m2—O5—Si2 | 72.7 (6) |
Ti_m1(2)ii—Na_a—W1 | 100.6 (4) | Fe_m2—O5—Si2vi | 72.7 (6) |
Ti_m1(2)ii—Na_a—W2iii | 95.5 (3) | Fe_m2—O5—O1 | 37.7 (3) |
Si1—Na_a—Si1iii | 96.3 (6) | Fe_m2—O5—O1vi | 37.7 (3) |
Si1—Na_a—Si2iv | 53.7 (3) | Fe_m2—O5—O2 | 92.9 (4) |
Si1—Na_a—Si2ii | 70.6 (5) | Fe_m2—O5—O2vi | 92.9 (4) |
Si1—Na_a—O1ii | 76.7 (5) | Fe_m2—O5—O3 | 83.8 (3) |
Si1—Na_a—O2iv | 79.3 (6) | Fe_m2—O5—O3vi | 83.8 (3) |
Si1—Na_a—O3iii | 116.6 (7) | Fe_m2—O5—O4ix | 128.0 (8) |
Si1—Na_a—O6 | 24.2 (4) | Fe_m2—O5—O7ix | 90.8 (6) |
Si1—Na_a—O7 | 28.1 (2) | Fe_m2—O5—O7xiii | 90.8 (6) |
Si1—Na_a—O7iii | 87.4 (7) | Fe_m2—O5—Ba | 37.76 (19) |
Si1—Na_a—Ohiii | 136.6 (4) | Fe_m2—O5—W_c | 37.76 (19) |
Si1—Na_a—Ohv | 84.4 (4) | Fe_m2—O5—Ti_m2 | 0.0 (5) |
Si1—Na_a—W1 | 85.3 (4) | Fe_m2—O5—Mg_m2 | 0.0 (5) |
Si1—Na_a—W2iii | 152.1 (5) | Si2—O5—Si2vi | 129.2 (14) |
Si1iii—Na_a—Si2iv | 67.6 (4) | Si2—O5—O1 | 35.0 (4) |
Si1iii—Na_a—Si2ii | 54.2 (3) | Si2—O5—O1vi | 101.9 (10) |
Si1iii—Na_a—O1ii | 81.1 (5) | Si2—O5—O2 | 35.4 (4) |
Si1iii—Na_a—O2iv | 57.9 (4) | Si2—O5—O2vi | 163.4 (12) |
Si1iii—Na_a—O3iii | 26.4 (3) | Si2—O5—O3 | 79.1 (4) |
Si1iii—Na_a—O6 | 111.1 (9) | Si2—O5—O3vi | 131.7 (4) |
Si1iii—Na_a—O7 | 73.9 (5) | Si2—O5—O4ix | 86.6 (4) |
Si1iii—Na_a—O7iii | 24.5 (2) | Si2—O5—O7ix | 35.9 (3) |
Si1iii—Na_a—Ohiii | 74.4 (4) | Si2—O5—O7xiii | 110.0 (9) |
Si1iii—Na_a—Ohv | 138.5 (5) | Si2—O5—Ba | 87.4 (4) |
Si1iii—Na_a—W1 | 140.7 (4) | Si2—O5—W_c | 87.4 (4) |
Si1iii—Na_a—W2iii | 89.2 (4) | Si2—O5—Ti_m2 | 72.7 (6) |
Si2iv—Na_a—Si2ii | 89.8 (6) | Si2—O5—Mg_m2 | 72.7 (6) |
Si2iv—Na_a—O1ii | 115.1 (8) | Si2vi—O5—O1 | 101.9 (10) |
Si2iv—Na_a—O2iv | 25.5 (3) | Si2vi—O5—O1vi | 35.0 (4) |
Si2iv—Na_a—O3iii | 72.6 (4) | Si2vi—O5—O2 | 163.4 (12) |
Si2iv—Na_a—O6 | 77.8 (6) | Si2vi—O5—O2vi | 35.4 (4) |
Si2iv—Na_a—O7 | 28.2 (2) | Si2vi—O5—O3 | 131.7 (4) |
Si2iv—Na_a—O7iii | 79.6 (6) | Si2vi—O5—O3vi | 79.1 (4) |
Si2iv—Na_a—Ohiii | 84.4 (3) | Si2vi—O5—O4ix | 86.6 (4) |
Si2iv—Na_a—Ohv | 135.9 (5) | Si2vi—O5—O7ix | 110.0 (9) |
Si2iv—Na_a—W1 | 82.7 (4) | Si2vi—O5—O7xiii | 35.9 (3) |
Si2iv—Na_a—W2iii | 150.3 (4) | Si2vi—O5—Ba | 87.4 (4) |
Si2ii—Na_a—O1ii | 30.1 (3) | Si2vi—O5—W_c | 87.4 (4) |
Si2ii—Na_a—O2iv | 99.5 (8) | Si2vi—O5—Ti_m2 | 72.7 (6) |
Si2ii—Na_a—O3iii | 78.9 (4) | Si2vi—O5—Mg_m2 | 72.7 (6) |
Si2ii—Na_a—O6 | 68.8 (6) | O1—O5—O1vi | 69.2 (6) |
Si2ii—Na_a—O7 | 70.9 (5) | O1—O5—O2 | 61.6 (4) |
Si2ii—Na_a—O7iii | 30.2 (3) | O1—O5—O2vi | 129.8 (7) |
Si2ii—Na_a—Ohiii | 126.0 (5) | O1—O5—O3 | 81.1 (4) |
Si2ii—Na_a—Ohv | 87.9 (4) | O1—O5—O3vi | 112.5 (3) |
Si2ii—Na_a—W1 | 154.2 (6) | O1—O5—O4ix | 107.9 (6) |
Si2ii—Na_a—W2iii | 91.1 (4) | O1—O5—O7ix | 58.2 (4) |
O1ii—Na_a—O2iv | 129.2 (11) | O1—O5—O7xiii | 101.4 (8) |
O1ii—Na_a—O3iii | 102.0 (5) | O1—O5—Ba | 61.0 (3) |
O1ii—Na_a—O6 | 62.4 (4) | O1—O5—W_c | 61.0 (3) |
O1ii—Na_a—O7 | 90.1 (7) | O1—O5—Ti_m2 | 37.7 (3) |
O1ii—Na_a—O7iii | 56.8 (4) | O1—O5—Mg_m2 | 37.7 (3) |
O1ii—Na_a—Ohiii | 139.8 (4) | O1vi—O5—O2 | 129.8 (7) |
O1ii—Na_a—Ohv | 58.5 (4) | O1vi—O5—O2vi | 61.6 (4) |
O1ii—Na_a—W1 | 136.5 (5) | O1vi—O5—O3 | 112.5 (3) |
O1ii—Na_a—W2iii | 77.1 (4) | O1vi—O5—O3vi | 81.1 (4) |
O2iv—Na_a—O3iii | 52.5 (3) | O1vi—O5—O4ix | 107.9 (6) |
O2iv—Na_a—O6 | 103.3 (8) | O1vi—O5—O7ix | 101.4 (8) |
O2iv—Na_a—O7 | 52.9 (5) | O1vi—O5—O7xiii | 58.2 (4) |
O2iv—Na_a—O7iii | 78.1 (7) | O1vi—O5—Ba | 61.0 (3) |
O2iv—Na_a—Ohiii | 59.6 (4) | O1vi—O5—W_c | 61.0 (3) |
O2iv—Na_a—Ohv | 158.6 (4) | O1vi—O5—Ti_m2 | 37.7 (3) |
O2iv—Na_a—W1 | 84.2 (4) | O1vi—O5—Mg_m2 | 37.7 (3) |
O2iv—Na_a—W2iii | 125.7 (5) | O2—O5—O2vi | 158.1 (9) |
O3iii—Na_a—O6 | 135.8 (10) | O2—O5—O3 | 51.8 (3) |
O3iii—Na_a—O7 | 89.9 (5) | O2—O5—O3vi | 108.1 (5) |
O3iii—Na_a—O7iii | 48.8 (3) | O2—O5—O4ix | 96.5 (2) |
O3iii—Na_a—Ohiii | 48.2 (4) | O2—O5—O7ix | 60.9 (3) |
O3iii—Na_a—Ohv | 148.9 (4) | O2—O5—O7xiii | 140.0 (6) |
O3iii—Na_a—W1 | 121.5 (5) | O2—O5—Ba | 85.9 (2) |
O3iii—Na_a—W2iii | 78.4 (3) | O2—O5—W_c | 85.9 (2) |
O6—Na_a—O7 | 51.9 (5) | O2—O5—Ti_m2 | 92.9 (4) |
O6—Na_a—O7iii | 94.4 (9) | O2—O5—Mg_m2 | 92.9 (4) |
O6—Na_a—Ohiii | 157.1 (4) | O2vi—O5—O3 | 108.1 (5) |
O6—Na_a—Ohv | 60.5 (5) | O2vi—O5—O3vi | 51.8 (3) |
O6—Na_a—W1 | 85.5 (4) | O2vi—O5—O4ix | 96.5 (2) |
O6—Na_a—W2iii | 129.7 (5) | O2vi—O5—O7ix | 140.0 (6) |
O7—Na_a—O7iii | 73.9 (7) | O2vi—O5—O7xiii | 60.9 (3) |
O7—Na_a—Ohiii | 112.4 (5) | O2vi—O5—Ba | 85.9 (2) |
O7—Na_a—Ohv | 112.4 (5) | O2vi—O5—W_c | 85.9 (2) |
O7—Na_a—W1 | 92.1 (5) | O2vi—O5—Ti_m2 | 92.9 (4) |
O7—Na_a—W2iii | 160.3 (9) | O2vi—O5—Mg_m2 | 92.9 (4) |
O7iii—Na_a—Ohiii | 96.5 (4) | O3—O5—O3vi | 56.5 (3) |
O7iii—Na_a—Ohv | 115.0 (5) | O3—O5—O4ix | 139.1 (6) |
O7iii—Na_a—W1 | 161.8 (8) | O3—O5—O7ix | 111.9 (2) |
O7iii—Na_a—W2iii | 86.5 (5) | O3—O5—O7xiii | 167.6 (2) |
Ohiii—Na_a—Ohv | 130.6 (10) | O3—O5—Ba | 51.6 (2) |
Ohiii—Na_a—W1 | 77.9 (6) | O3—O5—W_c | 51.6 (2) |
Ohiii—Na_a—W2iii | 71.2 (5) | O3—O5—Ti_m2 | 83.8 (3) |
Ohv—Na_a—W1 | 80.8 (6) | O3—O5—Mg_m2 | 83.8 (3) |
Ohv—Na_a—W2iii | 73.8 (5) | O3vi—O5—O4ix | 139.1 (6) |
W1—Na_a—W2iii | 107.5 (12) | O3vi—O5—O7ix | 167.6 (2) |
Si1—K_b—Si1vi | 51.93 (7) | O3vi—O5—O7xiii | 111.9 (2) |
Si1—K_b—O2 | 76.10 (16) | O3vi—O5—Ba | 51.6 (2) |
Si1—K_b—O2vi | 114.6 (2) | O3vi—O5—W_c | 51.6 (2) |
Si1—K_b—O3 | 27.5 (3) | O3vi—O5—Ti_m2 | 83.8 (3) |
Si1—K_b—O3vi | 67.28 (16) | O3vi—O5—Mg_m2 | 83.8 (3) |
Si1—K_b—O4 | 28.72 (18) | O4ix—O5—O7ix | 52.0 (3) |
Si1—K_b—O4vii | 89.7 (3) | O4ix—O5—O7xiii | 52.0 (3) |
Si1—K_b—O5 | 102.4 (3) | O4ix—O5—Ba | 165.8 (9) |
Si1—K_b—O6vii | 68.51 (17) | O4ix—O5—W_c | 165.8 (9) |
Si1—K_b—O6viii | 106.7 (2) | O4ix—O5—Ti_m2 | 128.0 (8) |
Si1—K_b—W1ix | 108.54 (15) | O4ix—O5—Mg_m2 | 128.0 (8) |
Si1—K_b—W1viii | 160.34 (17) | O7ix—O5—O7xiii | 79.2 (5) |
Si1vi—K_b—O2 | 114.6 (2) | O7ix—O5—Ba | 118.9 (6) |
Si1vi—K_b—O2vi | 76.10 (16) | O7ix—O5—W_c | 118.9 (6) |
Si1vi—K_b—O3 | 67.28 (16) | O7ix—O5—Ti_m2 | 90.8 (6) |
Si1vi—K_b—O3vi | 27.5 (3) | O7ix—O5—Mg_m2 | 90.8 (6) |
Si1vi—K_b—O4 | 28.72 (18) | O7xiii—O5—Ba | 118.9 (6) |
Si1vi—K_b—O4vii | 89.7 (3) | O7xiii—O5—W_c | 118.9 (6) |
Si1vi—K_b—O5 | 102.4 (3) | O7xiii—O5—Ti_m2 | 90.8 (6) |
Si1vi—K_b—O6vii | 106.7 (2) | O7xiii—O5—Mg_m2 | 90.8 (6) |
Si1vi—K_b—O6viii | 68.51 (17) | Ba—O5—W_c | 0.0 (5) |
Si1vi—K_b—W1ix | 160.34 (17) | Ba—O5—Ti_m2 | 37.76 (19) |
Si1vi—K_b—W1viii | 108.54 (15) | Ba—O5—Mg_m2 | 37.76 (19) |
O2—K_b—O2vi | 97.2 (4) | W_c—O5—Ti_m2 | 37.76 (19) |
O2—K_b—O3 | 50.9 (3) | W_c—O5—Mg_m2 | 37.76 (19) |
O2—K_b—O3vi | 103.1 (4) | Ti_m2—O5—Mg_m2 | 0.0 (5) |
O2—K_b—O4 | 103.9 (3) | Na_a—O6—K_bvii | 93.2 (6) |
O2—K_b—O4vii | 130.9 (2) | Na_a—O6—Ti_m1(1) | 123.7 (6) |
O2—K_b—O5 | 48.8 (2) | Na_a—O6—Ti_m1(2)ii | 100.3 (5) |
O2—K_b—O6vii | 82.9 (3) | Na_a—O6—Si1 | 116.9 (5) |
O2—K_b—O6viii | 176.82 (18) | Na_a—O6—Si2ii | 66.9 (5) |
O2—K_b—W1ix | 54.95 (18) | Na_a—O6—O1ii | 67.4 (4) |
O2—K_b—W1viii | 119.6 (3) | Na_a—O6—O2ii | 89.8 (6) |
O2vi—K_b—O3 | 103.1 (4) | Na_a—O6—O3 | 137.2 (8) |
O2vi—K_b—O3vi | 50.9 (3) | Na_a—O6—O4 | 118.4 (5) |
O2vi—K_b—O4 | 103.9 (3) | Na_a—O6—O6vii | 128.9 (8) |
O2vi—K_b—O4vii | 130.9 (2) | Na_a—O6—O7 | 82.1 (5) |
O2vi—K_b—O5 | 48.8 (2) | Na_a—O6—Ohii | 125.2 (4) |
O2vi—K_b—O6vii | 176.82 (18) | Na_a—O6—Ohv | 68.3 (6) |
O2vi—K_b—O6viii | 82.9 (3) | Na_a—O6—W1 | 41.5 (5) |
O2vi—K_b—W1ix | 119.6 (3) | Na_a—O6—Nb_m1(1) | 123.7 (6) |
O2vi—K_b—W1viii | 54.95 (18) | K_bvii—O6—Ti_m1(1) | 141.7 (3) |
O3—K_b—O3vi | 69.7 (2) | K_bvii—O6—Ti_m1(2)ii | 110.1 (6) |
O3—K_b—O4 | 53.2 (4) | K_bvii—O6—Si1 | 91.5 (4) |
O3—K_b—O4vii | 114.3 (4) | K_bvii—O6—Si2ii | 159.9 (5) |
O3—K_b—O5 | 76.5 (4) | K_bvii—O6—O1ii | 140.6 (7) |
O3—K_b—O6vii | 79.5 (3) | K_bvii—O6—O2ii | 163.8 (4) |
O3—K_b—O6viii | 132.2 (3) | K_bvii—O6—O3 | 111.2 (3) |
O3—K_b—W1ix | 96.15 (19) | K_bvii—O6—O4 | 53.3 (6) |
O3—K_b—W1viii | 157.1 (5) | K_bvii—O6—O6vii | 78.9 (4) |
O3vi—K_b—O4 | 53.2 (4) | K_bvii—O6—O7 | 101.4 (3) |
O3vi—K_b—O4vii | 114.3 (4) | K_bvii—O6—Ohii | 132.6 (3) |
O3vi—K_b—O5 | 76.5 (4) | K_bvii—O6—Ohv | 79.2 (5) |
O3vi—K_b—O6vii | 132.2 (3) | K_bvii—O6—W1 | 51.9 (3) |
O3vi—K_b—O6viii | 79.5 (3) | K_bvii—O6—Nb_m1(1) | 141.7 (3) |
O3vi—K_b—W1ix | 157.1 (5) | Ti_m1(1)—O6—Ti_m1(2)ii | 76.0 (4) |
O3vi—K_b—W1viii | 96.15 (19) | Ti_m1(1)—O6—Si1 | 64.2 (6) |
O4—K_b—O4vii | 77.0 (5) | Ti_m1(1)—O6—Si2ii | 58.3 (3) |
O4—K_b—O5 | 116.6 (5) | Ti_m1(1)—O6—O1ii | 71.6 (4) |
O4—K_b—O6vii | 79.1 (3) | Ti_m1(1)—O6—O2ii | 34.2 (2) |
O4—K_b—O6viii | 79.1 (3) | Ti_m1(1)—O6—O3 | 34.5 (2) |
O4—K_b—W1ix | 132.3 (2) | Ti_m1(1)—O6—O4 | 95.6 (7) |
O4—K_b—W1viii | 132.3 (2) | Ti_m1(1)—O6—O6vii | 84.4 (4) |
O4vii—K_b—O5 | 166.4 (3) | Ti_m1(1)—O6—O7 | 76.4 (5) |
O4vii—K_b—O6vii | 48.5 (3) | Ti_m1(1)—O6—Ohii | 33.5 (3) |
O4vii—K_b—O6viii | 48.5 (3) | Ti_m1(1)—O6—Ohv | 121.4 (3) |
O4vii—K_b—W1ix | 87.7 (2) | Ti_m1(1)—O6—W1 | 161.0 (3) |
O4vii—K_b—W1viii | 87.7 (2) | Ti_m1(1)—O6—Nb_m1(1) | 0.0 (5) |
O5—K_b—O6vii | 130.9 (3) | Ti_m1(2)ii—O6—Si1 | 135.9 (8) |
O5—K_b—O6viii | 130.9 (3) | Ti_m1(2)ii—O6—Si2ii | 72.6 (3) |
O5—K_b—W1ix | 82.8 (2) | Ti_m1(2)ii—O6—O1ii | 46.4 (2) |
O5—K_b—W1viii | 82.8 (2) | Ti_m1(2)ii—O6—O2ii | 84.9 (4) |
O6vii—K_b—O6viii | 96.7 (4) | Ti_m1(2)ii—O6—O3 | 103.1 (5) |
O6vii—K_b—W1ix | 57.9 (2) | Ti_m1(2)ii—O6—O4 | 137.0 (4) |
O6vii—K_b—W1viii | 122.2 (3) | Ti_m1(2)ii—O6—O6vii | 40.9 (2) |
O6viii—K_b—W1ix | 122.2 (3) | Ti_m1(2)ii—O6—O7 | 148.1 (8) |
O6viii—K_b—W1viii | 57.9 (2) | Ti_m1(2)ii—O6—Ohii | 43.4 (4) |
W1ix—K_b—W1viii | 90.8 (2) | Ti_m1(2)ii—O6—Ohv | 46.3 (4) |
Si1—Ti_m1(1)—Si1ii | 180.0 (5) | Ti_m1(2)ii—O6—W1 | 114.8 (7) |
Si1—Ti_m1(1)—Si2 | 106.35 (9) | Ti_m1(2)ii—O6—Nb_m1(1) | 76.0 (4) |
Si1—Ti_m1(1)—Si2ii | 73.65 (9) | Si1—O6—Si2ii | 100.0 (7) |
Si1—Ti_m1(1)—O2 | 111.3 (3) | Si1—O6—O1ii | 127.7 (9) |
Si1—Ti_m1(1)—O2ii | 68.7 (3) | Si1—O6—O2ii | 73.1 (6) |
Si1—Ti_m1(1)—O3 | 26.1 (4) | Si1—O6—O3 | 33.0 (4) |
Si1—Ti_m1(1)—O3ii | 153.9 (4) | Si1—O6—O4 | 38.6 (5) |
Si1—Ti_m1(1)—O6 | 27.07 (18) | Si1—O6—O6vii | 113.7 (5) |
Si1—Ti_m1(1)—O6ii | 152.93 (18) | Si1—O6—O7 | 35.6 (3) |
Si1—Ti_m1(1)—Oh | 101.0 (3) | Si1—O6—Ohii | 93.7 (7) |
Si1—Ti_m1(1)—Ohii | 79.0 (3) | Si1—O6—Ohv | 169.7 (6) |
Si1—Ti_m1(1)—Nb_m1(1) | 0 | Si1—O6—W1 | 108.8 (4) |
Si1ii—Ti_m1(1)—Si2 | 73.65 (9) | Si1—O6—Nb_m1(1) | 64.2 (6) |
Si1ii—Ti_m1(1)—Si2ii | 106.35 (9) | Si2ii—O6—O1ii | 29.8 (3) |
Si1ii—Ti_m1(1)—O2 | 68.7 (3) | Si2ii—O6—O2ii | 29.3 (2) |
Si1ii—Ti_m1(1)—O2ii | 111.3 (3) | Si2ii—O6—O3 | 86.8 (5) |
Si1ii—Ti_m1(1)—O3 | 153.9 (4) | Si2ii—O6—O4 | 138.1 (7) |
Si1ii—Ti_m1(1)—O3ii | 26.1 (4) | Si2ii—O6—O6vii | 110.8 (3) |
Si1ii—Ti_m1(1)—O6 | 152.93 (18) | Si2ii—O6—O7 | 79.5 (4) |
Si1ii—Ti_m1(1)—O6ii | 27.07 (18) | Si2ii—O6—Ohii | 63.6 (3) |
Si1ii—Ti_m1(1)—Oh | 79.0 (3) | Si2ii—O6—Ohv | 90.2 (3) |
Si1ii—Ti_m1(1)—Ohii | 101.0 (3) | Si2ii—O6—W1 | 108.4 (3) |
Si1ii—Ti_m1(1)—Nb_m1(1) | 0 | Si2ii—O6—Nb_m1(1) | 58.3 (3) |
Si2—Ti_m1(1)—Si2ii | 180.0 (5) | O1ii—O6—O2ii | 54.6 (4) |
Si2—Ti_m1(1)—O2 | 21.0 (3) | O1ii—O6—O3 | 105.7 (6) |
Si2—Ti_m1(1)—O2ii | 159.0 (3) | O1ii—O6—O4 | 166.1 (10) |
Si2—Ti_m1(1)—O3 | 80.8 (3) | O1ii—O6—O6vii | 87.3 (3) |
Si2—Ti_m1(1)—O3ii | 99.2 (3) | O1ii—O6—O7 | 108.9 (5) |
Si2—Ti_m1(1)—O6 | 122.78 (14) | O1ii—O6—Ohii | 58.0 (3) |
Si2—Ti_m1(1)—O6ii | 57.22 (14) | O1ii—O6—Ohv | 62.0 (4) |
Si2—Ti_m1(1)—Oh | 71.3 (2) | O1ii—O6—W1 | 103.8 (5) |
Si2—Ti_m1(1)—Ohii | 108.7 (2) | O1ii—O6—Nb_m1(1) | 71.6 (4) |
Si2—Ti_m1(1)—Nb_m1(1) | 0 | O2ii—O6—O3 | 57.7 (4) |
Si2ii—Ti_m1(1)—O2 | 159.0 (3) | O2ii—O6—O4 | 111.7 (8) |
Si2ii—Ti_m1(1)—O2ii | 21.0 (3) | O2ii—O6—O6vii | 111.2 (4) |
Si2ii—Ti_m1(1)—O3 | 99.2 (3) | O2ii—O6—O7 | 63.3 (4) |
Si2ii—Ti_m1(1)—O3ii | 80.8 (3) | O2ii—O6—Ohii | 55.3 (4) |
Si2ii—Ti_m1(1)—O6 | 57.22 (14) | O2ii—O6—Ohv | 116.6 (3) |
Si2ii—Ti_m1(1)—O6ii | 122.78 (14) | O2ii—O6—W1 | 128.1 (3) |
Si2ii—Ti_m1(1)—Oh | 108.7 (2) | O2ii—O6—Nb_m1(1) | 34.2 (2) |
Si2ii—Ti_m1(1)—Ohii | 71.3 (2) | O3—O6—O4 | 61.1 (6) |
Si2ii—Ti_m1(1)—Nb_m1(1) | 0 | O3—O6—O6vii | 91.0 (5) |
O2—Ti_m1(1)—O2ii | 180.0 (5) | O3—O6—O7 | 59.6 (5) |
O2—Ti_m1(1)—O3 | 89.2 (3) | O3—O6—Ohii | 60.8 (4) |
O2—Ti_m1(1)—O3ii | 90.8 (3) | O3—O6—Ohv | 148.2 (4) |
O2—Ti_m1(1)—O6 | 118.0 (4) | O3—O6—W1 | 141.8 (3) |
O2—Ti_m1(1)—O6ii | 62.0 (4) | O3—O6—Nb_m1(1) | 34.5 (2) |
O2—Ti_m1(1)—Oh | 90.7 (5) | O4—O6—O6vii | 96.9 (3) |
O2—Ti_m1(1)—Ohii | 89.3 (5) | O4—O6—O7 | 61.6 (4) |
O2—Ti_m1(1)—Nb_m1(1) | 0 | O4—O6—Ohii | 113.8 (6) |
O2ii—Ti_m1(1)—O3 | 90.8 (3) | O4—O6—Ohv | 131.4 (8) |
O2ii—Ti_m1(1)—O3ii | 89.2 (3) | O4—O6—W1 | 86.6 (5) |
O2ii—Ti_m1(1)—O6 | 62.0 (4) | O4—O6—Nb_m1(1) | 95.6 (7) |
O2ii—Ti_m1(1)—O6ii | 118.0 (4) | O6vii—O6—O7 | 149.0 (6) |
O2ii—Ti_m1(1)—Oh | 89.3 (5) | O6vii—O6—Ohii | 56.0 (4) |
O2ii—Ti_m1(1)—Ohii | 90.7 (5) | O6vii—O6—Ohv | 60.6 (4) |
O2ii—Ti_m1(1)—Nb_m1(1) | 0 | O6vii—O6—W1 | 114.2 (6) |
O3—Ti_m1(1)—O3ii | 180.0 (5) | O6vii—O6—Nb_m1(1) | 84.4 (4) |
O3—Ti_m1(1)—O6 | 50.3 (5) | O7—O6—Ohii | 109.8 (7) |
O3—Ti_m1(1)—O6ii | 129.7 (5) | O7—O6—Ohv | 150.3 (5) |
O3—Ti_m1(1)—Oh | 88.0 (5) | O7—O6—W1 | 88.1 (4) |
O3—Ti_m1(1)—Ohii | 92.0 (5) | O7—O6—Nb_m1(1) | 76.4 (5) |
O3—Ti_m1(1)—Nb_m1(1) | 0 | Ohii—O6—Ohv | 89.7 (4) |
O3ii—Ti_m1(1)—O6 | 129.7 (5) | Ohii—O6—W1 | 157.4 (5) |
O3ii—Ti_m1(1)—O6ii | 50.3 (5) | Ohii—O6—Nb_m1(1) | 33.5 (3) |
O3ii—Ti_m1(1)—Oh | 92.0 (5) | Ohv—O6—W1 | 68.7 (4) |
O3ii—Ti_m1(1)—Ohii | 88.0 (5) | Ohv—O6—Nb_m1(1) | 121.4 (3) |
O3ii—Ti_m1(1)—Nb_m1(1) | 0 | W1—O6—Nb_m1(1) | 161.0 (3) |
O6—Ti_m1(1)—O6ii | 180.0 (5) | Na_a—O7—Na_aiii | 106.1 (5) |
O6—Ti_m1(1)—Oh | 125.0 (3) | Na_a—O7—Si1 | 79.4 (6) |
O6—Ti_m1(1)—Ohii | 55.0 (3) | Na_a—O7—Si2iv | 77.1 (6) |
O6—Ti_m1(1)—Nb_m1(1) | 0 | Na_a—O7—O1iv | 105.3 (5) |
O6ii—Ti_m1(1)—Oh | 55.0 (3) | Na_a—O7—O2iv | 44.6 (3) |
O6ii—Ti_m1(1)—Ohii | 125.0 (3) | Na_a—O7—O2ii | 75.7 (4) |
O6ii—Ti_m1(1)—Nb_m1(1) | 0 | Na_a—O7—O3 | 104.6 (4) |
Oh—Ti_m1(1)—Ohii | 180.0 (5) | Na_a—O7—O4 | 90.3 (6) |
Oh—Ti_m1(1)—Nb_m1(1) | 0 | Na_a—O7—O5iv | 88.1 (6) |
Ohii—Ti_m1(1)—Nb_m1(1) | 0 | Na_a—O7—O6 | 46.0 (4) |
Na_aii—Ti_m1(2)—Na_ax | 174.2 (2) | Na_a—O7—O7vi | 124.9 (6) |
Na_aii—Ti_m1(2)—Fe_m2 | 92.91 (15) | Na_a—O7—W2 | 148.0 (4) |
Na_aii—Ti_m1(2)—Si1ii | 62.7 (3) | Na_aiii—O7—Si1 | 117.6 (6) |
Na_aii—Ti_m1(2)—Si1x | 112.9 (3) | Na_aiii—O7—Si2iv | 101.0 (5) |
Na_aii—Ti_m1(2)—Si2 | 57.9 (4) | Na_aiii—O7—O1iv | 70.8 (5) |
Na_aii—Ti_m1(2)—Si2xi | 125.4 (4) | Na_aiii—O7—O2iv | 99.4 (5) |
Na_aii—Ti_m1(2)—O1 | 59.6 (3) | Na_aiii—O7—O2ii | 49.7 (4) |
Na_aii—Ti_m1(2)—O1xi | 125.6 (4) | Na_aiii—O7—O3 | 87.3 (6) |
Na_aii—Ti_m1(2)—O2 | 69.7 (4) | Na_aiii—O7—O4 | 146.7 (7) |
Na_aii—Ti_m1(2)—O2xi | 111.1 (4) | Na_aiii—O7—O5iv | 131.6 (5) |
Na_aii—Ti_m1(2)—O6ii | 45.2 (4) | Na_aiii—O7—O6 | 114.8 (4) |
Na_aii—Ti_m1(2)—O6x | 129.6 (4) | Na_aiii—O7—O7vi | 128.1 (7) |
Na_aii—Ti_m1(2)—Oh | 121.2 (5) | Na_aiii—O7—W2 | 42.0 (5) |
Na_aii—Ti_m1(2)—Ohxi | 59.0 (5) | Si1—O7—Si2iv | 139.0 (11) |
Na_aii—Ti_m1(2)—Ti_m2 | 92.91 (15) | Si1—O7—O1iv | 169.3 (4) |
Na_aii—Ti_m1(2)—Mg_m2 | 92.91 (15) | Si1—O7—O2iv | 120.3 (9) |
Na_ax—Ti_m1(2)—Fe_m2 | 92.91 (15) | Si1—O7—O2ii | 74.1 (3) |
Na_ax—Ti_m1(2)—Si1ii | 112.9 (3) | Si1—O7—O3 | 35.0 (5) |
Na_ax—Ti_m1(2)—Si1x | 62.7 (3) | Si1—O7—O4 | 36.2 (3) |
Na_ax—Ti_m1(2)—Si2 | 125.4 (4) | Si1—O7—O5iv | 110.4 (7) |
Na_ax—Ti_m1(2)—Si2xi | 57.9 (4) | Si1—O7—O6 | 34.0 (4) |
Na_ax—Ti_m1(2)—O1 | 125.6 (4) | Si1—O7—O7vi | 83.6 (3) |
Na_ax—Ti_m1(2)—O1xi | 59.6 (3) | Si1—O7—W2 | 113.9 (7) |
Na_ax—Ti_m1(2)—O2 | 111.1 (4) | Si2iv—O7—O1iv | 36.9 (5) |
Na_ax—Ti_m1(2)—O2xi | 69.7 (4) | Si2iv—O7—O2iv | 33.8 (3) |
Na_ax—Ti_m1(2)—O6ii | 129.6 (4) | Si2iv—O7—O2ii | 130.1 (3) |
Na_ax—Ti_m1(2)—O6x | 45.2 (4) | Si2iv—O7—O3 | 170.8 (5) |
Na_ax—Ti_m1(2)—Oh | 59.0 (5) | Si2iv—O7—O4 | 111.0 (7) |
Na_ax—Ti_m1(2)—Ohxi | 121.2 (5) | Si2iv—O7—O5iv | 36.4 (3) |
Na_ax—Ti_m1(2)—Ti_m2 | 92.91 (15) | Si2iv—O7—O6 | 118.0 (9) |
Na_ax—Ti_m1(2)—Mg_m2 | 92.91 (15) | Si2iv—O7—O7vi | 83.0 (3) |
Fe_m2—Ti_m1(2)—Si1ii | 134.06 (7) | Si2iv—O7—W2 | 103.7 (6) |
Fe_m2—Ti_m1(2)—Si1x | 134.06 (7) | O1iv—O7—O2iv | 61.9 (4) |
Fe_m2—Ti_m1(2)—Si2 | 61.58 (6) | O1iv—O7—O2ii | 116.2 (4) |
Fe_m2—Ti_m1(2)—Si2xi | 61.58 (6) | O1iv—O7—O3 | 146.8 (9) |
Fe_m2—Ti_m1(2)—O1 | 41.2 (2) | O1iv—O7—O4 | 133.3 (3) |
Fe_m2—Ti_m1(2)—O1xi | 41.2 (2) | O1iv—O7—O5iv | 60.8 (4) |
Fe_m2—Ti_m1(2)—O2 | 82.68 (10) | O1iv—O7—O6 | 151.2 (7) |
Fe_m2—Ti_m1(2)—O2xi | 82.68 (10) | O1iv—O7—O7vi | 85.9 (2) |
Fe_m2—Ti_m1(2)—O6ii | 130.9 (2) | O1iv—O7—W2 | 67.2 (5) |
Fe_m2—Ti_m1(2)—O6x | 130.9 (2) | O2iv—O7—O2ii | 103.5 (3) |
Fe_m2—Ti_m1(2)—Oh | 88.32 (17) | O2iv—O7—O3 | 149.2 (6) |
Fe_m2—Ti_m1(2)—Ohxi | 88.32 (17) | O2iv—O7—O4 | 112.2 (8) |
Fe_m2—Ti_m1(2)—Ti_m2 | 0.0 (5) | O2iv—O7—O5iv | 59.1 (4) |
Fe_m2—Ti_m1(2)—Mg_m2 | 0.0 (5) | O2iv—O7—O6 | 89.4 (6) |
Si1ii—Ti_m1(2)—Si1x | 91.88 (11) | O2iv—O7—O7vi | 109.4 (4) |
Si1ii—Ti_m1(2)—Si2 | 72.53 (9) | O2iv—O7—W2 | 124.6 (4) |
Si1ii—Ti_m1(2)—Si2xi | 164.17 (9) | O2ii—O7—O3 | 58.6 (2) |
Si1ii—Ti_m1(2)—O1 | 94.4 (3) | O2ii—O7—O4 | 110.2 (3) |
Si1ii—Ti_m1(2)—O1xi | 165.7 (5) | O2ii—O7—O5iv | 162.2 (6) |
Si1ii—Ti_m1(2)—O2 | 53.22 (13) | O2ii—O7—O6 | 65.3 (4) |
Si1ii—Ti_m1(2)—O2xi | 140.89 (15) | O2ii—O7—O7vi | 146.4 (4) |
Si1ii—Ti_m1(2)—O6ii | 19.7 (5) | O2ii—O7—W2 | 80.3 (5) |
Si1ii—Ti_m1(2)—O6x | 91.7 (3) | O3—O7—O4 | 60.2 (4) |
Si1ii—Ti_m1(2)—Oh | 75.1 (2) | O3—O7—O5iv | 134.4 (4) |
Si1ii—Ti_m1(2)—Ohxi | 107.3 (2) | O3—O7—O6 | 60.8 (5) |
Si1ii—Ti_m1(2)—Ti_m2 | 134.06 (7) | O3—O7—O7vi | 88.8 (2) |
Si1ii—Ti_m1(2)—Mg_m2 | 134.06 (7) | O3—O7—W2 | 79.8 (5) |
Si1x—Ti_m1(2)—Si2 | 164.17 (9) | O4—O7—O5iv | 76.5 (4) |
Si1x—Ti_m1(2)—Si2xi | 72.53 (9) | O4—O7—O6 | 57.6 (4) |
Si1x—Ti_m1(2)—O1 | 165.7 (5) | O4—O7—O7vi | 50.7 (3) |
Si1x—Ti_m1(2)—O1xi | 94.4 (3) | O4—O7—W2 | 118.0 (6) |
Si1x—Ti_m1(2)—O2 | 140.89 (15) | O5iv—O7—O6 | 108.2 (8) |
Si1x—Ti_m1(2)—O2xi | 53.22 (13) | O5iv—O7—O7vi | 50.4 (3) |
Si1x—Ti_m1(2)—O6ii | 91.7 (3) | O5iv—O7—W2 | 111.8 (5) |
Si1x—Ti_m1(2)—O6x | 19.7 (5) | O6—O7—O7vi | 107.9 (4) |
Si1x—Ti_m1(2)—Oh | 107.3 (2) | O6—O7—W2 | 136.9 (5) |
Si1x—Ti_m1(2)—Ohxi | 75.1 (2) | O7vi—O7—W2 | 86.4 (4) |
Si1x—Ti_m1(2)—Ti_m2 | 134.06 (7) | Na_aiii—Oh—Na_ax | 48.5 (6) |
Si1x—Ti_m1(2)—Mg_m2 | 134.06 (7) | Na_aiii—Oh—Ti_m1(1) | 90.7 (7) |
Si2—Ti_m1(2)—Si2xi | 123.17 (10) | Na_aiii—Oh—Ti_m1(2) | 133.8 (7) |
Si2—Ti_m1(2)—O1 | 24.0 (4) | Na_aiii—Oh—Si1ii | 128.9 (3) |
Si2—Ti_m1(2)—O1xi | 101.4 (3) | Na_aiii—Oh—Si2 | 147.7 (6) |
Si2—Ti_m1(2)—O2 | 27.30 (16) | Na_aiii—Oh—O1 | 150.3 (3) |
Si2—Ti_m1(2)—O2xi | 140.12 (14) | Na_aiii—Oh—O1xi | 101.6 (5) |
Si2—Ti_m1(2)—O6ii | 72.7 (3) | Na_aiii—Oh—O2 | 132.3 (8) |
Si2—Ti_m1(2)—O6x | 157.1 (5) | Na_aiii—Oh—O2ii | 48.4 (4) |
Si2—Ti_m1(2)—Oh | 72.0 (2) | Na_aiii—Oh—O3 | 76.0 (5) |
Si2—Ti_m1(2)—Ohxi | 106.4 (2) | Na_aiii—Oh—O3ii | 104.5 (5) |
Si2—Ti_m1(2)—Ti_m2 | 61.58 (6) | Na_aiii—Oh—O6ii | 146.4 (3) |
Si2—Ti_m1(2)—Mg_m2 | 61.58 (6) | Na_aiii—Oh—O6x | 93.2 (5) |
Si2xi—Ti_m1(2)—O1 | 101.4 (3) | Na_aiii—Oh—Ba | 88.4 (3) |
Si2xi—Ti_m1(2)—O1xi | 24.0 (4) | Na_aiii—Oh—W1iii | 37.3 (3) |
Si2xi—Ti_m1(2)—O2 | 140.12 (14) | Na_aiii—Oh—W2 | 40.3 (3) |
Si2xi—Ti_m1(2)—O2xi | 27.30 (16) | Na_aiii—Oh—W_c | 88.4 (3) |
Si2xi—Ti_m1(2)—O6ii | 157.1 (5) | Na_aiii—Oh—Nb_m1(1) | 90.7 (7) |
Si2xi—Ti_m1(2)—O6x | 72.7 (3) | Na_ax—Oh—Ti_m1(1) | 137.0 (7) |
Si2xi—Ti_m1(2)—Oh | 106.4 (2) | Na_ax—Oh—Ti_m1(2) | 85.4 (7) |
Si2xi—Ti_m1(2)—Ohxi | 72.0 (2) | Na_ax—Oh—Si1ii | 124.3 (4) |
Si2xi—Ti_m1(2)—Ti_m2 | 61.58 (6) | Na_ax—Oh—Si2 | 147.0 (6) |
Si2xi—Ti_m1(2)—Mg_m2 | 61.58 (6) | Na_ax—Oh—O1 | 118.3 (7) |
O1—Ti_m1(2)—O1xi | 82.4 (3) | Na_ax—Oh—O1xi | 61.2 (5) |
O1—Ti_m1(2)—O2 | 50.8 (4) | Na_ax—Oh—O2 | 176.4 (4) |
O1—Ti_m1(2)—O2xi | 116.1 (4) | Na_ax—Oh—O2ii | 91.0 (5) |
O1—Ti_m1(2)—O6ii | 89.9 (3) | Na_ax—Oh—O3 | 118.1 (5) |
O1—Ti_m1(2)—O6x | 170.7 (3) | Na_ax—Oh—O3ii | 123.1 (3) |
O1—Ti_m1(2)—Oh | 86.7 (5) | Na_ax—Oh—O6ii | 114.6 (7) |
O1—Ti_m1(2)—Ohxi | 90.7 (5) | Na_ax—Oh—O6x | 51.2 (5) |
O1—Ti_m1(2)—Ti_m2 | 41.2 (2) | Na_ax—Oh—Ba | 88.7 (3) |
O1—Ti_m1(2)—Mg_m2 | 41.2 (2) | Na_ax—Oh—W1iii | 37.7 (3) |
O1xi—Ti_m1(2)—O2 | 116.1 (4) | Na_ax—Oh—W2 | 41.0 (3) |
O1xi—Ti_m1(2)—O2xi | 50.8 (4) | Na_ax—Oh—W_c | 88.7 (3) |
O1xi—Ti_m1(2)—O6ii | 170.7 (3) | Na_ax—Oh—Nb_m1(1) | 137.0 (7) |
O1xi—Ti_m1(2)—O6x | 89.9 (3) | Ti_m1(1)—Oh—Ti_m1(2) | 132.1 (3) |
O1xi—Ti_m1(2)—Oh | 90.7 (5) | Ti_m1(1)—Oh—Si1ii | 66.8 (2) |
O1xi—Ti_m1(2)—Ohxi | 86.7 (5) | Ti_m1(1)—Oh—Si2 | 74.4 (2) |
O1xi—Ti_m1(2)—Ti_m2 | 41.2 (2) | Ti_m1(1)—Oh—O1 | 104.2 (4) |
O1xi—Ti_m1(2)—Mg_m2 | 41.2 (2) | Ti_m1(1)—Oh—O1xi | 158.4 (3) |
O2—Ti_m1(2)—O2xi | 165.36 (14) | Ti_m1(1)—Oh—O2 | 45.3 (3) |
O2—Ti_m1(2)—O6ii | 61.7 (5) | Ti_m1(1)—Oh—O2ii | 46.0 (3) |
O2—Ti_m1(2)—O6x | 129.9 (5) | Ti_m1(1)—Oh—O3 | 46.9 (4) |
O2—Ti_m1(2)—Oh | 52.1 (3) | Ti_m1(1)—Oh—O3ii | 44.9 (3) |
O2—Ti_m1(2)—Ohxi | 127.4 (3) | Ti_m1(1)—Oh—O6ii | 91.6 (4) |
O2—Ti_m1(2)—Ti_m2 | 82.68 (10) | Ti_m1(1)—Oh—O6x | 137.1 (3) |
O2—Ti_m1(2)—Mg_m2 | 82.68 (10) | Ti_m1(1)—Oh—Ba | 105.6 (5) |
O2xi—Ti_m1(2)—O6ii | 129.9 (5) | Ti_m1(1)—Oh—W1iii | 102.7 (4) |
O2xi—Ti_m1(2)—O6x | 61.7 (5) | Ti_m1(1)—Oh—W2 | 118.5 (6) |
O2xi—Ti_m1(2)—Oh | 127.4 (3) | Ti_m1(1)—Oh—W_c | 105.6 (5) |
O2xi—Ti_m1(2)—Ohxi | 52.1 (3) | Ti_m1(1)—Oh—Nb_m1(1) | 0.0 (5) |
O2xi—Ti_m1(2)—Ti_m2 | 82.68 (10) | Ti_m1(2)—Oh—Si1ii | 70.4 (2) |
O2xi—Ti_m1(2)—Mg_m2 | 82.68 (10) | Ti_m1(2)—Oh—Si2 | 72.7 (3) |
O6ii—Ti_m1(2)—O6x | 98.1 (3) | Ti_m1(2)—Oh—O1 | 47.7 (4) |
O6ii—Ti_m1(2)—Oh | 94.0 (5) | Ti_m1(2)—Oh—O1xi | 45.6 (4) |
O6ii—Ti_m1(2)—Ohxi | 88.2 (5) | Ti_m1(2)—Oh—O2 | 93.8 (4) |
O6ii—Ti_m1(2)—Ti_m2 | 130.9 (2) | Ti_m1(2)—Oh—O2ii | 151.1 (3) |
O6ii—Ti_m1(2)—Mg_m2 | 130.9 (2) | Ti_m1(2)—Oh—O3 | 143.1 (3) |
O6x—Ti_m1(2)—Oh | 88.2 (5) | Ti_m1(2)—Oh—O3ii | 98.4 (4) |
O6x—Ti_m1(2)—Ohxi | 94.0 (5) | Ti_m1(2)—Oh—O6ii | 42.6 (4) |
O6x—Ti_m1(2)—Ti_m2 | 130.9 (2) | Ti_m1(2)—Oh—O6x | 45.5 (4) |
O6x—Ti_m1(2)—Mg_m2 | 130.9 (2) | Ti_m1(2)—Oh—Ba | 94.0 (4) |
Oh—Ti_m1(2)—Ohxi | 176.6 (3) | Ti_m1(2)—Oh—W1iii | 105.7 (4) |
Oh—Ti_m1(2)—Ti_m2 | 88.32 (17) | Ti_m1(2)—Oh—W2 | 108.6 (5) |
Oh—Ti_m1(2)—Mg_m2 | 88.32 (17) | Ti_m1(2)—Oh—W_c | 94.0 (4) |
Ohxi—Ti_m1(2)—Ti_m2 | 88.32 (17) | Ti_m1(2)—Oh—Nb_m1(1) | 132.1 (3) |
Ohxi—Ti_m1(2)—Mg_m2 | 88.32 (17) | Si1ii—Oh—Si2 | 71.59 (13) |
Ti_m2—Ti_m1(2)—Mg_m2 | 0.0 (5) | Si1ii—Oh—O1 | 80.8 (2) |
Ti_m1(2)—Fe_m2—Ti_m1(2)xii | 180.0 (5) | Si1ii—Oh—O1xi | 116.0 (5) |
Ti_m1(2)—Fe_m2—Si2 | 62.28 (5) | Si1ii—Oh—O2 | 58.59 (19) |
Ti_m1(2)—Fe_m2—Si2xi | 62.28 (5) | Si1ii—Oh—O2ii | 88.4 (3) |
Ti_m1(2)—Fe_m2—Si2xii | 117.72 (5) | Si1ii—Oh—O3 | 110.5 (4) |
Ti_m1(2)—Fe_m2—Si2vi | 117.72 (5) | Si1ii—Oh—O3ii | 28.6 (3) |
Ti_m1(2)—Fe_m2—O1 | 41.5 (2) | Si1ii—Oh—O6ii | 28.2 (3) |
Ti_m1(2)—Fe_m2—O1xi | 41.5 (2) | Si1ii—Oh—O6x | 77.9 (3) |
Ti_m1(2)—Fe_m2—O1xii | 138.5 (2) | Si1ii—Oh—Ba | 140.4 (2) |
Ti_m1(2)—Fe_m2—O1vi | 138.5 (2) | Si1ii—Oh—W1iii | 101.4 (2) |
Ti_m1(2)—Fe_m2—O5 | 90 | Si1ii—Oh—W2 | 164.2 (3) |
Ti_m1(2)—Fe_m2—O5xi | 90 | Si1ii—Oh—W_c | 140.4 (2) |
Ti_m1(2)—Fe_m2—Ba | 90 | Si1ii—Oh—Nb_m1(1) | 66.8 (2) |
Ti_m1(2)—Fe_m2—Baxi | 90 | Si2—Oh—O1 | 30.0 (3) |
Ti_m1(2)—Fe_m2—W_c | 90 | Si2—Oh—O1xi | 86.0 (3) |
Ti_m1(2)—Fe_m2—W_cxi | 90 | Si2—Oh—O2 | 29.9 (3) |
Ti_m1(2)—Fe_m2—Ti_m2 | 0 | Si2—Oh—O2ii | 119.9 (5) |
Ti_m1(2)—Fe_m2—Mg_m2 | 0 | Si2—Oh—O3 | 72.9 (3) |
Ti_m1(2)xii—Fe_m2—Si2 | 117.72 (5) | Si2—Oh—O3ii | 85.1 (2) |
Ti_m1(2)xii—Fe_m2—Si2xi | 117.72 (5) | Si2—Oh—O6ii | 64.1 (2) |
Ti_m1(2)xii—Fe_m2—Si2xii | 62.28 (5) | Si2—Oh—O6x | 117.3 (5) |
Ti_m1(2)xii—Fe_m2—Si2vi | 62.28 (5) | Si2—Oh—Ba | 69.06 (12) |
Ti_m1(2)xii—Fe_m2—O1 | 138.5 (2) | Si2—Oh—W1iii | 173.0 (2) |
Ti_m1(2)xii—Fe_m2—O1xi | 138.5 (2) | Si2—Oh—W2 | 123.8 (2) |
Ti_m1(2)xii—Fe_m2—O1xii | 41.5 (2) | Si2—Oh—W_c | 69.06 (12) |
Ti_m1(2)xii—Fe_m2—O1vi | 41.5 (2) | Si2—Oh—Nb_m1(1) | 74.4 (2) |
Ti_m1(2)xii—Fe_m2—O5 | 90 | O1—Oh—O1xi | 57.3 (4) |
Ti_m1(2)xii—Fe_m2—O5xi | 90 | O1—Oh—O2 | 59.1 (4) |
Ti_m1(2)xii—Fe_m2—Ba | 90 | O1—Oh—O2ii | 149.9 (6) |
Ti_m1(2)xii—Fe_m2—Baxi | 90 | O1—Oh—O3 | 95.4 (4) |
Ti_m1(2)xii—Fe_m2—W_c | 90 | O1—Oh—O3ii | 104.2 (3) |
Ti_m1(2)xii—Fe_m2—W_cxi | 90 | O1—Oh—O6ii | 60.1 (3) |
Ti_m1(2)xii—Fe_m2—Ti_m2 | 0 | O1—Oh—O6x | 92.9 (6) |
Ti_m1(2)xii—Fe_m2—Mg_m2 | 0 | O1—Oh—Ba | 63.0 (2) |
Si2—Fe_m2—Si2xi | 124.57 (8) | O1—Oh—W1iii | 151.4 (7) |
Si2—Fe_m2—Si2xii | 180.0 (5) | O1—Oh—W2 | 110.6 (3) |
Si2—Fe_m2—Si2vi | 55.43 (8) | O1—Oh—W_c | 63.0 (2) |
Si2—Fe_m2—O1 | 24.4 (4) | O1—Oh—Nb_m1(1) | 104.2 (4) |
Si2—Fe_m2—O1xi | 102.4 (3) | O1xi—Oh—O2 | 115.9 (4) |
Si2—Fe_m2—O1xii | 155.6 (4) | O1xi—Oh—O2ii | 149.9 (3) |
Si2—Fe_m2—O1vi | 77.6 (3) | O1xi—Oh—O3 | 118.8 (3) |
Si2—Fe_m2—O5 | 29.44 (12) | O1xi—Oh—O3ii | 143.8 (6) |
Si2—Fe_m2—O5xi | 150.56 (12) | O1xi—Oh—O6ii | 87.9 (6) |
Si2—Fe_m2—Ba | 80.24 (13) | O1xi—Oh—O6x | 60.6 (4) |
Si2—Fe_m2—Baxi | 99.76 (13) | O1xi—Oh—Ba | 57.7 (3) |
Si2—Fe_m2—W_c | 80.24 (13) | O1xi—Oh—W1iii | 97.7 (3) |
Si2—Fe_m2—W_cxi | 99.76 (13) | O1xi—Oh—W2 | 65.3 (3) |
Si2—Fe_m2—Ti_m2 | 0 | O1xi—Oh—W_c | 57.7 (3) |
Si2—Fe_m2—Mg_m2 | 0 | O1xi—Oh—Nb_m1(1) | 158.4 (3) |
Si2xi—Fe_m2—Si2xii | 55.43 (8) | O2—Oh—O2ii | 91.3 (5) |
Si2xi—Fe_m2—Si2vi | 180.0 (5) | O2—Oh—O3 | 60.8 (4) |
Si2xi—Fe_m2—O1 | 102.4 (3) | O2—Oh—O3ii | 60.5 (3) |
Si2xi—Fe_m2—O1xi | 24.4 (4) | O2—Oh—O6ii | 66.7 (4) |
Si2xi—Fe_m2—O1xii | 77.6 (3) | O2—Oh—O6x | 130.0 (5) |
Si2xi—Fe_m2—O1vi | 155.6 (4) | O2—Oh—Ba | 87.8 (2) |
Si2xi—Fe_m2—O5 | 150.56 (12) | O2—Oh—W1iii | 145.6 (5) |
Si2xi—Fe_m2—O5xi | 29.44 (12) | O2—Oh—W2 | 136.4 (4) |
Si2xi—Fe_m2—Ba | 99.76 (13) | O2—Oh—W_c | 87.8 (2) |
Si2xi—Fe_m2—Baxi | 80.24 (13) | O2—Oh—Nb_m1(1) | 45.3 (3) |
Si2xi—Fe_m2—W_c | 99.76 (13) | O2ii—Oh—O3 | 62.2 (5) |
Si2xi—Fe_m2—W_cxi | 80.24 (13) | O2ii—Oh—O3ii | 60.1 (4) |
Si2xi—Fe_m2—Ti_m2 | 0 | O2ii—Oh—O6ii | 116.0 (4) |
Si2xi—Fe_m2—Mg_m2 | 0 | O2ii—Oh—O6x | 112.3 (4) |
Si2xii—Fe_m2—Si2vi | 124.57 (8) | O2ii—Oh—Ba | 114.6 (5) |
Si2xii—Fe_m2—O1 | 155.6 (4) | O2ii—Oh—W1iii | 58.3 (2) |
Si2xii—Fe_m2—O1xi | 77.6 (3) | O2ii—Oh—W2 | 86.4 (3) |
Si2xii—Fe_m2—O1xii | 24.4 (4) | O2ii—Oh—W_c | 114.6 (5) |
Si2xii—Fe_m2—O1vi | 102.4 (3) | O2ii—Oh—Nb_m1(1) | 46.0 (3) |
Si2xii—Fe_m2—O5 | 150.56 (12) | O3—Oh—O3ii | 91.8 (6) |
Si2xii—Fe_m2—O5xi | 29.44 (12) | O3—Oh—O6ii | 127.3 (4) |
Si2xii—Fe_m2—Ba | 99.76 (13) | O3—Oh—O6x | 169.0 (3) |
Si2xii—Fe_m2—Baxi | 80.24 (13) | O3—Oh—Ba | 61.1 (3) |
Si2xii—Fe_m2—W_c | 99.76 (13) | O3—Oh—W1iii | 110.0 (4) |
Si2xii—Fe_m2—W_cxi | 80.24 (13) | O3—Oh—W2 | 80.1 (3) |
Si2xii—Fe_m2—Ti_m2 | 0 | O3—Oh—W_c | 61.1 (3) |
Si2xii—Fe_m2—Mg_m2 | 0 | O3—Oh—Nb_m1(1) | 46.9 (4) |
Si2vi—Fe_m2—O1 | 77.6 (3) | O3ii—Oh—O6ii | 56.8 (4) |
Si2vi—Fe_m2—O1xi | 155.6 (4) | O3ii—Oh—O6x | 93.1 (4) |
Si2vi—Fe_m2—O1xii | 102.4 (3) | O3ii—Oh—Ba | 146.6 (5) |
Si2vi—Fe_m2—O1vi | 24.4 (4) | O3ii—Oh—W1iii | 88.4 (3) |
Si2vi—Fe_m2—O5 | 29.44 (12) | O3ii—Oh—W2 | 144.8 (5) |
Si2vi—Fe_m2—O5xi | 150.56 (12) | O3ii—Oh—W_c | 146.6 (5) |
Si2vi—Fe_m2—Ba | 80.24 (13) | O3ii—Oh—Nb_m1(1) | 44.9 (3) |
Si2vi—Fe_m2—Baxi | 99.76 (13) | O6ii—Oh—O6x | 63.4 (4) |
Si2vi—Fe_m2—W_c | 80.24 (13) | O6ii—Oh—Ba | 123.0 (4) |
Si2vi—Fe_m2—W_cxi | 99.76 (13) | O6ii—Oh—W1iii | 109.9 (3) |
Si2vi—Fe_m2—Ti_m2 | 0 | O6ii—Oh—W2 | 149.8 (7) |
Si2vi—Fe_m2—Mg_m2 | 0 | O6ii—Oh—W_c | 123.0 (4) |
O1—Fe_m2—O1xi | 83.1 (3) | O6ii—Oh—Nb_m1(1) | 91.6 (4) |
O1—Fe_m2—O1xii | 180.0 (5) | O6x—Oh—Ba | 117.2 (5) |
O1—Fe_m2—O1vi | 96.9 (3) | O6x—Oh—W1iii | 60.3 (3) |
O1—Fe_m2—O5 | 53.8 (4) | O6x—Oh—W2 | 90.2 (3) |
O1—Fe_m2—O5xi | 126.2 (4) | O6x—Oh—W_c | 117.2 (5) |
O1—Fe_m2—Ba | 93.7 (4) | O6x—Oh—Nb_m1(1) | 137.1 (3) |
O1—Fe_m2—Baxi | 86.3 (4) | Ba—Oh—W1iii | 118.0 (2) |
O1—Fe_m2—W_c | 93.7 (4) | Ba—Oh—W2 | 54.71 (19) |
O1—Fe_m2—W_cxi | 86.3 (4) | Ba—Oh—W_c | 0.0 (5) |
O1—Fe_m2—Ti_m2 | 0 | Ba—Oh—Nb_m1(1) | 105.6 (5) |
O1—Fe_m2—Mg_m2 | 0 | W1iii—Oh—W2 | 63.2 (2) |
O1xi—Fe_m2—O1xii | 96.9 (3) | W1iii—Oh—W_c | 118.0 (2) |
O1xi—Fe_m2—O1vi | 180.0 (5) | W1iii—Oh—Nb_m1(1) | 102.7 (4) |
O1xi—Fe_m2—O5 | 126.2 (4) | W2—Oh—W_c | 54.71 (19) |
O1xi—Fe_m2—O5xi | 53.8 (4) | W2—Oh—Nb_m1(1) | 118.5 (6) |
O1xi—Fe_m2—Ba | 86.3 (4) | W_c—Oh—Nb_m1(1) | 105.6 (5) |
O1xi—Fe_m2—Baxi | 93.7 (4) | Fe_m2—Ba—Si2 | 63.84 (12) |
O1xi—Fe_m2—W_c | 86.3 (4) | Fe_m2—Ba—Si2vi | 63.84 (12) |
O1xi—Fe_m2—W_cxi | 93.7 (4) | Fe_m2—Ba—O1 | 42.0 (3) |
O1xi—Fe_m2—Ti_m2 | 0 | Fe_m2—Ba—O1xi | 45.6 (2) |
O1xi—Fe_m2—Mg_m2 | 0 | Fe_m2—Ba—O1xii | 45.6 (2) |
O1xii—Fe_m2—O1vi | 83.1 (3) | Fe_m2—Ba—O1vi | 42.0 (3) |
O1xii—Fe_m2—O5 | 126.2 (4) | Fe_m2—Ba—O3 | 127.8 (2) |
O1xii—Fe_m2—O5xi | 53.8 (4) | Fe_m2—Ba—O3vi | 127.8 (2) |
O1xii—Fe_m2—Ba | 86.3 (4) | Fe_m2—Ba—O5 | 73.6 (4) |
O1xii—Fe_m2—Baxi | 93.7 (4) | Fe_m2—Ba—Oh | 86.8 (3) |
O1xii—Fe_m2—W_c | 86.3 (4) | Fe_m2—Ba—Ohvi | 86.8 (3) |
O1xii—Fe_m2—W_cxi | 93.7 (4) | Fe_m2—Ba—W2 | 114.03 (18) |
O1xii—Fe_m2—Ti_m2 | 0 | Fe_m2—Ba—W2xiv | 114.03 (18) |
O1xii—Fe_m2—Mg_m2 | 0 | Fe_m2—Ba—W_c | 0 |
O1vi—Fe_m2—O5 | 53.8 (4) | Fe_m2—Ba—Ti_m2 | 0.0 (5) |
O1vi—Fe_m2—O5xi | 126.2 (4) | Fe_m2—Ba—Mg_m2 | 0.0 (5) |
O1vi—Fe_m2—Ba | 93.7 (4) | Si2—Ba—Si2vi | 50.12 (6) |
O1vi—Fe_m2—Baxi | 86.3 (4) | Si2—Ba—O1 | 27.0 (3) |
O1vi—Fe_m2—W_c | 93.7 (4) | Si2—Ba—O1xi | 80.68 (17) |
O1vi—Fe_m2—W_cxi | 86.3 (4) | Si2—Ba—O1xii | 107.0 (2) |
O1vi—Fe_m2—Ti_m2 | 0 | Si2—Ba—O1vi | 62.28 (14) |
O1vi—Fe_m2—Mg_m2 | 0 | Si2—Ba—O3 | 66.0 (2) |
O5—Fe_m2—O5xi | 180.0 (5) | Si2—Ba—O3vi | 94.09 (17) |
O5—Fe_m2—Ba | 68.6 (3) | Si2—Ba—O5 | 27.93 (18) |
O5—Fe_m2—Baxi | 111.4 (3) | Si2—Ba—Oh | 58.49 (11) |
O5—Fe_m2—W_c | 68.6 (3) | Si2—Ba—Ohvi | 108.61 (12) |
O5—Fe_m2—W_cxi | 111.4 (3) | Si2—Ba—W2 | 122.25 (18) |
O5—Fe_m2—Ti_m2 | 0 | Si2—Ba—W2xiv | 172.37 (18) |
O5—Fe_m2—Mg_m2 | 0 | Si2—Ba—W_c | 0 |
O5xi—Fe_m2—Ba | 111.4 (3) | Si2—Ba—Ti_m2 | 63.84 (12) |
O5xi—Fe_m2—Baxi | 68.6 (3) | Si2—Ba—Mg_m2 | 63.84 (12) |
O5xi—Fe_m2—W_c | 111.4 (3) | Si2vi—Ba—O1 | 62.28 (14) |
O5xi—Fe_m2—W_cxi | 68.6 (3) | Si2vi—Ba—O1xi | 107.0 (2) |
O5xi—Fe_m2—Ti_m2 | 0 | Si2vi—Ba—O1xii | 80.68 (17) |
O5xi—Fe_m2—Mg_m2 | 0 | Si2vi—Ba—O1vi | 27.0 (3) |
Ba—Fe_m2—Baxi | 180.0 (5) | Si2vi—Ba—O3 | 94.09 (17) |
Ba—Fe_m2—W_c | 0.0 (5) | Si2vi—Ba—O3vi | 66.0 (2) |
Ba—Fe_m2—W_cxi | 180.0 (5) | Si2vi—Ba—O5 | 27.93 (18) |
Ba—Fe_m2—Ti_m2 | 0 | Si2vi—Ba—Oh | 108.61 (12) |
Ba—Fe_m2—Mg_m2 | 0 | Si2vi—Ba—Ohvi | 58.49 (11) |
Baxi—Fe_m2—W_c | 180.0 (5) | Si2vi—Ba—W2 | 172.37 (18) |
Baxi—Fe_m2—W_cxi | 0.0 (5) | Si2vi—Ba—W2xiv | 122.25 (18) |
Baxi—Fe_m2—Ti_m2 | 0 | Si2vi—Ba—W_c | 0 |
Baxi—Fe_m2—Mg_m2 | 0 | Si2vi—Ba—Ti_m2 | 63.84 (12) |
W_c—Fe_m2—W_cxi | 180.0 (5) | Si2vi—Ba—Mg_m2 | 63.84 (12) |
W_c—Fe_m2—Ti_m2 | 0 | O1—Ba—O1xi | 54.6 (3) |
W_c—Fe_m2—Mg_m2 | 0 | O1—Ba—O1xii | 87.6 (3) |
W_cxi—Fe_m2—Ti_m2 | 0 | O1—Ba—O1vi | 60.31 (19) |
W_cxi—Fe_m2—Mg_m2 | 0 | O1—Ba—O3 | 85.8 (3) |
Ti_m2—Fe_m2—Mg_m2 | 0 | O1—Ba—O3vi | 119.6 (3) |
Na_a—Si1—Na_aiii | 83.7 (5) | O1—Ba—O5 | 50.6 (4) |
Na_a—Si1—K_b | 136.1 (3) | O1—Ba—Oh | 54.3 (2) |
Na_a—Si1—Ti_m1(1) | 105.2 (2) | O1—Ba—Ohvi | 114.5 (2) |
Na_a—Si1—Ti_m1(2)ii | 60.11 (18) | O1—Ba—W2 | 110.9 (2) |
Na_a—Si1—Si1vi | 127.5 (3) | O1—Ba—W2xiv | 154.1 (4) |
Na_a—Si1—Si2iv | 62.0 (2) | O1—Ba—W_c | 0 |
Na_a—Si1—O2ii | 74.2 (4) | O1—Ba—Ti_m2 | 42.0 (3) |
Na_a—Si1—O3 | 137.9 (3) | O1—Ba—Mg_m2 | 42.0 (3) |
Na_a—Si1—O4 | 109.4 (8) | O1xi—Ba—O1xii | 64.8 (3) |
Na_a—Si1—O6 | 38.9 (3) | O1xi—Ba—O1vi | 87.6 (3) |
Na_a—Si1—O7 | 72.4 (6) | O1xi—Ba—O3 | 112.9 (3) |
Na_a—Si1—Ohii | 87.3 (3) | O1xi—Ba—O3vi | 173.0 (2) |
Na_a—Si1—Nb_m1(1) | 105.2 (2) | O1xi—Ba—O5 | 104.8 (4) |
Na_aiii—Si1—K_b | 131.7 (4) | O1xi—Ba—Oh | 58.4 (4) |
Na_aiii—Si1—Ti_m1(1) | 64.8 (2) | O1xi—Ba—Ohvi | 122.7 (4) |
Na_aiii—Si1—Ti_m1(2)ii | 106.9 (2) | O1xi—Ba—W2 | 69.38 (19) |
Na_aiii—Si1—Si1vi | 118.7 (3) | O1xi—Ba—W2xiv | 103.1 (2) |
Na_aiii—Si1—Si2iv | 57.3 (3) | O1xi—Ba—W_c | 0 |
Na_aiii—Si1—O2ii | 41.4 (2) | O1xi—Ba—Ti_m2 | 45.6 (2) |
Na_aiii—Si1—O3 | 76.6 (5) | O1xi—Ba—Mg_m2 | 45.6 (2) |
Na_aiii—Si1—O4 | 139.4 (5) | O1xii—Ba—O1vi | 54.6 (3) |
Na_aiii—Si1—O6 | 108.3 (4) | O1xii—Ba—O3 | 173.0 (2) |
Na_aiii—Si1—O7 | 37.9 (5) | O1xii—Ba—O3vi | 112.9 (3) |
Na_aiii—Si1—Ohii | 90.9 (3) | O1xii—Ba—O5 | 104.8 (4) |
Na_aiii—Si1—Nb_m1(1) | 64.8 (2) | O1xii—Ba—Oh | 122.7 (4) |
K_b—Si1—Ti_m1(1) | 76.78 (13) | O1xii—Ba—Ohvi | 58.4 (4) |
K_b—Si1—Ti_m1(2)ii | 82.24 (11) | O1xii—Ba—W2 | 103.1 (2) |
K_b—Si1—Si1vi | 64.03 (6) | O1xii—Ba—W2xiv | 69.38 (19) |
K_b—Si1—Si2iv | 153.55 (9) | O1xii—Ba—W_c | 0 |
K_b—Si1—O2ii | 113.19 (19) | O1xii—Ba—Ti_m2 | 45.6 (2) |
K_b—Si1—O3 | 55.6 (4) | O1xii—Ba—Mg_m2 | 45.6 (2) |
K_b—Si1—O4 | 63.3 (4) | O1vi—Ba—O3 | 119.6 (3) |
K_b—Si1—O6 | 98.5 (3) | O1vi—Ba—O3vi | 85.8 (3) |
K_b—Si1—O7 | 151.1 (5) | O1vi—Ba—O5 | 50.6 (4) |
K_b—Si1—Ohii | 70.00 (11) | O1vi—Ba—Oh | 114.5 (2) |
K_b—Si1—Nb_m1(1) | 76.78 (13) | O1vi—Ba—Ohvi | 54.3 (2) |
Ti_m1(1)—Si1—Ti_m1(2)ii | 67.32 (5) | O1vi—Ba—W2 | 154.1 (4) |
Ti_m1(1)—Si1—Si1vi | 127.2 (2) | O1vi—Ba—W2xiv | 110.9 (2) |
Ti_m1(1)—Si1—Si2iv | 121.44 (17) | O1vi—Ba—W_c | 0 |
Ti_m1(1)—Si1—O2ii | 37.10 (17) | O1vi—Ba—Ti_m2 | 42.0 (3) |
Ti_m1(1)—Si1—O3 | 32.7 (2) | O1vi—Ba—Mg_m2 | 42.0 (3) |
Ti_m1(1)—Si1—O4 | 139.1 (5) | O3—Ba—O3vi | 68.6 (3) |
Ti_m1(1)—Si1—O6 | 88.7 (5) | O3—Ba—O5 | 69.0 (3) |
Ti_m1(1)—Si1—O7 | 102.7 (5) | O3—Ba—Oh | 54.5 (4) |
Ti_m1(1)—Si1—Ohii | 34.3 (3) | O3—Ba—Ohvi | 122.7 (4) |
Ti_m1(1)—Si1—Nb_m1(1) | 0.0 (5) | O3—Ba—W2 | 81.57 (18) |
Ti_m1(2)ii—Si1—Si1vi | 134.06 (18) | O3—Ba—W2xiv | 117.5 (2) |
Ti_m1(2)ii—Si1—Si2iv | 121.30 (15) | O3—Ba—W_c | 0 |
Ti_m1(2)ii—Si1—O2ii | 67.3 (2) | O3—Ba—Ti_m2 | 127.8 (2) |
Ti_m1(2)ii—Si1—O3 | 90.5 (3) | O3—Ba—Mg_m2 | 127.8 (2) |
Ti_m1(2)ii—Si1—O4 | 112.9 (6) | O3vi—Ba—O5 | 69.0 (3) |
Ti_m1(2)ii—Si1—O6 | 24.4 (4) | O3vi—Ba—Oh | 122.7 (4) |
Ti_m1(2)ii—Si1—O7 | 124.8 (3) | O3vi—Ba—Ohvi | 54.5 (4) |
Ti_m1(2)ii—Si1—Ohii | 34.5 (3) | O3vi—Ba—W2 | 117.5 (2) |
Ti_m1(2)ii—Si1—Nb_m1(1) | 67.32 (5) | O3vi—Ba—W2xiv | 81.57 (18) |
Si1vi—Si1—Si2iv | 89.68 (8) | O3vi—Ba—W_c | 0 |
Si1vi—Si1—O2ii | 153.5 (4) | O3vi—Ba—Ti_m2 | 127.8 (2) |
Si1vi—Si1—O3 | 94.6 (3) | O3vi—Ba—Mg_m2 | 127.8 (2) |
Si1vi—Si1—O4 | 24.4 (7) | O5—Ba—Oh | 83.72 (13) |
Si1vi—Si1—O6 | 129.3 (5) | O5—Ba—Ohvi | 83.72 (13) |
Si1vi—Si1—O7 | 96.4 (2) | O5—Ba—W2 | 145.2 (2) |
Si1vi—Si1—Ohii | 134.02 (13) | O5—Ba—W2xiv | 145.2 (2) |
Si1vi—Si1—Nb_m1(1) | 127.2 (2) | O5—Ba—W_c | 0 |
Si2iv—Si1—O2ii | 88.82 (14) | O5—Ba—Ti_m2 | 73.6 (4) |
Si2iv—Si1—O3 | 128.9 (5) | O5—Ba—Mg_m2 | 73.6 (4) |
Si2iv—Si1—O4 | 94.2 (3) | Oh—Ba—Ohvi | 167.10 (16) |
Si2iv—Si1—O6 | 100.7 (3) | Oh—Ba—W2 | 63.8 (2) |
Si2iv—Si1—O7 | 20.4 (6) | Oh—Ba—W2xiv | 129.1 (2) |
Si2iv—Si1—Ohii | 136.11 (12) | Oh—Ba—W_c | 0 |
Si2iv—Si1—Nb_m1(1) | 121.44 (17) | Oh—Ba—Ti_m2 | 86.8 (3) |
O2ii—Si1—O3 | 66.4 (3) | Oh—Ba—Mg_m2 | 86.8 (3) |
O2ii—Si1—O4 | 176.1 (6) | Ohvi—Ba—W2 | 129.1 (2) |
O2ii—Si1—O6 | 76.9 (5) | Ohvi—Ba—W2xiv | 63.8 (2) |
O2ii—Si1—O7 | 74.3 (3) | Ohvi—Ba—W_c | 0 |
O2ii—Si1—Ohii | 51.0 (2) | Ohvi—Ba—Ti_m2 | 86.8 (3) |
O2ii—Si1—Nb_m1(1) | 37.10 (17) | Ohvi—Ba—Mg_m2 | 86.8 (3) |
O3—Si1—O4 | 109.7 (7) | W2—Ba—W2xiv | 65.4 (3) |
O3—Si1—O6 | 114.7 (5) | W2—Ba—W_c | 0 |
O3—Si1—O7 | 109.0 (8) | W2—Ba—Ti_m2 | 114.03 (18) |
O3—Si1—Ohii | 56.6 (4) | W2—Ba—Mg_m2 | 114.03 (18) |
O3—Si1—Nb_m1(1) | 32.7 (2) | W2xiv—Ba—W_c | 0 |
O4—Si1—O6 | 104.9 (9) | W2xiv—Ba—Ti_m2 | 114.03 (18) |
O4—Si1—O7 | 107.9 (4) | W2xiv—Ba—Mg_m2 | 114.03 (18) |
O4—Si1—Ohii | 126.9 (4) | W_c—Ba—Ti_m2 | 0 |
O4—Si1—Nb_m1(1) | 139.1 (5) | W_c—Ba—Mg_m2 | 0 |
O6—Si1—O7 | 110.4 (5) | Ti_m2—Ba—Mg_m2 | 0.0 (5) |
O6—Si1—Ohii | 58.1 (5) | Na_a—W1—Na_ai | 74.1 (9) |
O6—Si1—Nb_m1(1) | 88.7 (5) | Na_a—W1—K_biv | 126.4 (4) |
O7—Si1—Ohii | 125.2 (3) | Na_a—W1—K_bvii | 122.9 (4) |
O7—Si1—Nb_m1(1) | 102.7 (5) | Na_a—W1—O2iv | 53.0 (4) |
Ohii—Si1—Nb_m1(1) | 34.3 (3) | Na_a—W1—O2vii | 106.4 (6) |
Na_aix—Si2—Na_aii | 90.2 (5) | Na_a—W1—O6 | 53.0 (5) |
Na_aix—Si2—Ti_m1(1) | 65.2 (2) | Na_a—W1—O6i | 109.4 (6) |
Na_aix—Si2—Ti_m1(2) | 111.3 (2) | Na_a—W1—Ohiii | 64.8 (4) |
Na_aix—Si2—Fe_m2 | 163.1 (2) | Na_a—W1—Ohv | 61.5 (4) |
Na_aix—Si2—Si1ix | 64.3 (2) | Na_a—W1—W2iii | 37.0 (6) |
Na_aix—Si2—Si2vi | 128.8 (3) | Na_ai—W1—K_biv | 122.9 (4) |
Na_aix—Si2—O1 | 140.7 (3) | Na_ai—W1—K_bvii | 126.4 (4) |
Na_aix—Si2—O1vi | 156.9 (4) | Na_ai—W1—O2iv | 106.4 (6) |
Na_aix—Si2—O2 | 39.4 (3) | Na_ai—W1—O2vii | 53.0 (4) |
Na_aix—Si2—O5 | 108.2 (7) | Na_ai—W1—O6 | 109.4 (6) |
Na_aix—Si2—O6ii | 81.1 (4) | Na_ai—W1—O6i | 53.0 (5) |
Na_aix—Si2—O7ix | 74.7 (6) | Na_ai—W1—Ohiii | 61.5 (4) |
Na_aix—Si2—Oh | 96.0 (3) | Na_ai—W1—Ohv | 64.8 (4) |
Na_aix—Si2—Ba | 131.7 (3) | Na_ai—W1—W2iii | 37.0 (6) |
Na_aix—Si2—W_c | 131.7 (3) | K_biv—W1—K_bvii | 89.2 (3) |
Na_aix—Si2—Nb_m1(1) | 65.2 (2) | K_biv—W1—O2iv | 73.7 (2) |
Na_aix—Si2—Ti_m2 | 163.1 (2) | K_biv—W1—O2vii | 124.5 (3) |
Na_aix—Si2—Mg_m2 | 163.1 (2) | K_biv—W1—O6 | 125.4 (3) |
Na_aii—Si2—Ti_m1(1) | 107.7 (2) | K_biv—W1—O6i | 70.2 (2) |
Na_aii—Si2—Ti_m1(2) | 63.0 (2) | K_biv—W1—Ohiii | 79.82 (11) |
Na_aii—Si2—Fe_m2 | 92.8 (3) | K_biv—W1—Ohv | 169.0 (3) |
Na_aii—Si2—Si1ix | 68.4 (2) | K_biv—W1—W2iii | 135.42 (15) |
Na_aii—Si2—Si2vi | 122.4 (3) | K_bvii—W1—O2iv | 124.5 (3) |
Na_aii—Si2—O1 | 65.3 (5) | K_bvii—W1—O2vii | 73.7 (2) |
Na_aii—Si2—O1vi | 106.1 (4) | K_bvii—W1—O6 | 70.2 (2) |
Na_aii—Si2—O2 | 104.4 (5) | K_bvii—W1—O6i | 125.4 (3) |
Na_aii—Si2—O5 | 145.9 (7) | K_bvii—W1—Ohiii | 169.0 (3) |
Na_aii—Si2—O6ii | 44.3 (3) | K_bvii—W1—Ohv | 79.82 (11) |
Na_aii—Si2—O7ix | 48.8 (5) | K_bvii—W1—W2iii | 135.42 (15) |
Na_aii—Si2—Oh | 93.8 (3) | O2iv—W1—O2vii | 157.0 (4) |
Na_aii—Si2—Ba | 123.1 (3) | O2iv—W1—O6 | 77.9 (3) |
Na_aii—Si2—W_c | 123.1 (3) | O2iv—W1—O6i | 98.1 (3) |
Na_aii—Si2—Nb_m1(1) | 107.7 (2) | O2iv—W1—Ohiii | 52.0 (4) |
Na_aii—Si2—Ti_m2 | 92.8 (3) | O2iv—W1—Ohv | 113.0 (4) |
Na_aii—Si2—Mg_m2 | 92.8 (3) | O2iv—W1—W2iii | 78.5 (2) |
Ti_m1(1)—Si2—Ti_m1(2) | 65.93 (5) | O2vii—W1—O6 | 98.1 (3) |
Ti_m1(1)—Si2—Fe_m2 | 98.07 (6) | O2vii—W1—O6i | 77.9 (3) |
Ti_m1(1)—Si2—Si1ix | 129.30 (16) | O2vii—W1—Ohiii | 113.0 (4) |
Ti_m1(1)—Si2—Si2vi | 125.70 (16) | O2vii—W1—Ohv | 52.0 (4) |
Ti_m1(1)—Si2—O1 | 92.3 (4) | O2vii—W1—W2iii | 78.5 (2) |
Ti_m1(1)—Si2—O1vi | 122.39 (16) | O6—W1—O6i | 160.6 (4) |
Ti_m1(1)—Si2—O2 | 26.0 (2) | O6—W1—Ohiii | 116.0 (4) |
Ti_m1(1)—Si2—O5 | 106.1 (6) | O6—W1—Ohv | 51.0 (4) |
Ti_m1(1)—Si2—O6ii | 64.5 (3) | O6—W1—W2iii | 80.3 (2) |
Ti_m1(1)—Si2—O7ix | 133.7 (3) | O6i—W1—Ohiii | 51.0 (4) |
Ti_m1(1)—Si2—Oh | 34.3 (3) | O6i—W1—Ohv | 116.0 (4) |
Ti_m1(1)—Si2—Ba | 71.22 (8) | O6i—W1—W2iii | 80.3 (2) |
Ti_m1(1)—Si2—W_c | 71.22 (8) | Ohiii—W1—Ohv | 111.2 (3) |
Ti_m1(1)—Si2—Nb_m1(1) | 0.0 (5) | Ohiii—W1—W2iii | 55.60 (18) |
Ti_m1(1)—Si2—Ti_m2 | 98.07 (6) | Ohv—W1—W2iii | 55.60 (18) |
Ti_m1(1)—Si2—Mg_m2 | 98.07 (6) | Na_aiii—W2—Na_ax | 70.9 (9) |
Ti_m1(2)—Si2—Fe_m2 | 56.13 (9) | Na_aiii—W2—O1iv | 63.1 (5) |
Ti_m1(2)—Si2—Si1ix | 131.29 (19) | Na_aiii—W2—O1xi | 116.6 (5) |
Ti_m1(2)—Si2—Si2vi | 118.42 (16) | Na_aiii—W2—O7 | 51.6 (6) |
Ti_m1(2)—Si2—O1 | 30.8 (2) | Na_aiii—W2—O7xv | 121.4 (7) |
Ti_m1(2)—Si2—O1vi | 90.9 (2) | Na_aiii—W2—Oh | 68.5 (4) |
Ti_m1(2)—Si2—O2 | 85.2 (4) | Na_aiii—W2—Ohxv | 65.2 (4) |
Ti_m1(2)—Si2—O5 | 129.7 (4) | Na_aiii—W2—Ba | 117.7 (3) |
Ti_m1(2)—Si2—O6ii | 34.72 (16) | Na_aiii—W2—Baxv | 114.5 (3) |
Ti_m1(2)—Si2—O7ix | 111.7 (5) | Na_aiii—W2—W1iii | 35.4 (6) |
Ti_m1(2)—Si2—Oh | 35.3 (3) | Na_aiii—W2—W2xiv | 144.6 (6) |
Ti_m1(2)—Si2—Ba | 65.97 (9) | Na_aiii—W2—W_c | 117.7 (3) |
Ti_m1(2)—Si2—W_c | 65.97 (9) | Na_aiii—W2—W_cxv | 114.5 (3) |
Ti_m1(2)—Si2—Nb_m1(1) | 65.93 (5) | Na_ax—W2—O1iv | 116.6 (5) |
Ti_m1(2)—Si2—Ti_m2 | 56.13 (9) | Na_ax—W2—O1xi | 63.1 (5) |
Ti_m1(2)—Si2—Mg_m2 | 56.13 (9) | Na_ax—W2—O7 | 121.4 (7) |
Fe_m2—Si2—Si1ix | 132.0 (2) | Na_ax—W2—O7xv | 51.6 (6) |
Fe_m2—Si2—Si2vi | 62.28 (10) | Na_ax—W2—Oh | 65.2 (4) |
Fe_m2—Si2—O1 | 31.1 (2) | Na_ax—W2—Ohxv | 68.5 (4) |
Fe_m2—Si2—O1vi | 35.28 (15) | Na_ax—W2—Ba | 114.5 (3) |
Fe_m2—Si2—O2 | 124.0 (2) | Na_ax—W2—Baxv | 117.7 (3) |
Fe_m2—Si2—O5 | 77.9 (5) | Na_ax—W2—W1iii | 35.4 (6) |
Fe_m2—Si2—O6ii | 89.5 (2) | Na_ax—W2—W2xiv | 144.6 (6) |
Fe_m2—Si2—O7ix | 119.2 (6) | Na_ax—W2—W_c | 114.5 (3) |
Fe_m2—Si2—Oh | 67.2 (2) | Na_ax—W2—W_cxv | 117.7 (3) |
Fe_m2—Si2—Ba | 35.93 (10) | O1iv—W2—O1xi | 179.8 (4) |
Fe_m2—Si2—W_c | 35.93 (10) | O1iv—W2—O7 | 48.4 (2) |
Fe_m2—Si2—Nb_m1(1) | 98.07 (6) | O1iv—W2—O7xv | 131.6 (2) |
Fe_m2—Si2—Ti_m2 | 0.0 (5) | O1iv—W2—Oh | 125.8 (4) |
Fe_m2—Si2—Mg_m2 | 0.0 (5) | O1iv—W2—Ohxv | 54.0 (3) |
Si1ix—Si2—Si2vi | 90.32 (8) | O1iv—W2—Ba | 124.3 (3) |
Si1ix—Si2—O1 | 125.2 (5) | O1iv—W2—Baxv | 55.8 (2) |
Si1ix—Si2—O1vi | 106.09 (15) | O1iv—W2—W1iii | 89.9 (2) |
Si1ix—Si2—O2 | 103.7 (3) | O1iv—W2—W2xiv | 90.1 (2) |
Si1ix—Si2—O5 | 93.5 (3) | O1iv—W2—W_c | 124.3 (3) |
Si1ix—Si2—O6ii | 103.16 (17) | O1iv—W2—W_cxv | 55.8 (2) |
Si1ix—Si2—O7ix | 20.6 (5) | O1xi—W2—O7 | 131.6 (2) |
Si1ix—Si2—Oh | 152.27 (13) | O1xi—W2—O7xv | 48.4 (2) |
Si1ix—Si2—Ba | 155.25 (8) | O1xi—W2—Oh | 54.0 (3) |
Si1ix—Si2—W_c | 155.25 (8) | O1xi—W2—Ohxv | 125.8 (4) |
Si1ix—Si2—Nb_m1(1) | 129.30 (16) | O1xi—W2—Ba | 55.8 (2) |
Si1ix—Si2—Ti_m2 | 132.0 (2) | O1xi—W2—Baxv | 124.3 (3) |
Si1ix—Si2—Mg_m2 | 132.0 (2) | O1xi—W2—W1iii | 89.9 (2) |
Si2vi—Si2—O1 | 90.5 (2) | O1xi—W2—W2xiv | 90.1 (2) |
Si2vi—Si2—O1vi | 28.2 (2) | O1xi—W2—W_c | 55.8 (2) |
Si2vi—Si2—O2 | 133.0 (5) | O1xi—W2—W_cxv | 124.3 (3) |
Si2vi—Si2—O5 | 25.4 (7) | O7—W2—O7xv | 172.9 (4) |
Si2vi—Si2—O6ii | 150.0 (3) | O7—W2—Oh | 82.8 (3) |
Si2vi—Si2—O7ix | 97.0 (2) | O7—W2—Ohxv | 93.8 (3) |
Si2vi—Si2—Oh | 117.39 (12) | O7—W2—Ba | 86.60 (18) |
Si2vi—Si2—Ba | 64.94 (6) | O7—W2—Baxv | 97.3 (2) |
Si2vi—Si2—W_c | 64.94 (6) | O7—W2—W1iii | 86.4 (2) |
Si2vi—Si2—Nb_m1(1) | 125.70 (16) | O7—W2—W2xiv | 93.6 (2) |
Si2vi—Si2—Ti_m2 | 62.28 (10) | O7—W2—W_c | 86.60 (18) |
Si2vi—Si2—Mg_m2 | 62.28 (10) | O7—W2—W_cxv | 97.3 (2) |
O1—Si2—O1vi | 62.3 (3) | O7xv—W2—Oh | 93.8 (3) |
O1—Si2—O2 | 114.9 (5) | O7xv—W2—Ohxv | 82.8 (3) |
O1—Si2—O5 | 108.9 (6) | O7xv—W2—Ba | 97.3 (2) |
O1—Si2—O6ii | 59.8 (3) | O7xv—W2—Baxv | 86.60 (18) |
O1—Si2—O7ix | 105.5 (8) | O7xv—W2—W1iii | 86.4 (2) |
O1—Si2—Oh | 58.1 (5) | O7xv—W2—W2xiv | 93.6 (2) |
O1—Si2—Ba | 58.0 (4) | O7xv—W2—W_c | 97.3 (2) |
O1—Si2—W_c | 58.0 (4) | O7xv—W2—W_cxv | 86.60 (18) |
O1—Si2—Nb_m1(1) | 92.3 (4) | Oh—W2—Ohxv | 122.3 (4) |
O1—Si2—Ti_m2 | 31.1 (2) | Oh—W2—Ba | 61.53 (10) |
O1—Si2—Mg_m2 | 31.1 (2) | Oh—W2—Baxv | 176.2 (4) |
O1vi—Si2—O2 | 143.4 (4) | Oh—W2—W1iii | 61.16 (19) |
O1vi—Si2—O5 | 49.7 (7) | Oh—W2—W2xiv | 118.84 (19) |
O1vi—Si2—O6ii | 122.0 (4) | Oh—W2—W_c | 61.53 (10) |
O1vi—Si2—O7ix | 103.6 (4) | Oh—W2—W_cxv | 176.2 (4) |
O1vi—Si2—Oh | 99.09 (19) | Ohxv—W2—Ba | 176.2 (4) |
O1vi—Si2—Ba | 51.27 (14) | Ohxv—W2—Baxv | 61.53 (10) |
O1vi—Si2—W_c | 51.27 (14) | Ohxv—W2—W1iii | 61.16 (19) |
O1vi—Si2—Nb_m1(1) | 122.39 (16) | Ohxv—W2—W2xiv | 118.84 (19) |
O1vi—Si2—Ti_m2 | 35.28 (15) | Ohxv—W2—W_c | 176.2 (4) |
O1vi—Si2—Mg_m2 | 35.28 (15) | Ohxv—W2—W_cxv | 61.53 (10) |
O2—Si2—O5 | 107.9 (9) | Ba—W2—Baxv | 114.6 (4) |
O2—Si2—O6ii | 70.1 (5) | Ba—W2—W1iii | 122.69 (18) |
O2—Si2—O7ix | 111.7 (5) | Ba—W2—W2xiv | 57.31 (18) |
O2—Si2—Oh | 58.9 (4) | Ba—W2—W_c | 0.0 (5) |
O2—Si2—Ba | 94.7 (2) | Ba—W2—W_cxv | 114.6 (4) |
O2—Si2—W_c | 94.7 (2) | Baxv—W2—W1iii | 122.69 (18) |
O2—Si2—Nb_m1(1) | 26.0 (2) | Baxv—W2—W2xiv | 57.31 (18) |
O2—Si2—Ti_m2 | 124.0 (2) | Baxv—W2—W_c | 114.6 (4) |
O2—Si2—Mg_m2 | 124.0 (2) | Baxv—W2—W_cxv | 0.0 (5) |
O5—Si2—O6ii | 163.2 (3) | W1iii—W2—W2xiv | 180.0 (5) |
O5—Si2—O7ix | 107.7 (4) | W1iii—W2—W_c | 122.69 (18) |
O5—Si2—Oh | 111.8 (4) | W1iii—W2—W_cxv | 122.69 (18) |
O5—Si2—Ba | 64.7 (3) | W2xiv—W2—W_c | 57.31 (18) |
O5—Si2—W_c | 64.7 (3) | W2xiv—W2—W_cxv | 57.31 (18) |
O5—Si2—Nb_m1(1) | 106.1 (6) | W_c—W2—W_cxv | 114.6 (4) |
O5—Si2—Ti_m2 | 77.9 (5) | Fe_m2—W_c—Si2 | 63.84 (12) |
O5—Si2—Mg_m2 | 77.9 (5) | Fe_m2—W_c—Si2vi | 63.84 (12) |
O6ii—Si2—O7ix | 88.0 (4) | Fe_m2—W_c—O1 | 42.0 (3) |
O6ii—Si2—Oh | 52.3 (2) | Fe_m2—W_c—O1xi | 45.6 (2) |
O6ii—Si2—Ba | 98.61 (14) | Fe_m2—W_c—O1xii | 45.6 (2) |
O6ii—Si2—W_c | 98.61 (14) | Fe_m2—W_c—O1vi | 42.0 (3) |
O6ii—Si2—Nb_m1(1) | 64.5 (3) | Fe_m2—W_c—O3 | 127.8 (2) |
O6ii—Si2—Ti_m2 | 89.5 (2) | Fe_m2—W_c—O3vi | 127.8 (2) |
O6ii—Si2—Mg_m2 | 89.5 (2) | Fe_m2—W_c—O5 | 73.6 (4) |
O7ix—Si2—Oh | 140.3 (4) | Fe_m2—W_c—Oh | 86.8 (3) |
O7ix—Si2—Ba | 153.4 (5) | Fe_m2—W_c—Ohvi | 86.8 (3) |
O7ix—Si2—W_c | 153.4 (5) | Fe_m2—W_c—Ba | 0 |
O7ix—Si2—Nb_m1(1) | 133.7 (3) | Fe_m2—W_c—W2 | 114.03 (18) |
O7ix—Si2—Ti_m2 | 119.2 (6) | Fe_m2—W_c—W2xiv | 114.03 (18) |
O7ix—Si2—Mg_m2 | 119.2 (6) | Fe_m2—W_c—Ti_m2 | 0.0 (5) |
Oh—Si2—Ba | 52.45 (10) | Fe_m2—W_c—Mg_m2 | 0.0 (5) |
Oh—Si2—W_c | 52.45 (10) | Si2—W_c—Si2vi | 50.12 (6) |
Oh—Si2—Nb_m1(1) | 34.3 (3) | Si2—W_c—O1 | 27.0 (3) |
Oh—Si2—Ti_m2 | 67.2 (2) | Si2—W_c—O1xi | 80.68 (17) |
Oh—Si2—Mg_m2 | 67.2 (2) | Si2—W_c—O1xii | 107.0 (2) |
Ba—Si2—W_c | 0.0 (5) | Si2—W_c—O1vi | 62.28 (14) |
Ba—Si2—Nb_m1(1) | 71.22 (8) | Si2—W_c—O3 | 66.0 (2) |
Ba—Si2—Ti_m2 | 35.93 (10) | Si2—W_c—O3vi | 94.09 (17) |
Ba—Si2—Mg_m2 | 35.93 (10) | Si2—W_c—O5 | 27.93 (18) |
W_c—Si2—Nb_m1(1) | 71.22 (8) | Si2—W_c—Oh | 58.49 (11) |
W_c—Si2—Ti_m2 | 35.93 (10) | Si2—W_c—Ohvi | 108.61 (12) |
W_c—Si2—Mg_m2 | 35.93 (10) | Si2—W_c—Ba | 0 |
Nb_m1(1)—Si2—Ti_m2 | 98.07 (6) | Si2—W_c—W2 | 122.25 (18) |
Nb_m1(1)—Si2—Mg_m2 | 98.07 (6) | Si2—W_c—W2xiv | 172.37 (18) |
Ti_m2—Si2—Mg_m2 | 0.0 (5) | Si2—W_c—Ti_m2 | 63.84 (12) |
Na_aii—O1—Ti_m1(2) | 83.6 (4) | Si2—W_c—Mg_m2 | 63.84 (12) |
Na_aii—O1—Fe_m2 | 139.7 (9) | Si2vi—W_c—O1 | 62.28 (14) |
Na_aii—O1—Si2 | 84.5 (5) | Si2vi—W_c—O1xi | 107.0 (2) |
Na_aii—O1—Si2vi | 117.7 (3) | Si2vi—W_c—O1xii | 80.68 (17) |
Na_aii—O1—O1xi | 119.6 (6) | Si2vi—W_c—O1vi | 27.0 (3) |
Na_aii—O1—O1vi | 125.6 (4) | Si2vi—W_c—O3 | 94.09 (17) |
Na_aii—O1—O2 | 88.1 (5) | Si2vi—W_c—O3vi | 66.0 (2) |
Na_aii—O1—O5 | 113.4 (4) | Si2vi—W_c—O5 | 27.93 (18) |
Na_aii—O1—O6ii | 50.2 (3) | Si2vi—W_c—Oh | 108.61 (12) |
Na_aii—O1—O7ix | 52.4 (5) | Si2vi—W_c—Ohvi | 58.49 (11) |
Na_aii—O1—Oh | 111.8 (3) | Si2vi—W_c—Ba | 0 |
Na_aii—O1—Ohxi | 60.3 (5) | Si2vi—W_c—W2 | 172.37 (18) |
Na_aii—O1—Ba | 174.5 (4) | Si2vi—W_c—W2xiv | 122.25 (18) |
Na_aii—O1—Baxi | 91.7 (6) | Si2vi—W_c—Ti_m2 | 63.84 (12) |
Na_aii—O1—W2ix | 39.7 (4) | Si2vi—W_c—Mg_m2 | 63.84 (12) |
Na_aii—O1—W_c | 174.5 (4) | O1—W_c—O1xi | 54.6 (3) |
Na_aii—O1—W_cxi | 91.7 (6) | O1—W_c—O1xii | 87.6 (3) |
Na_aii—O1—Ti_m2 | 139.7 (9) | O1—W_c—O1vi | 60.31 (19) |
Na_aii—O1—Mg_m2 | 139.7 (9) | O1—W_c—O3 | 85.8 (3) |
Ti_m1(2)—O1—Fe_m2 | 97.2 (3) | O1—W_c—O3vi | 119.6 (3) |
Ti_m1(2)—O1—Si2 | 125.1 (6) | O1—W_c—O5 | 50.6 (4) |
Ti_m1(2)—O1—Si2vi | 158.7 (4) | O1—W_c—Oh | 54.3 (2) |
Ti_m1(2)—O1—O1xi | 48.8 (2) | O1—W_c—Ohvi | 114.5 (2) |
Ti_m1(2)—O1—O1vi | 138.8 (4) | O1—W_c—Ba | 0 |
Ti_m1(2)—O1—O2 | 93.7 (4) | O1—W_c—W2 | 110.9 (2) |
Ti_m1(2)—O1—O5 | 145.5 (8) | O1—W_c—W2xiv | 154.1 (4) |
Ti_m1(2)—O1—O6ii | 43.6 (2) | O1—W_c—Ti_m2 | 42.0 (3) |
Ti_m1(2)—O1—O7ix | 126.7 (3) | O1—W_c—Mg_m2 | 42.0 (3) |
Ti_m1(2)—O1—Oh | 45.6 (3) | O1xi—W_c—O1xii | 64.8 (3) |
Ti_m1(2)—O1—Ohxi | 43.6 (3) | O1xi—W_c—O1vi | 87.6 (3) |
Ti_m1(2)—O1—Ba | 92.3 (2) | O1xi—W_c—O3 | 112.9 (3) |
Ti_m1(2)—O1—Baxi | 97.9 (5) | O1xi—W_c—O3vi | 173.0 (2) |
Ti_m1(2)—O1—W2ix | 102.2 (5) | O1xi—W_c—O5 | 104.8 (4) |
Ti_m1(2)—O1—W_c | 92.3 (2) | O1xi—W_c—Oh | 58.4 (4) |
Ti_m1(2)—O1—W_cxi | 97.9 (5) | O1xi—W_c—Ohvi | 122.7 (4) |
Ti_m1(2)—O1—Ti_m2 | 97.2 (3) | O1xi—W_c—Ba | 0 |
Ti_m1(2)—O1—Mg_m2 | 97.2 (3) | O1xi—W_c—W2 | 69.38 (19) |
Fe_m2—O1—Si2 | 124.5 (6) | O1xi—W_c—W2xiv | 103.1 (2) |
Fe_m2—O1—Si2vi | 67.09 (19) | O1xi—W_c—Ti_m2 | 45.6 (2) |
Fe_m2—O1—O1xi | 48.5 (2) | O1xi—W_c—Mg_m2 | 45.6 (2) |
Fe_m2—O1—O1vi | 41.53 (18) | O1xii—W_c—O1vi | 54.6 (3) |
Fe_m2—O1—O2 | 131.7 (7) | O1xii—W_c—O3 | 173.0 (2) |
Fe_m2—O1—O5 | 88.5 (4) | O1xii—W_c—O3vi | 112.9 (3) |
Fe_m2—O1—O6ii | 140.6 (4) | O1xii—W_c—O5 | 104.8 (4) |
Fe_m2—O1—O7ix | 135.3 (3) | O1xii—W_c—Oh | 122.7 (4) |
Fe_m2—O1—Oh | 95.9 (3) | O1xii—W_c—Ohvi | 58.4 (4) |
Fe_m2—O1—Ohxi | 92.9 (5) | O1xii—W_c—Ba | 0 |
Fe_m2—O1—Ba | 44.3 (2) | O1xii—W_c—W2 | 103.1 (2) |
Fe_m2—O1—Baxi | 48.1 (3) | O1xii—W_c—W2xiv | 69.38 (19) |
Fe_m2—O1—W2ix | 102.1 (5) | O1xii—W_c—Ti_m2 | 45.6 (2) |
Fe_m2—O1—W_c | 44.3 (2) | O1xii—W_c—Mg_m2 | 45.6 (2) |
Fe_m2—O1—W_cxi | 48.1 (3) | O1vi—W_c—O3 | 119.6 (3) |
Fe_m2—O1—Ti_m2 | 0.0 (5) | O1vi—W_c—O3vi | 85.8 (3) |
Fe_m2—O1—Mg_m2 | 0.0 (5) | O1vi—W_c—O5 | 50.6 (4) |
Si2—O1—Si2vi | 61.3 (3) | O1vi—W_c—Oh | 114.5 (2) |
Si2—O1—O1xi | 149.7 (8) | O1vi—W_c—Ohvi | 54.3 (2) |
Si2—O1—O1vi | 89.5 (4) | O1vi—W_c—Ba | 0 |
Si2—O1—O2 | 32.5 (3) | O1vi—W_c—W2 | 154.1 (4) |
Si2—O1—O5 | 36.1 (3) | O1vi—W_c—W2xiv | 110.9 (2) |
Si2—O1—O6ii | 90.3 (4) | O1vi—W_c—Ti_m2 | 42.0 (3) |
Si2—O1—O7ix | 37.6 (4) | O1vi—W_c—Mg_m2 | 42.0 (3) |
Si2—O1—Oh | 91.9 (7) | O3—W_c—O3vi | 68.6 (3) |
Si2—O1—Ohxi | 142.2 (4) | O3—W_c—O5 | 69.0 (3) |
Si2—O1—Ba | 95.0 (6) | O3—W_c—Oh | 54.5 (4) |
Si2—O1—Baxi | 135.8 (3) | O3—W_c—Ohvi | 122.7 (4) |
Si2—O1—W2ix | 101.7 (3) | O3—W_c—Ba | 0 |
Si2—O1—W_c | 95.0 (6) | O3—W_c—W2 | 81.57 (18) |
Si2—O1—W_cxi | 135.8 (3) | O3—W_c—W2xiv | 117.5 (2) |
Si2—O1—Ti_m2 | 124.5 (6) | O3—W_c—Ti_m2 | 127.8 (2) |
Si2—O1—Mg_m2 | 124.5 (6) | O3—W_c—Mg_m2 | 127.8 (2) |
Si2vi—O1—O1xi | 114.1 (2) | O3vi—W_c—O5 | 69.0 (3) |
Si2vi—O1—O1vi | 28.2 (3) | O3vi—W_c—Oh | 122.7 (4) |
Si2vi—O1—O2 | 87.2 (4) | O3vi—W_c—Ohvi | 54.5 (4) |
Si2vi—O1—O5 | 28.4 (3) | O3vi—W_c—Ba | 0 |
Si2vi—O1—O6ii | 151.3 (5) | O3vi—W_c—W2 | 117.5 (2) |
Si2vi—O1—O7ix | 71.9 (3) | O3vi—W_c—W2xiv | 81.57 (18) |
Si2vi—O1—Oh | 119.1 (5) | O3vi—W_c—Ti_m2 | 127.8 (2) |
Si2vi—O1—Ohxi | 145.8 (5) | O3vi—W_c—Mg_m2 | 127.8 (2) |
Si2vi—O1—Ba | 66.45 (19) | O5—W_c—Oh | 83.72 (13) |
Si2vi—O1—Baxi | 82.48 (19) | O5—W_c—Ohvi | 83.72 (13) |
Si2vi—O1—W2ix | 95.4 (3) | O5—W_c—Ba | 0 |
Si2vi—O1—W_c | 66.45 (19) | O5—W_c—W2 | 145.2 (2) |
Si2vi—O1—W_cxi | 82.48 (19) | O5—W_c—W2xiv | 145.2 (2) |
Si2vi—O1—Ti_m2 | 67.09 (19) | O5—W_c—Ti_m2 | 73.6 (4) |
Si2vi—O1—Mg_m2 | 67.09 (19) | O5—W_c—Mg_m2 | 73.6 (4) |
O1xi—O1—O1vi | 90.0 (3) | Oh—W_c—Ohvi | 167.10 (16) |
O1xi—O1—O2 | 123.6 (5) | Oh—W_c—Ba | 0 |
O1xi—O1—O5 | 127.0 (4) | Oh—W_c—W2 | 63.8 (2) |
O1xi—O1—O6ii | 92.3 (3) | Oh—W_c—W2xiv | 129.1 (2) |
O1xi—O1—O7ix | 171.8 (8) | Oh—W_c—Ti_m2 | 86.8 (3) |
O1xi—O1—Oh | 63.3 (4) | Oh—W_c—Mg_m2 | 86.8 (3) |
O1xi—O1—Ohxi | 59.5 (4) | Ohvi—W_c—Ba | 0 |
O1xi—O1—Ba | 59.2 (3) | Ohvi—W_c—W2 | 129.1 (2) |
O1xi—O1—Baxi | 66.3 (4) | Ohvi—W_c—W2xiv | 63.8 (2) |
O1xi—O1—W2ix | 108.6 (6) | Ohvi—W_c—Ti_m2 | 86.8 (3) |
O1xi—O1—W_c | 59.2 (3) | Ohvi—W_c—Mg_m2 | 86.8 (3) |
O1xi—O1—W_cxi | 66.3 (4) | Ba—W_c—W2 | 0 |
O1xi—O1—Ti_m2 | 48.5 (2) | Ba—W_c—W2xiv | 0 |
O1xi—O1—Mg_m2 | 48.5 (2) | Ba—W_c—Ti_m2 | 0 |
O1vi—O1—O2 | 113.5 (6) | Ba—W_c—Mg_m2 | 0 |
O1vi—O1—O5 | 55.4 (4) | W2—W_c—W2xiv | 65.4 (3) |
O1vi—O1—O6ii | 175.7 (5) | W2—W_c—Ti_m2 | 114.03 (18) |
O1vi—O1—O7ix | 94.1 (3) | W2—W_c—Mg_m2 | 114.03 (18) |
O1vi—O1—Oh | 122.4 (4) | W2xiv—W_c—Ti_m2 | 114.03 (18) |
O1vi—O1—Ohxi | 121.2 (6) | W2xiv—W_c—Mg_m2 | 114.03 (18) |
O1vi—O1—Ba | 59.8 (2) | Ti_m2—W_c—Mg_m2 | 0.0 (5) |
O1vi—O1—Baxi | 57.6 (4) | Ti_m1(1)—Nb_m1(1)—Si1 | 0 |
O1vi—O1—W2ix | 89.9 (4) | Ti_m1(1)—Nb_m1(1)—Si1ii | 0 |
O1vi—O1—W_c | 59.8 (2) | Ti_m1(1)—Nb_m1(1)—Si2 | 0 |
O1vi—O1—W_cxi | 57.6 (4) | Ti_m1(1)—Nb_m1(1)—Si2ii | 0 |
O1vi—O1—Ti_m2 | 41.53 (18) | Ti_m1(1)—Nb_m1(1)—O2 | 0 |
O1vi—O1—Mg_m2 | 41.53 (18) | Ti_m1(1)—Nb_m1(1)—O2ii | 0 |
O2—O1—O5 | 58.9 (5) | Ti_m1(1)—Nb_m1(1)—O3 | 0 |
O2—O1—O6ii | 68.1 (4) | Ti_m1(1)—Nb_m1(1)—O3ii | 0 |
O2—O1—O7ix | 60.9 (4) | Ti_m1(1)—Nb_m1(1)—O6 | 0 |
O2—O1—Oh | 60.8 (4) | Ti_m1(1)—Nb_m1(1)—O6ii | 0 |
O2—O1—Ohxi | 125.3 (3) | Ti_m1(1)—Nb_m1(1)—Oh | 0 |
O2—O1—Ba | 88.6 (5) | Ti_m1(1)—Nb_m1(1)—Ohii | 0 |
O2—O1—Baxi | 168.3 (3) | Si1—Nb_m1(1)—Si1ii | 180.0 (5) |
O2—O1—W2ix | 121.2 (3) | Si1—Nb_m1(1)—Si2 | 106.35 (9) |
O2—O1—W_c | 88.6 (5) | Si1—Nb_m1(1)—Si2ii | 73.65 (9) |
O2—O1—W_cxi | 168.3 (3) | Si1—Nb_m1(1)—O2 | 111.3 (3) |
O2—O1—Ti_m2 | 131.7 (7) | Si1—Nb_m1(1)—O2ii | 68.7 (3) |
O2—O1—Mg_m2 | 131.7 (7) | Si1—Nb_m1(1)—O3 | 26.1 (4) |
O5—O1—O6ii | 125.3 (6) | Si1—Nb_m1(1)—O3ii | 153.9 (4) |
O5—O1—O7ix | 61.0 (4) | Si1—Nb_m1(1)—O6 | 27.07 (18) |
O5—O1—Oh | 100.0 (7) | Si1—Nb_m1(1)—O6ii | 152.93 (18) |
O5—O1—Ohxi | 170.5 (5) | Si1—Nb_m1(1)—Oh | 101.0 (3) |
O5—O1—Ba | 68.4 (3) | Si1—Nb_m1(1)—Ohii | 79.0 (3) |
O5—O1—Baxi | 110.8 (4) | Si1ii—Nb_m1(1)—Si2 | 73.65 (9) |
O5—O1—W2ix | 109.8 (4) | Si1ii—Nb_m1(1)—Si2ii | 106.35 (9) |
O5—O1—W_c | 68.4 (3) | Si1ii—Nb_m1(1)—O2 | 68.7 (3) |
O5—O1—W_cxi | 110.8 (4) | Si1ii—Nb_m1(1)—O2ii | 111.3 (3) |
O5—O1—Ti_m2 | 88.5 (4) | Si1ii—Nb_m1(1)—O3 | 153.9 (4) |
O5—O1—Mg_m2 | 88.5 (4) | Si1ii—Nb_m1(1)—O3ii | 26.1 (4) |
O6ii—O1—O7ix | 83.1 (3) | Si1ii—Nb_m1(1)—O6 | 152.93 (18) |
O6ii—O1—Oh | 61.9 (3) | Si1ii—Nb_m1(1)—O6ii | 27.07 (18) |
O6ii—O1—Ohxi | 57.4 (4) | Si1ii—Nb_m1(1)—Oh | 79.0 (3) |
O6ii—O1—Ba | 124.4 (4) | Si1ii—Nb_m1(1)—Ohii | 101.0 (3) |
O6ii—O1—Baxi | 120.2 (6) | Si2—Nb_m1(1)—Si2ii | 180.0 (5) |
O6ii—O1—W2ix | 86.0 (4) | Si2—Nb_m1(1)—O2 | 21.0 (3) |
O6ii—O1—W_c | 124.4 (4) | Si2—Nb_m1(1)—O2ii | 159.0 (3) |
O6ii—O1—W_cxi | 120.2 (6) | Si2—Nb_m1(1)—O3 | 80.8 (3) |
O6ii—O1—Ti_m2 | 140.6 (4) | Si2—Nb_m1(1)—O3ii | 99.2 (3) |
O6ii—O1—Mg_m2 | 140.6 (4) | Si2—Nb_m1(1)—O6 | 122.78 (14) |
O7ix—O1—Oh | 119.6 (6) | Si2—Nb_m1(1)—O6ii | 57.22 (14) |
O7ix—O1—Ohxi | 112.4 (5) | Si2—Nb_m1(1)—Oh | 71.3 (2) |
O7ix—O1—Ba | 129.0 (6) | Si2—Nb_m1(1)—Ohii | 108.7 (2) |
O7ix—O1—Baxi | 110.2 (5) | Si2ii—Nb_m1(1)—O2 | 159.0 (3) |
O7ix—O1—W2ix | 64.4 (4) | Si2ii—Nb_m1(1)—O2ii | 21.0 (3) |
O7ix—O1—W_c | 129.0 (6) | Si2ii—Nb_m1(1)—O3 | 99.2 (3) |
O7ix—O1—W_cxi | 110.2 (5) | Si2ii—Nb_m1(1)—O3ii | 80.8 (3) |
O7ix—O1—Ti_m2 | 135.3 (3) | Si2ii—Nb_m1(1)—O6 | 57.22 (14) |
O7ix—O1—Mg_m2 | 135.3 (3) | Si2ii—Nb_m1(1)—O6ii | 122.78 (14) |
Oh—O1—Ohxi | 89.2 (4) | Si2ii—Nb_m1(1)—Oh | 108.7 (2) |
Oh—O1—Ba | 62.7 (3) | Si2ii—Nb_m1(1)—Ohii | 71.3 (2) |
Oh—O1—Baxi | 129.5 (4) | O2—Nb_m1(1)—O2ii | 180.0 (5) |
Oh—O1—W2ix | 145.2 (4) | O2—Nb_m1(1)—O3 | 89.2 (3) |
Oh—O1—W_c | 62.7 (3) | O2—Nb_m1(1)—O3ii | 90.8 (3) |
Oh—O1—W_cxi | 129.5 (4) | O2—Nb_m1(1)—O6 | 118.0 (4) |
Oh—O1—Ti_m2 | 95.9 (3) | O2—Nb_m1(1)—O6ii | 62.0 (4) |
Oh—O1—Mg_m2 | 95.9 (3) | O2—Nb_m1(1)—Oh | 90.7 (5) |
Ohxi—O1—Ba | 118.6 (3) | O2—Nb_m1(1)—Ohii | 89.3 (5) |
Ohxi—O1—Baxi | 64.0 (4) | O2ii—Nb_m1(1)—O3 | 90.8 (3) |
Ohxi—O1—W2ix | 60.7 (4) | O2ii—Nb_m1(1)—O3ii | 89.2 (3) |
Ohxi—O1—W_c | 118.6 (3) | O2ii—Nb_m1(1)—O6 | 62.0 (4) |
Ohxi—O1—W_cxi | 64.0 (4) | O2ii—Nb_m1(1)—O6ii | 118.0 (4) |
Ohxi—O1—Ti_m2 | 92.9 (5) | O2ii—Nb_m1(1)—Oh | 89.3 (5) |
Ohxi—O1—Mg_m2 | 92.9 (5) | O2ii—Nb_m1(1)—Ohii | 90.7 (5) |
Ba—O1—Baxi | 92.4 (2) | O3—Nb_m1(1)—O3ii | 180.0 (5) |
Ba—O1—W2ix | 145.3 (4) | O3—Nb_m1(1)—O6 | 50.3 (5) |
Ba—O1—W_c | 0.0 (5) | O3—Nb_m1(1)—O6ii | 129.7 (5) |
Ba—O1—W_cxi | 92.4 (2) | O3—Nb_m1(1)—Oh | 88.0 (5) |
Ba—O1—Ti_m2 | 44.3 (2) | O3—Nb_m1(1)—Ohii | 92.0 (5) |
Ba—O1—Mg_m2 | 44.3 (2) | O3ii—Nb_m1(1)—O6 | 129.7 (5) |
Baxi—O1—W2ix | 54.8 (3) | O3ii—Nb_m1(1)—O6ii | 50.3 (5) |
Baxi—O1—W_c | 92.4 (2) | O3ii—Nb_m1(1)—Oh | 92.0 (5) |
Baxi—O1—W_cxi | 0.0 (5) | O3ii—Nb_m1(1)—Ohii | 88.0 (5) |
Baxi—O1—Ti_m2 | 48.1 (3) | O6—Nb_m1(1)—O6ii | 180.0 (5) |
Baxi—O1—Mg_m2 | 48.1 (3) | O6—Nb_m1(1)—Oh | 125.0 (3) |
W2ix—O1—W_c | 145.3 (4) | O6—Nb_m1(1)—Ohii | 55.0 (3) |
W2ix—O1—W_cxi | 54.8 (3) | O6ii—Nb_m1(1)—Oh | 55.0 (3) |
W2ix—O1—Ti_m2 | 102.1 (5) | O6ii—Nb_m1(1)—Ohii | 125.0 (3) |
W2ix—O1—Mg_m2 | 102.1 (5) | Oh—Nb_m1(1)—Ohii | 180.0 (5) |
W_c—O1—W_cxi | 92.4 (2) | Ti_m1(2)—Ti_m2—Ti_m1(2)xii | 180.0 (5) |
W_c—O1—Ti_m2 | 44.3 (2) | Ti_m1(2)—Ti_m2—Fe_m2 | 0 |
W_c—O1—Mg_m2 | 44.3 (2) | Ti_m1(2)—Ti_m2—Si2 | 62.28 (5) |
W_cxi—O1—Ti_m2 | 48.1 (3) | Ti_m1(2)—Ti_m2—Si2xi | 62.28 (5) |
W_cxi—O1—Mg_m2 | 48.1 (3) | Ti_m1(2)—Ti_m2—Si2xii | 117.72 (5) |
Ti_m2—O1—Mg_m2 | 0.0 (5) | Ti_m1(2)—Ti_m2—Si2vi | 117.72 (5) |
Na_aix—O2—K_b | 94.1 (6) | Ti_m1(2)—Ti_m2—O1 | 41.5 (2) |
Na_aix—O2—Ti_m1(1) | 111.6 (6) | Ti_m1(2)—Ti_m2—O1xi | 41.5 (2) |
Na_aix—O2—Ti_m1(2) | 136.8 (6) | Ti_m1(2)—Ti_m2—O1xii | 138.5 (2) |
Na_aix—O2—Si1ii | 80.7 (4) | Ti_m1(2)—Ti_m2—O1vi | 138.5 (2) |
Na_aix—O2—Si2 | 115.1 (5) | Ti_m1(2)—Ti_m2—O5 | 90 |
Na_aix—O2—O1 | 137.5 (7) | Ti_m1(2)—Ti_m2—O5xi | 90 |
Na_aix—O2—O3 | 126.9 (9) | Ti_m1(2)—Ti_m2—Ba | 90 |
Na_aix—O2—O3ii | 85.5 (3) | Ti_m1(2)—Ti_m2—Baxi | 90 |
Na_aix—O2—O5 | 114.0 (4) | Ti_m1(2)—Ti_m2—W_c | 90 |
Na_aix—O2—O6ii | 103.4 (6) | Ti_m1(2)—Ti_m2—W_cxi | 90 |
Na_aix—O2—O7ix | 82.5 (5) | Ti_m1(2)—Ti_m2—Mg_m2 | 0 |
Na_aix—O2—O7ii | 52.2 (5) | Ti_m1(2)xii—Ti_m2—Fe_m2 | 0 |
Na_aix—O2—Oh | 146.0 (3) | Ti_m1(2)xii—Ti_m2—Si2 | 117.72 (5) |
Na_aix—O2—Ohii | 71.9 (6) | Ti_m1(2)xii—Ti_m2—Si2xi | 117.72 (5) |
Na_aix—O2—W1ix | 42.8 (5) | Ti_m1(2)xii—Ti_m2—Si2xii | 62.28 (5) |
Na_aix—O2—Nb_m1(1) | 111.6 (6) | Ti_m1(2)xii—Ti_m2—Si2vi | 62.28 (5) |
K_b—O2—Ti_m1(1) | 94.3 (4) | Ti_m1(2)xii—Ti_m2—O1 | 138.5 (2) |
K_b—O2—Ti_m1(2) | 128.7 (2) | Ti_m1(2)xii—Ti_m2—O1xi | 138.5 (2) |
K_b—O2—Si1ii | 164.4 (5) | Ti_m1(2)xii—Ti_m2—O1xii | 41.5 (2) |
K_b—O2—Si2 | 87.6 (3) | Ti_m1(2)xii—Ti_m2—O1vi | 41.5 (2) |
K_b—O2—O1 | 106.1 (3) | Ti_m1(2)xii—Ti_m2—O5 | 90 |
K_b—O2—O3 | 53.6 (3) | Ti_m1(2)xii—Ti_m2—O5xi | 90 |
K_b—O2—O3ii | 133.7 (5) | Ti_m1(2)xii—Ti_m2—Ba | 90 |
K_b—O2—O5 | 51.1 (5) | Ti_m1(2)xii—Ti_m2—Baxi | 90 |
K_b—O2—O6ii | 161.9 (4) | Ti_m1(2)xii—Ti_m2—W_c | 90 |
K_b—O2—O7ix | 101.6 (3) | Ti_m1(2)xii—Ti_m2—W_cxi | 90 |
K_b—O2—O7ii | 146.2 (4) | Ti_m1(2)xii—Ti_m2—Mg_m2 | 0 |
K_b—O2—Oh | 108.9 (3) | Fe_m2—Ti_m2—Si2 | 0 |
K_b—O2—Ohii | 77.3 (4) | Fe_m2—Ti_m2—Si2xi | 0 |
K_b—O2—W1ix | 51.4 (3) | Fe_m2—Ti_m2—Si2xii | 0 |
K_b—O2—Nb_m1(1) | 94.3 (4) | Fe_m2—Ti_m2—Si2vi | 0 |
Ti_m1(1)—O2—Ti_m1(2) | 75.3 (3) | Fe_m2—Ti_m2—O1 | 0 |
Ti_m1(1)—O2—Si1ii | 74.2 (2) | Fe_m2—Ti_m2—O1xi | 0 |
Ti_m1(1)—O2—Si2 | 133.0 (5) | Fe_m2—Ti_m2—O1xii | 0 |
Ti_m1(1)—O2—O1 | 103.9 (4) | Fe_m2—Ti_m2—O1vi | 0 |
Ti_m1(1)—O2—O3 | 45.6 (2) | Fe_m2—Ti_m2—O5 | 0 |
Ti_m1(1)—O2—O3ii | 44.9 (2) | Fe_m2—Ti_m2—O5xi | 0 |
Ti_m1(1)—O2—O5 | 123.2 (3) | Fe_m2—Ti_m2—Ba | 0 |
Ti_m1(1)—O2—O6ii | 83.9 (3) | Fe_m2—Ti_m2—Baxi | 0 |
Ti_m1(1)—O2—O7ix | 158.0 (7) | Fe_m2—Ti_m2—W_c | 0 |
Ti_m1(1)—O2—O7ii | 98.4 (2) | Fe_m2—Ti_m2—W_cxi | 0 |
Ti_m1(1)—O2—Oh | 44.0 (3) | Fe_m2—Ti_m2—Mg_m2 | 0 |
Ti_m1(1)—O2—Ohii | 44.7 (3) | Si2—Ti_m2—Si2xi | 124.57 (8) |
Ti_m1(1)—O2—W1ix | 112.6 (6) | Si2—Ti_m2—Si2xii | 180.0 (5) |
Ti_m1(1)—O2—Nb_m1(1) | 0.0 (5) | Si2—Ti_m2—Si2vi | 55.43 (8) |
Ti_m1(2)—O2—Si1ii | 59.5 (2) | Si2—Ti_m2—O1 | 24.4 (4) |
Ti_m1(2)—O2—Si2 | 67.5 (5) | Si2—Ti_m2—O1xi | 102.4 (3) |
Ti_m1(2)—O2—O1 | 35.5 (2) | Si2—Ti_m2—O1xii | 155.6 (4) |
Ti_m1(2)—O2—O3 | 89.4 (4) | Si2—Ti_m2—O1vi | 77.6 (3) |
Ti_m1(2)—O2—O3ii | 69.8 (4) | Si2—Ti_m2—O5 | 29.44 (12) |
Ti_m1(2)—O2—O5 | 92.8 (5) | Si2—Ti_m2—O5xi | 150.56 (12) |
Ti_m1(2)—O2—O6ii | 33.5 (2) | Si2—Ti_m2—Ba | 80.24 (13) |
Ti_m1(2)—O2—O7ix | 82.9 (5) | Si2—Ti_m2—Baxi | 99.76 (13) |
Ti_m1(2)—O2—O7ii | 84.9 (4) | Si2—Ti_m2—W_c | 80.24 (13) |
Ti_m1(2)—O2—Oh | 34.1 (4) | Si2—Ti_m2—W_cxi | 99.76 (13) |
Ti_m1(2)—O2—Ohii | 118.3 (3) | Si2—Ti_m2—Mg_m2 | 0 |
Ti_m1(2)—O2—W1ix | 172.0 (4) | Si2xi—Ti_m2—Si2xii | 55.43 (8) |
Ti_m1(2)—O2—Nb_m1(1) | 75.3 (3) | Si2xi—Ti_m2—Si2vi | 180.0 (5) |
Si1ii—O2—Si2 | 107.9 (7) | Si2xi—Ti_m2—O1 | 102.4 (3) |
Si1ii—O2—O1 | 87.3 (4) | Si2xi—Ti_m2—O1xi | 24.4 (4) |
Si1ii—O2—O3 | 118.5 (2) | Si2xi—Ti_m2—O1xii | 77.6 (3) |
Si1ii—O2—O3ii | 31.7 (3) | Si2xi—Ti_m2—O1vi | 155.6 (4) |
Si1ii—O2—O5 | 144.4 (8) | Si2xi—Ti_m2—O5 | 150.56 (12) |
Si1ii—O2—O6ii | 30.0 (3) | Si2xi—Ti_m2—O5xi | 29.44 (12) |
Si1ii—O2—O7ix | 92.4 (4) | Si2xi—Ti_m2—Ba | 99.76 (13) |
Si1ii—O2—O7ii | 31.60 (18) | Si2xi—Ti_m2—Baxi | 80.24 (13) |
Si1ii—O2—Oh | 70.4 (3) | Si2xi—Ti_m2—W_c | 99.76 (13) |
Si1ii—O2—Ohii | 87.1 (3) | Si2xi—Ti_m2—W_cxi | 80.24 (13) |
Si1ii—O2—W1ix | 122.7 (3) | Si2xi—Ti_m2—Mg_m2 | 0 |
Si1ii—O2—Nb_m1(1) | 74.2 (2) | Si2xii—Ti_m2—Si2vi | 124.57 (8) |
Si2—O2—O1 | 32.6 (3) | Si2xii—Ti_m2—O1 | 155.6 (4) |
Si2—O2—O3 | 105.3 (3) | Si2xii—Ti_m2—O1xi | 77.6 (3) |
Si2—O2—O3ii | 134.0 (8) | Si2xii—Ti_m2—O1xii | 24.4 (4) |
Si2—O2—O5 | 36.6 (5) | Si2xii—Ti_m2—O1vi | 102.4 (3) |
Si2—O2—O6ii | 80.6 (6) | Si2xii—Ti_m2—O5 | 150.56 (12) |
Si2—O2—O7ix | 34.5 (3) | Si2xii—Ti_m2—O5xi | 29.44 (12) |
Si2—O2—O7ii | 105.5 (6) | Si2xii—Ti_m2—Ba | 99.76 (13) |
Si2—O2—Oh | 91.2 (5) | Si2xii—Ti_m2—Baxi | 80.24 (13) |
Si2—O2—Ohii | 164.0 (6) | Si2xii—Ti_m2—W_c | 99.76 (13) |
Si2—O2—W1ix | 105.0 (4) | Si2xii—Ti_m2—W_cxi | 80.24 (13) |
Si2—O2—Nb_m1(1) | 133.0 (5) | Si2xii—Ti_m2—Mg_m2 | 0 |
O1—O2—O3 | 94.6 (4) | Si2vi—Ti_m2—O1 | 77.6 (3) |
O1—O2—O3ii | 104.8 (5) | Si2vi—Ti_m2—O1xi | 155.6 (4) |
O1—O2—O5 | 59.5 (5) | Si2vi—Ti_m2—O1xii | 102.4 (3) |
O1—O2—O6ii | 57.3 (4) | Si2vi—Ti_m2—O1vi | 24.4 (4) |
O1—O2—O7ix | 57.3 (4) | Si2vi—Ti_m2—O5 | 29.44 (12) |
O1—O2—O7ii | 101.0 (6) | Si2vi—Ti_m2—O5xi | 150.56 (12) |
O1—O2—Oh | 60.1 (4) | Si2vi—Ti_m2—Ba | 80.24 (13) |
O1—O2—Ohii | 148.2 (3) | Si2vi—Ti_m2—Baxi | 99.76 (13) |
O1—O2—W1ix | 137.4 (3) | Si2vi—Ti_m2—W_c | 80.24 (13) |
O1—O2—Nb_m1(1) | 103.9 (4) | Si2vi—Ti_m2—W_cxi | 99.76 (13) |
O3—O2—O3ii | 90.5 (3) | Si2vi—Ti_m2—Mg_m2 | 0 |
O3—O2—O5 | 79.7 (4) | O1—Ti_m2—O1xi | 83.1 (3) |
O3—O2—O6ii | 116.4 (4) | O1—Ti_m2—O1xii | 180.0 (5) |
O3—O2—O7ix | 138.3 (3) | O1—Ti_m2—O1vi | 96.9 (3) |
O3—O2—O7ii | 143.6 (3) | O1—Ti_m2—O5 | 53.8 (4) |
O3—O2—Oh | 58.6 (4) | O1—Ti_m2—O5xi | 126.2 (4) |
O3—O2—Ohii | 61.3 (4) | O1—Ti_m2—Ba | 93.7 (4) |
O3—O2—W1ix | 95.4 (5) | O1—Ti_m2—Baxi | 86.3 (4) |
O3—O2—Nb_m1(1) | 45.6 (2) | O1—Ti_m2—W_c | 93.7 (4) |
O3ii—O2—O5 | 160.3 (5) | O1—Ti_m2—W_cxi | 86.3 (4) |
O3ii—O2—O6ii | 54.0 (4) | O1—Ti_m2—Mg_m2 | 0 |
O3ii—O2—O7ix | 124.1 (5) | O1xi—Ti_m2—O1xii | 96.9 (3) |
O3ii—O2—O7ii | 53.9 (2) | O1xi—Ti_m2—O1vi | 180.0 (5) |
O3ii—O2—Oh | 60.5 (3) | O1xi—Ti_m2—O5 | 126.2 (4) |
O3ii—O2—Ohii | 58.6 (4) | O1xi—Ti_m2—O5xi | 53.8 (4) |
O3ii—O2—W1ix | 116.4 (5) | O1xi—Ti_m2—Ba | 86.3 (4) |
O3ii—O2—Nb_m1(1) | 44.9 (2) | O1xi—Ti_m2—Baxi | 93.7 (4) |
O5—O2—O6ii | 115.5 (7) | O1xi—Ti_m2—W_c | 86.3 (4) |
O5—O2—O7ix | 59.9 (4) | O1xi—Ti_m2—W_cxi | 93.7 (4) |
O5—O2—O7ii | 136.3 (5) | O1xi—Ti_m2—Mg_m2 | 0 |
O5—O2—Oh | 99.9 (4) | O1xii—Ti_m2—O1vi | 83.1 (3) |
O5—O2—Ohii | 127.8 (7) | O1xii—Ti_m2—O5 | 126.2 (4) |
O5—O2—W1ix | 81.8 (5) | O1xii—Ti_m2—O5xi | 53.8 (4) |
O5—O2—Nb_m1(1) | 123.2 (3) | O1xii—Ti_m2—Ba | 86.3 (4) |
O6ii—O2—O7ix | 76.3 (5) | O1xii—Ti_m2—Baxi | 93.7 (4) |
O6ii—O2—O7ii | 51.4 (3) | O1xii—Ti_m2—W_c | 86.3 (4) |
O6ii—O2—Oh | 58.0 (4) | O1xii—Ti_m2—W_cxi | 93.7 (4) |
O6ii—O2—Ohii | 112.6 (3) | O1xii—Ti_m2—Mg_m2 | 0 |
O6ii—O2—W1ix | 145.4 (3) | O1vi—Ti_m2—O5 | 53.8 (4) |
O6ii—O2—Nb_m1(1) | 83.9 (3) | O1vi—Ti_m2—O5xi | 126.2 (4) |
O7ix—O2—O7ii | 76.5 (4) | O1vi—Ti_m2—Ba | 93.7 (4) |
O7ix—O2—Oh | 115.4 (7) | O1vi—Ti_m2—Baxi | 86.3 (4) |
O7ix—O2—Ohii | 154.2 (4) | O1vi—Ti_m2—W_c | 93.7 (4) |
O7ix—O2—W1ix | 89.3 (3) | O1vi—Ti_m2—W_cxi | 86.3 (4) |
O7ix—O2—Nb_m1(1) | 158.0 (7) | O1vi—Ti_m2—Mg_m2 | 0 |
O7ii—O2—Oh | 101.9 (4) | O5—Ti_m2—O5xi | 180.0 (5) |
O7ii—O2—Ohii | 90.2 (4) | O5—Ti_m2—Ba | 68.6 (3) |
O7ii—O2—W1ix | 94.9 (4) | O5—Ti_m2—Baxi | 111.4 (3) |
O7ii—O2—Nb_m1(1) | 98.4 (2) | O5—Ti_m2—W_c | 68.6 (3) |
Oh—O2—Ohii | 88.7 (4) | O5—Ti_m2—W_cxi | 111.4 (3) |
Oh—O2—W1ix | 152.7 (6) | O5—Ti_m2—Mg_m2 | 0 |
Oh—O2—Nb_m1(1) | 44.0 (3) | O5xi—Ti_m2—Ba | 111.4 (3) |
Ohii—O2—W1ix | 69.7 (4) | O5xi—Ti_m2—Baxi | 68.6 (3) |
Ohii—O2—Nb_m1(1) | 44.7 (3) | O5xi—Ti_m2—W_c | 111.4 (3) |
W1ix—O2—Nb_m1(1) | 112.6 (6) | O5xi—Ti_m2—W_cxi | 68.6 (3) |
Na_aiii—O3—K_b | 170.4 (3) | O5xi—Ti_m2—Mg_m2 | 0 |
Na_aiii—O3—Ti_m1(1) | 75.5 (3) | Ba—Ti_m2—Baxi | 180.0 (5) |
Na_aiii—O3—Si1 | 77.0 (4) | Ba—Ti_m2—W_c | 0.0 (5) |
Na_aiii—O3—O2 | 113.3 (5) | Ba—Ti_m2—W_cxi | 180.0 (5) |
Na_aiii—O3—O2ii | 42.0 (3) | Ba—Ti_m2—Mg_m2 | 0 |
Na_aiii—O3—O3vi | 116.4 (3) | Baxi—Ti_m2—W_c | 180.0 (5) |
Na_aiii—O3—O4 | 104.0 (4) | Baxi—Ti_m2—W_cxi | 0.0 (5) |
Na_aiii—O3—O5 | 132.7 (7) | Baxi—Ti_m2—Mg_m2 | 0 |
Na_aiii—O3—O6 | 86.5 (5) | W_c—Ti_m2—W_cxi | 180.0 (5) |
Na_aiii—O3—O7 | 43.9 (4) | W_c—Ti_m2—Mg_m2 | 0 |
Na_aiii—O3—Oh | 55.8 (4) | W_cxi—Ti_m2—Mg_m2 | 0 |
Na_aiii—O3—Ohii | 100.9 (3) | Ti_m1(2)—Mg_m2—Ti_m1(2)xii | 180.0 (5) |
Na_aiii—O3—Ba | 80.5 (4) | Ti_m1(2)—Mg_m2—Fe_m2 | 0 |
Na_aiii—O3—W_c | 80.5 (4) | Ti_m1(2)—Mg_m2—Si2 | 62.28 (5) |
Na_aiii—O3—Nb_m1(1) | 75.5 (3) | Ti_m1(2)—Mg_m2—Si2xi | 62.28 (5) |
K_b—O3—Ti_m1(1) | 114.1 (2) | Ti_m1(2)—Mg_m2—Si2xii | 117.72 (5) |
K_b—O3—Si1 | 96.9 (6) | Ti_m1(2)—Mg_m2—Si2vi | 117.72 (5) |
K_b—O3—O2 | 75.5 (3) | Ti_m1(2)—Mg_m2—O1 | 41.5 (2) |
K_b—O3—O2ii | 145.4 (4) | Ti_m1(2)—Mg_m2—O1xi | 41.5 (2) |
K_b—O3—O3vi | 55.14 (19) | Ti_m1(2)—Mg_m2—O1xii | 138.5 (2) |
K_b—O3—O4 | 67.6 (3) | Ti_m1(2)—Mg_m2—O1vi | 138.5 (2) |
K_b—O3—O5 | 49.9 (4) | Ti_m1(2)—Mg_m2—O5 | 90 |
K_b—O3—O6 | 92.2 (5) | Ti_m1(2)—Mg_m2—O5xi | 90 |
K_b—O3—O7 | 127.9 (6) | Ti_m1(2)—Mg_m2—Ba | 90 |
K_b—O3—Oh | 130.8 (5) | Ti_m1(2)—Mg_m2—Baxi | 90 |
K_b—O3—Ohii | 86.9 (3) | Ti_m1(2)—Mg_m2—W_c | 90 |
K_b—O3—Ba | 96.2 (3) | Ti_m1(2)—Mg_m2—W_cxi | 90 |
K_b—O3—W_c | 96.2 (3) | Ti_m1(2)—Mg_m2—Ti_m2 | 0 |
K_b—O3—Nb_m1(1) | 114.1 (2) | Ti_m1(2)xii—Mg_m2—Fe_m2 | 0 |
Ti_m1(1)—O3—Si1 | 121.2 (5) | Ti_m1(2)xii—Mg_m2—Si2 | 117.72 (5) |
Ti_m1(1)—O3—O2 | 45.1 (2) | Ti_m1(2)xii—Mg_m2—Si2xi | 117.72 (5) |
Ti_m1(1)—O3—O2ii | 44.4 (2) | Ti_m1(2)xii—Mg_m2—Si2xii | 62.28 (5) |
Ti_m1(1)—O3—O3vi | 153.2 (6) | Ti_m1(2)xii—Mg_m2—Si2vi | 62.28 (5) |
Ti_m1(1)—O3—O4 | 152.2 (8) | Ti_m1(2)xii—Mg_m2—O1 | 138.5 (2) |
Ti_m1(1)—O3—O5 | 92.3 (4) | Ti_m1(2)xii—Mg_m2—O1xi | 138.5 (2) |
Ti_m1(1)—O3—O6 | 95.1 (4) | Ti_m1(2)xii—Mg_m2—O1xii | 41.5 (2) |
Ti_m1(1)—O3—O7 | 111.5 (3) | Ti_m1(2)xii—Mg_m2—O1vi | 41.5 (2) |
Ti_m1(1)—O3—Oh | 45.1 (3) | Ti_m1(2)xii—Mg_m2—O5 | 90 |
Ti_m1(1)—O3—Ohii | 43.1 (3) | Ti_m1(2)xii—Mg_m2—O5xi | 90 |
Ti_m1(1)—O3—Ba | 107.0 (7) | Ti_m1(2)xii—Mg_m2—Ba | 90 |
Ti_m1(1)—O3—W_c | 107.0 (7) | Ti_m1(2)xii—Mg_m2—Baxi | 90 |
Ti_m1(1)—O3—Nb_m1(1) | 0.0 (5) | Ti_m1(2)xii—Mg_m2—W_c | 90 |
Si1—O3—O2 | 152.2 (7) | Ti_m1(2)xii—Mg_m2—W_cxi | 90 |
Si1—O3—O2ii | 81.9 (4) | Ti_m1(2)xii—Mg_m2—Ti_m2 | 0 |
Si1—O3—O3vi | 85.4 (4) | Fe_m2—Mg_m2—Si2 | 0 |
Si1—O3—O4 | 35.8 (3) | Fe_m2—Mg_m2—Si2xi | 0 |
Si1—O3—O5 | 142.2 (5) | Fe_m2—Mg_m2—Si2xii | 0 |
Si1—O3—O6 | 32.4 (3) | Fe_m2—Mg_m2—Si2vi | 0 |
Si1—O3—O7 | 36.0 (4) | Fe_m2—Mg_m2—O1 | 0 |
Si1—O3—Oh | 132.3 (4) | Fe_m2—Mg_m2—O1xi | 0 |
Si1—O3—Ohii | 94.7 (6) | Fe_m2—Mg_m2—O1xii | 0 |
Si1—O3—Ba | 118.2 (3) | Fe_m2—Mg_m2—O1vi | 0 |
Si1—O3—W_c | 118.2 (3) | Fe_m2—Mg_m2—O5 | 0 |
Si1—O3—Nb_m1(1) | 121.2 (5) | Fe_m2—Mg_m2—O5xi | 0 |
O2—O3—O2ii | 89.5 (3) | Fe_m2—Mg_m2—Ba | 0 |
O2—O3—O3vi | 110.1 (3) | Fe_m2—Mg_m2—Baxi | 0 |
O2—O3—O4 | 142.5 (4) | Fe_m2—Mg_m2—W_c | 0 |
O2—O3—O5 | 48.5 (2) | Fe_m2—Mg_m2—W_cxi | 0 |
O2—O3—O6 | 120.1 (4) | Fe_m2—Mg_m2—Ti_m2 | 0 |
O2—O3—O7 | 155.8 (4) | Si2—Mg_m2—Si2xi | 124.57 (8) |
O2—O3—Oh | 60.5 (4) | Si2—Mg_m2—Si2xii | 180.0 (5) |
O2—O3—Ohii | 58.6 (4) | Si2—Mg_m2—Si2vi | 55.43 (8) |
O2—O3—Ba | 89.4 (5) | Si2—Mg_m2—O1 | 24.4 (4) |
O2—O3—W_c | 89.4 (5) | Si2—Mg_m2—O1xi | 102.4 (3) |
O2—O3—Nb_m1(1) | 45.1 (2) | Si2—Mg_m2—O1xii | 155.6 (4) |
O2ii—O3—O3vi | 157.1 (3) | Si2—Mg_m2—O1vi | 77.6 (3) |
O2ii—O3—O4 | 117.7 (5) | Si2—Mg_m2—O5 | 29.44 (12) |
O2ii—O3—O5 | 135.2 (5) | Si2—Mg_m2—O5xi | 150.56 (12) |
O2ii—O3—O6 | 68.3 (4) | Si2—Mg_m2—Ba | 80.24 (13) |
O2ii—O3—O7 | 67.5 (2) | Si2—Mg_m2—Baxi | 99.76 (13) |
O2ii—O3—Oh | 59.3 (4) | Si2—Mg_m2—W_c | 80.24 (13) |
O2ii—O3—Ohii | 59.0 (2) | Si2—Mg_m2—W_cxi | 99.76 (13) |
O2ii—O3—Ba | 115.0 (5) | Si2—Mg_m2—Ti_m2 | 0 |
O2ii—O3—W_c | 115.0 (5) | Si2xi—Mg_m2—Si2xii | 55.43 (8) |
O2ii—O3—Nb_m1(1) | 44.4 (2) | Si2xi—Mg_m2—Si2vi | 180.0 (5) |
O3vi—O3—O4 | 52.2 (4) | Si2xi—Mg_m2—O1 | 102.4 (3) |
O3vi—O3—O5 | 61.8 (2) | Si2xi—Mg_m2—O1xi | 24.4 (4) |
O3vi—O3—O6 | 109.0 (5) | Si2xi—Mg_m2—O1xii | 77.6 (3) |
O3vi—O3—O7 | 91.2 (3) | Si2xi—Mg_m2—O1vi | 155.6 (4) |
O3vi—O3—Oh | 119.6 (6) | Si2xi—Mg_m2—O5 | 150.56 (12) |
O3vi—O3—Ohii | 141.6 (4) | Si2xi—Mg_m2—O5xi | 29.44 (12) |
O3vi—O3—Ba | 55.7 (3) | Si2xi—Mg_m2—Ba | 99.76 (13) |
O3vi—O3—W_c | 55.7 (3) | Si2xi—Mg_m2—Baxi | 80.24 (13) |
O3vi—O3—Nb_m1(1) | 153.2 (6) | Si2xi—Mg_m2—W_c | 99.76 (13) |
O4—O3—O5 | 106.7 (3) | Si2xi—Mg_m2—W_cxi | 80.24 (13) |
O4—O3—O6 | 57.3 (5) | Si2xi—Mg_m2—Ti_m2 | 0 |
O4—O3—O7 | 60.4 (4) | Si2xii—Mg_m2—Si2vi | 124.57 (8) |
O4—O3—Oh | 154.9 (4) | Si2xii—Mg_m2—O1 | 155.6 (4) |
O4—O3—Ohii | 112.0 (7) | Si2xii—Mg_m2—O1xi | 77.6 (3) |
O4—O3—Ba | 100.2 (4) | Si2xii—Mg_m2—O1xii | 24.4 (4) |
O4—O3—W_c | 100.2 (4) | Si2xii—Mg_m2—O1vi | 102.4 (3) |
O4—O3—Nb_m1(1) | 152.2 (8) | Si2xii—Mg_m2—O5 | 150.56 (12) |
O5—O3—O6 | 140.6 (5) | Si2xii—Mg_m2—O5xi | 29.44 (12) |
O5—O3—O7 | 148.9 (4) | Si2xii—Mg_m2—Ba | 99.76 (13) |
O5—O3—Oh | 83.1 (5) | Si2xii—Mg_m2—Baxi | 80.24 (13) |
O5—O3—Ohii | 99.9 (3) | Si2xii—Mg_m2—W_c | 99.76 (13) |
O5—O3—Ba | 59.4 (3) | Si2xii—Mg_m2—W_cxi | 80.24 (13) |
O5—O3—W_c | 59.4 (3) | Si2xii—Mg_m2—Ti_m2 | 0 |
O5—O3—Nb_m1(1) | 92.3 (4) | Si2vi—Mg_m2—O1 | 77.6 (3) |
O6—O3—O7 | 59.6 (4) | Si2vi—Mg_m2—O1xi | 155.6 (4) |
O6—O3—Oh | 127.6 (3) | Si2vi—Mg_m2—O1xii | 102.4 (3) |
O6—O3—Ohii | 62.4 (4) | Si2vi—Mg_m2—O1vi | 24.4 (4) |
O6—O3—Ba | 150.4 (3) | Si2vi—Mg_m2—O5 | 29.44 (12) |
O6—O3—W_c | 150.4 (3) | Si2vi—Mg_m2—O5xi | 150.56 (12) |
O6—O3—Nb_m1(1) | 95.1 (4) | Si2vi—Mg_m2—Ba | 80.24 (13) |
O7—O3—Oh | 99.3 (4) | Si2vi—Mg_m2—Baxi | 99.76 (13) |
O7—O3—Ohii | 111.2 (5) | Si2vi—Mg_m2—W_c | 80.24 (13) |
O7—O3—Ba | 93.5 (4) | Si2vi—Mg_m2—W_cxi | 99.76 (13) |
O7—O3—W_c | 93.5 (4) | Si2vi—Mg_m2—Ti_m2 | 0 |
O7—O3—Nb_m1(1) | 111.5 (3) | O1—Mg_m2—O1xi | 83.1 (3) |
Oh—O3—Ohii | 88.2 (4) | O1—Mg_m2—O1xii | 180.0 (5) |
Oh—O3—Ba | 64.4 (4) | O1—Mg_m2—O1vi | 96.9 (3) |
Oh—O3—W_c | 64.4 (4) | O1—Mg_m2—O5 | 53.8 (4) |
Oh—O3—Nb_m1(1) | 45.1 (3) | O1—Mg_m2—O5xi | 126.2 (4) |
Ohii—O3—Ba | 146.1 (6) | O1—Mg_m2—Ba | 93.7 (4) |
Ohii—O3—W_c | 146.1 (6) | O1—Mg_m2—Baxi | 86.3 (4) |
Ohii—O3—Nb_m1(1) | 43.1 (3) | O1—Mg_m2—W_c | 93.7 (4) |
Ba—O3—W_c | 0.0 (5) | O1—Mg_m2—W_cxi | 86.3 (4) |
Ba—O3—Nb_m1(1) | 107.0 (7) | O1—Mg_m2—Ti_m2 | 0 |
W_c—O3—Nb_m1(1) | 107.0 (7) | O1xi—Mg_m2—O1xii | 96.9 (3) |
K_b—O4—K_bvii | 103.0 (5) | O1xi—Mg_m2—O1vi | 180.0 (5) |
K_b—O4—Si1 | 88.0 (5) | O1xi—Mg_m2—O5 | 126.2 (4) |
K_b—O4—Si1vi | 88.0 (5) | O1xi—Mg_m2—O5xi | 53.8 (4) |
K_b—O4—O3 | 59.2 (3) | O1xi—Mg_m2—Ba | 86.3 (4) |
K_b—O4—O3vi | 59.2 (3) | O1xi—Mg_m2—Baxi | 93.7 (4) |
K_b—O4—O5iv | 164.8 (9) | O1xi—Mg_m2—W_c | 86.3 (4) |
K_b—O4—O6 | 89.7 (3) | O1xi—Mg_m2—W_cxi | 93.7 (4) |
K_b—O4—O6vi | 89.7 (3) | O1xi—Mg_m2—Ti_m2 | 0 |
K_b—O4—O7 | 118.7 (6) | O1xii—Mg_m2—O1vi | 83.1 (3) |
K_b—O4—O7vi | 118.7 (6) | O1xii—Mg_m2—O5 | 126.2 (4) |
K_bvii—O4—Si1 | 114.2 (8) | O1xii—Mg_m2—O5xi | 53.8 (4) |
K_bvii—O4—Si1vi | 114.2 (8) | O1xii—Mg_m2—Ba | 86.3 (4) |
K_bvii—O4—O3 | 134.5 (4) | O1xii—Mg_m2—Baxi | 93.7 (4) |
K_bvii—O4—O3vi | 134.5 (4) | O1xii—Mg_m2—W_c | 86.3 (4) |
K_bvii—O4—O5iv | 92.2 (6) | O1xii—Mg_m2—W_cxi | 93.7 (4) |
K_bvii—O4—O6 | 78.3 (6) | O1xii—Mg_m2—Ti_m2 | 0 |
K_bvii—O4—O6vi | 78.3 (6) | O1vi—Mg_m2—O5 | 53.8 (4) |
K_bvii—O4—O7 | 118.9 (6) | O1vi—Mg_m2—O5xi | 126.2 (4) |
K_bvii—O4—O7vi | 118.9 (6) | O1vi—Mg_m2—Ba | 93.7 (4) |
Si1—O4—Si1vi | 131.2 (15) | O1vi—Mg_m2—Baxi | 86.3 (4) |
Si1—O4—O3 | 34.5 (5) | O1vi—Mg_m2—W_c | 93.7 (4) |
Si1—O4—O3vi | 107.0 (11) | O1vi—Mg_m2—W_cxi | 86.3 (4) |
Si1—O4—O5iv | 85.7 (3) | O1vi—Mg_m2—Ti_m2 | 0 |
Si1—O4—O6 | 36.5 (5) | O5—Mg_m2—O5xi | 180.0 (5) |
Si1—O4—O6vi | 167.6 (13) | O5—Mg_m2—Ba | 68.6 (3) |
Si1—O4—O7 | 35.9 (3) | O5—Mg_m2—Baxi | 111.4 (3) |
Si1—O4—O7vi | 110.1 (9) | O5—Mg_m2—W_c | 68.6 (3) |
Si1vi—O4—O3 | 107.0 (11) | O5—Mg_m2—W_cxi | 111.4 (3) |
Si1vi—O4—O3vi | 34.5 (5) | O5—Mg_m2—Ti_m2 | 0 |
Si1vi—O4—O5iv | 85.7 (3) | O5xi—Mg_m2—Ba | 111.4 (3) |
Si1vi—O4—O6 | 167.6 (13) | O5xi—Mg_m2—Baxi | 68.6 (3) |
Si1vi—O4—O6vi | 36.5 (5) | O5xi—Mg_m2—W_c | 111.4 (3) |
Si1vi—O4—O7 | 110.1 (9) | O5xi—Mg_m2—W_cxi | 68.6 (3) |
Si1vi—O4—O7vi | 35.9 (3) | O5xi—Mg_m2—Ti_m2 | 0 |
O3—O4—O3vi | 75.7 (7) | Ba—Mg_m2—Baxi | 180.0 (5) |
O3—O4—O5iv | 109.6 (5) | Ba—Mg_m2—W_c | 0.0 (5) |
O3—O4—O6 | 61.6 (5) | Ba—Mg_m2—W_cxi | 180.0 (5) |
O3—O4—O6vi | 136.3 (8) | Ba—Mg_m2—Ti_m2 | 0 |
O3—O4—O7 | 59.4 (4) | Baxi—Mg_m2—W_c | 180.0 (5) |
O3—O4—O7vi | 105.6 (9) | Baxi—Mg_m2—W_cxi | 0.0 (5) |
O3vi—O4—O5iv | 109.6 (5) | Baxi—Mg_m2—Ti_m2 | 0 |
O3vi—O4—O6 | 136.3 (8) | W_c—Mg_m2—W_cxi | 180.0 (5) |
O3vi—O4—O6vi | 61.6 (5) | W_c—Mg_m2—Ti_m2 | 0 |
O3vi—O4—O7 | 105.6 (9) | W_cxi—Mg_m2—Ti_m2 | 0 |
O3vi—O4—O7vi | 59.4 (4) | | |
Symmetry codes: (i) −x+1, y, −z; (ii) −x+1/2, −y+1/2, −z+1; (iii) −x+1/2, −y+1/2, −z; (iv) x, y, z−1; (v) x+1/2, −y+1/2, z; (vi) x, −y, z; (vii) −x+1, y, −z+1; (viii) −x+1, −y, −z+1; (ix) x, y, z+1; (x) x−1/2, −y+1/2, z; (xi) −x, y, −z+1; (xii) −x, −y, −z+1; (xiii) x, −y, z+1; (xiv) −x, −y, −z; (xv) −x, y, −z. |
Crystal data top
Ba0.7Fe0.5K2.1Mg0.05Na2Nb0.1O33Si8Ti4 | Z = 2 |
Mr = 1206.8 | F(000) = 1167 |
Monoclinic, C2/m | Dx = 3.202 Mg m−3 |
Hall symbol: -C 2y | Synchrotron radiation, λ = 0.414 Å |
a = 13.862 (12) Å | Cell parameters from 2907 reflections |
b = 13.4214 (4) Å | θ = 1.8–19.0° |
c = 7.515 (3) Å | µ = 0.85 mm−1 |
β = 116.50 (6)° | T = 293 K |
V = 1251.3 (13) Å3 | Anhedral grain |
Data collection top
ESRF ID 09 diffractometer | θmax = 19.0°, θmin = 1.8° |
2907 measured reflections | h = −7→8 |
901 independent reflections | k = −20→20 |
679 reflections with I > 2σ(I) | l = −10→10 |
Rint = 0.057 | |
Refinement top
Refinement on F | 0 restraints |
R[F2 > 2σ(F2)] = 0.071 | 6 constraints |
wR(F2) = 0.130 | Weighting scheme based on measured s.u.'s w = 1/(σ2(F) + 0.0120999999F2) |
S = 0.97 | (Δ/σ)max = 0.046 |
901 reflections | Δρmax = 0.94 e Å−3 |
71 parameters | Δρmin = −0.80 e Å−3 |
Fractional atomic coordinates and isotropic or equivalent isotropic displacement parameters (Å2) top | x | y | z | Uiso*/Ueq | Occ. (<1) |
Na_a | 0.4175 (16) | 0.2673 (6) | 0.0163 (12) | 0.033 (10) | 0.5 |
K_b | 0.4272 (6) | 0 | 0.7147 (4) | 0.020 (4) | |
Ti_m1(1) | 0.25 | 0.25 | 0.5 | 0.0119 (5)* | 0.95 |
Ti_m1(2) | 0 | 0.22129 (14) | 0.5 | 0.0101 (5)* | |
Fe_m2 | 0 | 0 | 0.5 | 0.0243 (11)* | 0.5 |
Si1 | 0.3247 (4) | 0.11052 (13) | 0.2605 (3) | 0.0061 (5)* | |
Si2 | 0.2108 (4) | 0.10950 (13) | 0.8108 (3) | 0.0060 (5)* | |
O1 | 0.0818 (10) | 0.1099 (3) | 0.6767 (8) | 0.0089 (11)* | |
O2 | 0.2731 (10) | 0.1920 (4) | 0.7542 (7) | 0.0074 (11)* | |
O3 | 0.2741 (10) | 0.1187 (3) | 0.4156 (8) | 0.0083 (11)* | |
O4 | 0.3816 (16) | 0 | 0.2792 (11) | 0.0121 (16)* | |
O5 | 0.2601 (14) | 0 | 0.7934 (10) | 0.0070 (14)* | |
O6 | 0.4198 (11) | 0.1858 (4) | 0.2949 (8) | 0.0159 (13)* | |
O7 | 0.2269 (11) | 0.1225 (4) | 0.0364 (8) | 0.0095 (11)* | |
Oh | 0.0990 (10) | 0.2161 (3) | 0.3885 (7) | 0.0085 (11)* | |
Ba | 0.0900 (3) | 0 | 0.3412 (2) | 0.0127 (5)* | 0.35 |
W1 | 0.5 | 0.1445 (7) | 0 | 0.037 (13) | |
W2 | 0 | 0.1119 (8) | 0 | 0.059 (19) | |
W_c | 0.0900 (3) | 0 | 0.3412 (2) | 0.0127 (5)* | 0.65 |
Nb_m1(1) | 0.25 | 0.25 | 0.5 | 0.0119 (5)* | 0.05 |
Ti_m2 | 0 | 0 | 0.5 | 0.0243 (11)* | 0.1 |
Mg_m2 | 0 | 0 | 0.5 | 0.0243 (11)* | 0.05 |
Atomic displacement parameters (Å2) top | U11 | U22 | U33 | U12 | U13 | U23 |
Na_a | 0.05 (2) | 0.019 (3) | 0.028 (4) | −0.007 (5) | 0.016 (6) | −0.001 (3) |
K_b | 0.010 (8) | 0.0343 (14) | 0.0127 (11) | 0 | 0.002 (2) | 0 |
W1 | 0.06 (3) | 0.022 (4) | 0.017 (4) | 0 | 0.008 (7) | 0 |
W2 | 0.10 (4) | 0.037 (6) | 0.025 (6) | 0 | 0.018 (10) | 0 |
Geometric parameters (Å, º) top
Na_a—Na_ai | 2.41 (3) | Ti_m1(2)—Ohxii | 1.902 (13) |
Na_a—K_bii | 4.278 (10) | Ti_m1(2)—Ba | 3.624 (3) |
Na_a—K_biii | 4.208 (10) | Ti_m1(2)—Baxii | 3.624 (3) |
Na_a—Ti_m1(1)ii | 3.530 (10) | Ti_m1(2)—Ti_m2 | 2.9700 (18) |
Na_a—Ti_m1(2)iv | 3.292 (10) | Ti_m1(2)—Mg_m2 | 2.9700 (18) |
Na_a—Si2iv | 3.106 (19) | Fe_m2—O1 | 1.971 (6) |
Na_a—O2ii | 2.321 (14) | Fe_m2—O1xii | 1.971 (6) |
Na_a—O6 | 2.349 (15) | Fe_m2—O1xiv | 1.971 (6) |
Na_a—O7v | 2.38 (2) | Fe_m2—O1x | 1.971 (6) |
Na_a—Bavi | 4.028 (10) | Fe_m2—Ba | 2.076 (5) |
Na_a—Bavii | 4.091 (10) | Fe_m2—Baxii | 2.076 (5) |
Na_a—W1 | 2.040 (16) | Fe_m2—W_c | 2.076 (5) |
Na_a—W2v | 2.019 (17) | Fe_m2—W_cxii | 2.076 (5) |
Na_a—Nb_m1(1)ii | 3.530 (10) | Fe_m2—Ti_m2 | 0 |
K_b—K_biii | 4.505 (10) | Fe_m2—Mg_m2 | 0 |
K_b—K_bviii | 3.839 (6) | Si1—O3 | 1.611 (13) |
K_b—Si1 | 3.398 (4) | Si1—O4 | 1.657 (10) |
K_b—Si1iii | 3.673 (11) | Si1—O6 | 1.589 (13) |
K_b—Si1ix | 3.673 (11) | Si1—O7 | 1.632 (8) |
K_b—Si1x | 3.398 (4) | Si2—O1 | 1.613 (13) |
K_b—Si2 | 3.690 (10) | Si2—O2 | 1.575 (11) |
K_b—Si2x | 3.690 (10) | Si2—O5 | 1.650 (10) |
K_b—O3 | 2.800 (9) | Si2—O7xi | 1.618 (8) |
K_b—O3x | 2.800 (9) | Si2—Ba | 3.485 (4) |
K_b—O4iii | 2.63 (2) | O1—Baxii | 2.754 (14) |
K_b—O5 | 2.63 (2) | O1—Ti_m2 | 1.971 (6) |
K_b—Ba | 4.245 (12) | O1—Mg_m2 | 1.971 (6) |
K_b—W1xi | 2.729 (7) | O2—Nb_m1(1) | 1.952 (7) |
K_b—W1ix | 2.729 (7) | O3—Ba | 2.844 (13) |
Ti_m1(1)—O2 | 1.952 (7) | O3—Nb_m1(1) | 1.951 (7) |
Ti_m1(1)—O2iv | 1.952 (7) | Oh—Nb_m1(1) | 1.930 (13) |
Ti_m1(1)—O3 | 1.951 (7) | Ba—Baxv | 4.595 (6) |
Ti_m1(1)—O3iv | 1.951 (7) | Ba—Baxii | 4.152 (7) |
Ti_m1(1)—Oh | 1.930 (13) | Ba—W2 | 2.745 (6) |
Ti_m1(1)—Ohiv | 1.930 (13) | Ba—W2xvi | 2.745 (6) |
Ti_m1(1)—Nb_m1(1) | 0 | Ba—W_c | 0 |
Ti_m1(2)—O1 | 1.985 (6) | Ba—Ti_m2 | 2.076 (5) |
Ti_m1(2)—O1xii | 1.985 (6) | Ba—Mg_m2 | 2.076 (5) |
Ti_m1(2)—O6iv | 1.907 (6) | W_c—Ti_m2 | 2.076 (5) |
Ti_m1(2)—O6xiii | 1.907 (6) | W_c—Mg_m2 | 2.076 (5) |
Ti_m1(2)—Oh | 1.902 (13) | Ti_m2—Mg_m2 | 0 |
| | | |
Na_ai—Na_a—K_bii | 71.9 (4) | O7xi—Si2—Ba | 152.4 (4) |
Na_ai—Na_a—K_biii | 75.1 (4) | Ti_m1(2)—O1—Fe_m2 | 97.3 (3) |
Na_ai—Na_a—Ti_m1(1)ii | 94.4 (5) | Ti_m1(2)—O1—Si2 | 124.3 (5) |
Na_ai—Na_a—Ti_m1(2)iv | 103.6 (5) | Ti_m1(2)—O1—Baxii | 98.5 (5) |
Na_ai—Na_a—Si2iv | 142.2 (4) | Ti_m1(2)—O1—Ti_m2 | 97.3 (3) |
Na_ai—Na_a—O2ii | 114.3 (7) | Ti_m1(2)—O1—Mg_m2 | 97.3 (3) |
Na_ai—Na_a—O6 | 117.1 (7) | Fe_m2—O1—Si2 | 124.2 (5) |
Na_ai—Na_a—O7v | 138.7 (6) | Fe_m2—O1—Baxii | 48.7 (3) |
Na_ai—Na_a—Bavi | 74.2 (4) | Fe_m2—O1—Ti_m2 | 0.0 (5) |
Na_ai—Na_a—Bavii | 71.3 (4) | Fe_m2—O1—Mg_m2 | 0.0 (5) |
Na_ai—Na_a—W1 | 53.9 (6) | Si2—O1—Baxii | 136.2 (3) |
Na_ai—Na_a—W2v | 53.4 (6) | Si2—O1—Ti_m2 | 124.2 (5) |
Na_ai—Na_a—Nb_m1(1)ii | 94.4 (5) | Si2—O1—Mg_m2 | 124.2 (5) |
K_bii—Na_a—K_biii | 53.79 (14) | Baxii—O1—Ti_m2 | 48.7 (3) |
K_bii—Na_a—Ti_m1(1)ii | 61.52 (14) | Baxii—O1—Mg_m2 | 48.7 (3) |
K_bii—Na_a—Ti_m1(2)iv | 123.1 (2) | Ti_m2—O1—Mg_m2 | 0.0 (5) |
K_bii—Na_a—Si2iv | 145.8 (6) | Na_axi—O2—Ti_m1(1) | 111.1 (6) |
K_bii—Na_a—O2ii | 53.4 (3) | Na_axi—O2—Si2 | 116.5 (4) |
K_bii—Na_a—O6 | 95.2 (3) | Na_axi—O2—Nb_m1(1) | 111.1 (6) |
K_bii—Na_a—O7v | 131.1 (5) | Ti_m1(1)—O2—Si2 | 132.4 (4) |
K_bii—Na_a—Bavi | 145.2 (6) | Ti_m1(1)—O2—Nb_m1(1) | 0.0 (5) |
K_bii—Na_a—Bavii | 106.8 (3) | Si2—O2—Nb_m1(1) | 132.4 (4) |
K_bii—Na_a—W1 | 30.67 (19) | K_b—O3—Ti_m1(1) | 115.6 (2) |
K_bii—Na_a—W2v | 119.3 (7) | K_b—O3—Si1 | 97.1 (5) |
K_bii—Na_a—Nb_m1(1)ii | 61.52 (14) | K_b—O3—Ba | 97.5 (3) |
K_biii—Na_a—Ti_m1(1)ii | 114.6 (2) | K_b—O3—Nb_m1(1) | 115.6 (2) |
K_biii—Na_a—Ti_m1(2)iv | 70.00 (16) | Ti_m1(1)—O3—Si1 | 119.3 (4) |
K_biii—Na_a—Si2iv | 121.2 (4) | Ti_m1(1)—O3—Ba | 107.5 (6) |
K_biii—Na_a—O2ii | 95.7 (3) | Ti_m1(1)—O3—Nb_m1(1) | 0.0 (5) |
K_biii—Na_a—O6 | 51.3 (3) | Si1—O3—Ba | 117.5 (3) |
K_biii—Na_a—O7v | 145.4 (7) | Si1—O3—Nb_m1(1) | 119.3 (4) |
K_biii—Na_a—Bavi | 109.4 (3) | Ba—O3—Nb_m1(1) | 107.5 (6) |
K_biii—Na_a—Bavii | 145.5 (6) | K_biii—O4—Si1 | 116.1 (7) |
K_biii—Na_a—W1 | 32.87 (19) | K_biii—O4—Si1x | 116.1 (7) |
K_biii—Na_a—W2v | 122.1 (7) | Si1—O4—Si1x | 127.1 (14) |
K_biii—Na_a—Nb_m1(1)ii | 114.6 (2) | K_b—O5—Si2 | 117.0 (6) |
Ti_m1(1)ii—Na_a—Ti_m1(2)iv | 162.0 (7) | K_b—O5—Si2x | 117.0 (6) |
Ti_m1(1)ii—Na_a—Si2iv | 106.0 (5) | Si2—O5—Si2x | 125.9 (13) |
Ti_m1(1)ii—Na_a—O2ii | 31.1 (2) | Na_a—O6—Ti_m1(2)iv | 100.8 (4) |
Ti_m1(1)ii—Na_a—O6 | 133.6 (6) | Na_a—O6—Si1 | 118.1 (5) |
Ti_m1(1)ii—Na_a—O7v | 76.4 (3) | Ti_m1(2)iv—O6—Si1 | 133.6 (7) |
Ti_m1(1)ii—Na_a—Bavi | 129.7 (2) | Na_av—O7—Si1 | 118.9 (5) |
Ti_m1(1)ii—Na_a—Bavii | 61.10 (14) | Na_av—O7—Si2ii | 100.4 (4) |
Ti_m1(1)ii—Na_a—W1 | 89.6 (3) | Si1—O7—Si2ii | 137.2 (10) |
Ti_m1(1)ii—Na_a—W2v | 95.7 (3) | Ti_m1(1)—Oh—Ti_m1(2) | 131.0 (3) |
Ti_m1(1)ii—Na_a—Nb_m1(1)ii | 0.0 (5) | Ti_m1(1)—Oh—Nb_m1(1) | 0.0 (5) |
Ti_m1(2)iv—Na_a—Si2iv | 59.7 (3) | Ti_m1(2)—Oh—Nb_m1(1) | 131.0 (3) |
Ti_m1(2)iv—Na_a—O2ii | 134.5 (8) | Na_axviii—Ba—Na_axix | 34.5 (4) |
Ti_m1(2)iv—Na_a—O6 | 34.7 (2) | Na_axviii—Ba—Na_av | 111.07 (18) |
Ti_m1(2)iv—Na_a—O7v | 90.4 (5) | Na_axviii—Ba—Na_axiii | 101.7 (2) |
Ti_m1(2)iv—Na_a—Bavi | 58.31 (14) | Na_axviii—Ba—K_b | 125.6 (3) |
Ti_m1(2)iv—Na_a—Bavii | 125.7 (2) | Na_axviii—Ba—Ti_m1(2) | 129.5 (3) |
Ti_m1(2)iv—Na_a—W1 | 100.1 (3) | Na_axviii—Ba—Ti_m1(2)xiv | 50.62 (17) |
Ti_m1(2)iv—Na_a—W2v | 95.9 (3) | Na_axviii—Ba—Fe_m2 | 90.1 (3) |
Ti_m1(2)iv—Na_a—Nb_m1(1)ii | 162.0 (7) | Na_axviii—Ba—Si2 | 145.9 (2) |
Si2iv—Na_a—O2ii | 98.6 (8) | Na_axviii—Ba—Si2x | 100.01 (13) |
Si2iv—Na_a—O6 | 70.0 (5) | Na_axviii—Ba—O1xii | 96.8 (3) |
Si2iv—Na_a—O7v | 30.8 (3) | Na_axviii—Ba—O1xiv | 44.6 (3) |
Si2iv—Na_a—Bavi | 68.25 (19) | Na_axviii—Ba—O3 | 142.3 (4) |
Si2iv—Na_a—Bavii | 91.0 (2) | Na_axviii—Ba—O3x | 85.6 (3) |
Si2iv—Na_a—W1 | 153.6 (6) | Na_axviii—Ba—Baxv | 56.18 (14) |
Si2iv—Na_a—W2v | 92.5 (4) | Na_axviii—Ba—Baxii | 90.1 (3) |
Si2iv—Na_a—Nb_m1(1)ii | 106.0 (5) | Na_axviii—Ba—W2 | 87.6 (2) |
O2ii—Na_a—O6 | 102.6 (7) | Na_axviii—Ba—W2xvi | 27.1 (3) |
O2ii—Na_a—O7v | 77.7 (6) | Na_axviii—Ba—W_c | 0 |
O2ii—Na_a—Bavi | 154.9 (4) | Na_axviii—Ba—Ti_m2 | 90.1 (3) |
O2ii—Na_a—Bavii | 90.9 (3) | Na_axviii—Ba—Mg_m2 | 90.1 (3) |
O2ii—Na_a—W1 | 83.8 (4) | Na_axix—Ba—Na_av | 99.5 (2) |
O2ii—Na_a—W2v | 126.5 (4) | Na_axix—Ba—Na_axiii | 111.07 (18) |
O2ii—Na_a—Nb_m1(1)ii | 31.1 (2) | Na_axix—Ba—K_b | 97.6 (3) |
O6—Na_a—O7v | 96.5 (8) | Na_axix—Ba—Ti_m1(2) | 158.5 (2) |
O6—Na_a—Bavi | 93.0 (3) | Na_axix—Ba—Ti_m1(2)xiv | 71.3 (2) |
O6—Na_a—Bavii | 157.9 (4) | Na_axix—Ba—Fe_m2 | 122.1 (3) |
O6—Na_a—W1 | 83.8 (4) | Na_axix—Ba—Si2 | 147.89 (19) |
O6—Na_a—W2v | 130.2 (5) | Na_axix—Ba—Si2x | 101.72 (12) |
O6—Na_a—Nb_m1(1)ii | 133.6 (6) | Na_axix—Ba—O1xii | 127.5 (3) |
O7v—Na_a—Bavi | 81.2 (3) | Na_axix—Ba—O1xiv | 77.9 (3) |
O7v—Na_a—Bavii | 69.0 (3) | Na_axix—Ba—O3 | 108.3 (4) |
O7v—Na_a—W1 | 161.1 (7) | Na_axix—Ba—O3x | 57.3 (3) |
O7v—Na_a—W2v | 87.0 (4) | Na_axix—Ba—Baxv | 54.89 (13) |
O7v—Na_a—Nb_m1(1)ii | 76.4 (3) | Na_axix—Ba—Baxii | 122.1 (3) |
Bavi—Na_a—Bavii | 68.93 (18) | Na_axix—Ba—W2 | 86.3 (2) |
Bavi—Na_a—W1 | 117.7 (7) | Na_axix—Ba—W2xvi | 26.0 (2) |
Bavi—Na_a—W2v | 38.28 (17) | Na_axix—Ba—W_c | 0 |
Bavi—Na_a—Nb_m1(1)ii | 129.7 (2) | Na_axix—Ba—Ti_m2 | 122.1 (3) |
Bavii—Na_a—W1 | 115.3 (7) | Na_axix—Ba—Mg_m2 | 122.1 (3) |
Bavii—Na_a—W2v | 36.50 (17) | Na_av—Ba—Na_axiii | 34.5 (4) |
Bavii—Na_a—Nb_m1(1)ii | 61.10 (14) | Na_av—Ba—K_b | 97.6 (3) |
W1—Na_a—W2v | 107.3 (10) | Na_av—Ba—Ti_m1(2) | 71.3 (2) |
W1—Na_a—Nb_m1(1)ii | 89.6 (3) | Na_av—Ba—Ti_m1(2)xiv | 158.5 (2) |
W2v—Na_a—Nb_m1(1)ii | 95.7 (3) | Na_av—Ba—Fe_m2 | 122.1 (3) |
Na_axi—K_b—Na_aiii | 32.9 (4) | Na_av—Ba—Si2 | 101.72 (12) |
Na_axi—K_b—Na_aix | 126.21 (18) | Na_av—Ba—Si2x | 147.89 (19) |
Na_axi—K_b—Na_axvii | 114.0 (3) | Na_av—Ba—O1xii | 77.9 (3) |
Na_axi—K_b—K_biii | 120.6 (3) | Na_av—Ba—O1xiv | 127.5 (3) |
Na_axi—K_b—K_bviii | 62.18 (12) | Na_av—Ba—O3 | 57.3 (3) |
Na_axi—K_b—Si1 | 93.92 (12) | Na_av—Ba—O3x | 108.3 (4) |
Na_axi—K_b—Si1iii | 83.4 (3) | Na_av—Ba—Baxv | 54.89 (13) |
Na_axi—K_b—Si1ix | 124.2 (3) | Na_av—Ba—Baxii | 122.1 (3) |
Na_axi—K_b—Si1x | 143.19 (16) | Na_av—Ba—W2 | 26.0 (2) |
Na_axi—K_b—Si2 | 48.8 (3) | Na_av—Ba—W2xvi | 86.3 (2) |
Na_axi—K_b—Si2x | 90.6 (3) | Na_av—Ba—W_c | 0 |
Na_axi—K_b—O3 | 75.90 (19) | Na_av—Ba—Ti_m2 | 122.1 (3) |
Na_axi—K_b—O3x | 135.3 (4) | Na_av—Ba—Mg_m2 | 122.1 (3) |
Na_axi—K_b—O4iii | 105.1 (3) | Na_axiii—Ba—K_b | 125.6 (3) |
Na_axi—K_b—O5 | 69.0 (3) | Na_axiii—Ba—Ti_m1(2) | 50.62 (17) |
Na_axi—K_b—Ba | 93.7 (3) | Na_axiii—Ba—Ti_m1(2)xiv | 129.5 (3) |
Na_axi—K_b—W1xi | 22.4 (2) | Na_axiii—Ba—Fe_m2 | 90.1 (3) |
Na_axi—K_b—W1ix | 105.5 (2) | Na_axiii—Ba—Si2 | 100.01 (13) |
Na_aiii—K_b—Na_aix | 117.0 (3) | Na_axiii—Ba—Si2x | 145.9 (2) |
Na_aiii—K_b—Na_axvii | 126.21 (18) | Na_axiii—Ba—O1xii | 44.6 (3) |
Na_aiii—K_b—K_biii | 92.7 (3) | Na_axiii—Ba—O1xiv | 96.8 (3) |
Na_aiii—K_b—K_bviii | 64.03 (13) | Na_axiii—Ba—O3 | 85.6 (3) |
Na_aiii—K_b—Si1 | 90.31 (13) | Na_axiii—Ba—O3x | 142.3 (4) |
Na_aiii—K_b—Si1iii | 50.5 (3) | Na_axiii—Ba—Baxv | 56.18 (14) |
Na_aiii—K_b—Si1ix | 93.1 (3) | Na_axiii—Ba—Baxii | 90.1 (3) |
Na_aiii—K_b—Si1x | 138.6 (2) | Na_axiii—Ba—W2 | 27.1 (3) |
Na_aiii—K_b—Si2 | 81.5 (3) | Na_axiii—Ba—W2xvi | 87.6 (2) |
Na_aiii—K_b—Si2x | 122.1 (3) | Na_axiii—Ba—W_c | 0 |
Na_aiii—K_b—O3 | 86.7 (2) | Na_axiii—Ba—Ti_m2 | 90.1 (3) |
Na_aiii—K_b—O3x | 155.91 (18) | Na_axiii—Ba—Mg_m2 | 90.1 (3) |
Na_aiii—K_b—O4iii | 72.3 (3) | K_b—Ba—Ti_m1(2) | 102.81 (7) |
Na_aiii—K_b—O5 | 101.8 (3) | K_b—Ba—Ti_m1(2)xiv | 102.81 (7) |
Na_aiii—K_b—Ba | 119.6 (3) | K_b—Ba—Fe_m2 | 112.76 (12) |
Na_aiii—K_b—W1xi | 23.9 (2) | K_b—Ba—Si2 | 55.99 (13) |
Na_aiii—K_b—W1ix | 107.3 (2) | K_b—Ba—Si2x | 55.99 (13) |
Na_aix—K_b—Na_axvii | 32.9 (4) | K_b—Ba—O1xii | 134.89 (15) |
Na_aix—K_b—K_biii | 92.7 (3) | K_b—Ba—O1xiv | 134.89 (15) |
Na_aix—K_b—K_bviii | 64.03 (13) | K_b—Ba—O3 | 40.84 (14) |
Na_aix—K_b—Si1 | 138.6 (2) | K_b—Ba—O3x | 40.84 (14) |
Na_aix—K_b—Si1iii | 93.1 (3) | K_b—Ba—Baxv | 128.87 (15) |
Na_aix—K_b—Si1ix | 50.5 (3) | K_b—Ba—Baxii | 112.76 (11) |
Na_aix—K_b—Si1x | 90.31 (13) | K_b—Ba—W2 | 121.69 (16) |
Na_aix—K_b—Si2 | 122.1 (3) | K_b—Ba—W2xvi | 121.69 (16) |
Na_aix—K_b—Si2x | 81.5 (3) | K_b—Ba—W_c | 0 |
Na_aix—K_b—O3 | 155.91 (18) | K_b—Ba—Ti_m2 | 112.76 (12) |
Na_aix—K_b—O3x | 86.7 (2) | K_b—Ba—Mg_m2 | 112.76 (12) |
Na_aix—K_b—O4iii | 72.3 (3) | Ti_m1(2)—Ba—Ti_m1(2)xiv | 110.09 (12) |
Na_aix—K_b—O5 | 101.8 (3) | Ti_m1(2)—Ba—Fe_m2 | 55.05 (6) |
Na_aix—K_b—Ba | 119.6 (3) | Ti_m1(2)—Ba—Si2 | 53.22 (8) |
Na_aix—K_b—W1xi | 107.3 (2) | Ti_m1(2)—Ba—Si2x | 95.32 (8) |
Na_aix—K_b—W1ix | 23.9 (2) | Ti_m1(2)—Ba—O1xii | 32.81 (15) |
Na_axvii—K_b—K_biii | 120.6 (3) | Ti_m1(2)—Ba—O1xiv | 92.2 (2) |
Na_axvii—K_b—K_bviii | 62.18 (12) | Ti_m1(2)—Ba—O3 | 83.5 (2) |
Na_axvii—K_b—Si1 | 143.19 (16) | Ti_m1(2)—Ba—O3x | 143.61 (15) |
Na_axvii—K_b—Si1iii | 124.2 (3) | Ti_m1(2)—Ba—Baxv | 105.80 (7) |
Na_axvii—K_b—Si1ix | 83.4 (3) | Ti_m1(2)—Ba—Baxii | 55.05 (6) |
Na_axvii—K_b—Si1x | 93.92 (12) | Ti_m1(2)—Ba—W2 | 77.26 (16) |
Na_axvii—K_b—Si2 | 90.6 (3) | Ti_m1(2)—Ba—W2xvi | 132.56 (18) |
Na_axvii—K_b—Si2x | 48.8 (3) | Ti_m1(2)—Ba—W_c | 0 |
Na_axvii—K_b—O3 | 135.3 (4) | Ti_m1(2)—Ba—Ti_m2 | 55.05 (6) |
Na_axvii—K_b—O3x | 75.90 (19) | Ti_m1(2)—Ba—Mg_m2 | 55.05 (6) |
Na_axvii—K_b—O4iii | 105.1 (3) | Ti_m1(2)xiv—Ba—Fe_m2 | 55.05 (6) |
Na_axvii—K_b—O5 | 69.0 (3) | Ti_m1(2)xiv—Ba—Si2 | 95.32 (8) |
Na_axvii—K_b—Ba | 93.7 (3) | Ti_m1(2)xiv—Ba—Si2x | 53.22 (8) |
Na_axvii—K_b—W1xi | 105.5 (2) | Ti_m1(2)xiv—Ba—O1xii | 92.2 (2) |
Na_axvii—K_b—W1ix | 22.4 (2) | Ti_m1(2)xiv—Ba—O1xiv | 32.81 (15) |
K_biii—K_b—K_bviii | 128.3 (2) | Ti_m1(2)xiv—Ba—O3 | 143.61 (15) |
K_biii—K_b—Si1 | 53.17 (15) | Ti_m1(2)xiv—Ba—O3x | 83.5 (2) |
K_biii—K_b—Si1iii | 47.77 (12) | Ti_m1(2)xiv—Ba—Baxv | 105.80 (7) |
K_biii—K_b—Si1ix | 47.77 (12) | Ti_m1(2)xiv—Ba—Baxii | 55.05 (6) |
K_biii—K_b—Si1x | 53.17 (15) | Ti_m1(2)xiv—Ba—W2 | 132.56 (18) |
K_biii—K_b—Si2 | 143.44 (9) | Ti_m1(2)xiv—Ba—W2xvi | 77.26 (16) |
K_biii—K_b—Si2x | 143.44 (9) | Ti_m1(2)xiv—Ba—W_c | 0 |
K_biii—K_b—O3 | 81.2 (3) | Ti_m1(2)xiv—Ba—Ti_m2 | 55.05 (6) |
K_biii—K_b—O3x | 81.2 (3) | Ti_m1(2)xiv—Ba—Mg_m2 | 55.05 (6) |
K_biii—K_b—O4iii | 40.8 (2) | Fe_m2—Ba—Si2 | 63.79 (12) |
K_biii—K_b—O5 | 151.7 (2) | Fe_m2—Ba—Si2x | 63.79 (12) |
K_biii—K_b—Ba | 103.84 (12) | Fe_m2—Ba—O1xii | 45.53 (19) |
K_biii—K_b—W1xi | 115.9 (2) | Fe_m2—Ba—O1xiv | 45.53 (19) |
K_biii—K_b—W1ix | 115.9 (2) | Fe_m2—Ba—O3 | 127.13 (19) |
K_bviii—K_b—Si1 | 153.90 (5) | Fe_m2—Ba—O3x | 127.13 (19) |
K_bviii—K_b—Si1iii | 85.97 (17) | Fe_m2—Ba—Baxv | 118.37 (16) |
K_bviii—K_b—Si1ix | 85.97 (17) | Fe_m2—Ba—Baxii | 0.0 (5) |
K_bviii—K_b—Si1x | 153.90 (5) | Fe_m2—Ba—W2 | 113.44 (17) |
K_bviii—K_b—Si2 | 81.34 (17) | Fe_m2—Ba—W2xvi | 113.44 (17) |
K_bviii—K_b—Si2x | 81.34 (17) | Fe_m2—Ba—W_c | 0 |
K_bviii—K_b—O3 | 136.8 (2) | Fe_m2—Ba—Ti_m2 | 0.0 (5) |
K_bviii—K_b—O3x | 136.8 (2) | Fe_m2—Ba—Mg_m2 | 0.0 (5) |
K_bviii—K_b—O4iii | 87.6 (3) | Si2—Ba—Si2x | 49.89 (5) |
K_bviii—K_b—O5 | 80.0 (2) | Si2—Ba—O1xii | 80.67 (17) |
K_bviii—K_b—Ba | 127.8 (2) | Si2—Ba—O1xiv | 106.8 (2) |
K_bviii—K_b—W1xi | 45.30 (14) | Si2—Ba—O3 | 65.24 (18) |
K_bviii—K_b—W1ix | 45.30 (14) | Si2—Ba—O3x | 93.08 (16) |
Si1—K_b—Si1iii | 80.62 (17) | Si2—Ba—Baxv | 155.04 (3) |
Si1—K_b—Si1ix | 100.9 (2) | Si2—Ba—Baxii | 63.79 (13) |
Si1—K_b—Si1x | 51.77 (6) | Si2—Ba—W2 | 121.88 (19) |
Si1—K_b—Si2 | 90.61 (16) | Si2—Ba—W2xvi | 171.75 (19) |
Si1—K_b—Si2x | 111.0 (2) | Si2—Ba—W_c | 0 |
Si1—K_b—O3 | 28.1 (3) | Si2—Ba—Ti_m2 | 63.79 (12) |
Si1—K_b—O3x | 67.32 (15) | Si2—Ba—Mg_m2 | 63.79 (12) |
Si1—K_b—O4iii | 89.1 (2) | Si2x—Ba—O1xii | 106.8 (2) |
Si1—K_b—O5 | 102.1 (2) | Si2x—Ba—O1xiv | 80.67 (17) |
Si1—K_b—Ba | 59.48 (14) | Si2x—Ba—O3 | 93.08 (16) |
Si1—K_b—W1xi | 108.75 (14) | Si2x—Ba—O3x | 65.24 (18) |
Si1—K_b—W1ix | 160.39 (16) | Si2x—Ba—Baxv | 155.04 (3) |
Si1iii—K_b—Si1ix | 47.64 (12) | Si2x—Ba—Baxii | 63.79 (13) |
Si1iii—K_b—Si1x | 100.9 (2) | Si2x—Ba—W2 | 171.75 (19) |
Si1iii—K_b—Si2 | 130.83 (8) | Si2x—Ba—W2xvi | 121.88 (19) |
Si1iii—K_b—Si2x | 167.31 (10) | Si2x—Ba—W_c | 0 |
Si1iii—K_b—O3 | 99.7 (3) | Si2x—Ba—Ti_m2 | 63.79 (12) |
Si1iii—K_b—O3x | 128.9 (3) | Si2x—Ba—Mg_m2 | 63.79 (12) |
Si1iii—K_b—O4iii | 23.90 (7) | O1xii—Ba—O1xiv | 64.8 (3) |
Si1iii—K_b—O5 | 152.36 (11) | O1xii—Ba—O3 | 113.0 (3) |
Si1iii—K_b—Ba | 139.76 (10) | O1xii—Ba—O3x | 172.1 (2) |
Si1iii—K_b—W1xi | 70.34 (14) | O1xii—Ba—Baxv | 85.30 (15) |
Si1iii—K_b—W1ix | 103.7 (2) | O1xii—Ba—Baxii | 45.53 (18) |
Si1ix—K_b—Si1x | 80.62 (17) | O1xii—Ba—W2 | 68.79 (18) |
Si1ix—K_b—Si2 | 167.31 (10) | O1xii—Ba—W2xvi | 103.0 (2) |
Si1ix—K_b—Si2x | 130.83 (8) | O1xii—Ba—W_c | 0 |
Si1ix—K_b—O3 | 128.9 (3) | O1xii—Ba—Ti_m2 | 45.53 (19) |
Si1ix—K_b—O3x | 99.7 (3) | O1xii—Ba—Mg_m2 | 45.53 (19) |
Si1ix—K_b—O4iii | 23.90 (7) | O1xiv—Ba—O3 | 172.1 (2) |
Si1ix—K_b—O5 | 152.36 (11) | O1xiv—Ba—O3x | 113.0 (3) |
Si1ix—K_b—Ba | 139.76 (10) | O1xiv—Ba—Baxv | 85.30 (15) |
Si1ix—K_b—W1xi | 103.7 (2) | O1xiv—Ba—Baxii | 45.53 (18) |
Si1ix—K_b—W1ix | 70.34 (14) | O1xiv—Ba—W2 | 103.0 (2) |
Si1x—K_b—Si2 | 111.0 (2) | O1xiv—Ba—W2xvi | 68.79 (18) |
Si1x—K_b—Si2x | 90.61 (16) | O1xiv—Ba—W_c | 0 |
Si1x—K_b—O3 | 67.32 (15) | O1xiv—Ba—Ti_m2 | 45.53 (19) |
Si1x—K_b—O3x | 28.1 (3) | O1xiv—Ba—Mg_m2 | 45.53 (19) |
Si1x—K_b—O4iii | 89.1 (2) | O3—Ba—O3x | 68.2 (3) |
Si1x—K_b—O5 | 102.1 (2) | O3—Ba—Baxv | 102.25 (16) |
Si1x—K_b—Ba | 59.48 (14) | O3—Ba—Baxii | 127.13 (19) |
Si1x—K_b—W1xi | 160.39 (16) | O3—Ba—W2 | 82.59 (18) |
Si1x—K_b—W1ix | 108.75 (14) | O3—Ba—W2xvi | 119.0 (2) |
Si2—K_b—Si2x | 46.95 (12) | O3—Ba—W_c | 0 |
Si2—K_b—O3 | 62.5 (3) | O3—Ba—Ti_m2 | 127.13 (19) |
Si2—K_b—O3x | 89.6 (3) | O3—Ba—Mg_m2 | 127.13 (19) |
Si2—K_b—O4iii | 153.84 (11) | O3x—Ba—Baxv | 102.25 (16) |
Si2—K_b—O5 | 23.48 (7) | O3x—Ba—Baxii | 127.13 (19) |
Si2—K_b—Ba | 51.52 (12) | O3x—Ba—W2 | 119.0 (2) |
Si2—K_b—W1xi | 67.11 (15) | O3x—Ba—W2xvi | 82.59 (18) |
Si2—K_b—W1ix | 100.2 (2) | O3x—Ba—W_c | 0 |
Si2x—K_b—O3 | 89.6 (3) | O3x—Ba—Ti_m2 | 127.13 (19) |
Si2x—K_b—O3x | 62.5 (3) | O3x—Ba—Mg_m2 | 127.13 (19) |
Si2x—K_b—O4iii | 153.84 (11) | Baxv—Ba—Baxii | 118.37 (14) |
Si2x—K_b—O5 | 23.48 (7) | Baxv—Ba—W2 | 33.17 (18) |
Si2x—K_b—Ba | 51.52 (12) | Baxv—Ba—W2xvi | 33.17 (18) |
Si2x—K_b—W1xi | 100.2 (2) | Baxv—Ba—W_c | 0 |
Si2x—K_b—W1ix | 67.11 (15) | Baxv—Ba—Ti_m2 | 118.37 (16) |
O3—K_b—O3x | 69.4 (2) | Baxv—Ba—Mg_m2 | 118.37 (16) |
O3—K_b—O4iii | 114.3 (4) | Baxii—Ba—W2 | 113.44 (15) |
O3—K_b—O5 | 75.7 (4) | Baxii—Ba—W2xvi | 113.44 (15) |
O3—K_b—Ba | 41.6 (3) | Baxii—Ba—W_c | 0 |
O3—K_b—W1xi | 96.22 (18) | Baxii—Ba—Ti_m2 | 0.0 (5) |
O3—K_b—W1ix | 156.5 (4) | Baxii—Ba—Mg_m2 | 0.0 (5) |
O3x—K_b—O4iii | 114.3 (4) | W2—Ba—W2xvi | 66.3 (3) |
O3x—K_b—O5 | 75.7 (4) | W2—Ba—W_c | 0 |
O3x—K_b—Ba | 41.6 (3) | W2—Ba—Ti_m2 | 113.44 (17) |
O3x—K_b—W1xi | 156.5 (4) | W2—Ba—Mg_m2 | 113.44 (17) |
O3x—K_b—W1ix | 96.22 (18) | W2xvi—Ba—W_c | 0 |
O4iii—K_b—O5 | 167.5 (3) | W2xvi—Ba—Ti_m2 | 113.44 (17) |
O4iii—K_b—Ba | 144.6 (2) | W2xvi—Ba—Mg_m2 | 113.44 (17) |
O4iii—K_b—W1xi | 88.3 (2) | W_c—Ba—Ti_m2 | 0 |
O4iii—K_b—W1ix | 88.3 (2) | W_c—Ba—Mg_m2 | 0 |
O5—K_b—Ba | 47.9 (2) | Ti_m2—Ba—Mg_m2 | 0.0 (5) |
O5—K_b—W1xi | 83.0 (2) | Na_a—W1—Na_ai | 72.3 (8) |
O5—K_b—W1ix | 83.0 (2) | Na_a—W1—K_bii | 126.9 (4) |
Ba—K_b—W1xi | 115.6 (2) | Na_a—W1—K_biii | 123.2 (4) |
Ba—K_b—W1ix | 115.6 (2) | Na_ai—W1—K_bii | 123.2 (4) |
W1xi—K_b—W1ix | 90.6 (2) | Na_ai—W1—K_biii | 126.9 (4) |
Na_axi—Ti_m1(1)—Na_av | 180.0 (5) | K_bii—W1—K_biii | 89.4 (3) |
Na_axi—Ti_m1(1)—O2 | 37.8 (4) | Na_av—W2—Na_axiii | 73.2 (8) |
Na_axi—Ti_m1(1)—O2iv | 142.2 (4) | Na_av—W2—Ba | 117.5 (3) |
Na_axi—Ti_m1(1)—O3 | 107.0 (2) | Na_av—W2—Baxv | 114.6 (3) |
Na_axi—Ti_m1(1)—O3iv | 73.0 (2) | Na_axiii—W2—Ba | 114.6 (3) |
Na_axi—Ti_m1(1)—Oh | 123.1 (4) | Na_axiii—W2—Baxv | 117.5 (3) |
Na_axi—Ti_m1(1)—Ohiv | 56.9 (4) | Ba—W2—Baxv | 113.7 (4) |
Na_axi—Ti_m1(1)—Nb_m1(1) | 0 | Fe_m2—W_c—Ba | 0 |
Na_av—Ti_m1(1)—O2 | 142.2 (4) | Fe_m2—W_c—Ti_m2 | 0.0 (5) |
Na_av—Ti_m1(1)—O2iv | 37.8 (4) | Fe_m2—W_c—Mg_m2 | 0.0 (5) |
Na_av—Ti_m1(1)—O3 | 73.0 (2) | Ba—W_c—Ti_m2 | 0 |
Na_av—Ti_m1(1)—O3iv | 107.0 (2) | Ba—W_c—Mg_m2 | 0 |
Na_av—Ti_m1(1)—Oh | 56.9 (4) | Ti_m2—W_c—Mg_m2 | 0.0 (5) |
Na_av—Ti_m1(1)—Ohiv | 123.1 (4) | Na_axi—Nb_m1(1)—Na_av | 180.0 (5) |
Na_av—Ti_m1(1)—Nb_m1(1) | 0 | Na_axi—Nb_m1(1)—Ti_m1(1) | 0 |
O2—Ti_m1(1)—O2iv | 180.0 (5) | Na_axi—Nb_m1(1)—O2 | 37.8 (4) |
O2—Ti_m1(1)—O3 | 88.9 (3) | Na_axi—Nb_m1(1)—O2iv | 142.2 (4) |
O2—Ti_m1(1)—O3iv | 91.1 (3) | Na_axi—Nb_m1(1)—O3 | 107.0 (2) |
O2—Ti_m1(1)—Oh | 90.2 (4) | Na_axi—Nb_m1(1)—O3iv | 73.0 (2) |
O2—Ti_m1(1)—Ohiv | 89.8 (4) | Na_axi—Nb_m1(1)—Oh | 123.1 (4) |
O2—Ti_m1(1)—Nb_m1(1) | 0 | Na_axi—Nb_m1(1)—Ohiv | 56.9 (4) |
O2iv—Ti_m1(1)—O3 | 91.1 (3) | Na_av—Nb_m1(1)—Ti_m1(1) | 0 |
O2iv—Ti_m1(1)—O3iv | 88.9 (3) | Na_av—Nb_m1(1)—O2 | 142.2 (4) |
O2iv—Ti_m1(1)—Oh | 89.8 (4) | Na_av—Nb_m1(1)—O2iv | 37.8 (4) |
O2iv—Ti_m1(1)—Ohiv | 90.2 (4) | Na_av—Nb_m1(1)—O3 | 73.0 (2) |
O2iv—Ti_m1(1)—Nb_m1(1) | 0 | Na_av—Nb_m1(1)—O3iv | 107.0 (2) |
O3—Ti_m1(1)—O3iv | 180.0 (5) | Na_av—Nb_m1(1)—Oh | 56.9 (4) |
O3—Ti_m1(1)—Oh | 87.5 (4) | Na_av—Nb_m1(1)—Ohiv | 123.1 (4) |
O3—Ti_m1(1)—Ohiv | 92.5 (4) | Ti_m1(1)—Nb_m1(1)—O2 | 0 |
O3—Ti_m1(1)—Nb_m1(1) | 0 | Ti_m1(1)—Nb_m1(1)—O2iv | 0 |
O3iv—Ti_m1(1)—Oh | 92.5 (4) | Ti_m1(1)—Nb_m1(1)—O3 | 0 |
O3iv—Ti_m1(1)—Ohiv | 87.5 (4) | Ti_m1(1)—Nb_m1(1)—O3iv | 0 |
O3iv—Ti_m1(1)—Nb_m1(1) | 0 | Ti_m1(1)—Nb_m1(1)—Oh | 0 |
Oh—Ti_m1(1)—Ohiv | 180.0 (5) | Ti_m1(1)—Nb_m1(1)—Ohiv | 0 |
Oh—Ti_m1(1)—Nb_m1(1) | 0 | O2—Nb_m1(1)—O2iv | 180.0 (5) |
Ohiv—Ti_m1(1)—Nb_m1(1) | 0 | O2—Nb_m1(1)—O3 | 88.9 (3) |
Na_aiv—Ti_m1(2)—Na_axiii | 174.66 (19) | O2—Nb_m1(1)—O3iv | 91.1 (3) |
Na_aiv—Ti_m1(2)—O1 | 58.9 (3) | O2—Nb_m1(1)—Oh | 90.2 (4) |
Na_aiv—Ti_m1(2)—O1xii | 126.0 (3) | O2—Nb_m1(1)—Ohiv | 89.8 (4) |
Na_aiv—Ti_m1(2)—O6iv | 44.5 (3) | O2iv—Nb_m1(1)—O3 | 91.1 (3) |
Na_aiv—Ti_m1(2)—O6xiii | 130.7 (3) | O2iv—Nb_m1(1)—O3iv | 88.9 (3) |
Na_aiv—Ti_m1(2)—Oh | 121.6 (4) | O2iv—Nb_m1(1)—Oh | 89.8 (4) |
Na_aiv—Ti_m1(2)—Ohxii | 58.6 (4) | O2iv—Nb_m1(1)—Ohiv | 90.2 (4) |
Na_aiv—Ti_m1(2)—Ba | 113.6 (2) | O3—Nb_m1(1)—O3iv | 180.0 (5) |
Na_aiv—Ti_m1(2)—Baxii | 71.1 (2) | O3—Nb_m1(1)—Oh | 87.5 (4) |
Na_aiv—Ti_m1(2)—Ti_m2 | 92.67 (13) | O3—Nb_m1(1)—Ohiv | 92.5 (4) |
Na_aiv—Ti_m1(2)—Mg_m2 | 92.67 (13) | O3iv—Nb_m1(1)—Oh | 92.5 (4) |
Na_axiii—Ti_m1(2)—O1 | 126.0 (3) | O3iv—Nb_m1(1)—Ohiv | 87.5 (4) |
Na_axiii—Ti_m1(2)—O1xii | 58.9 (3) | Oh—Nb_m1(1)—Ohiv | 180.0 (5) |
Na_axiii—Ti_m1(2)—O6iv | 130.7 (3) | Ti_m1(2)—Ti_m2—Ti_m1(2)xiv | 180.0 (5) |
Na_axiii—Ti_m1(2)—O6xiii | 44.5 (3) | Ti_m1(2)—Ti_m2—Fe_m2 | 0 |
Na_axiii—Ti_m1(2)—Oh | 58.6 (4) | Ti_m1(2)—Ti_m2—O1 | 41.52 (18) |
Na_axiii—Ti_m1(2)—Ohxii | 121.6 (4) | Ti_m1(2)—Ti_m2—O1xii | 41.52 (18) |
Na_axiii—Ti_m1(2)—Ba | 71.1 (2) | Ti_m1(2)—Ti_m2—O1xiv | 138.48 (18) |
Na_axiii—Ti_m1(2)—Baxii | 113.6 (2) | Ti_m1(2)—Ti_m2—O1x | 138.48 (18) |
Na_axiii—Ti_m1(2)—Ti_m2 | 92.67 (13) | Ti_m1(2)—Ti_m2—Ba | 90 |
Na_axiii—Ti_m1(2)—Mg_m2 | 92.67 (13) | Ti_m1(2)—Ti_m2—Baxii | 90 |
O1—Ti_m1(2)—O1xii | 82.3 (3) | Ti_m1(2)—Ti_m2—W_c | 90 |
O1—Ti_m1(2)—O6iv | 89.9 (3) | Ti_m1(2)—Ti_m2—W_cxii | 90 |
O1—Ti_m1(2)—O6xiii | 170.4 (3) | Ti_m1(2)—Ti_m2—Mg_m2 | 0 |
O1—Ti_m1(2)—Oh | 87.6 (4) | Ti_m1(2)xiv—Ti_m2—Fe_m2 | 0 |
O1—Ti_m1(2)—Ohxii | 89.3 (4) | Ti_m1(2)xiv—Ti_m2—O1 | 138.48 (18) |
O1—Ti_m1(2)—Ba | 54.9 (2) | Ti_m1(2)xiv—Ti_m2—O1xii | 138.48 (18) |
O1—Ti_m1(2)—Baxii | 48.7 (4) | Ti_m1(2)xiv—Ti_m2—O1xiv | 41.52 (18) |
O1—Ti_m1(2)—Ti_m2 | 41.15 (18) | Ti_m1(2)xiv—Ti_m2—O1x | 41.52 (18) |
O1—Ti_m1(2)—Mg_m2 | 41.15 (18) | Ti_m1(2)xiv—Ti_m2—Ba | 90 |
O1xii—Ti_m1(2)—O6iv | 170.4 (3) | Ti_m1(2)xiv—Ti_m2—Baxii | 90 |
O1xii—Ti_m1(2)—O6xiii | 89.9 (3) | Ti_m1(2)xiv—Ti_m2—W_c | 90 |
O1xii—Ti_m1(2)—Oh | 89.3 (4) | Ti_m1(2)xiv—Ti_m2—W_cxii | 90 |
O1xii—Ti_m1(2)—Ohxii | 87.6 (4) | Ti_m1(2)xiv—Ti_m2—Mg_m2 | 0 |
O1xii—Ti_m1(2)—Ba | 48.7 (4) | Fe_m2—Ti_m2—O1 | 0 |
O1xii—Ti_m1(2)—Baxii | 54.9 (2) | Fe_m2—Ti_m2—O1xii | 0 |
O1xii—Ti_m1(2)—Ti_m2 | 41.15 (18) | Fe_m2—Ti_m2—O1xiv | 0 |
O1xii—Ti_m1(2)—Mg_m2 | 41.15 (18) | Fe_m2—Ti_m2—O1x | 0 |
O6iv—Ti_m1(2)—O6xiii | 98.4 (3) | Fe_m2—Ti_m2—Ba | 0 |
O6iv—Ti_m1(2)—Oh | 96.0 (5) | Fe_m2—Ti_m2—Baxii | 0 |
O6iv—Ti_m1(2)—Ohxii | 86.7 (5) | Fe_m2—Ti_m2—W_c | 0 |
O6iv—Ti_m1(2)—Ba | 129.8 (4) | Fe_m2—Ti_m2—W_cxii | 0 |
O6iv—Ti_m1(2)—Baxii | 115.6 (3) | Fe_m2—Ti_m2—Mg_m2 | 0 |
O6iv—Ti_m1(2)—Ti_m2 | 130.82 (19) | O1—Ti_m2—O1xii | 83.0 (3) |
O6iv—Ti_m1(2)—Mg_m2 | 130.82 (19) | O1—Ti_m2—O1xiv | 180.0 (5) |
O6xiii—Ti_m1(2)—Oh | 86.7 (5) | O1—Ti_m2—O1x | 97.0 (3) |
O6xiii—Ti_m1(2)—Ohxii | 96.0 (5) | O1—Ti_m2—Ba | 94.3 (4) |
O6xiii—Ti_m1(2)—Ba | 115.6 (3) | O1—Ti_m2—Baxii | 85.7 (4) |
O6xiii—Ti_m1(2)—Baxii | 129.8 (4) | O1—Ti_m2—W_c | 94.3 (4) |
O6xiii—Ti_m1(2)—Ti_m2 | 130.82 (19) | O1—Ti_m2—W_cxii | 85.7 (4) |
O6xiii—Ti_m1(2)—Mg_m2 | 130.82 (19) | O1—Ti_m2—Mg_m2 | 0 |
Oh—Ti_m1(2)—Ohxii | 175.8 (2) | O1xii—Ti_m2—O1xiv | 97.0 (3) |
Oh—Ti_m1(2)—Ba | 53.33 (16) | O1xii—Ti_m2—O1x | 180.0 (5) |
Oh—Ti_m1(2)—Baxii | 122.51 (17) | O1xii—Ti_m2—Ba | 85.7 (4) |
Oh—Ti_m1(2)—Ti_m2 | 87.91 (15) | O1xii—Ti_m2—Baxii | 94.3 (4) |
Oh—Ti_m1(2)—Mg_m2 | 87.91 (15) | O1xii—Ti_m2—W_c | 85.7 (4) |
Ohxii—Ti_m1(2)—Ba | 122.51 (17) | O1xii—Ti_m2—W_cxii | 94.3 (4) |
Ohxii—Ti_m1(2)—Baxii | 53.33 (16) | O1xii—Ti_m2—Mg_m2 | 0 |
Ohxii—Ti_m1(2)—Ti_m2 | 87.91 (15) | O1xiv—Ti_m2—O1x | 83.0 (3) |
Ohxii—Ti_m1(2)—Mg_m2 | 87.91 (15) | O1xiv—Ti_m2—Ba | 85.7 (4) |
Ba—Ti_m1(2)—Baxii | 69.91 (9) | O1xiv—Ti_m2—Baxii | 94.3 (4) |
Ba—Ti_m1(2)—Ti_m2 | 34.95 (6) | O1xiv—Ti_m2—W_c | 85.7 (4) |
Ba—Ti_m1(2)—Mg_m2 | 34.95 (6) | O1xiv—Ti_m2—W_cxii | 94.3 (4) |
Baxii—Ti_m1(2)—Ti_m2 | 34.95 (6) | O1xiv—Ti_m2—Mg_m2 | 0 |
Baxii—Ti_m1(2)—Mg_m2 | 34.95 (6) | O1x—Ti_m2—Ba | 94.3 (4) |
Ti_m2—Ti_m1(2)—Mg_m2 | 0.0 (5) | O1x—Ti_m2—Baxii | 85.7 (4) |
O1—Fe_m2—O1xii | 83.0 (3) | O1x—Ti_m2—W_c | 94.3 (4) |
O1—Fe_m2—O1xiv | 180.0 (5) | O1x—Ti_m2—W_cxii | 85.7 (4) |
O1—Fe_m2—O1x | 97.0 (3) | O1x—Ti_m2—Mg_m2 | 0 |
O1—Fe_m2—Ba | 94.3 (4) | Ba—Ti_m2—Baxii | 180.0 (5) |
O1—Fe_m2—Baxii | 85.7 (4) | Ba—Ti_m2—W_c | 0.0 (5) |
O1—Fe_m2—W_c | 94.3 (4) | Ba—Ti_m2—W_cxii | 180.0 (5) |
O1—Fe_m2—W_cxii | 85.7 (4) | Ba—Ti_m2—Mg_m2 | 0 |
O1—Fe_m2—Ti_m2 | 0 | Baxii—Ti_m2—W_c | 180.0 (5) |
O1—Fe_m2—Mg_m2 | 0 | Baxii—Ti_m2—W_cxii | 0.0 (5) |
O1xii—Fe_m2—O1xiv | 97.0 (3) | Baxii—Ti_m2—Mg_m2 | 0 |
O1xii—Fe_m2—O1x | 180.0 (5) | W_c—Ti_m2—W_cxii | 180.0 (5) |
O1xii—Fe_m2—Ba | 85.7 (4) | W_c—Ti_m2—Mg_m2 | 0 |
O1xii—Fe_m2—Baxii | 94.3 (4) | W_cxii—Ti_m2—Mg_m2 | 0 |
O1xii—Fe_m2—W_c | 85.7 (4) | Ti_m1(2)—Mg_m2—Ti_m1(2)xiv | 180.0 (5) |
O1xii—Fe_m2—W_cxii | 94.3 (4) | Ti_m1(2)—Mg_m2—Fe_m2 | 0 |
O1xii—Fe_m2—Ti_m2 | 0 | Ti_m1(2)—Mg_m2—O1 | 41.52 (18) |
O1xii—Fe_m2—Mg_m2 | 0 | Ti_m1(2)—Mg_m2—O1xii | 41.52 (18) |
O1xiv—Fe_m2—O1x | 83.0 (3) | Ti_m1(2)—Mg_m2—O1xiv | 138.48 (18) |
O1xiv—Fe_m2—Ba | 85.7 (4) | Ti_m1(2)—Mg_m2—O1x | 138.48 (18) |
O1xiv—Fe_m2—Baxii | 94.3 (4) | Ti_m1(2)—Mg_m2—Ba | 90 |
O1xiv—Fe_m2—W_c | 85.7 (4) | Ti_m1(2)—Mg_m2—Baxii | 90 |
O1xiv—Fe_m2—W_cxii | 94.3 (4) | Ti_m1(2)—Mg_m2—W_c | 90 |
O1xiv—Fe_m2—Ti_m2 | 0 | Ti_m1(2)—Mg_m2—W_cxii | 90 |
O1xiv—Fe_m2—Mg_m2 | 0 | Ti_m1(2)—Mg_m2—Ti_m2 | 0 |
O1x—Fe_m2—Ba | 94.3 (4) | Ti_m1(2)xiv—Mg_m2—Fe_m2 | 0 |
O1x—Fe_m2—Baxii | 85.7 (4) | Ti_m1(2)xiv—Mg_m2—O1 | 138.48 (18) |
O1x—Fe_m2—W_c | 94.3 (4) | Ti_m1(2)xiv—Mg_m2—O1xii | 138.48 (18) |
O1x—Fe_m2—W_cxii | 85.7 (4) | Ti_m1(2)xiv—Mg_m2—O1xiv | 41.52 (18) |
O1x—Fe_m2—Ti_m2 | 0 | Ti_m1(2)xiv—Mg_m2—O1x | 41.52 (18) |
O1x—Fe_m2—Mg_m2 | 0 | Ti_m1(2)xiv—Mg_m2—Ba | 90 |
Ba—Fe_m2—Baxii | 180.0 (5) | Ti_m1(2)xiv—Mg_m2—Baxii | 90 |
Ba—Fe_m2—W_c | 0.0 (5) | Ti_m1(2)xiv—Mg_m2—W_c | 90 |
Ba—Fe_m2—W_cxii | 180.0 (5) | Ti_m1(2)xiv—Mg_m2—W_cxii | 90 |
Ba—Fe_m2—Ti_m2 | 0 | Ti_m1(2)xiv—Mg_m2—Ti_m2 | 0 |
Ba—Fe_m2—Mg_m2 | 0 | Fe_m2—Mg_m2—O1 | 0 |
Baxii—Fe_m2—W_c | 180.0 (5) | Fe_m2—Mg_m2—O1xii | 0 |
Baxii—Fe_m2—W_cxii | 0.0 (5) | Fe_m2—Mg_m2—O1xiv | 0 |
Baxii—Fe_m2—Ti_m2 | 0 | Fe_m2—Mg_m2—O1x | 0 |
Baxii—Fe_m2—Mg_m2 | 0 | Fe_m2—Mg_m2—Ba | 0 |
W_c—Fe_m2—W_cxii | 180.0 (5) | Fe_m2—Mg_m2—Baxii | 0 |
W_c—Fe_m2—Ti_m2 | 0 | Fe_m2—Mg_m2—W_c | 0 |
W_c—Fe_m2—Mg_m2 | 0 | Fe_m2—Mg_m2—W_cxii | 0 |
W_cxii—Fe_m2—Ti_m2 | 0 | Fe_m2—Mg_m2—Ti_m2 | 0 |
W_cxii—Fe_m2—Mg_m2 | 0 | O1—Mg_m2—O1xii | 83.0 (3) |
Ti_m2—Fe_m2—Mg_m2 | 0 | O1—Mg_m2—O1xiv | 180.0 (5) |
K_b—Si1—K_biii | 79.06 (17) | O1—Mg_m2—O1x | 97.0 (3) |
K_b—Si1—O3 | 54.9 (3) | O1—Mg_m2—Ba | 94.3 (4) |
K_b—Si1—O4 | 63.5 (4) | O1—Mg_m2—Baxii | 85.7 (4) |
K_b—Si1—O6 | 99.8 (3) | O1—Mg_m2—W_c | 94.3 (4) |
K_b—Si1—O7 | 149.6 (5) | O1—Mg_m2—W_cxii | 85.7 (4) |
K_biii—Si1—O3 | 133.7 (3) | O1—Mg_m2—Ti_m2 | 0 |
K_biii—Si1—O4 | 40.0 (7) | O1xii—Mg_m2—O1xiv | 97.0 (3) |
K_biii—Si1—O6 | 63.8 (4) | O1xii—Mg_m2—O1x | 180.0 (5) |
K_biii—Si1—O7 | 114.9 (5) | O1xii—Mg_m2—Ba | 85.7 (4) |
O3—Si1—O4 | 110.2 (6) | O1xii—Mg_m2—Baxii | 94.3 (4) |
O3—Si1—O6 | 115.9 (4) | O1xii—Mg_m2—W_c | 85.7 (4) |
O3—Si1—O7 | 108.1 (7) | O1xii—Mg_m2—W_cxii | 94.3 (4) |
O4—Si1—O6 | 103.1 (8) | O1xii—Mg_m2—Ti_m2 | 0 |
O4—Si1—O7 | 108.7 (4) | O1xiv—Mg_m2—O1x | 83.0 (3) |
O6—Si1—O7 | 110.6 (5) | O1xiv—Mg_m2—Ba | 85.7 (4) |
Na_aiv—Si2—K_b | 164.0 (3) | O1xiv—Mg_m2—Baxii | 94.3 (4) |
Na_aiv—Si2—O1 | 65.0 (4) | O1xiv—Mg_m2—W_c | 85.7 (4) |
Na_aiv—Si2—O2 | 103.0 (4) | O1xiv—Mg_m2—W_cxii | 94.3 (4) |
Na_aiv—Si2—O5 | 147.3 (6) | O1xiv—Mg_m2—Ti_m2 | 0 |
Na_aiv—Si2—O7xi | 48.8 (4) | O1x—Mg_m2—Ba | 94.3 (4) |
Na_aiv—Si2—Ba | 122.8 (3) | O1x—Mg_m2—Baxii | 85.7 (4) |
K_b—Si2—O1 | 130.6 (3) | O1x—Mg_m2—W_c | 94.3 (4) |
K_b—Si2—O2 | 68.6 (4) | O1x—Mg_m2—W_cxii | 85.7 (4) |
K_b—Si2—O5 | 39.5 (6) | O1x—Mg_m2—Ti_m2 | 0 |
K_b—Si2—O7xi | 120.3 (5) | Ba—Mg_m2—Baxii | 180.0 (5) |
K_b—Si2—Ba | 72.49 (14) | Ba—Mg_m2—W_c | 0.0 (5) |
O1—Si2—O2 | 114.7 (4) | Ba—Mg_m2—W_cxii | 180.0 (5) |
O1—Si2—O5 | 109.7 (5) | Ba—Mg_m2—Ti_m2 | 0 |
O1—Si2—O7xi | 104.5 (7) | Baxii—Mg_m2—W_c | 180.0 (5) |
O1—Si2—Ba | 58.1 (3) | Baxii—Mg_m2—W_cxii | 0.0 (5) |
O2—Si2—O5 | 107.9 (8) | Baxii—Mg_m2—Ti_m2 | 0 |
O2—Si2—O7xi | 111.8 (4) | W_c—Mg_m2—W_cxii | 180.0 (5) |
O2—Si2—Ba | 95.5 (2) | W_c—Mg_m2—Ti_m2 | 0 |
O5—Si2—O7xi | 108.1 (4) | W_cxii—Mg_m2—Ti_m2 | 0 |
O5—Si2—Ba | 64.7 (3) | | |
Symmetry codes: (i) −x+1, y, −z; (ii) x, y, z−1; (iii) −x+1, y, −z+1; (iv) −x+1/2, −y+1/2, −z+1; (v) −x+1/2, −y+1/2, −z; (vi) x+1/2, y+1/2, z; (vii) −x+1/2, y+1/2, −z; (viii) −x+1, y, −z+2; (ix) −x+1, −y, −z+1; (x) x, −y, z; (xi) x, y, z+1; (xii) −x, y, −z+1; (xiii) x−1/2, −y+1/2, z; (xiv) −x, −y, −z+1; (xv) −x, y, −z; (xvi) −x, −y, −z; (xvii) x, −y, z+1; (xviii) x−1/2, y−1/2, z; (xix) −x+1/2, y−1/2, −z. |
Crystal data top
Ba0.7Fe0.5K2.1Mg0.05Na2Nb0.1O33Si8Ti4 | Z = 2 |
Mr = 1206.8 | F(000) = 1167 |
Monoclinic, C2/m | Dx = 3.292 Mg m−3 |
Hall symbol: -C 2y | Synchrotron radiation, λ = 0.414 Å |
a = 13.739 (12) Å | Cell parameters from 2971 reflections |
b = 13.3221 (7) Å | θ = 1.8–19.1° |
c = 7.419 (2) Å | µ = 0.87 mm−1 |
β = 116.33 (5)° | T = 293 K |
V = 1217.1 (12) Å3 | Anhedral grain |
Data collection top
ESRF ID 09 diffractometer | θmax = 19.1°, θmin = 1.8° |
2971 measured reflections | h = −8→7 |
877 independent reflections | k = −20→20 |
687 reflections with I > 2σ(I) | l = −10→10 |
Rint = 0.051 | |
Refinement top
Refinement on F | 0 restraints |
R[F2 > 2σ(F2)] = 0.074 | 6 constraints |
wR(F2) = 0.137 | Weighting scheme based on measured s.u.'s w = 1/(σ2(F) + 0.0120999999F2) |
S = 1.06 | (Δ/σ)max = 0.043 |
877 reflections | Δρmax = 0.97 e Å−3 |
71 parameters | Δρmin = −0.95 e Å−3 |
Fractional atomic coordinates and isotropic or equivalent isotropic displacement parameters (Å2) top | x | y | z | Uiso*/Ueq | Occ. (<1) |
Na_a | 0.4191 (15) | 0.2682 (5) | 0.0155 (12) | 0.025 (9) | 0.5 |
K_b | 0.4289 (5) | 0 | 0.7197 (4) | 0.020 (4) | |
Ti_m1(1) | 0.25 | 0.25 | 0.5 | 0.0141 (5)* | 0.95 |
Ti_m1(2) | 0 | 0.21989 (14) | 0.5 | 0.0132 (6)* | |
Fe_m2 | 0 | 0 | 0.5 | 0.0255 (11)* | 0.5 |
Si1 | 0.3268 (4) | 0.11032 (13) | 0.2634 (3) | 0.0085 (5)* | |
Si2 | 0.2112 (4) | 0.10905 (13) | 0.8133 (3) | 0.0079 (5)* | |
O1 | 0.0815 (11) | 0.1091 (3) | 0.6797 (8) | 0.0087 (11)* | |
O2 | 0.2729 (10) | 0.1943 (4) | 0.7576 (7) | 0.0090 (11)* | |
O3 | 0.2783 (11) | 0.1182 (3) | 0.4237 (8) | 0.0100 (11)* | |
O4 | 0.3827 (16) | 0 | 0.2844 (11) | 0.0129 (16)* | |
O5 | 0.2628 (15) | 0 | 0.7928 (11) | 0.0117 (16)* | |
O6 | 0.4212 (11) | 0.1868 (4) | 0.2938 (9) | 0.0177 (14)* | |
O7 | 0.2253 (11) | 0.1196 (3) | 0.0393 (8) | 0.0106 (11)* | |
Oh | 0.0972 (10) | 0.2129 (4) | 0.3873 (8) | 0.0112 (11)* | |
Ba | 0.0917 (3) | 0 | 0.3401 (2) | 0.0137 (5)* | 0.35 |
W1 | 0.5 | 0.1440 (7) | 0 | 0.056 (13) | |
W2 | 0 | 0.1078 (7) | 0 | 0.038 (17) | |
W_c | 0.0917 (3) | 0 | 0.3401 (2) | 0.0137 (5)* | 0.65 |
Nb_m1(1) | 0.25 | 0.25 | 0.5 | 0.0141 (5)* | 0.05 |
Ti_m2 | 0 | 0 | 0.5 | 0.0255 (11)* | 0.1 |
Mg_m2 | 0 | 0 | 0.5 | 0.0255 (11)* | 0.05 |
Atomic displacement parameters (Å2) top | U11 | U22 | U33 | U12 | U13 | U23 |
Na_a | 0.02 (2) | 0.019 (3) | 0.034 (4) | −0.008 (5) | 0.008 (6) | −0.003 (3) |
K_b | 0.014 (8) | 0.0331 (14) | 0.0129 (11) | 0 | 0.0057 (19) | 0 |
W1 | 0.09 (3) | 0.027 (5) | 0.016 (4) | 0 | −0.009 (8) | 0 |
W2 | 0.05 (4) | 0.032 (5) | 0.034 (6) | 0 | 0.023 (9) | 0 |
Geometric parameters (Å, º) top
Na_a—Na_ai | 2.33 (3) | Ti_m1(2)—Ba | 3.592 (3) |
Na_a—K_bii | 4.226 (10) | Ti_m1(2)—Baxiii | 3.592 (3) |
Na_a—K_biii | 4.165 (10) | Ti_m1(2)—Ti_m2 | 2.9294 (19) |
Na_a—Ti_m1(1)ii | 3.493 (10) | Ti_m1(2)—Mg_m2 | 2.9294 (19) |
Na_a—Ti_m1(2)iv | 3.262 (10) | Fe_m2—O1 | 1.954 (6) |
Na_a—Si2iv | 3.084 (18) | Fe_m2—O1xiii | 1.954 (6) |
Na_a—O2ii | 2.294 (14) | Fe_m2—O1xv | 1.954 (6) |
Na_a—O6 | 2.321 (15) | Fe_m2—O1x | 1.954 (6) |
Na_a—O7v | 2.37 (2) | Fe_m2—Ba | 2.079 (5) |
Na_a—Bavi | 3.987 (10) | Fe_m2—Baxiii | 2.079 (5) |
Na_a—Bavii | 4.021 (10) | Fe_m2—W_c | 2.079 (5) |
Na_a—W1 | 2.025 (16) | Fe_m2—W_cxiii | 2.079 (5) |
Na_a—W2v | 2.022 (16) | Fe_m2—Ti_m2 | 0 |
Na_a—Nb_m1(1)ii | 3.493 (10) | Fe_m2—Mg_m2 | 0 |
K_b—K_biii | 4.484 (9) | Si1—O3 | 1.604 (13) |
K_b—K_bviii | 3.729 (6) | Si1—O4 | 1.634 (10) |
K_b—Si1 | 3.373 (4) | Si1—O6 | 1.585 (13) |
K_b—Si1iii | 3.616 (10) | Si1—O7 | 1.633 (8) |
K_b—Si1ix | 3.616 (10) | Si2—O1 | 1.610 (13) |
K_b—Si1x | 3.373 (4) | Si2—O2 | 1.577 (11) |
K_b—Si2 | 3.657 (10) | Si2—O5 | 1.652 (11) |
K_b—Si2x | 3.657 (10) | Si2—O7xi | 1.607 (8) |
K_b—O3 | 2.749 (9) | Si2—Ba | 3.467 (4) |
K_b—O3x | 2.749 (9) | O1—Baxiii | 2.736 (14) |
K_b—O4iii | 2.60 (2) | O1—Ti_m2 | 1.954 (6) |
K_b—O5 | 2.57 (2) | O1—Mg_m2 | 1.954 (6) |
K_b—Ba | 4.221 (12) | O2—Nb_m1(1) | 1.942 (7) |
K_b—W1xi | 2.675 (7) | O3—Ba | 2.833 (14) |
K_b—W1ix | 2.675 (7) | O3—Nb_m1(1) | 1.936 (7) |
Ti_m1(1)—O2 | 1.942 (7) | Oh—Ba | 2.855 (5) |
Ti_m1(1)—O2iv | 1.942 (7) | Oh—Nb_m1(1) | 1.948 (13) |
Ti_m1(1)—O3 | 1.936 (7) | Ba—Baxvi | 4.532 (6) |
Ti_m1(1)—O3iv | 1.936 (7) | Ba—Baxiii | 4.157 (7) |
Ti_m1(1)—Oh | 1.948 (13) | Ba—W2 | 2.683 (6) |
Ti_m1(1)—Ohiv | 1.948 (13) | Ba—W2xvii | 2.683 (6) |
Ti_m1(1)—Ba | 3.865 (3) | Ba—W_c | 0 |
Ti_m1(1)—Baxii | 3.865 (3) | Ba—Nb_m1(1) | 3.865 (3) |
Ti_m1(1)—Nb_m1(1) | 0 | Ba—Nb_m1(1)xviii | 3.865 (3) |
Ti_m1(2)—O1 | 1.971 (6) | Ba—Ti_m2 | 2.079 (5) |
Ti_m1(2)—O1xiii | 1.971 (6) | Ba—Mg_m2 | 2.079 (5) |
Ti_m1(2)—O6iv | 1.895 (6) | W_c—Ti_m2 | 2.079 (5) |
Ti_m1(2)—O6xiv | 1.895 (6) | W_c—Mg_m2 | 2.079 (5) |
Ti_m1(2)—Oh | 1.866 (13) | Ti_m2—Mg_m2 | 0 |
Ti_m1(2)—Ohxiii | 1.866 (13) | | |
| | | |
Na_ai—Na_a—K_bii | 72.4 (4) | Na_axx—Ba—Nb_m1(1) | 162.89 (19) |
Na_ai—Na_a—K_biii | 75.3 (4) | Na_axx—Ba—Nb_m1(1)xviii | 67.7 (2) |
Na_ai—Na_a—Ti_m1(1)ii | 95.3 (5) | Na_axx—Ba—Ti_m2 | 89.8 (3) |
Na_ai—Na_a—Ti_m1(2)iv | 103.6 (5) | Na_axx—Ba—Mg_m2 | 89.8 (3) |
Na_ai—Na_a—Si2iv | 142.5 (4) | Na_axxi—Ba—Na_av | 100.3 (2) |
Na_ai—Na_a—O2ii | 116.0 (7) | Na_axxi—Ba—Na_axiv | 111.06 (18) |
Na_ai—Na_a—O6 | 116.8 (7) | Na_axxi—Ba—K_b | 98.5 (3) |
Na_ai—Na_a—O7v | 138.1 (6) | Na_axxi—Ba—Ti_m1(1) | 135.7 (3) |
Na_ai—Na_a—Bavi | 73.9 (4) | Na_axxi—Ba—Ti_m1(1)xviii | 52.54 (14) |
Na_ai—Na_a—Bavii | 72.3 (4) | Na_axxi—Ba—Ti_m1(2) | 157.9 (2) |
Na_ai—Na_a—W1 | 54.8 (5) | Na_axxi—Ba—Ti_m1(2)xv | 71.0 (2) |
Na_ai—Na_a—W2v | 54.8 (5) | Na_axxi—Ba—Fe_m2 | 121.3 (3) |
Na_ai—Na_a—Nb_m1(1)ii | 95.3 (5) | Na_axxi—Ba—Si2 | 148.14 (18) |
K_bii—Na_a—K_biii | 52.76 (13) | Na_axxi—Ba—Si2x | 101.87 (12) |
K_bii—Na_a—Ti_m1(1)ii | 62.07 (14) | Na_axxi—Ba—O1xiii | 126.5 (3) |
K_bii—Na_a—Ti_m1(2)iv | 122.7 (2) | Na_axxi—Ba—O1xv | 77.2 (3) |
K_bii—Na_a—Si2iv | 145.1 (5) | Na_axxi—Ba—O3 | 109.7 (4) |
K_bii—Na_a—O2ii | 54.7 (3) | Na_axxi—Ba—O3x | 58.9 (3) |
K_bii—Na_a—O6 | 94.3 (3) | Na_axxi—Ba—Oh | 146.6 (2) |
K_bii—Na_a—O7v | 131.4 (5) | Na_axxi—Ba—Ohx | 46.3 (2) |
K_bii—Na_a—Bavi | 145.2 (6) | Na_axxi—Ba—Baxvi | 55.17 (13) |
K_bii—Na_a—Bavii | 108.0 (3) | Na_axxi—Ba—Baxiii | 121.3 (3) |
K_bii—Na_a—W1 | 30.11 (18) | Na_axxi—Ba—W2 | 85.9 (2) |
K_bii—Na_a—W2v | 121.1 (7) | Na_axxi—Ba—W2xvii | 26.7 (2) |
K_bii—Na_a—Nb_m1(1)ii | 62.07 (14) | Na_axxi—Ba—W_c | 0 |
K_biii—Na_a—Ti_m1(1)ii | 114.1 (2) | Na_axxi—Ba—Nb_m1(1) | 135.7 (3) |
K_biii—Na_a—Ti_m1(2)iv | 70.58 (16) | Na_axxi—Ba—Nb_m1(1)xviii | 52.54 (14) |
K_biii—Na_a—Si2iv | 121.5 (4) | Na_axxi—Ba—Ti_m2 | 121.3 (3) |
K_biii—Na_a—O2ii | 95.5 (3) | Na_axxi—Ba—Mg_m2 | 121.3 (3) |
K_biii—Na_a—O6 | 51.2 (3) | Na_av—Ba—Na_axiv | 33.9 (4) |
K_biii—Na_a—O7v | 145.9 (7) | Na_av—Ba—K_b | 98.5 (3) |
K_biii—Na_a—Bavi | 109.9 (3) | Na_av—Ba—Ti_m1(1) | 52.54 (14) |
K_biii—Na_a—Bavii | 146.4 (6) | Na_av—Ba—Ti_m1(1)xviii | 135.7 (3) |
K_biii—Na_a—W1 | 32.07 (19) | Na_av—Ba—Ti_m1(2) | 71.0 (2) |
K_biii—Na_a—W2v | 123.7 (7) | Na_av—Ba—Ti_m1(2)xv | 157.9 (2) |
K_biii—Na_a—Nb_m1(1)ii | 114.1 (2) | Na_av—Ba—Fe_m2 | 121.3 (3) |
Ti_m1(1)ii—Na_a—Ti_m1(2)iv | 161.1 (7) | Na_av—Ba—Si2 | 101.87 (12) |
Ti_m1(1)ii—Na_a—Si2iv | 105.2 (5) | Na_av—Ba—Si2x | 148.14 (18) |
Ti_m1(1)ii—Na_a—O2ii | 31.3 (2) | Na_av—Ba—O1xiii | 77.2 (3) |
Ti_m1(1)ii—Na_a—O6 | 132.9 (6) | Na_av—Ba—O1xv | 126.5 (3) |
Ti_m1(1)ii—Na_a—O7v | 75.9 (3) | Na_av—Ba—O3 | 58.9 (3) |
Ti_m1(1)ii—Na_a—Bavi | 130.1 (2) | Na_av—Ba—O3x | 109.7 (4) |
Ti_m1(1)ii—Na_a—Bavii | 61.44 (14) | Na_av—Ba—Oh | 46.3 (2) |
Ti_m1(1)ii—Na_a—W1 | 89.8 (3) | Na_av—Ba—Ohx | 146.6 (2) |
Ti_m1(1)ii—Na_a—W2v | 96.3 (3) | Na_av—Ba—Baxvi | 55.17 (13) |
Ti_m1(1)ii—Na_a—Nb_m1(1)ii | 0.0 (5) | Na_av—Ba—Baxiii | 121.3 (3) |
Ti_m1(2)iv—Na_a—Si2iv | 59.8 (3) | Na_av—Ba—W2 | 26.7 (2) |
Ti_m1(2)iv—Na_a—O2ii | 133.2 (8) | Na_av—Ba—W2xvii | 85.9 (2) |
Ti_m1(2)iv—Na_a—O6 | 34.8 (2) | Na_av—Ba—W_c | 0 |
Ti_m1(2)iv—Na_a—O7v | 90.5 (5) | Na_av—Ba—Nb_m1(1) | 52.54 (14) |
Ti_m1(2)iv—Na_a—Bavi | 58.39 (14) | Na_av—Ba—Nb_m1(1)xviii | 135.7 (3) |
Ti_m1(2)iv—Na_a—Bavii | 125.5 (2) | Na_av—Ba—Ti_m2 | 121.3 (3) |
Ti_m1(2)iv—Na_a—W1 | 100.1 (3) | Na_av—Ba—Mg_m2 | 121.3 (3) |
Ti_m1(2)iv—Na_a—W2v | 95.5 (3) | Na_axiv—Ba—K_b | 125.9 (2) |
Ti_m1(2)iv—Na_a—Nb_m1(1)ii | 161.1 (7) | Na_axiv—Ba—Ti_m1(1) | 67.7 (2) |
Si2iv—Na_a—O2ii | 96.7 (7) | Na_axiv—Ba—Ti_m1(1)xviii | 162.89 (19) |
Si2iv—Na_a—O6 | 70.2 (5) | Na_axiv—Ba—Ti_m1(2) | 50.66 (17) |
Si2iv—Na_a—O7v | 30.9 (3) | Na_axiv—Ba—Ti_m1(2)xv | 129.0 (3) |
Si2iv—Na_a—Bavi | 68.84 (19) | Na_axiv—Ba—Fe_m2 | 89.8 (3) |
Si2iv—Na_a—Bavii | 90.2 (2) | Na_axiv—Ba—Si2 | 100.07 (13) |
Si2iv—Na_a—W1 | 152.9 (6) | Na_axiv—Ba—Si2x | 145.5 (2) |
Si2iv—Na_a—W2v | 91.4 (4) | Na_axiv—Ba—O1xiii | 44.4 (3) |
Si2iv—Na_a—Nb_m1(1)ii | 105.2 (5) | Na_axiv—Ba—O1xv | 96.2 (3) |
O2ii—Na_a—O6 | 101.6 (7) | Na_axiv—Ba—O3 | 86.5 (3) |
O2ii—Na_a—O7v | 76.7 (6) | Na_axiv—Ba—O3x | 143.2 (4) |
O2ii—Na_a—Bavi | 154.6 (4) | Na_axiv—Ba—Oh | 44.01 (19) |
O2ii—Na_a—Bavii | 91.1 (3) | Na_axiv—Ba—Ohx | 145.1 (3) |
O2ii—Na_a—W1 | 84.3 (4) | Na_axiv—Ba—Baxvi | 55.89 (13) |
O2ii—Na_a—W2v | 127.1 (4) | Na_axiv—Ba—Baxiii | 89.8 (3) |
O2ii—Na_a—Nb_m1(1)ii | 31.3 (2) | Na_axiv—Ba—W2 | 27.3 (2) |
O6—Na_a—O7v | 97.3 (8) | Na_axiv—Ba—W2xvii | 86.6 (2) |
O6—Na_a—Bavi | 93.2 (3) | Na_axiv—Ba—W_c | 0 |
O6—Na_a—Bavii | 157.6 (4) | Na_axiv—Ba—Nb_m1(1) | 67.7 (2) |
O6—Na_a—W1 | 83.0 (4) | Na_axiv—Ba—Nb_m1(1)xviii | 162.89 (19) |
O6—Na_a—W2v | 129.9 (4) | Na_axiv—Ba—Ti_m2 | 89.8 (3) |
O6—Na_a—Nb_m1(1)ii | 132.9 (6) | Na_axiv—Ba—Mg_m2 | 89.8 (3) |
O7v—Na_a—Bavi | 81.0 (3) | K_b—Ba—Ti_m1(1) | 59.58 (6) |
O7v—Na_a—Bavii | 67.6 (3) | K_b—Ba—Ti_m1(1)xviii | 59.58 (6) |
O7v—Na_a—W1 | 160.7 (7) | K_b—Ba—Ti_m1(2) | 102.80 (7) |
O7v—Na_a—W2v | 85.1 (4) | K_b—Ba—Ti_m1(2)xv | 102.80 (7) |
O7v—Na_a—Nb_m1(1)ii | 75.9 (3) | K_b—Ba—Fe_m2 | 112.51 (11) |
Bavi—Na_a—Bavii | 68.94 (17) | K_b—Ba—Si2 | 55.78 (13) |
Bavi—Na_a—W1 | 118.2 (7) | K_b—Ba—Si2x | 55.78 (13) |
Bavi—Na_a—W2v | 37.54 (17) | K_b—Ba—O1xiii | 134.98 (14) |
Bavi—Na_a—Nb_m1(1)ii | 130.1 (2) | K_b—Ba—O1xv | 134.98 (14) |
Bavii—Na_a—W1 | 116.9 (7) | K_b—Ba—O3 | 40.12 (14) |
Bavii—Na_a—W2v | 36.57 (17) | K_b—Ba—O3x | 40.12 (14) |
Bavii—Na_a—Nb_m1(1)ii | 61.44 (14) | K_b—Ba—Oh | 87.5 (2) |
W1—Na_a—W2v | 109.6 (10) | K_b—Ba—Ohx | 87.5 (2) |
W1—Na_a—Nb_m1(1)ii | 89.8 (3) | K_b—Ba—Baxvi | 130.29 (15) |
W2v—Na_a—Nb_m1(1)ii | 96.3 (3) | K_b—Ba—Baxiii | 112.51 (11) |
Na_axi—K_b—Na_aiii | 32.3 (4) | K_b—Ba—W2 | 123.11 (16) |
Na_axi—K_b—Na_aix | 127.24 (17) | K_b—Ba—W2xvii | 123.11 (16) |
Na_axi—K_b—Na_axix | 115.4 (3) | K_b—Ba—W_c | 0 |
Na_axi—K_b—K_biii | 120.1 (2) | K_b—Ba—Nb_m1(1) | 59.58 (6) |
Na_axi—K_b—K_bviii | 62.78 (12) | K_b—Ba—Nb_m1(1)xviii | 59.58 (6) |
Na_axi—K_b—Si1 | 93.32 (12) | K_b—Ba—Ti_m2 | 112.51 (11) |
Na_axi—K_b—Si1iii | 83.2 (3) | K_b—Ba—Mg_m2 | 112.51 (11) |
Na_axi—K_b—Si1ix | 124.6 (3) | Ti_m1(1)—Ba—Ti_m1(1)xviii | 119.01 (12) |
Na_axi—K_b—Si1x | 142.63 (16) | Ti_m1(1)—Ba—Ti_m1(2) | 55.11 (4) |
Na_axi—K_b—Si2 | 49.4 (3) | Ti_m1(1)—Ba—Ti_m1(2)xv | 146.45 (6) |
Na_axi—K_b—Si2x | 91.2 (3) | Ti_m1(1)—Ba—Fe_m2 | 103.05 (5) |
Na_axi—K_b—O3 | 75.20 (19) | Ti_m1(1)—Ba—Si2 | 51.60 (7) |
Na_axi—K_b—O3x | 135.5 (4) | Ti_m1(1)—Ba—Si2x | 95.80 (8) |
Na_axi—K_b—O4iii | 105.5 (3) | Ti_m1(1)—Ba—O1xiii | 85.21 (18) |
Na_axi—K_b—O5 | 69.8 (3) | Ti_m1(1)—Ba—O1xv | 146.3 (2) |
Na_axi—K_b—Ba | 93.9 (3) | Ti_m1(1)—Ba—O3 | 28.7 (2) |
Na_axi—K_b—W1xi | 22.3 (2) | Ti_m1(1)—Ba—O3x | 94.6 (2) |
Na_axi—K_b—W1ix | 106.7 (2) | Ti_m1(1)—Ba—Oh | 29.0 (3) |
Na_aiii—K_b—Na_aix | 118.2 (3) | Ti_m1(1)—Ba—Ohx | 146.9 (2) |
Na_aiii—K_b—Na_axix | 127.24 (17) | Ti_m1(1)—Ba—Baxvi | 107.52 (6) |
Na_aiii—K_b—K_biii | 93.1 (3) | Ti_m1(1)—Ba—Baxiii | 103.05 (6) |
Na_aiii—K_b—K_bviii | 64.46 (13) | Ti_m1(1)—Ba—W2 | 78.05 (17) |
Na_aiii—K_b—Si1 | 89.88 (13) | Ti_m1(1)—Ba—W2xvii | 135.68 (17) |
Na_aiii—K_b—Si1iii | 51.1 (3) | Ti_m1(1)—Ba—W_c | 0 |
Na_aiii—K_b—Si1ix | 93.9 (3) | Ti_m1(1)—Ba—Nb_m1(1) | 0.0 (5) |
Na_aiii—K_b—Si1x | 138.2 (2) | Ti_m1(1)—Ba—Nb_m1(1)xviii | 119.01 (12) |
Na_aiii—K_b—Si2 | 81.4 (3) | Ti_m1(1)—Ba—Ti_m2 | 103.05 (5) |
Na_aiii—K_b—Si2x | 122.2 (3) | Ti_m1(1)—Ba—Mg_m2 | 103.05 (5) |
Na_aiii—K_b—O3 | 85.8 (2) | Ti_m1(1)xviii—Ba—Ti_m1(2) | 146.45 (6) |
Na_aiii—K_b—O3x | 155.60 (18) | Ti_m1(1)xviii—Ba—Ti_m1(2)xv | 55.11 (4) |
Na_aiii—K_b—O4iii | 73.3 (3) | Ti_m1(1)xviii—Ba—Fe_m2 | 103.05 (5) |
Na_aiii—K_b—O5 | 101.9 (3) | Ti_m1(1)xviii—Ba—Si2 | 95.80 (8) |
Na_aiii—K_b—Ba | 119.1 (2) | Ti_m1(1)xviii—Ba—Si2x | 51.60 (7) |
Na_aiii—K_b—W1xi | 23.7 (2) | Ti_m1(1)xviii—Ba—O1xiii | 146.3 (2) |
Na_aiii—K_b—W1ix | 108.3 (2) | Ti_m1(1)xviii—Ba—O1xv | 85.21 (18) |
Na_aix—K_b—Na_axix | 32.3 (4) | Ti_m1(1)xviii—Ba—O3 | 94.6 (2) |
Na_aix—K_b—K_biii | 93.1 (3) | Ti_m1(1)xviii—Ba—O3x | 28.7 (2) |
Na_aix—K_b—K_bviii | 64.46 (13) | Ti_m1(1)xviii—Ba—Oh | 146.9 (2) |
Na_aix—K_b—Si1 | 138.2 (2) | Ti_m1(1)xviii—Ba—Ohx | 29.0 (3) |
Na_aix—K_b—Si1iii | 93.9 (3) | Ti_m1(1)xviii—Ba—Baxvi | 107.52 (6) |
Na_aix—K_b—Si1ix | 51.1 (3) | Ti_m1(1)xviii—Ba—Baxiii | 103.05 (6) |
Na_aix—K_b—Si1x | 89.88 (13) | Ti_m1(1)xviii—Ba—W2 | 135.68 (17) |
Na_aix—K_b—Si2 | 122.2 (3) | Ti_m1(1)xviii—Ba—W2xvii | 78.05 (17) |
Na_aix—K_b—Si2x | 81.4 (3) | Ti_m1(1)xviii—Ba—W_c | 0 |
Na_aix—K_b—O3 | 155.60 (18) | Ti_m1(1)xviii—Ba—Nb_m1(1) | 119.01 (12) |
Na_aix—K_b—O3x | 85.8 (2) | Ti_m1(1)xviii—Ba—Nb_m1(1)xviii | 0.0 (5) |
Na_aix—K_b—O4iii | 73.3 (3) | Ti_m1(1)xviii—Ba—Ti_m2 | 103.05 (5) |
Na_aix—K_b—O5 | 101.9 (3) | Ti_m1(1)xviii—Ba—Mg_m2 | 103.05 (5) |
Na_aix—K_b—Ba | 119.1 (2) | Ti_m1(2)—Ba—Ti_m1(2)xv | 109.28 (12) |
Na_aix—K_b—W1xi | 108.3 (2) | Ti_m1(2)—Ba—Fe_m2 | 54.64 (6) |
Na_aix—K_b—W1ix | 23.7 (2) | Ti_m1(2)—Ba—Si2 | 53.26 (8) |
Na_axix—K_b—K_biii | 120.1 (2) | Ti_m1(2)—Ba—Si2x | 94.90 (9) |
Na_axix—K_b—K_bviii | 62.78 (12) | Ti_m1(2)—Ba—O1xiii | 32.91 (15) |
Na_axix—K_b—Si1 | 142.63 (16) | Ti_m1(2)—Ba—O1xv | 91.5 (2) |
Na_axix—K_b—Si1iii | 124.6 (3) | Ti_m1(2)—Ba—O3 | 83.7 (2) |
Na_axix—K_b—Si1ix | 83.2 (3) | Ti_m1(2)—Ba—O3x | 142.85 (14) |
Na_axix—K_b—Si1x | 93.32 (12) | Ti_m1(2)—Ba—Oh | 31.0 (3) |
Na_axix—K_b—Si2 | 91.2 (3) | Ti_m1(2)—Ba—Ohx | 139.8 (3) |
Na_axix—K_b—Si2x | 49.4 (3) | Ti_m1(2)—Ba—Baxvi | 105.34 (7) |
Na_axix—K_b—O3 | 135.5 (4) | Ti_m1(2)—Ba—Baxiii | 54.64 (6) |
Na_axix—K_b—O3x | 75.20 (19) | Ti_m1(2)—Ba—W2 | 77.69 (16) |
Na_axix—K_b—O4iii | 105.5 (3) | Ti_m1(2)—Ba—W2xvii | 131.29 (17) |
Na_axix—K_b—O5 | 69.8 (3) | Ti_m1(2)—Ba—W_c | 0 |
Na_axix—K_b—Ba | 93.9 (3) | Ti_m1(2)—Ba—Nb_m1(1) | 55.11 (4) |
Na_axix—K_b—W1xi | 106.7 (2) | Ti_m1(2)—Ba—Nb_m1(1)xviii | 146.45 (6) |
Na_axix—K_b—W1ix | 22.3 (2) | Ti_m1(2)—Ba—Ti_m2 | 54.64 (6) |
K_biii—K_b—K_bviii | 129.0 (2) | Ti_m1(2)—Ba—Mg_m2 | 54.64 (6) |
K_biii—K_b—Si1 | 52.51 (15) | Ti_m1(2)xv—Ba—Fe_m2 | 54.64 (6) |
K_biii—K_b—Si1iii | 47.75 (11) | Ti_m1(2)xv—Ba—Si2 | 94.90 (9) |
K_biii—K_b—Si1ix | 47.75 (11) | Ti_m1(2)xv—Ba—Si2x | 53.26 (8) |
K_biii—K_b—Si1x | 52.51 (15) | Ti_m1(2)xv—Ba—O1xiii | 91.5 (2) |
K_biii—K_b—Si2 | 142.64 (9) | Ti_m1(2)xv—Ba—O1xv | 32.91 (15) |
K_biii—K_b—Si2x | 142.64 (9) | Ti_m1(2)xv—Ba—O3 | 142.85 (14) |
K_biii—K_b—O3 | 80.5 (3) | Ti_m1(2)xv—Ba—O3x | 83.7 (2) |
K_biii—K_b—O3x | 80.5 (3) | Ti_m1(2)xv—Ba—Oh | 139.8 (3) |
K_biii—K_b—O4iii | 40.1 (2) | Ti_m1(2)xv—Ba—Ohx | 31.0 (3) |
K_biii—K_b—O5 | 150.2 (2) | Ti_m1(2)xv—Ba—Baxvi | 105.34 (7) |
K_biii—K_b—Ba | 102.60 (11) | Ti_m1(2)xv—Ba—Baxiii | 54.64 (6) |
K_biii—K_b—W1xi | 116.0 (2) | Ti_m1(2)xv—Ba—W2 | 131.29 (17) |
K_biii—K_b—W1ix | 116.0 (2) | Ti_m1(2)xv—Ba—W2xvii | 77.69 (16) |
K_bviii—K_b—Si1 | 153.94 (5) | Ti_m1(2)xv—Ba—W_c | 0 |
K_bviii—K_b—Si1iii | 86.68 (17) | Ti_m1(2)xv—Ba—Nb_m1(1) | 146.45 (6) |
K_bviii—K_b—Si1ix | 86.68 (17) | Ti_m1(2)xv—Ba—Nb_m1(1)xviii | 55.11 (4) |
K_bviii—K_b—Si1x | 153.94 (5) | Ti_m1(2)xv—Ba—Ti_m2 | 54.64 (6) |
K_bviii—K_b—Si2 | 81.75 (17) | Ti_m1(2)xv—Ba—Mg_m2 | 54.64 (6) |
K_bviii—K_b—Si2x | 81.75 (17) | Fe_m2—Ba—Si2 | 63.70 (12) |
K_bviii—K_b—O3 | 136.7 (2) | Fe_m2—Ba—Si2x | 63.70 (12) |
K_bviii—K_b—O3x | 136.7 (2) | Fe_m2—Ba—O1xiii | 45.39 (18) |
K_bviii—K_b—O4iii | 88.9 (2) | Fe_m2—Ba—O1xv | 45.39 (18) |
K_bviii—K_b—O5 | 80.8 (2) | Fe_m2—Ba—O3 | 126.4 (2) |
K_bviii—K_b—Ba | 128.4 (2) | Fe_m2—Ba—O3x | 126.4 (2) |
K_bviii—K_b—W1xi | 45.81 (15) | Fe_m2—Ba—Oh | 85.4 (3) |
K_bviii—K_b—W1ix | 45.81 (15) | Fe_m2—Ba—Ohx | 85.4 (3) |
Si1—K_b—Si1iii | 79.86 (17) | Fe_m2—Ba—Baxvi | 117.19 (16) |
Si1—K_b—Si1ix | 100.3 (2) | Fe_m2—Ba—Baxiii | 0.0 (5) |
Si1—K_b—Si1x | 51.67 (6) | Fe_m2—Ba—W2 | 112.71 (17) |
Si1—K_b—Si2 | 90.37 (16) | Fe_m2—Ba—W2xvii | 112.71 (17) |
Si1—K_b—Si2x | 110.7 (2) | Fe_m2—Ba—W_c | 0 |
Si1—K_b—O3 | 28.1 (3) | Fe_m2—Ba—Nb_m1(1) | 103.05 (5) |
Si1—K_b—O3x | 67.48 (15) | Fe_m2—Ba—Nb_m1(1)xviii | 103.05 (5) |
Si1—K_b—O4iii | 87.8 (2) | Fe_m2—Ba—Ti_m2 | 0.0 (5) |
Si1—K_b—O5 | 101.5 (3) | Fe_m2—Ba—Mg_m2 | 0.0 (5) |
Si1—K_b—Ba | 59.04 (14) | Si2—Ba—Si2x | 49.55 (5) |
Si1—K_b—W1xi | 108.28 (15) | Si2—Ba—O1xiii | 80.91 (16) |
Si1—K_b—W1ix | 159.82 (17) | Si2—Ba—O1xv | 106.7 (2) |
Si1iii—K_b—Si1ix | 47.97 (12) | Si2—Ba—O3 | 64.49 (19) |
Si1iii—K_b—Si1x | 100.3 (2) | Si2—Ba—O3x | 92.02 (16) |
Si1iii—K_b—Si2 | 131.05 (8) | Si2—Ba—Oh | 58.98 (11) |
Si1iii—K_b—Si2x | 168.43 (10) | Si2—Ba—Ohx | 108.50 (12) |
Si1iii—K_b—O3 | 98.8 (3) | Si2—Ba—Baxvi | 155.15 (4) |
Si1iii—K_b—O3x | 128.2 (3) | Si2—Ba—Baxiii | 63.70 (13) |
Si1iii—K_b—O4iii | 24.11 (7) | Si2—Ba—W2 | 122.83 (18) |
Si1iii—K_b—O5 | 152.97 (11) | Si2—Ba—W2xvii | 172.21 (18) |
Si1iii—K_b—Ba | 138.62 (10) | Si2—Ba—W_c | 0 |
Si1iii—K_b—W1xi | 70.62 (14) | Si2—Ba—Nb_m1(1) | 51.60 (7) |
Si1iii—K_b—W1ix | 104.5 (2) | Si2—Ba—Nb_m1(1)xviii | 95.80 (8) |
Si1ix—K_b—Si1x | 79.86 (17) | Si2—Ba—Ti_m2 | 63.70 (12) |
Si1ix—K_b—Si2 | 168.43 (10) | Si2—Ba—Mg_m2 | 63.70 (12) |
Si1ix—K_b—Si2x | 131.05 (8) | Si2x—Ba—O1xiii | 106.7 (2) |
Si1ix—K_b—O3 | 128.2 (3) | Si2x—Ba—O1xv | 80.91 (16) |
Si1ix—K_b—O3x | 98.8 (3) | Si2x—Ba—O3 | 92.02 (16) |
Si1ix—K_b—O4iii | 24.11 (7) | Si2x—Ba—O3x | 64.49 (19) |
Si1ix—K_b—O5 | 152.97 (11) | Si2x—Ba—Oh | 108.50 (12) |
Si1ix—K_b—Ba | 138.62 (10) | Si2x—Ba—Ohx | 58.98 (11) |
Si1ix—K_b—W1xi | 104.5 (2) | Si2x—Ba—Baxvi | 155.15 (4) |
Si1ix—K_b—W1ix | 70.62 (14) | Si2x—Ba—Baxiii | 63.70 (13) |
Si1x—K_b—Si2 | 110.7 (2) | Si2x—Ba—W2 | 172.21 (18) |
Si1x—K_b—Si2x | 90.37 (16) | Si2x—Ba—W2xvii | 122.83 (18) |
Si1x—K_b—O3 | 67.48 (15) | Si2x—Ba—W_c | 0 |
Si1x—K_b—O3x | 28.1 (3) | Si2x—Ba—Nb_m1(1) | 95.80 (8) |
Si1x—K_b—O4iii | 87.8 (2) | Si2x—Ba—Nb_m1(1)xviii | 51.60 (7) |
Si1x—K_b—O5 | 101.5 (3) | Si2x—Ba—Ti_m2 | 63.70 (12) |
Si1x—K_b—Ba | 59.04 (14) | Si2x—Ba—Mg_m2 | 63.70 (12) |
Si1x—K_b—W1xi | 159.82 (17) | O1xiii—Ba—O1xv | 64.2 (3) |
Si1x—K_b—W1ix | 108.28 (15) | O1xiii—Ba—O3 | 113.4 (3) |
Si2—K_b—Si2x | 46.81 (12) | O1xiii—Ba—O3x | 171.1 (2) |
Si2—K_b—O3 | 62.3 (3) | O1xiii—Ba—Oh | 56.9 (3) |
Si2—K_b—O3x | 89.4 (4) | O1xiii—Ba—Ohx | 120.6 (4) |
Si2—K_b—O4iii | 154.63 (10) | O1xiii—Ba—Baxvi | 84.22 (15) |
Si2—K_b—O5 | 23.41 (7) | O1xiii—Ba—Baxiii | 45.39 (18) |
Si2—K_b—Ba | 51.61 (12) | O1xiii—Ba—W2 | 68.32 (18) |
Si2—K_b—W1xi | 67.37 (14) | O1xiii—Ba—W2xvii | 101.5 (2) |
Si2—K_b—W1ix | 100.7 (2) | O1xiii—Ba—W_c | 0 |
Si2x—K_b—O3 | 89.4 (4) | O1xiii—Ba—Nb_m1(1) | 85.21 (18) |
Si2x—K_b—O3x | 62.3 (3) | O1xiii—Ba—Nb_m1(1)xviii | 146.3 (2) |
Si2x—K_b—O4iii | 154.63 (10) | O1xiii—Ba—Ti_m2 | 45.39 (18) |
Si2x—K_b—O5 | 23.41 (7) | O1xiii—Ba—Mg_m2 | 45.39 (18) |
Si2x—K_b—Ba | 51.61 (12) | O1xv—Ba—O3 | 171.1 (2) |
Si2x—K_b—W1xi | 100.7 (2) | O1xv—Ba—O3x | 113.4 (3) |
Si2x—K_b—W1ix | 67.37 (14) | O1xv—Ba—Oh | 120.6 (4) |
O3—K_b—O3x | 69.9 (2) | O1xv—Ba—Ohx | 56.9 (3) |
O3—K_b—O4iii | 113.0 (4) | O1xv—Ba—Baxvi | 84.22 (15) |
O3—K_b—O5 | 75.2 (4) | O1xv—Ba—Baxiii | 45.39 (18) |
O3—K_b—Ba | 41.6 (3) | O1xv—Ba—W2 | 101.5 (2) |
O3—K_b—W1xi | 95.53 (19) | O1xv—Ba—W2xvii | 68.32 (18) |
O3—K_b—W1ix | 156.6 (4) | O1xv—Ba—W_c | 0 |
O3x—K_b—O4iii | 113.0 (4) | O1xv—Ba—Nb_m1(1) | 146.3 (2) |
O3x—K_b—O5 | 75.2 (4) | O1xv—Ba—Nb_m1(1)xviii | 85.21 (18) |
O3x—K_b—Ba | 41.6 (3) | O1xv—Ba—Ti_m2 | 45.39 (18) |
O3x—K_b—W1xi | 156.6 (4) | O1xv—Ba—Mg_m2 | 45.39 (18) |
O3x—K_b—W1ix | 95.53 (19) | O3—Ba—O3x | 67.6 (3) |
O4iii—K_b—O5 | 169.7 (3) | O3—Ba—Oh | 56.5 (3) |
O4iii—K_b—Ba | 142.7 (2) | O3—Ba—Ohx | 123.6 (3) |
O4iii—K_b—W1xi | 89.2 (2) | O3—Ba—Baxvi | 104.24 (16) |
O4iii—K_b—W1ix | 89.2 (2) | O3—Ba—Baxiii | 126.4 (2) |
O5—K_b—Ba | 47.6 (2) | O3—Ba—W2 | 84.84 (18) |
O5—K_b—W1xi | 83.6 (2) | O3—Ba—W2xvii | 120.4 (2) |
O5—K_b—W1ix | 83.6 (2) | O3—Ba—W_c | 0 |
Ba—K_b—W1xi | 115.7 (2) | O3—Ba—Nb_m1(1) | 28.7 (2) |
Ba—K_b—W1ix | 115.7 (2) | O3—Ba—Nb_m1(1)xviii | 94.6 (2) |
W1xi—K_b—W1ix | 91.6 (2) | O3—Ba—Ti_m2 | 126.4 (2) |
Na_axi—Ti_m1(1)—Na_av | 180.0 (5) | O3—Ba—Mg_m2 | 126.4 (2) |
Na_axi—Ti_m1(1)—O2 | 37.8 (4) | O3x—Ba—Oh | 123.6 (3) |
Na_axi—Ti_m1(1)—O2iv | 142.2 (4) | O3x—Ba—Ohx | 56.5 (3) |
Na_axi—Ti_m1(1)—O3 | 105.1 (3) | O3x—Ba—Baxvi | 104.24 (16) |
Na_axi—Ti_m1(1)—O3iv | 74.9 (3) | O3x—Ba—Baxiii | 126.4 (2) |
Na_axi—Ti_m1(1)—Oh | 123.7 (4) | O3x—Ba—W2 | 120.4 (2) |
Na_axi—Ti_m1(1)—Ohiv | 56.3 (4) | O3x—Ba—W2xvii | 84.84 (18) |
Na_axi—Ti_m1(1)—Ba | 113.98 (18) | O3x—Ba—W_c | 0 |
Na_axi—Ti_m1(1)—Baxii | 66.02 (18) | O3x—Ba—Nb_m1(1) | 94.6 (2) |
Na_axi—Ti_m1(1)—Nb_m1(1) | 0 | O3x—Ba—Nb_m1(1)xviii | 28.7 (2) |
Na_av—Ti_m1(1)—O2 | 142.2 (4) | O3x—Ba—Ti_m2 | 126.4 (2) |
Na_av—Ti_m1(1)—O2iv | 37.8 (4) | O3x—Ba—Mg_m2 | 126.4 (2) |
Na_av—Ti_m1(1)—O3 | 74.9 (3) | Oh—Ba—Ohx | 167.0 (2) |
Na_av—Ti_m1(1)—O3iv | 105.1 (3) | Oh—Ba—Baxvi | 96.19 (11) |
Na_av—Ti_m1(1)—Oh | 56.3 (4) | Oh—Ba—Baxiii | 85.4 (3) |
Na_av—Ti_m1(1)—Ohiv | 123.7 (4) | Oh—Ba—W2 | 63.9 (2) |
Na_av—Ti_m1(1)—Ba | 66.02 (18) | Oh—Ba—W2xvii | 128.5 (2) |
Na_av—Ti_m1(1)—Baxii | 113.98 (18) | Oh—Ba—W_c | 0 |
Na_av—Ti_m1(1)—Nb_m1(1) | 0 | Oh—Ba—Nb_m1(1) | 29.0 (3) |
O2—Ti_m1(1)—O2iv | 180.0 (5) | Oh—Ba—Nb_m1(1)xviii | 146.9 (2) |
O2—Ti_m1(1)—O3 | 88.6 (3) | Oh—Ba—Ti_m2 | 85.4 (3) |
O2—Ti_m1(1)—O3iv | 91.4 (3) | Oh—Ba—Mg_m2 | 85.4 (3) |
O2—Ti_m1(1)—Oh | 89.9 (4) | Ohx—Ba—Baxvi | 96.19 (11) |
O2—Ti_m1(1)—Ohiv | 90.1 (4) | Ohx—Ba—Baxiii | 85.4 (3) |
O2—Ti_m1(1)—Ba | 78.2 (2) | Ohx—Ba—W2 | 128.5 (2) |
O2—Ti_m1(1)—Baxii | 101.8 (2) | Ohx—Ba—W2xvii | 63.9 (2) |
O2—Ti_m1(1)—Nb_m1(1) | 0 | Ohx—Ba—W_c | 0 |
O2iv—Ti_m1(1)—O3 | 91.4 (3) | Ohx—Ba—Nb_m1(1) | 146.9 (2) |
O2iv—Ti_m1(1)—O3iv | 88.6 (3) | Ohx—Ba—Nb_m1(1)xviii | 29.0 (3) |
O2iv—Ti_m1(1)—Oh | 90.1 (4) | Ohx—Ba—Ti_m2 | 85.4 (3) |
O2iv—Ti_m1(1)—Ohiv | 89.9 (4) | Ohx—Ba—Mg_m2 | 85.4 (3) |
O2iv—Ti_m1(1)—Ba | 101.8 (2) | Baxvi—Ba—Baxiii | 117.19 (14) |
O2iv—Ti_m1(1)—Baxii | 78.2 (2) | Baxvi—Ba—W2 | 32.36 (17) |
O2iv—Ti_m1(1)—Nb_m1(1) | 0 | Baxvi—Ba—W2xvii | 32.36 (17) |
O3—Ti_m1(1)—O3iv | 180.0 (5) | Baxvi—Ba—W_c | 0 |
O3—Ti_m1(1)—Oh | 87.8 (5) | Baxvi—Ba—Nb_m1(1) | 107.52 (6) |
O3—Ti_m1(1)—Ohiv | 92.2 (5) | Baxvi—Ba—Nb_m1(1)xviii | 107.52 (6) |
O3—Ti_m1(1)—Ba | 44.6 (4) | Baxvi—Ba—Ti_m2 | 117.19 (16) |
O3—Ti_m1(1)—Baxii | 135.4 (4) | Baxvi—Ba—Mg_m2 | 117.19 (16) |
O3—Ti_m1(1)—Nb_m1(1) | 0 | Baxiii—Ba—W2 | 112.71 (15) |
O3iv—Ti_m1(1)—Oh | 92.2 (5) | Baxiii—Ba—W2xvii | 112.71 (15) |
O3iv—Ti_m1(1)—Ohiv | 87.8 (5) | Baxiii—Ba—W_c | 0 |
O3iv—Ti_m1(1)—Ba | 135.4 (4) | Baxiii—Ba—Nb_m1(1) | 103.05 (6) |
O3iv—Ti_m1(1)—Baxii | 44.6 (4) | Baxiii—Ba—Nb_m1(1)xviii | 103.05 (6) |
O3iv—Ti_m1(1)—Nb_m1(1) | 0 | Baxiii—Ba—Ti_m2 | 0.0 (5) |
Oh—Ti_m1(1)—Ohiv | 180.0 (5) | Baxiii—Ba—Mg_m2 | 0.0 (5) |
Oh—Ti_m1(1)—Ba | 45.35 (19) | W2—Ba—W2xvii | 64.7 (2) |
Oh—Ti_m1(1)—Baxii | 134.65 (19) | W2—Ba—W_c | 0 |
Oh—Ti_m1(1)—Nb_m1(1) | 0 | W2—Ba—Nb_m1(1) | 78.05 (17) |
Ohiv—Ti_m1(1)—Ba | 134.65 (19) | W2—Ba—Nb_m1(1)xviii | 135.68 (17) |
Ohiv—Ti_m1(1)—Baxii | 45.35 (19) | W2—Ba—Ti_m2 | 112.71 (17) |
Ohiv—Ti_m1(1)—Nb_m1(1) | 0 | W2—Ba—Mg_m2 | 112.71 (17) |
Ba—Ti_m1(1)—Baxii | 180.0 (5) | W2xvii—Ba—W_c | 0 |
Ba—Ti_m1(1)—Nb_m1(1) | 0 | W2xvii—Ba—Nb_m1(1) | 135.68 (17) |
Baxii—Ti_m1(1)—Nb_m1(1) | 0 | W2xvii—Ba—Nb_m1(1)xviii | 78.05 (17) |
Na_aiv—Ti_m1(2)—Na_axiv | 174.43 (19) | W2xvii—Ba—Ti_m2 | 112.71 (17) |
Na_aiv—Ti_m1(2)—O1 | 58.5 (3) | W2xvii—Ba—Mg_m2 | 112.71 (17) |
Na_aiv—Ti_m1(2)—O1xiii | 126.5 (3) | W_c—Ba—Nb_m1(1) | 0 |
Na_aiv—Ti_m1(2)—O6iv | 44.3 (3) | W_c—Ba—Nb_m1(1)xviii | 0 |
Na_aiv—Ti_m1(2)—O6xiv | 130.7 (3) | W_c—Ba—Ti_m2 | 0 |
Na_aiv—Ti_m1(2)—Oh | 122.3 (4) | W_c—Ba—Mg_m2 | 0 |
Na_aiv—Ti_m1(2)—Ohxiii | 58.0 (4) | Nb_m1(1)—Ba—Nb_m1(1)xviii | 119.01 (12) |
Na_aiv—Ti_m1(2)—Ba | 113.9 (2) | Nb_m1(1)—Ba—Ti_m2 | 103.05 (5) |
Na_aiv—Ti_m1(2)—Baxiii | 70.9 (2) | Nb_m1(1)—Ba—Mg_m2 | 103.05 (5) |
Na_aiv—Ti_m1(2)—Ti_m2 | 92.78 (13) | Nb_m1(1)xviii—Ba—Ti_m2 | 103.05 (5) |
Na_aiv—Ti_m1(2)—Mg_m2 | 92.78 (13) | Nb_m1(1)xviii—Ba—Mg_m2 | 103.05 (5) |
Na_axiv—Ti_m1(2)—O1 | 126.5 (3) | Ti_m2—Ba—Mg_m2 | 0.0 (5) |
Na_axiv—Ti_m1(2)—O1xiii | 58.5 (3) | Na_a—W1—Na_ai | 70.4 (8) |
Na_axiv—Ti_m1(2)—O6iv | 130.7 (3) | Na_a—W1—K_bii | 127.6 (3) |
Na_axiv—Ti_m1(2)—O6xiv | 44.3 (3) | Na_a—W1—K_biii | 124.2 (4) |
Na_axiv—Ti_m1(2)—Oh | 58.0 (4) | Na_ai—W1—K_bii | 124.2 (4) |
Na_axiv—Ti_m1(2)—Ohxiii | 122.3 (4) | Na_ai—W1—K_biii | 127.6 (3) |
Na_axiv—Ti_m1(2)—Ba | 70.9 (2) | K_bii—W1—K_biii | 88.4 (3) |
Na_axiv—Ti_m1(2)—Baxiii | 113.9 (2) | Na_av—W2—Na_axiv | 70.5 (8) |
Na_axiv—Ti_m1(2)—Ti_m2 | 92.78 (13) | Na_av—W2—Ba | 116.7 (3) |
Na_axiv—Ti_m1(2)—Mg_m2 | 92.78 (13) | Na_av—W2—Baxvi | 115.1 (3) |
O1—Ti_m1(2)—O1xiii | 83.0 (3) | Na_axiv—W2—Ba | 115.1 (3) |
O1—Ti_m1(2)—O6iv | 89.8 (3) | Na_axiv—W2—Baxvi | 116.7 (3) |
O1—Ti_m1(2)—O6xiv | 170.9 (3) | Ba—W2—Baxvi | 115.3 (3) |
O1—Ti_m1(2)—Oh | 87.8 (4) | Fe_m2—W_c—Ba | 0 |
O1—Ti_m1(2)—Ohxiii | 87.9 (5) | Fe_m2—W_c—Ti_m2 | 0.0 (5) |
O1—Ti_m1(2)—Ba | 55.6 (2) | Fe_m2—W_c—Mg_m2 | 0.0 (5) |
O1—Ti_m1(2)—Baxiii | 48.9 (4) | Ba—W_c—Ti_m2 | 0 |
O1—Ti_m1(2)—Ti_m2 | 41.50 (18) | Ba—W_c—Mg_m2 | 0 |
O1—Ti_m1(2)—Mg_m2 | 41.50 (18) | Ti_m2—W_c—Mg_m2 | 0.0 (5) |
O1xiii—Ti_m1(2)—O6iv | 170.9 (3) | Na_axi—Nb_m1(1)—Na_av | 180.0 (5) |
O1xiii—Ti_m1(2)—O6xiv | 89.8 (3) | Na_axi—Nb_m1(1)—Ti_m1(1) | 0 |
O1xiii—Ti_m1(2)—Oh | 87.9 (5) | Na_axi—Nb_m1(1)—O2 | 37.8 (4) |
O1xiii—Ti_m1(2)—Ohxiii | 87.8 (4) | Na_axi—Nb_m1(1)—O2iv | 142.2 (4) |
O1xiii—Ti_m1(2)—Ba | 48.9 (4) | Na_axi—Nb_m1(1)—O3 | 105.1 (3) |
O1xiii—Ti_m1(2)—Baxiii | 55.6 (2) | Na_axi—Nb_m1(1)—O3iv | 74.9 (3) |
O1xiii—Ti_m1(2)—Ti_m2 | 41.50 (18) | Na_axi—Nb_m1(1)—Oh | 123.7 (4) |
O1xiii—Ti_m1(2)—Mg_m2 | 41.50 (18) | Na_axi—Nb_m1(1)—Ohiv | 56.3 (4) |
O6iv—Ti_m1(2)—O6xiv | 98.0 (3) | Na_axi—Nb_m1(1)—Ba | 113.98 (18) |
O6iv—Ti_m1(2)—Oh | 97.4 (5) | Na_axi—Nb_m1(1)—Baxii | 66.02 (18) |
O6iv—Ti_m1(2)—Ohxiii | 86.4 (5) | Na_av—Nb_m1(1)—Ti_m1(1) | 0 |
O6iv—Ti_m1(2)—Ba | 130.1 (4) | Na_av—Nb_m1(1)—O2 | 142.2 (4) |
O6iv—Ti_m1(2)—Baxiii | 115.3 (3) | Na_av—Nb_m1(1)—O2iv | 37.8 (4) |
O6iv—Ti_m1(2)—Ti_m2 | 131.02 (19) | Na_av—Nb_m1(1)—O3 | 74.9 (3) |
O6iv—Ti_m1(2)—Mg_m2 | 131.02 (19) | Na_av—Nb_m1(1)—O3iv | 105.1 (3) |
O6xiv—Ti_m1(2)—Oh | 86.4 (5) | Na_av—Nb_m1(1)—Oh | 56.3 (4) |
O6xiv—Ti_m1(2)—Ohxiii | 97.4 (5) | Na_av—Nb_m1(1)—Ohiv | 123.7 (4) |
O6xiv—Ti_m1(2)—Ba | 115.3 (3) | Na_av—Nb_m1(1)—Ba | 66.02 (18) |
O6xiv—Ti_m1(2)—Baxiii | 130.1 (4) | Na_av—Nb_m1(1)—Baxii | 113.98 (18) |
O6xiv—Ti_m1(2)—Ti_m2 | 131.02 (19) | Ti_m1(1)—Nb_m1(1)—O2 | 0 |
O6xiv—Ti_m1(2)—Mg_m2 | 131.02 (19) | Ti_m1(1)—Nb_m1(1)—O2iv | 0 |
Oh—Ti_m1(2)—Ohxiii | 174.3 (2) | Ti_m1(1)—Nb_m1(1)—O3 | 0 |
Oh—Ti_m1(2)—Ba | 52.11 (17) | Ti_m1(1)—Nb_m1(1)—O3iv | 0 |
Oh—Ti_m1(2)—Baxiii | 122.21 (18) | Ti_m1(1)—Nb_m1(1)—Oh | 0 |
Oh—Ti_m1(2)—Ti_m2 | 87.15 (16) | Ti_m1(1)—Nb_m1(1)—Ohiv | 0 |
Oh—Ti_m1(2)—Mg_m2 | 87.15 (16) | Ti_m1(1)—Nb_m1(1)—Ba | 0 |
Ohxiii—Ti_m1(2)—Ba | 122.21 (18) | Ti_m1(1)—Nb_m1(1)—Baxii | 0 |
Ohxiii—Ti_m1(2)—Baxiii | 52.11 (17) | O2—Nb_m1(1)—O2iv | 180.0 (5) |
Ohxiii—Ti_m1(2)—Ti_m2 | 87.15 (16) | O2—Nb_m1(1)—O3 | 88.6 (3) |
Ohxiii—Ti_m1(2)—Mg_m2 | 87.15 (16) | O2—Nb_m1(1)—O3iv | 91.4 (3) |
Ba—Ti_m1(2)—Baxiii | 70.72 (9) | O2—Nb_m1(1)—Oh | 89.9 (4) |
Ba—Ti_m1(2)—Ti_m2 | 35.36 (6) | O2—Nb_m1(1)—Ohiv | 90.1 (4) |
Ba—Ti_m1(2)—Mg_m2 | 35.36 (6) | O2—Nb_m1(1)—Ba | 78.2 (2) |
Baxiii—Ti_m1(2)—Ti_m2 | 35.36 (6) | O2—Nb_m1(1)—Baxii | 101.8 (2) |
Baxiii—Ti_m1(2)—Mg_m2 | 35.36 (6) | O2iv—Nb_m1(1)—O3 | 91.4 (3) |
Ti_m2—Ti_m1(2)—Mg_m2 | 0.0 (5) | O2iv—Nb_m1(1)—O3iv | 88.6 (3) |
O1—Fe_m2—O1xiii | 83.9 (3) | O2iv—Nb_m1(1)—Oh | 90.1 (4) |
O1—Fe_m2—O1xv | 180.0 (5) | O2iv—Nb_m1(1)—Ohiv | 89.9 (4) |
O1—Fe_m2—O1x | 96.1 (3) | O2iv—Nb_m1(1)—Ba | 101.8 (2) |
O1—Fe_m2—Ba | 94.6 (4) | O2iv—Nb_m1(1)—Baxii | 78.2 (2) |
O1—Fe_m2—Baxiii | 85.4 (4) | O3—Nb_m1(1)—O3iv | 180.0 (5) |
O1—Fe_m2—W_c | 94.6 (4) | O3—Nb_m1(1)—Oh | 87.8 (5) |
O1—Fe_m2—W_cxiii | 85.4 (4) | O3—Nb_m1(1)—Ohiv | 92.2 (5) |
O1—Fe_m2—Ti_m2 | 0 | O3—Nb_m1(1)—Ba | 44.6 (4) |
O1—Fe_m2—Mg_m2 | 0 | O3—Nb_m1(1)—Baxii | 135.4 (4) |
O1xiii—Fe_m2—O1xv | 96.1 (3) | O3iv—Nb_m1(1)—Oh | 92.2 (5) |
O1xiii—Fe_m2—O1x | 180.0 (5) | O3iv—Nb_m1(1)—Ohiv | 87.8 (5) |
O1xiii—Fe_m2—Ba | 85.4 (4) | O3iv—Nb_m1(1)—Ba | 135.4 (4) |
O1xiii—Fe_m2—Baxiii | 94.6 (4) | O3iv—Nb_m1(1)—Baxii | 44.6 (4) |
O1xiii—Fe_m2—W_c | 85.4 (4) | Oh—Nb_m1(1)—Ohiv | 180.0 (5) |
O1xiii—Fe_m2—W_cxiii | 94.6 (4) | Oh—Nb_m1(1)—Ba | 45.35 (19) |
O1xiii—Fe_m2—Ti_m2 | 0 | Oh—Nb_m1(1)—Baxii | 134.65 (19) |
O1xiii—Fe_m2—Mg_m2 | 0 | Ohiv—Nb_m1(1)—Ba | 134.65 (19) |
O1xv—Fe_m2—O1x | 83.9 (3) | Ohiv—Nb_m1(1)—Baxii | 45.35 (19) |
O1xv—Fe_m2—Ba | 85.4 (4) | Ba—Nb_m1(1)—Baxii | 180.0 (5) |
O1xv—Fe_m2—Baxiii | 94.6 (4) | Ti_m1(2)—Ti_m2—Ti_m1(2)xv | 180.0 (5) |
O1xv—Fe_m2—W_c | 85.4 (4) | Ti_m1(2)—Ti_m2—Fe_m2 | 0 |
O1xv—Fe_m2—W_cxiii | 94.6 (4) | Ti_m1(2)—Ti_m2—O1 | 41.96 (18) |
O1xv—Fe_m2—Ti_m2 | 0 | Ti_m1(2)—Ti_m2—O1xiii | 41.96 (18) |
O1xv—Fe_m2—Mg_m2 | 0 | Ti_m1(2)—Ti_m2—O1xv | 138.04 (18) |
O1x—Fe_m2—Ba | 94.6 (4) | Ti_m1(2)—Ti_m2—O1x | 138.04 (18) |
O1x—Fe_m2—Baxiii | 85.4 (4) | Ti_m1(2)—Ti_m2—Ba | 90 |
O1x—Fe_m2—W_c | 94.6 (4) | Ti_m1(2)—Ti_m2—Baxiii | 90 |
O1x—Fe_m2—W_cxiii | 85.4 (4) | Ti_m1(2)—Ti_m2—W_c | 90 |
O1x—Fe_m2—Ti_m2 | 0 | Ti_m1(2)—Ti_m2—W_cxiii | 90 |
O1x—Fe_m2—Mg_m2 | 0 | Ti_m1(2)—Ti_m2—Mg_m2 | 0 |
Ba—Fe_m2—Baxiii | 180.0 (5) | Ti_m1(2)xv—Ti_m2—Fe_m2 | 0 |
Ba—Fe_m2—W_c | 0.0 (5) | Ti_m1(2)xv—Ti_m2—O1 | 138.04 (18) |
Ba—Fe_m2—W_cxiii | 180.0 (5) | Ti_m1(2)xv—Ti_m2—O1xiii | 138.04 (18) |
Ba—Fe_m2—Ti_m2 | 0 | Ti_m1(2)xv—Ti_m2—O1xv | 41.96 (18) |
Ba—Fe_m2—Mg_m2 | 0 | Ti_m1(2)xv—Ti_m2—O1x | 41.96 (18) |
Baxiii—Fe_m2—W_c | 180.0 (5) | Ti_m1(2)xv—Ti_m2—Ba | 90 |
Baxiii—Fe_m2—W_cxiii | 0.0 (5) | Ti_m1(2)xv—Ti_m2—Baxiii | 90 |
Baxiii—Fe_m2—Ti_m2 | 0 | Ti_m1(2)xv—Ti_m2—W_c | 90 |
Baxiii—Fe_m2—Mg_m2 | 0 | Ti_m1(2)xv—Ti_m2—W_cxiii | 90 |
W_c—Fe_m2—W_cxiii | 180.0 (5) | Ti_m1(2)xv—Ti_m2—Mg_m2 | 0 |
W_c—Fe_m2—Ti_m2 | 0 | Fe_m2—Ti_m2—O1 | 0 |
W_c—Fe_m2—Mg_m2 | 0 | Fe_m2—Ti_m2—O1xiii | 0 |
W_cxiii—Fe_m2—Ti_m2 | 0 | Fe_m2—Ti_m2—O1xv | 0 |
W_cxiii—Fe_m2—Mg_m2 | 0 | Fe_m2—Ti_m2—O1x | 0 |
Ti_m2—Fe_m2—Mg_m2 | 0 | Fe_m2—Ti_m2—Ba | 0 |
K_b—Si1—K_biii | 79.74 (16) | Fe_m2—Ti_m2—Baxiii | 0 |
K_b—Si1—O3 | 53.8 (3) | Fe_m2—Ti_m2—W_c | 0 |
K_b—Si1—O4 | 62.9 (4) | Fe_m2—Ti_m2—W_cxiii | 0 |
K_b—Si1—O6 | 100.8 (3) | Fe_m2—Ti_m2—Mg_m2 | 0 |
K_b—Si1—O7 | 147.4 (5) | O1—Ti_m2—O1xiii | 83.9 (3) |
K_biii—Si1—O3 | 133.3 (3) | O1—Ti_m2—O1xv | 180.0 (5) |
K_biii—Si1—O4 | 40.6 (7) | O1—Ti_m2—O1x | 96.1 (3) |
K_biii—Si1—O6 | 64.3 (4) | O1—Ti_m2—Ba | 94.6 (4) |
K_biii—Si1—O7 | 115.2 (5) | O1—Ti_m2—Baxiii | 85.4 (4) |
O3—Si1—O4 | 108.7 (6) | O1—Ti_m2—W_c | 94.6 (4) |
O3—Si1—O6 | 115.9 (5) | O1—Ti_m2—W_cxiii | 85.4 (4) |
O3—Si1—O7 | 107.6 (7) | O1—Ti_m2—Mg_m2 | 0 |
O4—Si1—O6 | 104.1 (8) | O1xiii—Ti_m2—O1xv | 96.1 (3) |
O4—Si1—O7 | 108.5 (4) | O1xiii—Ti_m2—O1x | 180.0 (5) |
O6—Si1—O7 | 111.8 (5) | O1xiii—Ti_m2—Ba | 85.4 (4) |
Na_aiv—Si2—K_b | 164.1 (3) | O1xiii—Ti_m2—Baxiii | 94.6 (4) |
Na_aiv—Si2—O1 | 64.3 (4) | O1xiii—Ti_m2—W_c | 85.4 (4) |
Na_aiv—Si2—O2 | 101.8 (4) | O1xiii—Ti_m2—W_cxiii | 94.6 (4) |
Na_aiv—Si2—O5 | 148.7 (6) | O1xiii—Ti_m2—Mg_m2 | 0 |
Na_aiv—Si2—O7xi | 49.2 (4) | O1xv—Ti_m2—O1x | 83.9 (3) |
Na_aiv—Si2—Ba | 122.6 (3) | O1xv—Ti_m2—Ba | 85.4 (4) |
K_b—Si2—O1 | 131.2 (3) | O1xv—Ti_m2—Baxiii | 94.6 (4) |
K_b—Si2—O2 | 69.9 (4) | O1xv—Ti_m2—W_c | 85.4 (4) |
K_b—Si2—O5 | 38.1 (7) | O1xv—Ti_m2—W_cxiii | 94.6 (4) |
K_b—Si2—O7xi | 120.2 (5) | O1xv—Ti_m2—Mg_m2 | 0 |
K_b—Si2—Ba | 72.61 (14) | O1x—Ti_m2—Ba | 94.6 (4) |
O1—Si2—O2 | 114.5 (4) | O1x—Ti_m2—Baxiii | 85.4 (4) |
O1—Si2—O5 | 110.2 (6) | O1x—Ti_m2—W_c | 94.6 (4) |
O1—Si2—O7xi | 103.3 (7) | O1x—Ti_m2—W_cxiii | 85.4 (4) |
O1—Si2—Ba | 58.6 (3) | O1x—Ti_m2—Mg_m2 | 0 |
O2—Si2—O5 | 107.9 (8) | Ba—Ti_m2—Baxiii | 180.0 (5) |
O2—Si2—O7xi | 112.4 (4) | Ba—Ti_m2—W_c | 0.0 (5) |
O2—Si2—Ba | 96.0 (2) | Ba—Ti_m2—W_cxiii | 180.0 (5) |
O5—Si2—O7xi | 108.3 (4) | Ba—Ti_m2—Mg_m2 | 0 |
O5—Si2—Ba | 64.4 (3) | Baxiii—Ti_m2—W_c | 180.0 (5) |
O7xi—Si2—Ba | 151.3 (4) | Baxiii—Ti_m2—W_cxiii | 0.0 (5) |
Ti_m1(2)—O1—Fe_m2 | 96.5 (3) | Baxiii—Ti_m2—Mg_m2 | 0 |
Ti_m1(2)—O1—Si2 | 123.9 (5) | W_c—Ti_m2—W_cxiii | 180.0 (5) |
Ti_m1(2)—O1—Baxiii | 98.2 (5) | W_c—Ti_m2—Mg_m2 | 0 |
Ti_m1(2)—O1—Ti_m2 | 96.5 (3) | W_cxiii—Ti_m2—Mg_m2 | 0 |
Ti_m1(2)—O1—Mg_m2 | 96.5 (3) | Ti_m1(2)—Mg_m2—Ti_m1(2)xv | 180.0 (5) |
Fe_m2—O1—Si2 | 124.2 (5) | Ti_m1(2)—Mg_m2—Fe_m2 | 0 |
Fe_m2—O1—Baxiii | 49.2 (3) | Ti_m1(2)—Mg_m2—O1 | 41.96 (18) |
Fe_m2—O1—Ti_m2 | 0.0 (5) | Ti_m1(2)—Mg_m2—O1xiii | 41.96 (18) |
Fe_m2—O1—Mg_m2 | 0.0 (5) | Ti_m1(2)—Mg_m2—O1xv | 138.04 (18) |
Si2—O1—Baxiii | 137.1 (3) | Ti_m1(2)—Mg_m2—O1x | 138.04 (18) |
Si2—O1—Ti_m2 | 124.2 (5) | Ti_m1(2)—Mg_m2—Ba | 90 |
Si2—O1—Mg_m2 | 124.2 (5) | Ti_m1(2)—Mg_m2—Baxiii | 90 |
Baxiii—O1—Ti_m2 | 49.2 (3) | Ti_m1(2)—Mg_m2—W_c | 90 |
Baxiii—O1—Mg_m2 | 49.2 (3) | Ti_m1(2)—Mg_m2—W_cxiii | 90 |
Ti_m2—O1—Mg_m2 | 0.0 (5) | Ti_m1(2)—Mg_m2—Ti_m2 | 0 |
Na_axi—O2—Ti_m1(1) | 110.9 (6) | Ti_m1(2)xv—Mg_m2—Fe_m2 | 0 |
Na_axi—O2—Si2 | 117.7 (4) | Ti_m1(2)xv—Mg_m2—O1 | 138.04 (18) |
Na_axi—O2—Nb_m1(1) | 110.9 (6) | Ti_m1(2)xv—Mg_m2—O1xiii | 138.04 (18) |
Ti_m1(1)—O2—Si2 | 131.5 (4) | Ti_m1(2)xv—Mg_m2—O1xv | 41.96 (18) |
Ti_m1(1)—O2—Nb_m1(1) | 0.0 (5) | Ti_m1(2)xv—Mg_m2—O1x | 41.96 (18) |
Si2—O2—Nb_m1(1) | 131.5 (4) | Ti_m1(2)xv—Mg_m2—Ba | 90 |
K_b—O3—Ti_m1(1) | 117.6 (2) | Ti_m1(2)xv—Mg_m2—Baxiii | 90 |
K_b—O3—Si1 | 98.1 (6) | Ti_m1(2)xv—Mg_m2—W_c | 90 |
K_b—O3—Ba | 98.3 (3) | Ti_m1(2)xv—Mg_m2—W_cxiii | 90 |
K_b—O3—Nb_m1(1) | 117.6 (2) | Ti_m1(2)xv—Mg_m2—Ti_m2 | 0 |
Ti_m1(1)—O3—Si1 | 118.7 (4) | Fe_m2—Mg_m2—O1 | 0 |
Ti_m1(1)—O3—Ba | 106.8 (6) | Fe_m2—Mg_m2—O1xiii | 0 |
Ti_m1(1)—O3—Nb_m1(1) | 0.0 (5) | Fe_m2—Mg_m2—O1xv | 0 |
Si1—O3—Ba | 115.8 (3) | Fe_m2—Mg_m2—O1x | 0 |
Si1—O3—Nb_m1(1) | 118.7 (4) | Fe_m2—Mg_m2—Ba | 0 |
Ba—O3—Nb_m1(1) | 106.8 (6) | Fe_m2—Mg_m2—Baxiii | 0 |
K_biii—O4—Si1 | 115.3 (7) | Fe_m2—Mg_m2—W_c | 0 |
K_biii—O4—Si1x | 115.3 (7) | Fe_m2—Mg_m2—W_cxiii | 0 |
Si1—O4—Si1x | 128.2 (14) | Fe_m2—Mg_m2—Ti_m2 | 0 |
K_b—O5—Si2 | 118.5 (7) | O1—Mg_m2—O1xiii | 83.9 (3) |
K_b—O5—Si2x | 118.5 (7) | O1—Mg_m2—O1xv | 180.0 (5) |
Si2—O5—Si2x | 123.1 (13) | O1—Mg_m2—O1x | 96.1 (3) |
Na_a—O6—Ti_m1(2)iv | 100.9 (4) | O1—Mg_m2—Ba | 94.6 (4) |
Na_a—O6—Si1 | 119.2 (5) | O1—Mg_m2—Baxiii | 85.4 (4) |
Ti_m1(2)iv—O6—Si1 | 132.4 (7) | O1—Mg_m2—W_c | 94.6 (4) |
Na_av—O7—Si1 | 119.6 (5) | O1—Mg_m2—W_cxiii | 85.4 (4) |
Na_av—O7—Si2ii | 99.9 (4) | O1—Mg_m2—Ti_m2 | 0 |
Si1—O7—Si2ii | 135.2 (10) | O1xiii—Mg_m2—O1xv | 96.1 (3) |
Ti_m1(1)—Oh—Ti_m1(2) | 130.1 (3) | O1xiii—Mg_m2—O1x | 180.0 (5) |
Ti_m1(1)—Oh—Ba | 105.6 (4) | O1xiii—Mg_m2—Ba | 85.4 (4) |
Ti_m1(1)—Oh—Nb_m1(1) | 0.0 (5) | O1xiii—Mg_m2—Baxiii | 94.6 (4) |
Ti_m1(2)—Oh—Ba | 96.9 (3) | O1xiii—Mg_m2—W_c | 85.4 (4) |
Ti_m1(2)—Oh—Nb_m1(1) | 130.1 (3) | O1xiii—Mg_m2—W_cxiii | 94.6 (4) |
Ba—Oh—Nb_m1(1) | 105.6 (4) | O1xiii—Mg_m2—Ti_m2 | 0 |
Na_axx—Ba—Na_axxi | 33.9 (4) | O1xv—Mg_m2—O1x | 83.9 (3) |
Na_axx—Ba—Na_av | 111.06 (18) | O1xv—Mg_m2—Ba | 85.4 (4) |
Na_axx—Ba—Na_axiv | 101.5 (2) | O1xv—Mg_m2—Baxiii | 94.6 (4) |
Na_axx—Ba—K_b | 125.9 (2) | O1xv—Mg_m2—W_c | 85.4 (4) |
Na_axx—Ba—Ti_m1(1) | 162.89 (19) | O1xv—Mg_m2—W_cxiii | 94.6 (4) |
Na_axx—Ba—Ti_m1(1)xviii | 67.7 (2) | O1xv—Mg_m2—Ti_m2 | 0 |
Na_axx—Ba—Ti_m1(2) | 129.0 (3) | O1x—Mg_m2—Ba | 94.6 (4) |
Na_axx—Ba—Ti_m1(2)xv | 50.66 (17) | O1x—Mg_m2—Baxiii | 85.4 (4) |
Na_axx—Ba—Fe_m2 | 89.8 (3) | O1x—Mg_m2—W_c | 94.6 (4) |
Na_axx—Ba—Si2 | 145.5 (2) | O1x—Mg_m2—W_cxiii | 85.4 (4) |
Na_axx—Ba—Si2x | 100.07 (13) | O1x—Mg_m2—Ti_m2 | 0 |
Na_axx—Ba—O1xiii | 96.2 (3) | Ba—Mg_m2—Baxiii | 180.0 (5) |
Na_axx—Ba—O1xv | 44.4 (3) | Ba—Mg_m2—W_c | 0.0 (5) |
Na_axx—Ba—O3 | 143.2 (4) | Ba—Mg_m2—W_cxiii | 180.0 (5) |
Na_axx—Ba—O3x | 86.5 (3) | Ba—Mg_m2—Ti_m2 | 0 |
Na_axx—Ba—Oh | 145.1 (3) | Baxiii—Mg_m2—W_c | 180.0 (5) |
Na_axx—Ba—Ohx | 44.01 (19) | Baxiii—Mg_m2—W_cxiii | 0.0 (5) |
Na_axx—Ba—Baxvi | 55.89 (13) | Baxiii—Mg_m2—Ti_m2 | 0 |
Na_axx—Ba—Baxiii | 89.8 (3) | W_c—Mg_m2—W_cxiii | 180.0 (5) |
Na_axx—Ba—W2 | 86.6 (2) | W_c—Mg_m2—Ti_m2 | 0 |
Na_axx—Ba—W2xvii | 27.3 (2) | W_cxiii—Mg_m2—Ti_m2 | 0 |
Na_axx—Ba—W_c | 0 | | |
Symmetry codes: (i) −x+1, y, −z; (ii) x, y, z−1; (iii) −x+1, y, −z+1; (iv) −x+1/2, −y+1/2, −z+1; (v) −x+1/2, −y+1/2, −z; (vi) x+1/2, y+1/2, z; (vii) −x+1/2, y+1/2, −z; (viii) −x+1, y, −z+2; (ix) −x+1, −y, −z+1; (x) x, −y, z; (xi) x, y, z+1; (xii) −x+1/2, y+1/2, −z+1; (xiii) −x, y, −z+1; (xiv) x−1/2, −y+1/2, z; (xv) −x, −y, −z+1; (xvi) −x, y, −z; (xvii) −x, −y, −z; (xviii) −x+1/2, y−1/2, −z+1; (xix) x, −y, z+1; (xx) x−1/2, y−1/2, z; (xxi) −x+1/2, y−1/2, −z. |
Crystal data top
Ba0.7Fe0.5K2.1Mg0.05Na2Nb0.1O33Si8Ti4 | Z = 2 |
Mr = 1206.8 | F(000) = 1167 |
Monoclinic, C2/m | Dx = 3.370 Mg m−3 |
Hall symbol: -C 2y | Synchrotron radiation, λ = 0.414 Å |
a = 13.645 (8) Å | Cell parameters from 2849 reflections |
b = 13.2460 (7) Å | θ = 1.8–19.0° |
c = 7.3265 (17) Å | µ = 0.89 mm−1 |
β = 116.11 (4)° | T = 293 K |
V = 1189.0 (8) Å3 | Anhedral grain |
Data collection top
ESRF ID 09 diffractometer | θmax = 19.0°, θmin = 1.8° |
2849 measured reflections | h = −8→7 |
857 independent reflections | k = −20→20 |
595 reflections with I > 2σ(I) | l = −10→10 |
Rint = 0.049 | |
Refinement top
Refinement on F | 0 restraints |
R[F2 > 2σ(F2)] = 0.075 | 6 constraints |
wR(F2) = 0.132 | Weighting scheme based on measured s.u.'s w = 1/(σ2(F) + 0.0100000007F2) |
S = 1.04 | (Δ/σ)max = 0.049 |
857 reflections | Δρmax = 0.99 e Å−3 |
68 parameters | Δρmin = −1.04 e Å−3 |
Fractional atomic coordinates and isotropic or equivalent isotropic displacement parameters (Å2) top | x | y | z | Uiso*/Ueq | Occ. (<1) |
Na_a | 0.4184 (17) | 0.2701 (6) | 0.0103 (14) | 0.029 (11) | 0.5 |
K_b | 0.4306 (6) | 0 | 0.7244 (4) | 0.028 (4) | |
Ti_m1(1) | 0.25 | 0.25 | 0.5 | 0.0151 (6)* | 0.95 |
Ti_m1(2) | 0 | 0.21864 (16) | 0.5 | 0.0139 (6)* | |
Fe_m2 | 0 | 0 | 0.5 | 0.0250 (12)* | 0.5 |
Si1 | 0.3284 (5) | 0.10984 (15) | 0.2667 (3) | 0.0082 (6)* | |
Si2 | 0.2109 (4) | 0.10896 (14) | 0.8159 (3) | 0.0074 (6)* | |
O1 | 0.0799 (11) | 0.1076 (4) | 0.6810 (9) | 0.0100 (13)* | |
O2 | 0.2721 (11) | 0.1962 (4) | 0.7605 (9) | 0.0105 (12)* | |
O3 | 0.2829 (12) | 0.1170 (4) | 0.4316 (9) | 0.0106 (12)* | |
O4 | 0.3859 (16) | 0 | 0.2875 (12) | 0.0091 (16)* | |
O5 | 0.2617 (16) | 0 | 0.7953 (12) | 0.0090 (16)* | |
O6 | 0.4212 (12) | 0.1889 (5) | 0.2901 (10) | 0.0182 (15)* | |
O7 | 0.2246 (12) | 0.1179 (4) | 0.0454 (9) | 0.0111 (13)* | |
Oh | 0.0983 (11) | 0.2117 (4) | 0.3840 (9) | 0.0102 (12)* | |
Ba | 0.0943 (4) | 0 | 0.3384 (3) | 0.0142 (5)* | 0.35 |
W1 | 0.5 | 0.1448 (8) | 0 | 0.055 (15) | |
W2 | 0 | 0.1075 (7) | 0 | 0.028 (3)* | |
W_c | 0.0943 (4) | 0 | 0.3384 (3) | 0.0142 (5)* | 0.65 |
Nb_m1(1) | 0.25 | 0.25 | 0.5 | 0.0151 (6)* | 0.05 |
Ti_m2 | 0 | 0 | 0.5 | 0.0250 (12)* | 0.1 |
Mg_m2 | 0 | 0 | 0.5 | 0.0250 (12)* | 0.05 |
Atomic displacement parameters (Å2) top | U11 | U22 | U33 | U12 | U13 | U23 |
Na_a | 0.02 (2) | 0.023 (4) | 0.034 (5) | −0.006 (5) | 0.007 (8) | −0.001 (3) |
K_b | 0.030 (10) | 0.0337 (16) | 0.0119 (12) | 0 | 0.003 (2) | 0 |
W1 | 0.10 (4) | 0.029 (5) | 0.019 (5) | 0 | 0.009 (9) | 0 |
Geometric parameters (Å, º) top
Na_a—Na_ai | 2.30 (3) | Ti_m1(2)—Ba | 3.576 (3) |
Na_a—K_bii | 4.186 (11) | Ti_m1(2)—Baxiii | 3.576 (3) |
Na_a—K_biii | 4.159 (10) | Ti_m1(2)—Ti_m2 | 2.896 (2) |
Na_a—Ti_m1(1)ii | 3.430 (10) | Ti_m1(2)—Mg_m2 | 2.896 (2) |
Na_a—Ti_m1(2)iv | 3.259 (10) | Fe_m2—O1 | 1.925 (6) |
Na_a—Si2iv | 3.05 (2) | Fe_m2—O1xiii | 1.925 (6) |
Na_a—O2ii | 2.253 (16) | Fe_m2—O1xv | 1.925 (6) |
Na_a—O6 | 2.301 (16) | Fe_m2—O1x | 1.925 (6) |
Na_a—O7v | 2.34 (2) | Fe_m2—Ba | 2.097 (5) |
Na_a—Bavi | 3.967 (11) | Fe_m2—Baxiii | 2.097 (5) |
Na_a—Bavii | 3.929 (11) | Fe_m2—W_c | 2.097 (5) |
Na_a—W1 | 2.018 (17) | Fe_m2—W_cxiii | 2.097 (5) |
Na_a—W2v | 1.987 (17) | Fe_m2—Ti_m2 | 0 |
Na_a—Nb_m1(1)ii | 3.430 (10) | Fe_m2—Mg_m2 | 0 |
K_b—K_biii | 4.459 (10) | Si1—O3 | 1.586 (15) |
K_b—K_bviii | 3.628 (5) | Si1—O4 | 1.628 (10) |
K_b—Si1 | 3.345 (4) | Si1—O6 | 1.593 (14) |
K_b—Si1iii | 3.571 (10) | Si1—O7 | 1.620 (9) |
K_b—Si1ix | 3.571 (10) | Si2—O1 | 1.618 (14) |
K_b—Si1x | 3.345 (4) | Si2—O2 | 1.580 (12) |
K_b—Si2 | 3.645 (10) | Si2—O5 | 1.636 (11) |
K_b—Si2x | 3.645 (10) | Si2—O7xi | 1.613 (9) |
K_b—O3 | 2.694 (9) | Si2—Ba | 3.457 (4) |
K_b—O3x | 2.694 (9) | O1—Baxiii | 2.721 (14) |
K_b—O4iii | 2.54 (2) | O1—Ti_m2 | 1.925 (6) |
K_b—O5 | 2.58 (2) | O1—Mg_m2 | 1.925 (6) |
K_b—Ba | 4.199 (10) | O2—Nb_m1(1) | 1.932 (7) |
K_b—W1xi | 2.640 (8) | O3—Ba | 2.818 (15) |
K_b—W1ix | 2.640 (8) | O3—Nb_m1(1) | 1.937 (8) |
Ti_m1(1)—O2 | 1.932 (7) | Oh—Ba | 2.821 (5) |
Ti_m1(1)—O2iv | 1.932 (7) | Oh—Nb_m1(1) | 1.928 (13) |
Ti_m1(1)—O3 | 1.937 (8) | Ba—Baxvi | 4.470 (5) |
Ti_m1(1)—O3iv | 1.937 (8) | Ba—Baxiii | 4.194 (7) |
Ti_m1(1)—Oh | 1.928 (13) | Ba—W2 | 2.650 (6) |
Ti_m1(1)—Ohiv | 1.928 (13) | Ba—W2xvii | 2.650 (6) |
Ti_m1(1)—Ba | 3.830 (3) | Ba—W_c | 0 |
Ti_m1(1)—Baxii | 3.830 (3) | Ba—Nb_m1(1) | 3.830 (3) |
Ti_m1(1)—Nb_m1(1) | 0 | Ba—Nb_m1(1)xviii | 3.830 (3) |
Ti_m1(2)—O1 | 1.960 (6) | Ba—Ti_m2 | 2.097 (5) |
Ti_m1(2)—O1xiii | 1.960 (6) | Ba—Mg_m2 | 2.097 (5) |
Ti_m1(2)—O6iv | 1.888 (7) | W_c—Ti_m2 | 2.097 (5) |
Ti_m1(2)—O6xiv | 1.888 (7) | W_c—Mg_m2 | 2.097 (5) |
Ti_m1(2)—Oh | 1.879 (14) | Ti_m2—Mg_m2 | 0 |
Ti_m1(2)—Ohxiii | 1.879 (14) | | |
| | | |
Na_ai—Na_a—K_bii | 73.4 (4) | Na_axx—Ba—Nb_m1(1) | 163.04 (19) |
Na_ai—Na_a—K_biii | 74.7 (4) | Na_axx—Ba—Nb_m1(1)xviii | 68.2 (2) |
Na_ai—Na_a—Ti_m1(1)ii | 97.6 (5) | Na_axx—Ba—Ti_m2 | 89.1 (3) |
Na_ai—Na_a—Ti_m1(2)iv | 101.6 (5) | Na_axx—Ba—Mg_m2 | 89.1 (3) |
Na_ai—Na_a—Si2iv | 141.6 (5) | Na_axxi—Ba—Na_av | 101.6 (2) |
Na_ai—Na_a—O2ii | 119.0 (8) | Na_axxi—Ba—Na_axiv | 111.0 (2) |
Na_ai—Na_a—O6 | 115.0 (7) | Na_axxi—Ba—K_b | 99.2 (3) |
Na_ai—Na_a—O7v | 138.3 (6) | Na_axxi—Ba—Ti_m1(1) | 136.9 (3) |
Na_ai—Na_a—Bavi | 72.2 (4) | Na_axxi—Ba—Ti_m1(1)xviii | 52.45 (16) |
Na_ai—Na_a—Bavii | 74.0 (4) | Na_axxi—Ba—Ti_m1(2) | 157.5 (3) |
Na_ai—Na_a—W1 | 55.3 (6) | Na_axxi—Ba—Ti_m1(2)xv | 70.6 (2) |
Na_ai—Na_a—W2v | 54.7 (6) | Na_axxi—Ba—Fe_m2 | 120.3 (3) |
Na_ai—Na_a—Nb_m1(1)ii | 97.6 (5) | Na_axxi—Ba—Si2 | 148.25 (19) |
K_bii—Na_a—K_biii | 51.54 (14) | Na_axxi—Ba—Si2x | 101.73 (14) |
K_bii—Na_a—Ti_m1(1)ii | 62.83 (16) | Na_axxi—Ba—O1xiii | 125.8 (3) |
K_bii—Na_a—Ti_m1(2)iv | 121.4 (2) | Na_axxi—Ba—O1xv | 76.9 (4) |
K_bii—Na_a—Si2iv | 144.7 (6) | Na_axxi—Ba—O3 | 111.0 (4) |
K_bii—Na_a—O2ii | 55.8 (4) | Na_axxi—Ba—O3x | 60.4 (3) |
K_bii—Na_a—O6 | 93.3 (3) | Na_axxi—Ba—Oh | 147.2 (3) |
K_bii—Na_a—O7v | 131.9 (5) | Na_axxi—Ba—Ohx | 45.6 (2) |
K_bii—Na_a—Bavi | 144.4 (6) | Na_axxi—Ba—Baxvi | 55.92 (15) |
K_bii—Na_a—Bavii | 109.7 (3) | Na_axxi—Ba—Baxiii | 120.3 (3) |
K_bii—Na_a—W1 | 30.1 (2) | Na_axxi—Ba—W2 | 86.8 (2) |
K_bii—Na_a—W2v | 122.2 (8) | Na_axxi—Ba—W2xvii | 27.2 (3) |
K_bii—Na_a—Nb_m1(1)ii | 62.83 (16) | Na_axxi—Ba—W_c | 0 |
K_biii—Na_a—Ti_m1(1)ii | 113.5 (2) | Na_axxi—Ba—Nb_m1(1) | 136.9 (3) |
K_biii—Na_a—Ti_m1(2)iv | 70.48 (17) | Na_axxi—Ba—Nb_m1(1)xviii | 52.45 (16) |
K_biii—Na_a—Si2iv | 121.1 (4) | Na_axxi—Ba—Ti_m2 | 120.3 (3) |
K_biii—Na_a—O2ii | 94.9 (3) | Na_axxi—Ba—Mg_m2 | 120.3 (3) |
K_biii—Na_a—O6 | 51.0 (4) | Na_av—Ba—Na_axiv | 33.8 (5) |
K_biii—Na_a—O7v | 146.2 (8) | Na_av—Ba—K_b | 99.2 (3) |
K_biii—Na_a—Bavi | 109.5 (3) | Na_av—Ba—Ti_m1(1) | 52.45 (16) |
K_biii—Na_a—Bavii | 147.3 (6) | Na_av—Ba—Ti_m1(1)xviii | 136.9 (3) |
K_biii—Na_a—W1 | 30.9 (2) | Na_av—Ba—Ti_m1(2) | 70.6 (2) |
K_biii—Na_a—W2v | 123.3 (8) | Na_av—Ba—Ti_m1(2)xv | 157.5 (3) |
K_biii—Na_a—Nb_m1(1)ii | 113.5 (2) | Na_av—Ba—Fe_m2 | 120.3 (3) |
Ti_m1(1)ii—Na_a—Ti_m1(2)iv | 160.7 (8) | Na_av—Ba—Si2 | 101.73 (14) |
Ti_m1(1)ii—Na_a—Si2iv | 105.3 (5) | Na_av—Ba—Si2x | 148.25 (19) |
Ti_m1(1)ii—Na_a—O2ii | 32.0 (3) | Na_av—Ba—O1xiii | 76.9 (4) |
Ti_m1(1)ii—Na_a—O6 | 132.5 (7) | Na_av—Ba—O1xv | 125.8 (3) |
Ti_m1(1)ii—Na_a—O7v | 75.6 (4) | Na_av—Ba—O3 | 60.4 (3) |
Ti_m1(1)ii—Na_a—Bavi | 131.0 (3) | Na_av—Ba—O3x | 111.0 (4) |
Ti_m1(1)ii—Na_a—Bavii | 62.28 (16) | Na_av—Ba—Oh | 45.6 (2) |
Ti_m1(1)ii—Na_a—W1 | 90.7 (3) | Na_av—Ba—Ohx | 147.2 (3) |
Ti_m1(1)ii—Na_a—W2v | 98.0 (4) | Na_av—Ba—Baxvi | 55.92 (15) |
Ti_m1(1)ii—Na_a—Nb_m1(1)ii | 0.0 (5) | Na_av—Ba—Baxiii | 120.3 (3) |
Ti_m1(2)iv—Na_a—Si2iv | 59.7 (3) | Na_av—Ba—W2 | 27.2 (3) |
Ti_m1(2)iv—Na_a—O2ii | 131.7 (8) | Na_av—Ba—W2xvii | 86.8 (2) |
Ti_m1(2)iv—Na_a—O6 | 34.6 (2) | Na_av—Ba—W_c | 0 |
Ti_m1(2)iv—Na_a—O7v | 91.0 (5) | Na_av—Ba—Nb_m1(1) | 52.45 (16) |
Ti_m1(2)iv—Na_a—Bavi | 58.34 (15) | Na_av—Ba—Nb_m1(1)xviii | 136.9 (3) |
Ti_m1(2)iv—Na_a—Bavii | 125.2 (2) | Na_av—Ba—Ti_m2 | 120.3 (3) |
Ti_m1(2)iv—Na_a—W1 | 98.7 (3) | Na_av—Ba—Mg_m2 | 120.3 (3) |
Ti_m1(2)iv—Na_a—W2v | 94.5 (3) | Na_axiv—Ba—K_b | 126.8 (3) |
Ti_m1(2)iv—Na_a—Nb_m1(1)ii | 160.7 (8) | Na_axiv—Ba—Ti_m1(1) | 68.2 (2) |
Si2iv—Na_a—O2ii | 95.7 (8) | Na_axiv—Ba—Ti_m1(1)xviii | 163.04 (19) |
Si2iv—Na_a—O6 | 70.0 (6) | Na_axiv—Ba—Ti_m1(2) | 50.87 (19) |
Si2iv—Na_a—O7v | 31.5 (3) | Na_axiv—Ba—Ti_m1(2)xv | 127.8 (3) |
Si2iv—Na_a—Bavi | 69.5 (2) | Na_axiv—Ba—Fe_m2 | 89.1 (3) |
Si2iv—Na_a—Bavii | 89.8 (2) | Na_axiv—Ba—Si2 | 100.31 (15) |
Si2iv—Na_a—W1 | 151.5 (6) | Na_axiv—Ba—Si2x | 145.1 (2) |
Si2iv—Na_a—W2v | 91.4 (4) | Na_axiv—Ba—O1xiii | 44.3 (4) |
Si2iv—Na_a—Nb_m1(1)ii | 105.3 (5) | Na_axiv—Ba—O1xv | 95.1 (4) |
O2ii—Na_a—O6 | 100.5 (8) | Na_axiv—Ba—O3 | 88.2 (3) |
O2ii—Na_a—O7v | 76.2 (7) | Na_axiv—Ba—O3x | 144.4 (4) |
O2ii—Na_a—Bavi | 155.4 (5) | Na_axiv—Ba—Oh | 44.3 (2) |
O2ii—Na_a—Bavii | 92.2 (3) | Na_axiv—Ba—Ohx | 144.1 (3) |
O2ii—Na_a—W1 | 85.3 (4) | Na_axiv—Ba—Baxvi | 55.13 (15) |
O2ii—Na_a—W2v | 129.4 (5) | Na_axiv—Ba—Baxiii | 89.1 (3) |
O2ii—Na_a—Nb_m1(1)ii | 32.0 (3) | Na_axiv—Ba—W2 | 26.5 (3) |
O6—Na_a—O7v | 97.9 (9) | Na_axiv—Ba—W2xvii | 86.0 (2) |
O6—Na_a—Bavi | 92.9 (3) | Na_axiv—Ba—W_c | 0 |
O6—Na_a—Bavii | 157.0 (5) | Na_axiv—Ba—Nb_m1(1) | 68.2 (2) |
O6—Na_a—W1 | 81.7 (4) | Na_axiv—Ba—Nb_m1(1)xviii | 163.04 (19) |
O6—Na_a—W2v | 128.7 (5) | Na_axiv—Ba—Ti_m2 | 89.1 (3) |
O6—Na_a—Nb_m1(1)ii | 132.5 (7) | Na_axiv—Ba—Mg_m2 | 89.1 (3) |
O7v—Na_a—Bavi | 81.6 (3) | K_b—Ba—Ti_m1(1) | 59.91 (6) |
O7v—Na_a—Bavii | 66.5 (4) | K_b—Ba—Ti_m1(1)xviii | 59.91 (6) |
O7v—Na_a—W1 | 161.1 (8) | K_b—Ba—Ti_m1(2) | 102.88 (7) |
O7v—Na_a—W2v | 85.1 (5) | K_b—Ba—Ti_m1(2)xv | 102.88 (7) |
O7v—Na_a—Nb_m1(1)ii | 75.6 (4) | K_b—Ba—Fe_m2 | 112.34 (11) |
Bavi—Na_a—Bavii | 68.95 (19) | K_b—Ba—Si2 | 55.86 (13) |
Bavi—Na_a—W1 | 117.2 (7) | K_b—Ba—Si2x | 55.86 (13) |
Bavi—Na_a—W2v | 36.57 (18) | K_b—Ba—O1xiii | 134.91 (16) |
Bavi—Na_a—Nb_m1(1)ii | 131.0 (3) | K_b—Ba—O1xv | 134.91 (16) |
Bavii—Na_a—W1 | 118.7 (7) | K_b—Ba—O3 | 39.31 (15) |
Bavii—Na_a—W2v | 37.63 (19) | K_b—Ba—O3x | 39.31 (15) |
Bavii—Na_a—Nb_m1(1)ii | 62.28 (16) | K_b—Ba—Oh | 87.8 (2) |
W1—Na_a—W2v | 110.0 (11) | K_b—Ba—Ohx | 87.8 (2) |
W1—Na_a—Nb_m1(1)ii | 90.7 (3) | K_b—Ba—Baxvi | 132.22 (16) |
W2v—Na_a—Nb_m1(1)ii | 98.0 (4) | K_b—Ba—Baxiii | 112.34 (11) |
Na_axi—K_b—Na_aiii | 32.0 (4) | K_b—Ba—W2 | 124.52 (17) |
Na_axi—K_b—Na_aix | 128.46 (19) | K_b—Ba—W2xvii | 124.52 (17) |
Na_axi—K_b—Na_axix | 117.5 (3) | K_b—Ba—W_c | 0 |
Na_axi—K_b—K_biii | 119.5 (3) | K_b—Ba—Nb_m1(1) | 59.91 (6) |
Na_axi—K_b—K_bviii | 63.85 (14) | K_b—Ba—Nb_m1(1)xviii | 59.91 (6) |
Na_axi—K_b—Si1 | 92.24 (14) | K_b—Ba—Ti_m2 | 112.34 (11) |
Na_axi—K_b—Si1iii | 83.2 (3) | K_b—Ba—Mg_m2 | 112.34 (11) |
Na_axi—K_b—Si1ix | 125.3 (3) | Ti_m1(1)—Ba—Ti_m1(1)xviii | 119.69 (12) |
Na_axi—K_b—Si1x | 141.49 (18) | Ti_m1(1)—Ba—Ti_m1(2) | 55.17 (3) |
Na_axi—K_b—Si2 | 49.7 (3) | Ti_m1(1)—Ba—Ti_m1(2)xv | 146.05 (7) |
Na_axi—K_b—Si2x | 91.7 (3) | Ti_m1(1)—Ba—Fe_m2 | 102.73 (6) |
Na_axi—K_b—O3 | 74.1 (2) | Ti_m1(1)—Ba—Si2 | 51.73 (7) |
Na_axi—K_b—O3x | 135.2 (5) | Ti_m1(1)—Ba—Si2x | 95.89 (8) |
Na_axi—K_b—O4iii | 105.9 (3) | Ti_m1(1)—Ba—O1xiii | 85.21 (19) |
Na_axi—K_b—O5 | 70.3 (3) | Ti_m1(1)—Ba—O1xv | 145.3 (2) |
Na_axi—K_b—Ba | 93.7 (3) | Ti_m1(1)—Ba—O3 | 29.1 (2) |
Na_axi—K_b—W1xi | 22.5 (3) | Ti_m1(1)—Ba—O3x | 94.4 (2) |
Na_axi—K_b—W1ix | 108.5 (2) | Ti_m1(1)—Ba—Oh | 29.0 (3) |
Na_aiii—K_b—Na_aix | 118.7 (3) | Ti_m1(1)—Ba—Ohx | 147.5 (3) |
Na_aiii—K_b—Na_axix | 128.46 (19) | Ti_m1(1)—Ba—Baxvi | 108.24 (6) |
Na_aiii—K_b—K_biii | 93.5 (3) | Ti_m1(1)—Ba—Baxiii | 102.73 (6) |
Na_aiii—K_b—K_bviii | 64.61 (15) | Ti_m1(1)—Ba—W2 | 78.43 (17) |
Na_aiii—K_b—Si1 | 89.81 (14) | Ti_m1(1)—Ba—W2xvii | 136.77 (18) |
Na_aiii—K_b—Si1iii | 51.5 (3) | Ti_m1(1)—Ba—W_c | 0 |
Na_aiii—K_b—Si1ix | 94.5 (3) | Ti_m1(1)—Ba—Nb_m1(1) | 0.0 (5) |
Na_aiii—K_b—Si1x | 138.1 (2) | Ti_m1(1)—Ba—Nb_m1(1)xviii | 119.69 (12) |
Na_aiii—K_b—Si2 | 81.5 (3) | Ti_m1(1)—Ba—Ti_m2 | 102.73 (6) |
Na_aiii—K_b—Si2x | 122.2 (3) | Ti_m1(1)—Ba—Mg_m2 | 102.73 (6) |
Na_aiii—K_b—O3 | 85.4 (2) | Ti_m1(1)xviii—Ba—Ti_m1(2) | 146.05 (7) |
Na_aiii—K_b—O3x | 155.5 (2) | Ti_m1(1)xviii—Ba—Ti_m1(2)xv | 55.17 (3) |
Na_aiii—K_b—O4iii | 73.9 (3) | Ti_m1(1)xviii—Ba—Fe_m2 | 102.73 (6) |
Na_aiii—K_b—O5 | 102.1 (3) | Ti_m1(1)xviii—Ba—Si2 | 95.89 (8) |
Na_aiii—K_b—Ba | 119.0 (3) | Ti_m1(1)xviii—Ba—Si2x | 51.73 (7) |
Na_aiii—K_b—W1xi | 23.1 (3) | Ti_m1(1)xviii—Ba—O1xiii | 145.3 (2) |
Na_aiii—K_b—W1ix | 109.3 (2) | Ti_m1(1)xviii—Ba—O1xv | 85.21 (19) |
Na_aix—K_b—Na_axix | 32.0 (4) | Ti_m1(1)xviii—Ba—O3 | 94.4 (2) |
Na_aix—K_b—K_biii | 93.5 (3) | Ti_m1(1)xviii—Ba—O3x | 29.1 (2) |
Na_aix—K_b—K_bviii | 64.61 (15) | Ti_m1(1)xviii—Ba—Oh | 147.5 (3) |
Na_aix—K_b—Si1 | 138.1 (2) | Ti_m1(1)xviii—Ba—Ohx | 29.0 (3) |
Na_aix—K_b—Si1iii | 94.5 (3) | Ti_m1(1)xviii—Ba—Baxvi | 108.24 (6) |
Na_aix—K_b—Si1ix | 51.5 (3) | Ti_m1(1)xviii—Ba—Baxiii | 102.73 (6) |
Na_aix—K_b—Si1x | 89.81 (14) | Ti_m1(1)xviii—Ba—W2 | 136.77 (18) |
Na_aix—K_b—Si2 | 122.2 (3) | Ti_m1(1)xviii—Ba—W2xvii | 78.43 (17) |
Na_aix—K_b—Si2x | 81.5 (3) | Ti_m1(1)xviii—Ba—W_c | 0 |
Na_aix—K_b—O3 | 155.5 (2) | Ti_m1(1)xviii—Ba—Nb_m1(1) | 119.69 (12) |
Na_aix—K_b—O3x | 85.4 (2) | Ti_m1(1)xviii—Ba—Nb_m1(1)xviii | 0.0 (5) |
Na_aix—K_b—O4iii | 73.9 (3) | Ti_m1(1)xviii—Ba—Ti_m2 | 102.73 (6) |
Na_aix—K_b—O5 | 102.1 (3) | Ti_m1(1)xviii—Ba—Mg_m2 | 102.73 (6) |
Na_aix—K_b—Ba | 119.0 (3) | Ti_m1(2)—Ba—Ti_m1(2)xv | 108.19 (13) |
Na_aix—K_b—W1xi | 109.3 (2) | Ti_m1(2)—Ba—Fe_m2 | 54.09 (7) |
Na_aix—K_b—W1ix | 23.1 (3) | Ti_m1(2)—Ba—Si2 | 53.08 (8) |
Na_axix—K_b—K_biii | 119.5 (3) | Ti_m1(2)—Ba—Si2x | 94.34 (9) |
Na_axix—K_b—K_bviii | 63.85 (14) | Ti_m1(2)—Ba—O1xiii | 32.84 (16) |
Na_axix—K_b—Si1 | 141.49 (18) | Ti_m1(2)—Ba—O1xv | 90.5 (2) |
Na_axix—K_b—Si1iii | 125.3 (3) | Ti_m1(2)—Ba—O3 | 84.1 (2) |
Na_axix—K_b—Si1ix | 83.2 (3) | Ti_m1(2)—Ba—O3x | 142.04 (15) |
Na_axix—K_b—Si1x | 92.24 (14) | Ti_m1(2)—Ba—Oh | 31.4 (3) |
Na_axix—K_b—Si2 | 91.7 (3) | Ti_m1(2)—Ba—Ohx | 139.2 (3) |
Na_axix—K_b—Si2x | 49.7 (3) | Ti_m1(2)—Ba—Baxvi | 104.59 (7) |
Na_axix—K_b—O3 | 135.2 (5) | Ti_m1(2)—Ba—Baxiii | 54.09 (7) |
Na_axix—K_b—O3x | 74.1 (2) | Ti_m1(2)—Ba—W2 | 77.13 (16) |
Na_axix—K_b—O4iii | 105.9 (3) | Ti_m1(2)—Ba—W2xvii | 130.37 (18) |
Na_axix—K_b—O5 | 70.3 (3) | Ti_m1(2)—Ba—W_c | 0 |
Na_axix—K_b—Ba | 93.7 (3) | Ti_m1(2)—Ba—Nb_m1(1) | 55.17 (3) |
Na_axix—K_b—W1xi | 108.5 (2) | Ti_m1(2)—Ba—Nb_m1(1)xviii | 146.05 (7) |
Na_axix—K_b—W1ix | 22.5 (3) | Ti_m1(2)—Ba—Ti_m2 | 54.09 (7) |
K_biii—K_b—K_bviii | 129.6 (3) | Ti_m1(2)—Ba—Mg_m2 | 54.09 (7) |
K_biii—K_b—Si1 | 52.11 (15) | Ti_m1(2)xv—Ba—Fe_m2 | 54.09 (7) |
K_biii—K_b—Si1iii | 47.67 (12) | Ti_m1(2)xv—Ba—Si2 | 94.34 (9) |
K_biii—K_b—Si1ix | 47.67 (12) | Ti_m1(2)xv—Ba—Si2x | 53.08 (8) |
K_biii—K_b—Si1x | 52.11 (15) | Ti_m1(2)xv—Ba—O1xiii | 90.5 (2) |
K_biii—K_b—Si2 | 141.84 (10) | Ti_m1(2)xv—Ba—O1xv | 32.84 (16) |
K_biii—K_b—Si2x | 141.84 (10) | Ti_m1(2)xv—Ba—O3 | 142.04 (15) |
K_biii—K_b—O3 | 79.9 (3) | Ti_m1(2)xv—Ba—O3x | 84.1 (2) |
K_biii—K_b—O3x | 79.9 (3) | Ti_m1(2)xv—Ba—Oh | 139.2 (3) |
K_biii—K_b—O4iii | 39.7 (2) | Ti_m1(2)xv—Ba—Ohx | 31.4 (3) |
K_biii—K_b—O5 | 149.0 (2) | Ti_m1(2)xv—Ba—Baxvi | 104.59 (7) |
K_biii—K_b—Ba | 101.33 (12) | Ti_m1(2)xv—Ba—Baxiii | 54.09 (7) |
K_biii—K_b—W1xi | 116.0 (2) | Ti_m1(2)xv—Ba—W2 | 130.37 (18) |
K_biii—K_b—W1ix | 116.0 (2) | Ti_m1(2)xv—Ba—W2xvii | 77.13 (16) |
K_bviii—K_b—Si1 | 154.01 (5) | Ti_m1(2)xv—Ba—W_c | 0 |
K_bviii—K_b—Si1iii | 87.37 (18) | Ti_m1(2)xv—Ba—Nb_m1(1) | 146.05 (7) |
K_bviii—K_b—Si1ix | 87.37 (18) | Ti_m1(2)xv—Ba—Nb_m1(1)xviii | 55.17 (3) |
K_bviii—K_b—Si1x | 154.01 (5) | Ti_m1(2)xv—Ba—Ti_m2 | 54.09 (7) |
K_bviii—K_b—Si2 | 82.19 (18) | Ti_m1(2)xv—Ba—Mg_m2 | 54.09 (7) |
K_bviii—K_b—Si2x | 82.19 (18) | Fe_m2—Ba—Si2 | 63.40 (12) |
K_bviii—K_b—O3 | 136.7 (3) | Fe_m2—Ba—Si2x | 63.40 (12) |
K_bviii—K_b—O3x | 136.7 (3) | Fe_m2—Ba—O1xiii | 44.8 (2) |
K_bviii—K_b—O4iii | 89.9 (3) | Fe_m2—Ba—O1xv | 44.8 (2) |
K_bviii—K_b—O5 | 81.4 (3) | Fe_m2—Ba—O3 | 125.8 (2) |
K_bviii—K_b—Ba | 129.1 (3) | Fe_m2—Ba—O3x | 125.8 (2) |
K_bviii—K_b—W1xi | 46.59 (17) | Fe_m2—Ba—Oh | 85.3 (3) |
K_bviii—K_b—W1ix | 46.59 (17) | Fe_m2—Ba—Ohx | 85.3 (3) |
Si1—K_b—Si1iii | 79.36 (17) | Fe_m2—Ba—Baxvi | 115.44 (16) |
Si1—K_b—Si1ix | 99.8 (2) | Fe_m2—Ba—Baxiii | 0.0 (5) |
Si1—K_b—Si1x | 51.56 (7) | Fe_m2—Ba—W2 | 111.24 (18) |
Si1—K_b—Si2 | 89.91 (17) | Fe_m2—Ba—W2xvii | 111.24 (18) |
Si1—K_b—Si2x | 110.1 (2) | Fe_m2—Ba—W_c | 0 |
Si1—K_b—O3 | 27.9 (3) | Fe_m2—Ba—Nb_m1(1) | 102.73 (6) |
Si1—K_b—O3x | 67.44 (17) | Fe_m2—Ba—Nb_m1(1)xviii | 102.73 (6) |
Si1—K_b—O4iii | 87.0 (3) | Fe_m2—Ba—Ti_m2 | 0.0 (5) |
Si1—K_b—O5 | 100.8 (3) | Fe_m2—Ba—Mg_m2 | 0.0 (5) |
Si1—K_b—Ba | 58.34 (14) | Si2—Ba—Si2x | 49.35 (5) |
Si1—K_b—W1xi | 107.56 (17) | Si2—Ba—O1xiii | 80.61 (17) |
Si1—K_b—W1ix | 159.01 (19) | Si2—Ba—O1xv | 105.9 (2) |
Si1iii—K_b—Si1ix | 48.09 (14) | Si2—Ba—O3 | 63.9 (2) |
Si1iii—K_b—Si1x | 99.8 (2) | Si2—Ba—O3x | 91.15 (17) |
Si1iii—K_b—Si2 | 131.36 (8) | Si2—Ba—Oh | 59.27 (12) |
Si1iii—K_b—Si2x | 169.54 (11) | Si2—Ba—Ohx | 108.59 (13) |
Si1iii—K_b—O3 | 98.1 (4) | Si2—Ba—Baxvi | 155.01 (5) |
Si1iii—K_b—O3x | 127.5 (4) | Si2—Ba—Baxiii | 63.40 (13) |
Si1iii—K_b—O4iii | 24.20 (8) | Si2—Ba—W2 | 122.69 (18) |
Si1iii—K_b—O5 | 153.51 (11) | Si2—Ba—W2xvii | 171.40 (19) |
Si1iii—K_b—Ba | 137.49 (10) | Si2—Ba—W_c | 0 |
Si1iii—K_b—W1xi | 70.88 (15) | Si2—Ba—Nb_m1(1) | 51.73 (7) |
Si1iii—K_b—W1ix | 105.3 (2) | Si2—Ba—Nb_m1(1)xviii | 95.89 (8) |
Si1ix—K_b—Si1x | 79.36 (17) | Si2—Ba—Ti_m2 | 63.40 (12) |
Si1ix—K_b—Si2 | 169.54 (11) | Si2—Ba—Mg_m2 | 63.40 (12) |
Si1ix—K_b—Si2x | 131.36 (8) | Si2x—Ba—O1xiii | 105.9 (2) |
Si1ix—K_b—O3 | 127.5 (4) | Si2x—Ba—O1xv | 80.61 (17) |
Si1ix—K_b—O3x | 98.1 (4) | Si2x—Ba—O3 | 91.15 (17) |
Si1ix—K_b—O4iii | 24.20 (8) | Si2x—Ba—O3x | 63.9 (2) |
Si1ix—K_b—O5 | 153.51 (11) | Si2x—Ba—Oh | 108.59 (13) |
Si1ix—K_b—Ba | 137.49 (10) | Si2x—Ba—Ohx | 59.27 (12) |
Si1ix—K_b—W1xi | 105.3 (2) | Si2x—Ba—Baxvi | 155.01 (5) |
Si1ix—K_b—W1ix | 70.88 (15) | Si2x—Ba—Baxiii | 63.40 (13) |
Si1x—K_b—Si2 | 110.1 (2) | Si2x—Ba—W2 | 171.40 (19) |
Si1x—K_b—Si2x | 89.91 (17) | Si2x—Ba—W2xvii | 122.69 (18) |
Si1x—K_b—O3 | 67.44 (17) | Si2x—Ba—W_c | 0 |
Si1x—K_b—O3x | 27.9 (3) | Si2x—Ba—Nb_m1(1) | 95.89 (8) |
Si1x—K_b—O4iii | 87.0 (3) | Si2x—Ba—Nb_m1(1)xviii | 51.73 (7) |
Si1x—K_b—O5 | 100.8 (3) | Si2x—Ba—Ti_m2 | 63.40 (12) |
Si1x—K_b—Ba | 58.34 (14) | Si2x—Ba—Mg_m2 | 63.40 (12) |
Si1x—K_b—W1xi | 159.01 (19) | O1xiii—Ba—O1xv | 63.2 (3) |
Si1x—K_b—W1ix | 107.56 (17) | O1xiii—Ba—O3 | 114.1 (3) |
Si2—K_b—Si2x | 46.65 (13) | O1xiii—Ba—O3x | 169.8 (2) |
Si2—K_b—O3 | 62.0 (3) | O1xiii—Ba—Oh | 57.1 (4) |
Si2—K_b—O3x | 89.2 (4) | O1xiii—Ba—Ohx | 119.8 (4) |
Si2—K_b—O4iii | 155.22 (10) | O1xiii—Ba—Baxvi | 83.04 (16) |
Si2—K_b—O5 | 23.33 (7) | O1xiii—Ba—Baxiii | 44.82 (19) |
Si2—K_b—Ba | 51.72 (12) | O1xiii—Ba—W2 | 67.44 (19) |
Si2—K_b—W1xi | 67.60 (15) | O1xiii—Ba—W2xvii | 100.3 (2) |
Si2—K_b—W1ix | 101.2 (2) | O1xiii—Ba—W_c | 0 |
Si2x—K_b—O3 | 89.2 (4) | O1xiii—Ba—Nb_m1(1) | 85.21 (19) |
Si2x—K_b—O3x | 62.0 (3) | O1xiii—Ba—Nb_m1(1)xviii | 145.3 (2) |
Si2x—K_b—O4iii | 155.22 (10) | O1xiii—Ba—Ti_m2 | 44.8 (2) |
Si2x—K_b—O5 | 23.33 (7) | O1xiii—Ba—Mg_m2 | 44.8 (2) |
Si2x—K_b—Ba | 51.72 (12) | O1xv—Ba—O3 | 169.8 (2) |
Si2x—K_b—W1xi | 101.2 (2) | O1xv—Ba—O3x | 114.1 (3) |
Si2x—K_b—W1ix | 67.60 (15) | O1xv—Ba—Oh | 119.8 (4) |
O3—K_b—O3x | 70.2 (2) | O1xv—Ba—Ohx | 57.1 (4) |
O3—K_b—O4iii | 112.1 (4) | O1xv—Ba—Baxvi | 83.04 (16) |
O3—K_b—O5 | 74.8 (4) | O1xv—Ba—Baxiii | 44.82 (19) |
O3—K_b—Ba | 41.5 (3) | O1xv—Ba—W2 | 100.3 (2) |
O3—K_b—W1xi | 94.7 (2) | O1xv—Ba—W2xvii | 67.44 (19) |
O3—K_b—W1ix | 156.6 (5) | O1xv—Ba—W_c | 0 |
O3x—K_b—O4iii | 112.1 (4) | O1xv—Ba—Nb_m1(1) | 145.3 (2) |
O3x—K_b—O5 | 74.8 (4) | O1xv—Ba—Nb_m1(1)xviii | 85.21 (19) |
O3x—K_b—Ba | 41.5 (3) | O1xv—Ba—Ti_m2 | 44.8 (2) |
O3x—K_b—W1xi | 156.6 (5) | O1xv—Ba—Mg_m2 | 44.8 (2) |
O3x—K_b—W1ix | 94.7 (2) | O3—Ba—O3x | 66.7 (3) |
O4iii—K_b—O5 | 171.3 (3) | O3—Ba—Oh | 57.1 (4) |
O4iii—K_b—Ba | 141.0 (2) | O3—Ba—Ohx | 123.4 (4) |
O4iii—K_b—W1xi | 89.9 (2) | O3—Ba—Baxvi | 106.69 (18) |
O4iii—K_b—W1ix | 89.9 (2) | O3—Ba—Baxiii | 125.8 (2) |
O5—K_b—Ba | 47.6 (2) | O3—Ba—W2 | 86.94 (19) |
O5—K_b—W1xi | 84.1 (2) | O3—Ba—W2xvii | 122.5 (3) |
O5—K_b—W1ix | 84.1 (2) | O3—Ba—W_c | 0 |
Ba—K_b—W1xi | 115.7 (2) | O3—Ba—Nb_m1(1) | 29.1 (2) |
Ba—K_b—W1ix | 115.7 (2) | O3—Ba—Nb_m1(1)xviii | 94.4 (2) |
W1xi—K_b—W1ix | 93.2 (3) | O3—Ba—Ti_m2 | 125.8 (2) |
Na_axi—Ti_m1(1)—Na_av | 180.0 (5) | O3—Ba—Mg_m2 | 125.8 (2) |
Na_axi—Ti_m1(1)—O2 | 38.2 (4) | O3x—Ba—Oh | 123.4 (4) |
Na_axi—Ti_m1(1)—O2iv | 141.8 (4) | O3x—Ba—Ohx | 57.1 (4) |
Na_axi—Ti_m1(1)—O3 | 103.4 (3) | O3x—Ba—Baxvi | 106.69 (18) |
Na_axi—Ti_m1(1)—O3iv | 76.6 (3) | O3x—Ba—Baxiii | 125.8 (2) |
Na_axi—Ti_m1(1)—Oh | 125.1 (5) | O3x—Ba—W2 | 122.5 (3) |
Na_axi—Ti_m1(1)—Ohiv | 54.9 (5) | O3x—Ba—W2xvii | 86.94 (19) |
Na_axi—Ti_m1(1)—Ba | 114.7 (2) | O3x—Ba—W_c | 0 |
Na_axi—Ti_m1(1)—Baxii | 65.3 (2) | O3x—Ba—Nb_m1(1) | 94.4 (2) |
Na_axi—Ti_m1(1)—Nb_m1(1) | 0 | O3x—Ba—Nb_m1(1)xviii | 29.1 (2) |
Na_av—Ti_m1(1)—O2 | 141.8 (4) | O3x—Ba—Ti_m2 | 125.8 (2) |
Na_av—Ti_m1(1)—O2iv | 38.2 (4) | O3x—Ba—Mg_m2 | 125.8 (2) |
Na_av—Ti_m1(1)—O3 | 76.6 (3) | Oh—Ba—Ohx | 167.2 (2) |
Na_av—Ti_m1(1)—O3iv | 103.4 (3) | Oh—Ba—Baxvi | 95.91 (12) |
Na_av—Ti_m1(1)—Oh | 54.9 (5) | Oh—Ba—Baxiii | 85.3 (3) |
Na_av—Ti_m1(1)—Ohiv | 125.1 (5) | Oh—Ba—W2 | 63.4 (2) |
Na_av—Ti_m1(1)—Ba | 65.3 (2) | Oh—Ba—W2xvii | 128.4 (2) |
Na_av—Ti_m1(1)—Baxii | 114.7 (2) | Oh—Ba—W_c | 0 |
Na_av—Ti_m1(1)—Nb_m1(1) | 0 | Oh—Ba—Nb_m1(1) | 29.0 (3) |
O2—Ti_m1(1)—O2iv | 180.0 (5) | Oh—Ba—Nb_m1(1)xviii | 147.5 (3) |
O2—Ti_m1(1)—O3 | 88.1 (3) | Oh—Ba—Ti_m2 | 85.3 (3) |
O2—Ti_m1(1)—O3iv | 91.9 (3) | Oh—Ba—Mg_m2 | 85.3 (3) |
O2—Ti_m1(1)—Oh | 90.5 (4) | Ohx—Ba—Baxvi | 95.91 (12) |
O2—Ti_m1(1)—Ohiv | 89.5 (4) | Ohx—Ba—Baxiii | 85.3 (3) |
O2—Ti_m1(1)—Ba | 79.1 (2) | Ohx—Ba—W2 | 128.4 (2) |
O2—Ti_m1(1)—Baxii | 100.9 (2) | Ohx—Ba—W2xvii | 63.4 (2) |
O2—Ti_m1(1)—Nb_m1(1) | 0 | Ohx—Ba—W_c | 0 |
O2iv—Ti_m1(1)—O3 | 91.9 (3) | Ohx—Ba—Nb_m1(1) | 147.5 (3) |
O2iv—Ti_m1(1)—O3iv | 88.1 (3) | Ohx—Ba—Nb_m1(1)xviii | 29.0 (3) |
O2iv—Ti_m1(1)—Oh | 89.5 (4) | Ohx—Ba—Ti_m2 | 85.3 (3) |
O2iv—Ti_m1(1)—Ohiv | 90.5 (4) | Ohx—Ba—Mg_m2 | 85.3 (3) |
O2iv—Ti_m1(1)—Ba | 100.9 (2) | Baxvi—Ba—Baxiii | 115.44 (14) |
O2iv—Ti_m1(1)—Baxii | 79.1 (2) | Baxvi—Ba—W2 | 32.50 (17) |
O2iv—Ti_m1(1)—Nb_m1(1) | 0 | Baxvi—Ba—W2xvii | 32.50 (17) |
O3—Ti_m1(1)—O3iv | 180.0 (5) | Baxvi—Ba—W_c | 0 |
O3—Ti_m1(1)—Oh | 88.4 (5) | Baxvi—Ba—Nb_m1(1) | 108.24 (6) |
O3—Ti_m1(1)—Ohiv | 91.6 (5) | Baxvi—Ba—Nb_m1(1)xviii | 108.24 (6) |
O3—Ti_m1(1)—Ba | 45.1 (5) | Baxvi—Ba—Ti_m2 | 115.44 (16) |
O3—Ti_m1(1)—Baxii | 134.9 (5) | Baxvi—Ba—Mg_m2 | 115.44 (16) |
O3—Ti_m1(1)—Nb_m1(1) | 0 | Baxiii—Ba—W2 | 111.24 (15) |
O3iv—Ti_m1(1)—Oh | 91.6 (5) | Baxiii—Ba—W2xvii | 111.24 (15) |
O3iv—Ti_m1(1)—Ohiv | 88.4 (5) | Baxiii—Ba—W_c | 0 |
O3iv—Ti_m1(1)—Ba | 134.9 (5) | Baxiii—Ba—Nb_m1(1) | 102.73 (6) |
O3iv—Ti_m1(1)—Baxii | 45.1 (5) | Baxiii—Ba—Nb_m1(1)xviii | 102.73 (6) |
O3iv—Ti_m1(1)—Nb_m1(1) | 0 | Baxiii—Ba—Ti_m2 | 0.0 (5) |
Oh—Ti_m1(1)—Ohiv | 180.0 (5) | Baxiii—Ba—Mg_m2 | 0.0 (5) |
Oh—Ti_m1(1)—Ba | 45.1 (2) | W2—Ba—W2xvii | 65.0 (2) |
Oh—Ti_m1(1)—Baxii | 134.9 (2) | W2—Ba—W_c | 0 |
Oh—Ti_m1(1)—Nb_m1(1) | 0 | W2—Ba—Nb_m1(1) | 78.43 (17) |
Ohiv—Ti_m1(1)—Ba | 134.9 (2) | W2—Ba—Nb_m1(1)xviii | 136.77 (18) |
Ohiv—Ti_m1(1)—Baxii | 45.1 (2) | W2—Ba—Ti_m2 | 111.24 (18) |
Ohiv—Ti_m1(1)—Nb_m1(1) | 0 | W2—Ba—Mg_m2 | 111.24 (18) |
Ba—Ti_m1(1)—Baxii | 180.0 (5) | W2xvii—Ba—W_c | 0 |
Ba—Ti_m1(1)—Nb_m1(1) | 0 | W2xvii—Ba—Nb_m1(1) | 136.77 (18) |
Baxii—Ti_m1(1)—Nb_m1(1) | 0 | W2xvii—Ba—Nb_m1(1)xviii | 78.43 (17) |
Na_aiv—Ti_m1(2)—Na_axiv | 174.8 (2) | W2xvii—Ba—Ti_m2 | 111.24 (18) |
Na_aiv—Ti_m1(2)—O1 | 58.0 (3) | W2xvii—Ba—Mg_m2 | 111.24 (18) |
Na_aiv—Ti_m1(2)—O1xiii | 126.7 (3) | W_c—Ba—Nb_m1(1) | 0 |
Na_aiv—Ti_m1(2)—O6iv | 43.7 (4) | W_c—Ba—Nb_m1(1)xviii | 0 |
Na_aiv—Ti_m1(2)—O6xiv | 131.5 (4) | W_c—Ba—Ti_m2 | 0 |
Na_aiv—Ti_m1(2)—Oh | 122.3 (5) | W_c—Ba—Mg_m2 | 0 |
Na_aiv—Ti_m1(2)—Ohxiii | 58.0 (5) | Nb_m1(1)—Ba—Nb_m1(1)xviii | 119.69 (12) |
Na_aiv—Ti_m1(2)—Ba | 113.8 (2) | Nb_m1(1)—Ba—Ti_m2 | 102.73 (6) |
Na_aiv—Ti_m1(2)—Baxiii | 70.8 (2) | Nb_m1(1)—Ba—Mg_m2 | 102.73 (6) |
Na_aiv—Ti_m1(2)—Ti_m2 | 92.62 (15) | Nb_m1(1)xviii—Ba—Ti_m2 | 102.73 (6) |
Na_aiv—Ti_m1(2)—Mg_m2 | 92.62 (15) | Nb_m1(1)xviii—Ba—Mg_m2 | 102.73 (6) |
Na_axiv—Ti_m1(2)—O1 | 126.7 (3) | Ti_m2—Ba—Mg_m2 | 0.0 (5) |
Na_axiv—Ti_m1(2)—O1xiii | 58.0 (3) | Na_a—W1—Na_ai | 69.4 (9) |
Na_axiv—Ti_m1(2)—O6iv | 131.5 (4) | Na_a—W1—K_bii | 127.4 (4) |
Na_axiv—Ti_m1(2)—O6xiv | 43.7 (4) | Na_a—W1—K_biii | 125.9 (4) |
Na_axiv—Ti_m1(2)—Oh | 58.0 (5) | Na_ai—W1—K_bii | 125.9 (4) |
Na_axiv—Ti_m1(2)—Ohxiii | 122.3 (5) | Na_ai—W1—K_biii | 127.4 (4) |
Na_axiv—Ti_m1(2)—Ba | 70.8 (2) | K_bii—W1—K_biii | 86.8 (3) |
Na_axiv—Ti_m1(2)—Baxiii | 113.8 (2) | Na_av—W2—Na_axiv | 70.6 (9) |
Na_axiv—Ti_m1(2)—Ti_m2 | 92.62 (15) | Na_av—W2—Ba | 115.1 (3) |
Na_axiv—Ti_m1(2)—Mg_m2 | 92.62 (15) | Na_av—W2—Baxvi | 116.9 (3) |
O1—Ti_m1(2)—O1xiii | 82.7 (3) | Na_axiv—W2—Ba | 116.9 (3) |
O1—Ti_m1(2)—O6iv | 89.3 (3) | Na_axiv—W2—Baxvi | 115.1 (3) |
O1—Ti_m1(2)—O6xiv | 170.4 (3) | Ba—W2—Baxvi | 115.0 (3) |
O1—Ti_m1(2)—Oh | 88.5 (5) | Fe_m2—W_c—Ba | 0 |
O1—Ti_m1(2)—Ohxiii | 87.3 (5) | Fe_m2—W_c—Ti_m2 | 0.0 (5) |
O1—Ti_m1(2)—Ba | 56.1 (3) | Fe_m2—W_c—Mg_m2 | 0.0 (5) |
O1—Ti_m1(2)—Baxiii | 48.8 (4) | Ba—W_c—Ti_m2 | 0 |
O1—Ti_m1(2)—Ti_m2 | 41.33 (19) | Ba—W_c—Mg_m2 | 0 |
O1—Ti_m1(2)—Mg_m2 | 41.33 (19) | Ti_m2—W_c—Mg_m2 | 0.0 (5) |
O1xiii—Ti_m1(2)—O6iv | 170.4 (3) | Na_axi—Nb_m1(1)—Na_av | 180.0 (5) |
O1xiii—Ti_m1(2)—O6xiv | 89.3 (3) | Na_axi—Nb_m1(1)—Ti_m1(1) | 0 |
O1xiii—Ti_m1(2)—Oh | 87.3 (5) | Na_axi—Nb_m1(1)—O2 | 38.2 (4) |
O1xiii—Ti_m1(2)—Ohxiii | 88.5 (5) | Na_axi—Nb_m1(1)—O2iv | 141.8 (4) |
O1xiii—Ti_m1(2)—Ba | 48.8 (4) | Na_axi—Nb_m1(1)—O3 | 103.4 (3) |
O1xiii—Ti_m1(2)—Baxiii | 56.1 (3) | Na_axi—Nb_m1(1)—O3iv | 76.6 (3) |
O1xiii—Ti_m1(2)—Ti_m2 | 41.33 (19) | Na_axi—Nb_m1(1)—Oh | 125.1 (5) |
O1xiii—Ti_m1(2)—Mg_m2 | 41.33 (19) | Na_axi—Nb_m1(1)—Ohiv | 54.9 (5) |
O6iv—Ti_m1(2)—O6xiv | 99.1 (3) | Na_axi—Nb_m1(1)—Ba | 114.7 (2) |
O6iv—Ti_m1(2)—Oh | 97.8 (6) | Na_axi—Nb_m1(1)—Baxii | 65.3 (2) |
O6iv—Ti_m1(2)—Ohxiii | 85.9 (5) | Na_av—Nb_m1(1)—Ti_m1(1) | 0 |
O6iv—Ti_m1(2)—Ba | 129.5 (4) | Na_av—Nb_m1(1)—O2 | 141.8 (4) |
O6iv—Ti_m1(2)—Baxiii | 114.5 (3) | Na_av—Nb_m1(1)—O2iv | 38.2 (4) |
O6iv—Ti_m1(2)—Ti_m2 | 130.4 (2) | Na_av—Nb_m1(1)—O3 | 76.6 (3) |
O6iv—Ti_m1(2)—Mg_m2 | 130.4 (2) | Na_av—Nb_m1(1)—O3iv | 103.4 (3) |
O6xiv—Ti_m1(2)—Oh | 85.9 (5) | Na_av—Nb_m1(1)—Oh | 54.9 (5) |
O6xiv—Ti_m1(2)—Ohxiii | 97.8 (6) | Na_av—Nb_m1(1)—Ohiv | 125.1 (5) |
O6xiv—Ti_m1(2)—Ba | 114.5 (3) | Na_av—Nb_m1(1)—Ba | 65.3 (2) |
O6xiv—Ti_m1(2)—Baxiii | 129.5 (4) | Na_av—Nb_m1(1)—Baxii | 114.7 (2) |
O6xiv—Ti_m1(2)—Ti_m2 | 130.4 (2) | Ti_m1(1)—Nb_m1(1)—O2 | 0 |
O6xiv—Ti_m1(2)—Mg_m2 | 130.4 (2) | Ti_m1(1)—Nb_m1(1)—O2iv | 0 |
Oh—Ti_m1(2)—Ohxiii | 174.4 (3) | Ti_m1(1)—Nb_m1(1)—O3 | 0 |
Oh—Ti_m1(2)—Ba | 51.55 (18) | Ti_m1(1)—Nb_m1(1)—O3iv | 0 |
Oh—Ti_m1(2)—Baxiii | 122.84 (19) | Ti_m1(1)—Nb_m1(1)—Oh | 0 |
Oh—Ti_m1(2)—Ti_m2 | 87.19 (17) | Ti_m1(1)—Nb_m1(1)—Ohiv | 0 |
Oh—Ti_m1(2)—Mg_m2 | 87.19 (17) | Ti_m1(1)—Nb_m1(1)—Ba | 0 |
Ohxiii—Ti_m1(2)—Ba | 122.84 (19) | Ti_m1(1)—Nb_m1(1)—Baxii | 0 |
Ohxiii—Ti_m1(2)—Baxiii | 51.55 (18) | O2—Nb_m1(1)—O2iv | 180.0 (5) |
Ohxiii—Ti_m1(2)—Ti_m2 | 87.19 (17) | O2—Nb_m1(1)—O3 | 88.1 (3) |
Ohxiii—Ti_m1(2)—Mg_m2 | 87.19 (17) | O2—Nb_m1(1)—O3iv | 91.9 (3) |
Ba—Ti_m1(2)—Baxiii | 71.81 (10) | O2—Nb_m1(1)—Oh | 90.5 (4) |
Ba—Ti_m1(2)—Ti_m2 | 35.91 (7) | O2—Nb_m1(1)—Ohiv | 89.5 (4) |
Ba—Ti_m1(2)—Mg_m2 | 35.91 (7) | O2—Nb_m1(1)—Ba | 79.1 (2) |
Baxiii—Ti_m1(2)—Ti_m2 | 35.91 (7) | O2—Nb_m1(1)—Baxii | 100.9 (2) |
Baxiii—Ti_m1(2)—Mg_m2 | 35.91 (7) | O2iv—Nb_m1(1)—O3 | 91.9 (3) |
Ti_m2—Ti_m1(2)—Mg_m2 | 0.0 (5) | O2iv—Nb_m1(1)—O3iv | 88.1 (3) |
O1—Fe_m2—O1xiii | 84.5 (3) | O2iv—Nb_m1(1)—Oh | 89.5 (4) |
O1—Fe_m2—O1xv | 180.0 (5) | O2iv—Nb_m1(1)—Ohiv | 90.5 (4) |
O1—Fe_m2—O1x | 95.5 (3) | O2iv—Nb_m1(1)—Ba | 100.9 (2) |
O1—Fe_m2—Ba | 95.0 (4) | O2iv—Nb_m1(1)—Baxii | 79.1 (2) |
O1—Fe_m2—Baxiii | 85.0 (4) | O3—Nb_m1(1)—O3iv | 180.0 (5) |
O1—Fe_m2—W_c | 95.0 (4) | O3—Nb_m1(1)—Oh | 88.4 (5) |
O1—Fe_m2—W_cxiii | 85.0 (4) | O3—Nb_m1(1)—Ohiv | 91.6 (5) |
O1—Fe_m2—Ti_m2 | 0 | O3—Nb_m1(1)—Ba | 45.1 (5) |
O1—Fe_m2—Mg_m2 | 0 | O3—Nb_m1(1)—Baxii | 134.9 (5) |
O1xiii—Fe_m2—O1xv | 95.5 (3) | O3iv—Nb_m1(1)—Oh | 91.6 (5) |
O1xiii—Fe_m2—O1x | 180.0 (5) | O3iv—Nb_m1(1)—Ohiv | 88.4 (5) |
O1xiii—Fe_m2—Ba | 85.0 (4) | O3iv—Nb_m1(1)—Ba | 134.9 (5) |
O1xiii—Fe_m2—Baxiii | 95.0 (4) | O3iv—Nb_m1(1)—Baxii | 45.1 (5) |
O1xiii—Fe_m2—W_c | 85.0 (4) | Oh—Nb_m1(1)—Ohiv | 180.0 (5) |
O1xiii—Fe_m2—W_cxiii | 95.0 (4) | Oh—Nb_m1(1)—Ba | 45.1 (2) |
O1xiii—Fe_m2—Ti_m2 | 0 | Oh—Nb_m1(1)—Baxii | 134.9 (2) |
O1xiii—Fe_m2—Mg_m2 | 0 | Ohiv—Nb_m1(1)—Ba | 134.9 (2) |
O1xv—Fe_m2—O1x | 84.5 (3) | Ohiv—Nb_m1(1)—Baxii | 45.1 (2) |
O1xv—Fe_m2—Ba | 85.0 (4) | Ba—Nb_m1(1)—Baxii | 180.0 (5) |
O1xv—Fe_m2—Baxiii | 95.0 (4) | Ti_m1(2)—Ti_m2—Ti_m1(2)xv | 180.0 (5) |
O1xv—Fe_m2—W_c | 85.0 (4) | Ti_m1(2)—Ti_m2—Fe_m2 | 0 |
O1xv—Fe_m2—W_cxiii | 95.0 (4) | Ti_m1(2)—Ti_m2—O1 | 42.25 (19) |
O1xv—Fe_m2—Ti_m2 | 0 | Ti_m1(2)—Ti_m2—O1xiii | 42.25 (19) |
O1xv—Fe_m2—Mg_m2 | 0 | Ti_m1(2)—Ti_m2—O1xv | 137.75 (19) |
O1x—Fe_m2—Ba | 95.0 (4) | Ti_m1(2)—Ti_m2—O1x | 137.75 (19) |
O1x—Fe_m2—Baxiii | 85.0 (4) | Ti_m1(2)—Ti_m2—Ba | 90 |
O1x—Fe_m2—W_c | 95.0 (4) | Ti_m1(2)—Ti_m2—Baxiii | 90 |
O1x—Fe_m2—W_cxiii | 85.0 (4) | Ti_m1(2)—Ti_m2—W_c | 90 |
O1x—Fe_m2—Ti_m2 | 0 | Ti_m1(2)—Ti_m2—W_cxiii | 90 |
O1x—Fe_m2—Mg_m2 | 0 | Ti_m1(2)—Ti_m2—Mg_m2 | 0 |
Ba—Fe_m2—Baxiii | 180.0 (5) | Ti_m1(2)xv—Ti_m2—Fe_m2 | 0 |
Ba—Fe_m2—W_c | 0.0 (5) | Ti_m1(2)xv—Ti_m2—O1 | 137.75 (19) |
Ba—Fe_m2—W_cxiii | 180.0 (5) | Ti_m1(2)xv—Ti_m2—O1xiii | 137.75 (19) |
Ba—Fe_m2—Ti_m2 | 0 | Ti_m1(2)xv—Ti_m2—O1xv | 42.25 (19) |
Ba—Fe_m2—Mg_m2 | 0 | Ti_m1(2)xv—Ti_m2—O1x | 42.25 (19) |
Baxiii—Fe_m2—W_c | 180.0 (5) | Ti_m1(2)xv—Ti_m2—Ba | 90 |
Baxiii—Fe_m2—W_cxiii | 0.0 (5) | Ti_m1(2)xv—Ti_m2—Baxiii | 90 |
Baxiii—Fe_m2—Ti_m2 | 0 | Ti_m1(2)xv—Ti_m2—W_c | 90 |
Baxiii—Fe_m2—Mg_m2 | 0 | Ti_m1(2)xv—Ti_m2—W_cxiii | 90 |
W_c—Fe_m2—W_cxiii | 180.0 (5) | Ti_m1(2)xv—Ti_m2—Mg_m2 | 0 |
W_c—Fe_m2—Ti_m2 | 0 | Fe_m2—Ti_m2—O1 | 0 |
W_c—Fe_m2—Mg_m2 | 0 | Fe_m2—Ti_m2—O1xiii | 0 |
W_cxiii—Fe_m2—Ti_m2 | 0 | Fe_m2—Ti_m2—O1xv | 0 |
W_cxiii—Fe_m2—Mg_m2 | 0 | Fe_m2—Ti_m2—O1x | 0 |
Ti_m2—Fe_m2—Mg_m2 | 0 | Fe_m2—Ti_m2—Ba | 0 |
K_b—Si1—K_biii | 80.22 (18) | Fe_m2—Ti_m2—Baxiii | 0 |
K_b—Si1—O3 | 52.6 (4) | Fe_m2—Ti_m2—W_c | 0 |
K_b—Si1—O4 | 63.0 (4) | Fe_m2—Ti_m2—W_cxiii | 0 |
K_b—Si1—O6 | 102.5 (3) | Fe_m2—Ti_m2—Mg_m2 | 0 |
K_b—Si1—O7 | 145.8 (5) | O1—Ti_m2—O1xiii | 84.5 (3) |
K_biii—Si1—O3 | 132.6 (4) | O1—Ti_m2—O1xv | 180.0 (5) |
K_biii—Si1—O4 | 39.8 (7) | O1—Ti_m2—O1x | 95.5 (3) |
K_biii—Si1—O6 | 65.4 (5) | O1—Ti_m2—Ba | 95.0 (4) |
K_biii—Si1—O7 | 116.0 (6) | O1—Ti_m2—Baxiii | 85.0 (4) |
O3—Si1—O4 | 108.4 (6) | O1—Ti_m2—W_c | 95.0 (4) |
O3—Si1—O6 | 115.9 (5) | O1—Ti_m2—W_cxiii | 85.0 (4) |
O3—Si1—O7 | 107.2 (8) | O1—Ti_m2—Mg_m2 | 0 |
O4—Si1—O6 | 104.5 (9) | O1xiii—Ti_m2—O1xv | 95.5 (3) |
O4—Si1—O7 | 109.0 (4) | O1xiii—Ti_m2—O1x | 180.0 (5) |
O6—Si1—O7 | 111.6 (5) | O1xiii—Ti_m2—Ba | 85.0 (4) |
Na_aiv—Si2—K_b | 163.7 (3) | O1xiii—Ti_m2—Baxiii | 95.0 (4) |
Na_aiv—Si2—O1 | 64.8 (5) | O1xiii—Ti_m2—W_c | 85.0 (4) |
Na_aiv—Si2—O2 | 101.1 (5) | O1xiii—Ti_m2—W_cxiii | 95.0 (4) |
Na_aiv—Si2—O5 | 148.1 (7) | O1xiii—Ti_m2—Mg_m2 | 0 |
Na_aiv—Si2—O7xi | 49.3 (5) | O1xv—Ti_m2—O1x | 84.5 (3) |
Na_aiv—Si2—Ba | 123.3 (3) | O1xv—Ti_m2—Ba | 85.0 (4) |
K_b—Si2—O1 | 131.3 (4) | O1xv—Ti_m2—Baxiii | 95.0 (4) |
K_b—Si2—O2 | 70.8 (5) | O1xv—Ti_m2—W_c | 85.0 (4) |
K_b—Si2—O5 | 38.6 (7) | O1xv—Ti_m2—W_cxiii | 95.0 (4) |
K_b—Si2—O7xi | 119.6 (5) | O1xv—Ti_m2—Mg_m2 | 0 |
K_b—Si2—Ba | 72.43 (14) | O1x—Ti_m2—Ba | 95.0 (4) |
O1—Si2—O2 | 114.7 (5) | O1x—Ti_m2—Baxiii | 85.0 (4) |
O1—Si2—O5 | 109.4 (6) | O1x—Ti_m2—W_c | 95.0 (4) |
O1—Si2—O7xi | 103.1 (8) | O1x—Ti_m2—W_cxiii | 85.0 (4) |
O1—Si2—Ba | 59.0 (4) | O1x—Ti_m2—Mg_m2 | 0 |
O2—Si2—O5 | 109.1 (9) | Ba—Ti_m2—Baxiii | 180.0 (5) |
O2—Si2—O7xi | 112.5 (4) | Ba—Ti_m2—W_c | 0.0 (5) |
O2—Si2—Ba | 96.0 (3) | Ba—Ti_m2—W_cxiii | 180.0 (5) |
O5—Si2—O7xi | 107.6 (4) | Ba—Ti_m2—Mg_m2 | 0 |
O5—Si2—Ba | 64.1 (3) | Baxiii—Ti_m2—W_c | 180.0 (5) |
O7xi—Si2—Ba | 151.2 (5) | Baxiii—Ti_m2—W_cxiii | 0.0 (5) |
Ti_m1(2)—O1—Fe_m2 | 96.4 (3) | Baxiii—Ti_m2—Mg_m2 | 0 |
Ti_m1(2)—O1—Si2 | 122.7 (6) | W_c—Ti_m2—W_cxiii | 180.0 (5) |
Ti_m1(2)—O1—Baxiii | 98.3 (5) | W_c—Ti_m2—Mg_m2 | 0 |
Ti_m1(2)—O1—Ti_m2 | 96.4 (3) | W_cxiii—Ti_m2—Mg_m2 | 0 |
Ti_m1(2)—O1—Mg_m2 | 96.4 (3) | Ti_m1(2)—Mg_m2—Ti_m1(2)xv | 180.0 (5) |
Fe_m2—O1—Si2 | 124.6 (6) | Ti_m1(2)—Mg_m2—Fe_m2 | 0 |
Fe_m2—O1—Baxiii | 50.2 (3) | Ti_m1(2)—Mg_m2—O1 | 42.25 (19) |
Fe_m2—O1—Ti_m2 | 0.0 (5) | Ti_m1(2)—Mg_m2—O1xiii | 42.25 (19) |
Fe_m2—O1—Mg_m2 | 0.0 (5) | Ti_m1(2)—Mg_m2—O1xv | 137.75 (19) |
Si2—O1—Baxiii | 138.0 (3) | Ti_m1(2)—Mg_m2—O1x | 137.75 (19) |
Si2—O1—Ti_m2 | 124.6 (6) | Ti_m1(2)—Mg_m2—Ba | 90 |
Si2—O1—Mg_m2 | 124.6 (6) | Ti_m1(2)—Mg_m2—Baxiii | 90 |
Baxiii—O1—Ti_m2 | 50.2 (3) | Ti_m1(2)—Mg_m2—W_c | 90 |
Baxiii—O1—Mg_m2 | 50.2 (3) | Ti_m1(2)—Mg_m2—W_cxiii | 90 |
Ti_m2—O1—Mg_m2 | 0.0 (5) | Ti_m1(2)—Mg_m2—Ti_m2 | 0 |
Na_axi—O2—Ti_m1(1) | 109.8 (6) | Ti_m1(2)xv—Mg_m2—Fe_m2 | 0 |
Na_axi—O2—Si2 | 119.2 (5) | Ti_m1(2)xv—Mg_m2—O1 | 137.75 (19) |
Na_axi—O2—Nb_m1(1) | 109.8 (6) | Ti_m1(2)xv—Mg_m2—O1xiii | 137.75 (19) |
Ti_m1(1)—O2—Si2 | 130.8 (4) | Ti_m1(2)xv—Mg_m2—O1xv | 42.25 (19) |
Ti_m1(1)—O2—Nb_m1(1) | 0.0 (5) | Ti_m1(2)xv—Mg_m2—O1x | 42.25 (19) |
Si2—O2—Nb_m1(1) | 130.8 (4) | Ti_m1(2)xv—Mg_m2—Ba | 90 |
K_b—O3—Ti_m1(1) | 119.6 (3) | Ti_m1(2)xv—Mg_m2—Baxiii | 90 |
K_b—O3—Si1 | 99.5 (7) | Ti_m1(2)xv—Mg_m2—W_c | 90 |
K_b—O3—Ba | 99.2 (3) | Ti_m1(2)xv—Mg_m2—W_cxiii | 90 |
K_b—O3—Nb_m1(1) | 119.6 (3) | Ti_m1(2)xv—Mg_m2—Ti_m2 | 0 |
Ti_m1(1)—O3—Si1 | 117.7 (4) | Fe_m2—Mg_m2—O1 | 0 |
Ti_m1(1)—O3—Ba | 105.8 (7) | Fe_m2—Mg_m2—O1xiii | 0 |
Ti_m1(1)—O3—Nb_m1(1) | 0.0 (5) | Fe_m2—Mg_m2—O1xv | 0 |
Si1—O3—Ba | 113.9 (3) | Fe_m2—Mg_m2—O1x | 0 |
Si1—O3—Nb_m1(1) | 117.7 (4) | Fe_m2—Mg_m2—Ba | 0 |
Ba—O3—Nb_m1(1) | 105.8 (7) | Fe_m2—Mg_m2—Baxiii | 0 |
K_biii—O4—Si1 | 116.0 (7) | Fe_m2—Mg_m2—W_c | 0 |
K_biii—O4—Si1x | 116.0 (7) | Fe_m2—Mg_m2—W_cxiii | 0 |
Si1—O4—Si1x | 126.7 (14) | Fe_m2—Mg_m2—Ti_m2 | 0 |
K_b—O5—Si2 | 118.1 (7) | O1—Mg_m2—O1xiii | 84.5 (3) |
K_b—O5—Si2x | 118.1 (7) | O1—Mg_m2—O1xv | 180.0 (5) |
Si2—O5—Si2x | 123.8 (14) | O1—Mg_m2—O1x | 95.5 (3) |
Na_a—O6—Ti_m1(2)iv | 101.7 (5) | O1—Mg_m2—Ba | 95.0 (4) |
Na_a—O6—Si1 | 120.7 (6) | O1—Mg_m2—Baxiii | 85.0 (4) |
Ti_m1(2)iv—O6—Si1 | 130.9 (8) | O1—Mg_m2—W_c | 95.0 (4) |
Na_av—O7—Si1 | 120.7 (5) | O1—Mg_m2—W_cxiii | 85.0 (4) |
Na_av—O7—Si2ii | 99.2 (5) | O1—Mg_m2—Ti_m2 | 0 |
Si1—O7—Si2ii | 133.4 (11) | O1xiii—Mg_m2—O1xv | 95.5 (3) |
Ti_m1(1)—Oh—Ti_m1(2) | 129.0 (3) | O1xiii—Mg_m2—O1x | 180.0 (5) |
Ti_m1(1)—Oh—Ba | 105.9 (4) | O1xiii—Mg_m2—Ba | 85.0 (4) |
Ti_m1(1)—Oh—Nb_m1(1) | 0.0 (5) | O1xiii—Mg_m2—Baxiii | 95.0 (4) |
Ti_m1(2)—Oh—Ba | 97.0 (4) | O1xiii—Mg_m2—W_c | 85.0 (4) |
Ti_m1(2)—Oh—Nb_m1(1) | 129.0 (3) | O1xiii—Mg_m2—W_cxiii | 95.0 (4) |
Ba—Oh—Nb_m1(1) | 105.9 (4) | O1xiii—Mg_m2—Ti_m2 | 0 |
Na_axx—Ba—Na_axxi | 33.8 (5) | O1xv—Mg_m2—O1x | 84.5 (3) |
Na_axx—Ba—Na_av | 111.0 (2) | O1xv—Mg_m2—Ba | 85.0 (4) |
Na_axx—Ba—Na_axiv | 100.3 (2) | O1xv—Mg_m2—Baxiii | 95.0 (4) |
Na_axx—Ba—K_b | 126.8 (3) | O1xv—Mg_m2—W_c | 85.0 (4) |
Na_axx—Ba—Ti_m1(1) | 163.04 (19) | O1xv—Mg_m2—W_cxiii | 95.0 (4) |
Na_axx—Ba—Ti_m1(1)xviii | 68.2 (2) | O1xv—Mg_m2—Ti_m2 | 0 |
Na_axx—Ba—Ti_m1(2) | 127.8 (3) | O1x—Mg_m2—Ba | 95.0 (4) |
Na_axx—Ba—Ti_m1(2)xv | 50.87 (19) | O1x—Mg_m2—Baxiii | 85.0 (4) |
Na_axx—Ba—Fe_m2 | 89.1 (3) | O1x—Mg_m2—W_c | 95.0 (4) |
Na_axx—Ba—Si2 | 145.1 (2) | O1x—Mg_m2—W_cxiii | 85.0 (4) |
Na_axx—Ba—Si2x | 100.31 (15) | O1x—Mg_m2—Ti_m2 | 0 |
Na_axx—Ba—O1xiii | 95.1 (4) | Ba—Mg_m2—Baxiii | 180.0 (5) |
Na_axx—Ba—O1xv | 44.3 (4) | Ba—Mg_m2—W_c | 0.0 (5) |
Na_axx—Ba—O3 | 144.4 (4) | Ba—Mg_m2—W_cxiii | 180.0 (5) |
Na_axx—Ba—O3x | 88.2 (3) | Ba—Mg_m2—Ti_m2 | 0 |
Na_axx—Ba—Oh | 144.1 (3) | Baxiii—Mg_m2—W_c | 180.0 (5) |
Na_axx—Ba—Ohx | 44.3 (2) | Baxiii—Mg_m2—W_cxiii | 0.0 (5) |
Na_axx—Ba—Baxvi | 55.13 (15) | Baxiii—Mg_m2—Ti_m2 | 0 |
Na_axx—Ba—Baxiii | 89.1 (3) | W_c—Mg_m2—W_cxiii | 180.0 (5) |
Na_axx—Ba—W2 | 86.0 (2) | W_c—Mg_m2—Ti_m2 | 0 |
Na_axx—Ba—W2xvii | 26.5 (3) | W_cxiii—Mg_m2—Ti_m2 | 0 |
Na_axx—Ba—W_c | 0 | | |
Symmetry codes: (i) −x+1, y, −z; (ii) x, y, z−1; (iii) −x+1, y, −z+1; (iv) −x+1/2, −y+1/2, −z+1; (v) −x+1/2, −y+1/2, −z; (vi) x+1/2, y+1/2, z; (vii) −x+1/2, y+1/2, −z; (viii) −x+1, y, −z+2; (ix) −x+1, −y, −z+1; (x) x, −y, z; (xi) x, y, z+1; (xii) −x+1/2, y+1/2, −z+1; (xiii) −x, y, −z+1; (xiv) x−1/2, −y+1/2, z; (xv) −x, −y, −z+1; (xvi) −x, y, −z; (xvii) −x, −y, −z; (xviii) −x+1/2, y−1/2, −z+1; (xix) x, −y, z+1; (xx) x−1/2, y−1/2, z; (xxi) −x+1/2, y−1/2, −z. |
Crystal data top
Ba0.7Fe0.5K2.1Mg0.05Na2Nb0.1O33Si8Ti4 | Z = 2 |
Mr = 1206.8 | F(000) = 1167 |
Monoclinic, C2/m | Dx = 3.476 Mg m−3 |
Hall symbol: -C 2y | Synchrotron radiation, λ = 0.414 Å |
a = 13.535 (8) Å | Cell parameters from 2728 reflections |
b = 13.1485 (5) Å | θ = 1.8–19.0° |
c = 7.2026 (17) Å | µ = 0.92 mm−1 |
β = 115.94 (4)° | T = 293 K |
V = 1152.7 (8) Å3 | Anhedral grain |
Data collection top
ESRF ID 09 diffractometer | θmax = 19.0°, θmin = 1.8° |
2728 measured reflections | h = −8→7 |
776 independent reflections | k = −20→20 |
501 reflections with I > 2σ(I) | l = −9→10 |
Rint = 0.047 | |
Refinement top
Refinement on F | 0 restraints |
R[F2 > 2σ(F2)] = 0.093 | 6 constraints |
wR(F2) = 0.148 | Weighting scheme based on measured s.u.'s w = 1/(σ2(F) + 0.0100000007F2) |
S = 1.11 | (Δ/σ)max = 0.048 |
776 reflections | Δρmax = 1.08 e Å−3 |
57 parameters | Δρmin = −1.32 e Å−3 |
Fractional atomic coordinates and isotropic or equivalent isotropic displacement parameters (Å2) top | x | y | z | Uiso*/Ueq | Occ. (<1) |
Na_a | 0.418 (2) | 0.2704 (8) | 0.0128 (17) | 0.035 (3)* | 0.5 |
K_b | 0.4358 (9) | 0 | 0.7315 (7) | 0.0362 (12)* | |
Ti_m1(1) | 0.25 | 0.25 | 0.5 | 0.0196 (7)* | 0.95 |
Ti_m1(2) | 0 | 0.2177 (2) | 0.5 | 0.0181 (7)* | |
Fe_m2 | 0 | 0 | 0.5 | 0.0309 (16)* | 0.5 |
Si1 | 0.3307 (6) | 0.10970 (19) | 0.2709 (4) | 0.0113 (7)* | |
Si2 | 0.2104 (5) | 0.10875 (18) | 0.8196 (4) | 0.0103 (7)* | |
O1 | 0.0805 (14) | 0.1047 (5) | 0.6816 (11) | 0.0149 (17)* | |
O2 | 0.2704 (14) | 0.1987 (5) | 0.7670 (11) | 0.0145 (16)* | |
O3 | 0.2876 (15) | 0.1156 (5) | 0.4395 (11) | 0.0141 (15)* | |
O4 | 0.3877 (19) | 0 | 0.2925 (15) | 0.013 (2)* | |
O5 | 0.272 (2) | 0 | 0.7986 (16) | 0.016 (2)* | |
O6 | 0.4180 (16) | 0.1883 (7) | 0.2876 (13) | 0.024 (2)* | |
O7 | 0.2200 (15) | 0.1143 (5) | 0.0522 (11) | 0.0145 (16)* | |
Oh | 0.0981 (14) | 0.2098 (5) | 0.3825 (11) | 0.0118 (15)* | |
Ba | 0.0963 (5) | 0 | 0.3344 (4) | 0.0179 (7)* | 0.35 |
W1 | 0.5 | 0.1435 (11) | 0 | 0.038 (4)* | |
W2 | 0 | 0.1077 (9) | 0 | 0.033 (3)* | |
W_c | 0.0963 (5) | 0 | 0.3344 (4) | 0.0179 (7)* | 0.65 |
Nb_m1(1) | 0.25 | 0.25 | 0.5 | 0.0196 (7)* | 0.05 |
Ti_m2 | 0 | 0 | 0.5 | 0.0309 (16)* | 0.1 |
Mg_m2 | 0 | 0 | 0.5 | 0.0309 (16)* | 0.05 |
Atomic displacement parameters (Å2) top | U11 | U22 | U33 | U12 | U13 | U23 |
? | ? | ? | ? | ? | ? | ? |
Geometric parameters (Å, º) top
Na_a—Na_ai | 2.30 (4) | Ti_m1(2)—Oh | 1.864 (18) |
Na_a—K_bii | 4.150 (14) | Ti_m1(2)—Ohxiii | 1.864 (18) |
Na_a—K_biii | 4.093 (13) | Ti_m1(2)—Ba | 3.560 (4) |
Na_a—Ti_m1(1)ii | 3.397 (12) | Ti_m1(2)—Baxiii | 3.560 (4) |
Na_a—Ti_m1(2)iv | 3.188 (13) | Ti_m1(2)—Ti_m2 | 2.862 (3) |
Na_a—Si2iv | 2.98 (2) | Ti_m1(2)—Mg_m2 | 2.862 (3) |
Na_a—O2ii | 2.22 (2) | Fe_m2—O1 | 1.883 (8) |
Na_a—O6 | 2.26 (2) | Fe_m2—O1xiii | 1.883 (8) |
Na_a—O7v | 2.29 (3) | Fe_m2—O1xv | 1.883 (8) |
Na_a—Bavi | 3.925 (14) | Fe_m2—O1x | 1.883 (8) |
Na_a—Bavii | 3.870 (13) | Fe_m2—Ba | 2.117 (6) |
Na_a—W1 | 2.03 (2) | Fe_m2—Baxiii | 2.117 (6) |
Na_a—W2v | 1.97 (2) | Fe_m2—W_c | 2.117 (6) |
Na_a—Nb_m1(1)ii | 3.397 (12) | Fe_m2—W_cxiii | 2.117 (6) |
K_b—K_biii | 4.384 (15) | Fe_m2—Ti_m2 | 0 |
K_b—K_bviii | 3.478 (7) | Fe_m2—Mg_m2 | 0 |
K_b—Si1 | 3.314 (5) | Si1—O3 | 1.562 (18) |
K_b—Si1iii | 3.481 (14) | Si1—O4 | 1.611 (12) |
K_b—Si1ix | 3.481 (14) | Si1—O6 | 1.535 (19) |
K_b—Si1x | 3.314 (5) | Si1—O7 | 1.633 (12) |
K_b—Si2 | 3.667 (14) | Si2—O1 | 1.597 (17) |
K_b—Si2x | 3.667 (14) | Si2—O2 | 1.572 (15) |
K_b—O3 | 2.657 (12) | Si2—O7xi | 1.625 (12) |
K_b—O3x | 2.657 (12) | Si2—Ba | 3.452 (4) |
K_b—O4iii | 2.47 (3) | O1—Baxiii | 2.720 (18) |
K_b—O5 | 2.46 (3) | O1—Ti_m2 | 1.883 (8) |
K_b—Ba | 4.218 (13) | O1—Mg_m2 | 1.883 (8) |
K_b—W1xi | 2.566 (12) | O2—Nb_m1(1) | 1.941 (10) |
K_b—W1ix | 2.566 (12) | O3—Ba | 2.806 (18) |
Ti_m1(1)—O2 | 1.941 (10) | O3—Nb_m1(1) | 1.941 (10) |
Ti_m1(1)—O2iv | 1.941 (10) | Oh—Ba | 2.778 (6) |
Ti_m1(1)—O3 | 1.941 (10) | Oh—Nb_m1(1) | 1.923 (17) |
Ti_m1(1)—O3iv | 1.941 (10) | Ba—Baxvi | 4.360 (5) |
Ti_m1(1)—Oh | 1.923 (17) | Ba—Baxiii | 4.234 (9) |
Ti_m1(1)—Ohiv | 1.923 (17) | Ba—W2 | 2.600 (7) |
Ti_m1(1)—Ba | 3.793 (3) | Ba—W2xvii | 2.600 (7) |
Ti_m1(1)—Baxii | 3.793 (3) | Ba—W_c | 0 |
Ti_m1(1)—Nb_m1(1) | 0 | Ba—Nb_m1(1) | 3.793 (3) |
Ti_m1(2)—Fe_m2 | 2.862 (3) | Ba—Nb_m1(1)xviii | 3.793 (3) |
Ti_m1(2)—O1 | 1.964 (8) | Ba—Ti_m2 | 2.117 (6) |
Ti_m1(2)—O1xiii | 1.964 (8) | Ba—Mg_m2 | 2.117 (6) |
Ti_m1(2)—O6iv | 1.901 (9) | W_c—Ti_m2 | 2.117 (6) |
Ti_m1(2)—O6xiv | 1.901 (9) | Ti_m2—Mg_m2 | 0 |
| | | |
Na_ai—Na_a—K_bii | 72.4 (5) | Ti_m1(2)—Oh—Nb_m1(1) | 128.4 (4) |
Na_ai—Na_a—K_biii | 75.2 (6) | Ba—Oh—Nb_m1(1) | 106.1 (6) |
Na_ai—Na_a—Ti_m1(1)ii | 97.1 (6) | Na_axx—Ba—Na_axxi | 34.3 (6) |
Na_ai—Na_a—Ti_m1(2)iv | 101.9 (7) | Na_axx—Ba—Na_av | 112.0 (3) |
Na_ai—Na_a—Si2iv | 141.9 (6) | Na_axx—Ba—Na_axiv | 100.6 (3) |
Na_ai—Na_a—O2ii | 120.0 (9) | Na_axx—Ba—K_b | 127.3 (3) |
Na_ai—Na_a—O6 | 116.2 (10) | Na_axx—Ba—Ti_m1(1) | 164.4 (2) |
Na_ai—Na_a—O7v | 135.4 (8) | Na_axx—Ba—Ti_m1(1)xviii | 68.3 (3) |
Na_ai—Na_a—Bavi | 71.5 (5) | Na_axx—Ba—Ti_m1(2) | 126.6 (4) |
Na_ai—Na_a—Bavii | 74.2 (6) | Na_axx—Ba—Ti_m1(2)xv | 50.1 (2) |
Na_ai—Na_a—W1 | 55.4 (8) | Na_axx—Ba—Fe_m2 | 87.8 (4) |
Na_ai—Na_a—W2v | 54.3 (8) | Na_axx—Ba—Si2 | 143.4 (3) |
Na_ai—Na_a—Nb_m1(1)ii | 97.1 (6) | Na_axx—Ba—Si2x | 99.56 (19) |
K_bii—Na_a—K_biii | 49.92 (18) | Na_axx—Ba—O1xiii | 93.6 (5) |
K_bii—Na_a—Ti_m1(1)ii | 63.6 (2) | Na_axx—Ba—O1xv | 44.3 (5) |
K_bii—Na_a—Ti_m1(2)iv | 120.9 (3) | Na_axx—Ba—O3 | 146.3 (5) |
K_bii—Na_a—Si2iv | 145.5 (8) | Na_axx—Ba—O3x | 89.9 (4) |
K_bii—Na_a—O2ii | 58.1 (5) | Na_axx—Ba—Oh | 143.8 (4) |
K_bii—Na_a—O6 | 92.3 (4) | Na_axx—Ba—Ohx | 43.9 (3) |
K_bii—Na_a—O7v | 133.1 (6) | Na_axx—Ba—Baxvi | 55.39 (18) |
K_bii—Na_a—Bavi | 142.7 (8) | Na_axx—Ba—Baxiii | 87.8 (4) |
K_bii—Na_a—Bavii | 110.5 (4) | Na_axx—Ba—W2 | 86.7 (3) |
K_bii—Na_a—W1 | 28.8 (3) | Na_axx—Ba—W2xvii | 26.4 (3) |
K_bii—Na_a—W2v | 121.4 (10) | Na_axx—Ba—W_c | 0 |
K_bii—Na_a—Nb_m1(1)ii | 63.6 (2) | Na_axx—Ba—Nb_m1(1) | 164.4 (2) |
K_biii—Na_a—Ti_m1(1)ii | 112.5 (3) | Na_axx—Ba—Nb_m1(1)xviii | 68.3 (3) |
K_biii—Na_a—Ti_m1(2)iv | 71.4 (2) | Na_axx—Ba—Ti_m2 | 87.8 (4) |
K_biii—Na_a—Si2iv | 122.3 (5) | Na_axx—Ba—Mg_m2 | 87.8 (4) |
K_biii—Na_a—O2ii | 94.5 (4) | Na_axxi—Ba—Na_av | 102.5 (3) |
K_biii—Na_a—O6 | 51.3 (5) | Na_axxi—Ba—Na_axiv | 112.0 (3) |
K_biii—Na_a—O7v | 149.0 (10) | Na_axxi—Ba—K_b | 99.8 (4) |
K_biii—Na_a—Bavi | 110.6 (4) | Na_axxi—Ba—Ti_m1(1) | 138.2 (4) |
K_biii—Na_a—Bavii | 147.8 (8) | Na_axxi—Ba—Ti_m1(1)xviii | 52.6 (2) |
K_biii—Na_a—W1 | 30.6 (3) | Na_axxi—Ba—Ti_m1(2) | 157.1 (4) |
K_biii—Na_a—W2v | 123.8 (10) | Na_axxi—Ba—Ti_m1(2)xv | 70.5 (3) |
K_biii—Na_a—Nb_m1(1)ii | 112.5 (3) | Na_axxi—Ba—Fe_m2 | 119.6 (4) |
Ti_m1(1)ii—Na_a—Ti_m1(2)iv | 161.0 (10) | Na_axxi—Ba—Si2 | 148.3 (2) |
Ti_m1(1)ii—Na_a—Si2iv | 104.5 (6) | Na_axxi—Ba—Si2x | 101.82 (17) |
Ti_m1(1)ii—Na_a—O2ii | 32.6 (4) | Na_axxi—Ba—O1xiii | 124.9 (4) |
Ti_m1(1)ii—Na_a—O6 | 131.2 (9) | Na_axxi—Ba—O1xv | 77.4 (5) |
Ti_m1(1)ii—Na_a—O7v | 74.4 (4) | Na_axxi—Ba—O3 | 112.1 (5) |
Ti_m1(1)ii—Na_a—Bavi | 130.5 (4) | Na_axxi—Ba—O3x | 62.1 (4) |
Ti_m1(1)ii—Na_a—Bavii | 62.5 (2) | Na_axxi—Ba—Oh | 148.2 (3) |
Ti_m1(1)ii—Na_a—W1 | 90.3 (4) | Na_axxi—Ba—Ohx | 45.7 (3) |
Ti_m1(1)ii—Na_a—W2v | 97.8 (5) | Na_axxi—Ba—Baxvi | 56.58 (19) |
Ti_m1(1)ii—Na_a—Nb_m1(1)ii | 0.0 (5) | Na_axxi—Ba—Baxiii | 119.6 (4) |
Ti_m1(2)iv—Na_a—Si2iv | 60.7 (4) | Na_axxi—Ba—W2 | 87.9 (3) |
Ti_m1(2)iv—Na_a—O2ii | 131.0 (11) | Na_axxi—Ba—W2xvii | 27.5 (3) |
Ti_m1(2)iv—Na_a—O6 | 36.0 (3) | Na_axxi—Ba—W_c | 0 |
Ti_m1(2)iv—Na_a—O7v | 93.0 (7) | Na_axxi—Ba—Nb_m1(1) | 138.2 (4) |
Ti_m1(2)iv—Na_a—Bavi | 59.0 (2) | Na_axxi—Ba—Nb_m1(1)xviii | 52.6 (2) |
Ti_m1(2)iv—Na_a—Bavii | 124.6 (3) | Na_axxi—Ba—Ti_m2 | 119.6 (4) |
Ti_m1(2)iv—Na_a—W1 | 99.0 (4) | Na_axxi—Ba—Mg_m2 | 119.6 (4) |
Ti_m1(2)iv—Na_a—W2v | 94.6 (4) | Na_av—Ba—Na_axiv | 34.3 (6) |
Ti_m1(2)iv—Na_a—Nb_m1(1)ii | 161.0 (10) | Na_av—Ba—K_b | 99.8 (4) |
Si2iv—Na_a—O2ii | 93.8 (10) | Na_av—Ba—Ti_m1(1) | 52.6 (2) |
Si2iv—Na_a—O6 | 71.0 (8) | Na_av—Ba—Ti_m1(1)xviii | 138.2 (4) |
Si2iv—Na_a—O7v | 32.8 (4) | Na_av—Ba—Ti_m1(2) | 70.5 (3) |
Si2iv—Na_a—Bavi | 70.5 (3) | Na_av—Ba—Ti_m1(2)xv | 157.1 (4) |
Si2iv—Na_a—Bavii | 88.4 (3) | Na_av—Ba—Fe_m2 | 119.6 (4) |
Si2iv—Na_a—W1 | 152.4 (8) | Na_av—Ba—Si2 | 101.82 (17) |
Si2iv—Na_a—W2v | 91.4 (5) | Na_av—Ba—Si2x | 148.3 (2) |
Si2iv—Na_a—Nb_m1(1)ii | 104.5 (6) | Na_av—Ba—O1xiii | 77.4 (5) |
O2ii—Na_a—O6 | 98.6 (10) | Na_av—Ba—O1xv | 124.9 (4) |
O2ii—Na_a—O7v | 75.4 (8) | Na_av—Ba—O3 | 62.1 (4) |
O2ii—Na_a—Bavi | 154.7 (6) | Na_av—Ba—O3x | 112.1 (5) |
O2ii—Na_a—Bavii | 92.5 (4) | Na_av—Ba—Oh | 45.7 (3) |
O2ii—Na_a—W1 | 86.2 (5) | Na_av—Ba—Ohx | 148.2 (3) |
O2ii—Na_a—W2v | 129.5 (6) | Na_av—Ba—Baxvi | 56.58 (19) |
O2ii—Na_a—Nb_m1(1)ii | 32.6 (4) | Na_av—Ba—Baxiii | 119.6 (4) |
O6—Na_a—O7v | 100.4 (12) | Na_av—Ba—W2 | 27.5 (3) |
O6—Na_a—Bavi | 95.0 (4) | Na_av—Ba—W2xvii | 87.9 (3) |
O6—Na_a—Bavii | 157.1 (7) | Na_av—Ba—W_c | 0 |
O6—Na_a—W1 | 81.7 (6) | Na_av—Ba—Nb_m1(1) | 52.6 (2) |
O6—Na_a—W2v | 130.2 (6) | Na_av—Ba—Nb_m1(1)xviii | 138.2 (4) |
O6—Na_a—Nb_m1(1)ii | 131.2 (9) | Na_av—Ba—Ti_m2 | 119.6 (4) |
O7v—Na_a—Bavi | 81.2 (4) | Na_av—Ba—Mg_m2 | 119.6 (4) |
O7v—Na_a—Bavii | 63.0 (5) | Na_axiv—Ba—K_b | 127.3 (3) |
O7v—Na_a—W1 | 161.6 (9) | Na_axiv—Ba—Ti_m1(1) | 68.3 (3) |
O7v—Na_a—W2v | 83.0 (6) | Na_axiv—Ba—Ti_m1(1)xviii | 164.4 (2) |
O7v—Na_a—Nb_m1(1)ii | 74.4 (4) | Na_axiv—Ba—Ti_m1(2) | 50.1 (2) |
Bavi—Na_a—Bavii | 68.0 (2) | Na_axiv—Ba—Ti_m1(2)xv | 126.6 (4) |
Bavi—Na_a—W1 | 117.0 (9) | Na_axiv—Ba—Fe_m2 | 87.8 (4) |
Bavi—Na_a—W2v | 35.9 (2) | Na_axiv—Ba—Si2 | 99.56 (19) |
Bavi—Na_a—Nb_m1(1)ii | 130.5 (4) | Na_axiv—Ba—Si2x | 143.4 (3) |
Bavii—Na_a—W1 | 119.2 (9) | Na_axiv—Ba—O1xiii | 44.3 (5) |
Bavii—Na_a—W2v | 37.5 (2) | Na_axiv—Ba—O1xv | 93.6 (5) |
Bavii—Na_a—Nb_m1(1)ii | 62.5 (2) | Na_axiv—Ba—O3 | 89.9 (4) |
W1—Na_a—W2v | 109.8 (14) | Na_axiv—Ba—O3x | 146.3 (5) |
W1—Na_a—Nb_m1(1)ii | 90.3 (4) | Na_axiv—Ba—Oh | 43.9 (3) |
W2v—Na_a—Nb_m1(1)ii | 97.8 (5) | Na_axiv—Ba—Ohx | 143.8 (4) |
Na_axi—K_b—Na_aiii | 32.4 (6) | Na_axiv—Ba—Baxvi | 55.39 (18) |
Na_axi—K_b—Na_aix | 130.1 (3) | Na_axiv—Ba—Baxiii | 87.8 (4) |
Na_axi—K_b—Na_axix | 117.9 (4) | Na_axiv—Ba—W2 | 26.4 (3) |
Na_axi—K_b—K_biii | 119.8 (3) | Na_axiv—Ba—W2xvii | 86.7 (3) |
Na_axi—K_b—K_bviii | 64.19 (18) | Na_axiv—Ba—W_c | 0 |
Na_axi—K_b—Si1 | 91.42 (18) | Na_axiv—Ba—Nb_m1(1) | 68.3 (3) |
Na_axi—K_b—Si1iii | 83.9 (4) | Na_axiv—Ba—Nb_m1(1)xviii | 164.4 (2) |
Na_axi—K_b—Si1ix | 127.1 (4) | Na_axiv—Ba—Ti_m2 | 87.8 (4) |
Na_axi—K_b—Si1x | 140.4 (2) | Na_axiv—Ba—Mg_m2 | 87.8 (4) |
Na_axi—K_b—Si2 | 49.6 (4) | K_b—Ba—Ti_m1(1) | 60.12 (7) |
Na_axi—K_b—Si2x | 91.2 (4) | K_b—Ba—Ti_m1(1)xviii | 60.12 (7) |
Na_axi—K_b—O3 | 73.3 (3) | K_b—Ba—Ti_m1(2) | 102.87 (9) |
Na_axi—K_b—O3x | 133.8 (6) | K_b—Ba—Ti_m1(2)xv | 102.87 (9) |
Na_axi—K_b—O4iii | 107.3 (4) | K_b—Ba—Fe_m2 | 111.99 (16) |
Na_axi—K_b—O5 | 69.9 (4) | K_b—Ba—Si2 | 56.05 (17) |
Na_axi—K_b—Ba | 93.0 (4) | K_b—Ba—Si2x | 56.05 (17) |
Na_axi—K_b—W1xi | 22.3 (3) | K_b—Ba—O1xiii | 134.9 (2) |
Na_axi—K_b—W1ix | 109.6 (3) | K_b—Ba—O1xv | 134.9 (2) |
Na_aiii—K_b—Na_aix | 120.6 (4) | K_b—Ba—O3 | 38.19 (19) |
Na_aiii—K_b—Na_axix | 130.1 (3) | K_b—Ba—O3x | 38.19 (19) |
Na_aiii—K_b—K_biii | 93.9 (4) | K_b—Ba—Oh | 88.2 (3) |
Na_aiii—K_b—K_bviii | 65.89 (19) | K_b—Ba—Ohx | 88.2 (3) |
Na_aiii—K_b—Si1 | 89.06 (18) | K_b—Ba—Baxvi | 134.1 (2) |
Na_aiii—K_b—Si1iii | 51.8 (4) | K_b—Ba—Baxiii | 111.99 (15) |
Na_aiii—K_b—Si1ix | 95.8 (5) | K_b—Ba—W2 | 125.7 (2) |
Na_aiii—K_b—Si1x | 137.7 (3) | K_b—Ba—W2xvii | 125.7 (2) |
Na_aiii—K_b—Si2 | 81.8 (4) | K_b—Ba—W_c | 0 |
Na_aiii—K_b—Si2x | 122.4 (4) | K_b—Ba—Nb_m1(1) | 60.12 (7) |
Na_aiii—K_b—O3 | 84.7 (3) | K_b—Ba—Nb_m1(1)xviii | 60.12 (7) |
Na_aiii—K_b—O3x | 154.3 (3) | K_b—Ba—Ti_m2 | 111.99 (16) |
Na_aiii—K_b—O4iii | 74.9 (4) | K_b—Ba—Mg_m2 | 111.99 (16) |
Na_aiii—K_b—O5 | 102.1 (4) | Ti_m1(1)—Ba—Ti_m1(1)xviii | 120.15 (15) |
Na_aiii—K_b—Ba | 118.2 (3) | Ti_m1(1)—Ba—Ti_m1(2) | 55.16 (4) |
Na_aiii—K_b—W1xi | 23.7 (4) | Ti_m1(1)—Ba—Ti_m1(2)xv | 145.32 (9) |
Na_aiii—K_b—W1ix | 111.2 (3) | Ti_m1(1)—Ba—Fe_m2 | 102.18 (7) |
Na_aix—K_b—Na_axix | 32.4 (6) | Ti_m1(1)—Ba—Si2 | 51.82 (8) |
Na_aix—K_b—K_biii | 93.9 (4) | Ti_m1(1)—Ba—Si2x | 95.73 (9) |
Na_aix—K_b—K_bviii | 65.89 (19) | Ti_m1(1)—Ba—O1xiii | 85.8 (2) |
Na_aix—K_b—Si1 | 137.7 (3) | Ti_m1(1)—Ba—O1xv | 143.5 (3) |
Na_aix—K_b—Si1iii | 95.8 (5) | Ti_m1(1)—Ba—O3 | 29.7 (3) |
Na_aix—K_b—Si1ix | 51.8 (4) | Ti_m1(1)—Ba—O3x | 94.0 (3) |
Na_aix—K_b—Si1x | 89.06 (18) | Ti_m1(1)—Ba—Oh | 29.2 (4) |
Na_aix—K_b—Si2 | 122.4 (4) | Ti_m1(1)—Ba—Ohx | 147.9 (3) |
Na_aix—K_b—Si2x | 81.8 (4) | Ti_m1(1)—Ba—Baxvi | 109.15 (7) |
Na_aix—K_b—O3 | 154.3 (3) | Ti_m1(1)—Ba—Baxiii | 102.18 (8) |
Na_aix—K_b—O3x | 84.7 (3) | Ti_m1(1)—Ba—W2 | 78.6 (2) |
Na_aix—K_b—O4iii | 74.9 (4) | Ti_m1(1)—Ba—W2xvii | 138.3 (2) |
Na_aix—K_b—O5 | 102.1 (4) | Ti_m1(1)—Ba—W_c | 0 |
Na_aix—K_b—Ba | 118.2 (3) | Ti_m1(1)—Ba—Nb_m1(1) | 0.0 (5) |
Na_aix—K_b—W1xi | 111.2 (3) | Ti_m1(1)—Ba—Nb_m1(1)xviii | 120.15 (15) |
Na_aix—K_b—W1ix | 23.7 (4) | Ti_m1(1)—Ba—Ti_m2 | 102.18 (7) |
Na_axix—K_b—K_biii | 119.8 (3) | Ti_m1(1)—Ba—Mg_m2 | 102.18 (7) |
Na_axix—K_b—K_bviii | 64.19 (18) | Ti_m1(1)xviii—Ba—Ti_m1(2) | 145.32 (9) |
Na_axix—K_b—Si1 | 140.4 (2) | Ti_m1(1)xviii—Ba—Ti_m1(2)xv | 55.16 (4) |
Na_axix—K_b—Si1iii | 127.1 (4) | Ti_m1(1)xviii—Ba—Fe_m2 | 102.18 (7) |
Na_axix—K_b—Si1ix | 83.9 (4) | Ti_m1(1)xviii—Ba—Si2 | 95.73 (9) |
Na_axix—K_b—Si1x | 91.42 (18) | Ti_m1(1)xviii—Ba—Si2x | 51.82 (8) |
Na_axix—K_b—Si2 | 91.2 (4) | Ti_m1(1)xviii—Ba—O1xiii | 143.5 (3) |
Na_axix—K_b—Si2x | 49.6 (4) | Ti_m1(1)xviii—Ba—O1xv | 85.8 (2) |
Na_axix—K_b—O3 | 133.8 (6) | Ti_m1(1)xviii—Ba—O3 | 94.0 (3) |
Na_axix—K_b—O3x | 73.3 (3) | Ti_m1(1)xviii—Ba—O3x | 29.7 (3) |
Na_axix—K_b—O4iii | 107.3 (4) | Ti_m1(1)xviii—Ba—Oh | 147.9 (3) |
Na_axix—K_b—O5 | 69.9 (4) | Ti_m1(1)xviii—Ba—Ohx | 29.2 (4) |
Na_axix—K_b—Ba | 93.0 (4) | Ti_m1(1)xviii—Ba—Baxvi | 109.15 (7) |
Na_axix—K_b—W1xi | 109.6 (3) | Ti_m1(1)xviii—Ba—Baxiii | 102.18 (8) |
Na_axix—K_b—W1ix | 22.3 (3) | Ti_m1(1)xviii—Ba—W2 | 138.3 (2) |
K_biii—K_b—K_bviii | 132.4 (4) | Ti_m1(1)xviii—Ba—W2xvii | 78.6 (2) |
K_biii—K_b—Si1 | 51.5 (2) | Ti_m1(1)xviii—Ba—W_c | 0 |
K_biii—K_b—Si1iii | 48.16 (18) | Ti_m1(1)xviii—Ba—Nb_m1(1) | 120.15 (15) |
K_biii—K_b—Si1ix | 48.16 (18) | Ti_m1(1)xviii—Ba—Nb_m1(1)xviii | 0.0 (5) |
K_biii—K_b—Si1x | 51.5 (2) | Ti_m1(1)xviii—Ba—Ti_m2 | 102.18 (7) |
K_biii—K_b—Si2 | 140.22 (15) | Ti_m1(1)xviii—Ba—Mg_m2 | 102.18 (7) |
K_biii—K_b—Si2x | 140.22 (15) | Ti_m1(2)—Ba—Ti_m1(2)xv | 107.03 (16) |
K_biii—K_b—O3 | 79.1 (4) | Ti_m1(2)—Ba—Fe_m2 | 53.51 (8) |
K_biii—K_b—O3x | 79.1 (4) | Ti_m1(2)—Ba—Si2 | 52.77 (10) |
K_biii—K_b—O4iii | 39.6 (3) | Ti_m1(2)—Ba—Si2x | 93.50 (12) |
K_biii—K_b—O5 | 147.0 (3) | Ti_m1(2)—Ba—O1xiii | 33.1 (2) |
K_biii—K_b—Ba | 99.28 (17) | Ti_m1(2)—Ba—O1xv | 88.7 (3) |
K_biii—K_b—W1xi | 117.2 (3) | Ti_m1(2)—Ba—O3 | 84.5 (3) |
K_biii—K_b—W1ix | 117.2 (3) | Ti_m1(2)—Ba—O3x | 140.80 (18) |
K_bviii—K_b—Si1 | 154.16 (6) | Ti_m1(2)—Ba—Oh | 31.2 (4) |
K_bviii—K_b—Si1iii | 89.6 (3) | Ti_m1(2)—Ba—Ohx | 137.8 (4) |
K_bviii—K_b—Si1ix | 89.6 (3) | Ti_m1(2)—Ba—Baxvi | 103.92 (10) |
K_bviii—K_b—Si1x | 154.16 (6) | Ti_m1(2)—Ba—Baxiii | 53.51 (8) |
K_bviii—K_b—Si2 | 81.8 (3) | Ti_m1(2)—Ba—W2 | 76.3 (2) |
K_bviii—K_b—Si2x | 81.8 (3) | Ti_m1(2)—Ba—W2xvii | 129.8 (2) |
K_bviii—K_b—O3 | 135.8 (4) | Ti_m1(2)—Ba—W_c | 0 |
K_bviii—K_b—O3x | 135.8 (4) | Ti_m1(2)—Ba—Nb_m1(1) | 55.16 (4) |
K_bviii—K_b—O4iii | 92.8 (4) | Ti_m1(2)—Ba—Nb_m1(1)xviii | 145.32 (9) |
K_bviii—K_b—O5 | 80.6 (4) | Ti_m1(2)—Ba—Ti_m2 | 53.51 (8) |
K_bviii—K_b—Ba | 128.3 (4) | Ti_m1(2)—Ba—Mg_m2 | 53.51 (8) |
K_bviii—K_b—W1xi | 47.3 (2) | Ti_m1(2)xv—Ba—Fe_m2 | 53.51 (8) |
K_bviii—K_b—W1ix | 47.3 (2) | Ti_m1(2)xv—Ba—Si2 | 93.50 (12) |
Si1—K_b—Si1iii | 78.9 (2) | Ti_m1(2)xv—Ba—Si2x | 52.77 (10) |
Si1—K_b—Si1ix | 99.7 (3) | Ti_m1(2)xv—Ba—O1xiii | 88.7 (3) |
Si1—K_b—Si1x | 51.61 (10) | Ti_m1(2)xv—Ba—O1xv | 33.1 (2) |
Si1—K_b—Si2 | 88.8 (2) | Ti_m1(2)xv—Ba—O3 | 140.80 (18) |
Si1—K_b—Si2x | 108.5 (3) | Ti_m1(2)xv—Ba—O3x | 84.5 (3) |
Si1—K_b—O3 | 27.6 (4) | Ti_m1(2)xv—Ba—Oh | 137.8 (4) |
Si1—K_b—O3x | 67.2 (2) | Ti_m1(2)xv—Ba—Ohx | 31.2 (4) |
Si1—K_b—O4iii | 86.2 (3) | Ti_m1(2)xv—Ba—Baxvi | 103.92 (10) |
Si1—K_b—O5 | 99.6 (4) | Ti_m1(2)xv—Ba—Baxiii | 53.51 (8) |
Si1—K_b—Ba | 57.19 (19) | Ti_m1(2)xv—Ba—W2 | 129.8 (2) |
Si1—K_b—W1xi | 106.9 (2) | Ti_m1(2)xv—Ba—W2xvii | 76.3 (2) |
Si1—K_b—W1ix | 158.4 (3) | Ti_m1(2)xv—Ba—W_c | 0 |
Si1iii—K_b—Si1ix | 49.0 (2) | Ti_m1(2)xv—Ba—Nb_m1(1) | 145.32 (9) |
Si1iii—K_b—Si1x | 99.7 (3) | Ti_m1(2)xv—Ba—Nb_m1(1)xviii | 55.16 (4) |
Si1iii—K_b—Si2 | 131.70 (9) | Ti_m1(2)xv—Ba—Ti_m2 | 53.51 (8) |
Si1iii—K_b—Si2x | 171.22 (16) | Ti_m1(2)xv—Ba—Mg_m2 | 53.51 (8) |
Si1iii—K_b—O3 | 97.6 (4) | Fe_m2—Ba—Si2 | 62.78 (14) |
Si1iii—K_b—O3x | 127.3 (5) | Fe_m2—Ba—Si2x | 62.78 (14) |
Si1iii—K_b—O4iii | 24.69 (11) | Fe_m2—Ba—O1xiii | 43.7 (2) |
Si1iii—K_b—O5 | 153.72 (15) | Fe_m2—Ba—O1xv | 43.7 (2) |
Si1iii—K_b—Ba | 135.94 (15) | Fe_m2—Ba—O3 | 124.8 (3) |
Si1iii—K_b—W1xi | 71.9 (2) | Fe_m2—Ba—O3x | 124.8 (3) |
Si1iii—K_b—W1ix | 107.4 (3) | Fe_m2—Ba—Oh | 84.5 (4) |
Si1ix—K_b—Si1x | 78.9 (2) | Fe_m2—Ba—Ohx | 84.5 (4) |
Si1ix—K_b—Si2 | 171.22 (16) | Fe_m2—Ba—Baxvi | 113.9 (2) |
Si1ix—K_b—Si2x | 131.70 (9) | Fe_m2—Ba—Baxiii | 0.0 (5) |
Si1ix—K_b—O3 | 127.3 (5) | Fe_m2—Ba—W2 | 109.8 (2) |
Si1ix—K_b—O3x | 97.6 (4) | Fe_m2—Ba—W2xvii | 109.8 (2) |
Si1ix—K_b—O4iii | 24.69 (11) | Fe_m2—Ba—W_c | 0 |
Si1ix—K_b—O5 | 153.72 (15) | Fe_m2—Ba—Nb_m1(1) | 102.18 (7) |
Si1ix—K_b—Ba | 135.94 (15) | Fe_m2—Ba—Nb_m1(1)xviii | 102.18 (7) |
Si1ix—K_b—W1xi | 107.4 (3) | Fe_m2—Ba—Ti_m2 | 0.0 (5) |
Si1ix—K_b—W1ix | 71.9 (2) | Fe_m2—Ba—Mg_m2 | 0.0 (5) |
Si1x—K_b—Si2 | 108.5 (3) | Si2—Ba—Si2x | 48.93 (7) |
Si1x—K_b—Si2x | 88.8 (2) | Si2—Ba—O1xiii | 80.1 (2) |
Si1x—K_b—O3 | 67.2 (2) | Si2—Ba—O1xv | 104.4 (3) |
Si1x—K_b—O3x | 27.6 (4) | Si2—Ba—O3 | 63.3 (3) |
Si1x—K_b—O4iii | 86.2 (3) | Si2—Ba—O3x | 90.0 (2) |
Si1x—K_b—O5 | 99.6 (4) | Si2—Ba—Oh | 59.14 (15) |
Si1x—K_b—Ba | 57.19 (19) | Si2—Ba—Ohx | 108.02 (16) |
Si1x—K_b—W1xi | 158.4 (3) | Si2—Ba—Baxvi | 154.78 (7) |
Si1x—K_b—W1ix | 106.9 (2) | Si2—Ba—Baxiii | 62.78 (16) |
Si2—K_b—Si2x | 45.90 (17) | Si2—Ba—W2 | 122.2 (2) |
Si2—K_b—O3 | 61.1 (4) | Si2—Ba—W2xvii | 169.8 (2) |
Si2—K_b—O3x | 87.9 (5) | Si2—Ba—W_c | 0 |
Si2—K_b—O4iii | 156.29 (12) | Si2—Ba—Nb_m1(1) | 51.82 (8) |
Si2—K_b—O5 | 22.95 (10) | Si2—Ba—Nb_m1(1)xviii | 95.73 (9) |
Si2—K_b—Ba | 51.35 (17) | Si2—Ba—Ti_m2 | 62.78 (14) |
Si2—K_b—W1xi | 67.4 (2) | Si2—Ba—Mg_m2 | 62.78 (14) |
Si2—K_b—W1ix | 100.9 (3) | Si2x—Ba—O1xiii | 104.4 (3) |
Si2x—K_b—O3 | 87.9 (5) | Si2x—Ba—O1xv | 80.1 (2) |
Si2x—K_b—O3x | 61.1 (4) | Si2x—Ba—O3 | 90.0 (2) |
Si2x—K_b—O4iii | 156.29 (12) | Si2x—Ba—O3x | 63.3 (3) |
Si2x—K_b—O5 | 22.95 (10) | Si2x—Ba—Oh | 108.02 (16) |
Si2x—K_b—Ba | 51.35 (17) | Si2x—Ba—Ohx | 59.14 (15) |
Si2x—K_b—W1xi | 100.9 (3) | Si2x—Ba—Baxvi | 154.78 (7) |
Si2x—K_b—W1ix | 67.4 (2) | Si2x—Ba—Baxiii | 62.78 (16) |
O3—K_b—O3x | 69.8 (3) | Si2x—Ba—W2 | 169.8 (2) |
O3—K_b—O4iii | 111.3 (5) | Si2x—Ba—W2xvii | 122.2 (2) |
O3—K_b—O5 | 74.0 (5) | Si2x—Ba—W_c | 0 |
O3—K_b—Ba | 40.8 (4) | Si2x—Ba—Nb_m1(1) | 95.73 (9) |
O3—K_b—W1xi | 93.8 (3) | Si2x—Ba—Nb_m1(1)xviii | 51.82 (8) |
O3—K_b—W1ix | 155.0 (6) | Si2x—Ba—Ti_m2 | 62.78 (14) |
O3x—K_b—O4iii | 111.3 (5) | Si2x—Ba—Mg_m2 | 62.78 (14) |
O3x—K_b—O5 | 74.0 (5) | O1xiii—Ba—O1xv | 60.8 (4) |
O3x—K_b—Ba | 40.8 (4) | O1xiii—Ba—O3 | 115.4 (4) |
O3x—K_b—W1xi | 155.0 (6) | O1xiii—Ba—O3x | 167.6 (3) |
O3x—K_b—W1ix | 93.8 (3) | O1xiii—Ba—Oh | 57.5 (5) |
O4iii—K_b—O5 | 173.4 (4) | O1xiii—Ba—Ohx | 117.9 (5) |
O4iii—K_b—Ba | 138.8 (3) | O1xiii—Ba—Baxvi | 82.16 (19) |
O4iii—K_b—W1xi | 91.9 (3) | O1xiii—Ba—Baxiii | 43.7 (2) |
O4iii—K_b—W1ix | 91.9 (3) | O1xiii—Ba—W2 | 67.0 (2) |
O5—K_b—Ba | 47.7 (3) | O1xiii—Ba—W2xvii | 99.3 (3) |
O5—K_b—W1xi | 83.7 (3) | O1xiii—Ba—W_c | 0 |
O5—K_b—W1ix | 83.7 (3) | O1xiii—Ba—Nb_m1(1) | 85.8 (2) |
Ba—K_b—W1xi | 114.9 (3) | O1xiii—Ba—Nb_m1(1)xviii | 143.5 (3) |
Ba—K_b—W1ix | 114.9 (3) | O1xiii—Ba—Ti_m2 | 43.7 (2) |
W1xi—K_b—W1ix | 94.7 (4) | O1xiii—Ba—Mg_m2 | 43.7 (2) |
Na_axi—Ti_m1(1)—Na_av | 180.0 (5) | O1xv—Ba—O3 | 167.6 (3) |
Na_axi—Ti_m1(1)—O2 | 38.1 (6) | O1xv—Ba—O3x | 115.4 (4) |
Na_axi—Ti_m1(1)—O2iv | 141.9 (6) | O1xv—Ba—Oh | 117.9 (5) |
Na_axi—Ti_m1(1)—O3 | 101.5 (4) | O1xv—Ba—Ohx | 57.5 (5) |
Na_axi—Ti_m1(1)—O3iv | 78.5 (4) | O1xv—Ba—Baxvi | 82.16 (19) |
Na_axi—Ti_m1(1)—Oh | 125.4 (6) | O1xv—Ba—Baxiii | 43.7 (2) |
Na_axi—Ti_m1(1)—Ohiv | 54.6 (6) | O1xv—Ba—W2 | 99.3 (3) |
Na_axi—Ti_m1(1)—Ba | 115.1 (3) | O1xv—Ba—W2xvii | 67.0 (2) |
Na_axi—Ti_m1(1)—Baxii | 64.9 (3) | O1xv—Ba—W_c | 0 |
Na_axi—Ti_m1(1)—Nb_m1(1) | 0 | O1xv—Ba—Nb_m1(1) | 143.5 (3) |
Na_av—Ti_m1(1)—O2 | 141.9 (6) | O1xv—Ba—Nb_m1(1)xviii | 85.8 (2) |
Na_av—Ti_m1(1)—O2iv | 38.1 (6) | O1xv—Ba—Ti_m2 | 43.7 (2) |
Na_av—Ti_m1(1)—O3 | 78.5 (4) | O1xv—Ba—Mg_m2 | 43.7 (2) |
Na_av—Ti_m1(1)—O3iv | 101.5 (4) | O3—Ba—O3x | 65.6 (4) |
Na_av—Ti_m1(1)—Oh | 54.6 (6) | O3—Ba—Oh | 58.1 (5) |
Na_av—Ti_m1(1)—Ohiv | 125.4 (6) | O3—Ba—Ohx | 123.2 (5) |
Na_av—Ti_m1(1)—Ba | 64.9 (3) | O3—Ba—Baxvi | 109.5 (2) |
Na_av—Ti_m1(1)—Baxii | 115.1 (3) | O3—Ba—Baxiii | 124.8 (3) |
Na_av—Ti_m1(1)—Nb_m1(1) | 0 | O3—Ba—W2 | 89.1 (2) |
O2—Ti_m1(1)—O2iv | 180.0 (5) | O3—Ba—W2xvii | 125.1 (3) |
O2—Ti_m1(1)—O3 | 88.2 (4) | O3—Ba—W_c | 0 |
O2—Ti_m1(1)—O3iv | 91.8 (4) | O3—Ba—Nb_m1(1) | 29.7 (3) |
O2—Ti_m1(1)—Oh | 90.1 (6) | O3—Ba—Nb_m1(1)xviii | 94.0 (3) |
O2—Ti_m1(1)—Ohiv | 89.9 (6) | O3—Ba—Ti_m2 | 124.8 (3) |
O2—Ti_m1(1)—Ba | 80.3 (3) | O3—Ba—Mg_m2 | 124.8 (3) |
O2—Ti_m1(1)—Baxii | 99.7 (3) | O3x—Ba—Oh | 123.2 (5) |
O2—Ti_m1(1)—Nb_m1(1) | 0 | O3x—Ba—Ohx | 58.1 (5) |
O2iv—Ti_m1(1)—O3 | 91.8 (4) | O3x—Ba—Baxvi | 109.5 (2) |
O2iv—Ti_m1(1)—O3iv | 88.2 (4) | O3x—Ba—Baxiii | 124.8 (3) |
O2iv—Ti_m1(1)—Oh | 89.9 (6) | O3x—Ba—W2 | 125.1 (3) |
O2iv—Ti_m1(1)—Ohiv | 90.1 (6) | O3x—Ba—W2xvii | 89.1 (2) |
O2iv—Ti_m1(1)—Ba | 99.7 (3) | O3x—Ba—W_c | 0 |
O2iv—Ti_m1(1)—Baxii | 80.3 (3) | O3x—Ba—Nb_m1(1) | 94.0 (3) |
O2iv—Ti_m1(1)—Nb_m1(1) | 0 | O3x—Ba—Nb_m1(1)xviii | 29.7 (3) |
O3—Ti_m1(1)—O3iv | 180.0 (5) | O3x—Ba—Ti_m2 | 124.8 (3) |
O3—Ti_m1(1)—Oh | 89.2 (6) | O3x—Ba—Mg_m2 | 124.8 (3) |
O3—Ti_m1(1)—Ohiv | 90.8 (6) | Oh—Ba—Ohx | 166.1 (3) |
O3—Ti_m1(1)—Ba | 45.7 (6) | Oh—Ba—Baxvi | 96.09 (15) |
O3—Ti_m1(1)—Baxii | 134.3 (6) | Oh—Ba—Baxiii | 84.5 (4) |
O3—Ti_m1(1)—Nb_m1(1) | 0 | Oh—Ba—W2 | 63.1 (3) |
O3iv—Ti_m1(1)—Oh | 90.8 (6) | Oh—Ba—W2xvii | 129.0 (3) |
O3iv—Ti_m1(1)—Ohiv | 89.2 (6) | Oh—Ba—W_c | 0 |
O3iv—Ti_m1(1)—Ba | 134.3 (6) | Oh—Ba—Nb_m1(1) | 29.2 (4) |
O3iv—Ti_m1(1)—Baxii | 45.7 (6) | Oh—Ba—Nb_m1(1)xviii | 147.9 (3) |
O3iv—Ti_m1(1)—Nb_m1(1) | 0 | Oh—Ba—Ti_m2 | 84.5 (4) |
Oh—Ti_m1(1)—Ohiv | 180.0 (5) | Oh—Ba—Mg_m2 | 84.5 (4) |
Oh—Ti_m1(1)—Ba | 44.7 (3) | Ohx—Ba—Baxvi | 96.09 (15) |
Oh—Ti_m1(1)—Baxii | 135.3 (3) | Ohx—Ba—Baxiii | 84.5 (4) |
Oh—Ti_m1(1)—Nb_m1(1) | 0 | Ohx—Ba—W2 | 129.0 (3) |
Ohiv—Ti_m1(1)—Ba | 135.3 (3) | Ohx—Ba—W2xvii | 63.1 (3) |
Ohiv—Ti_m1(1)—Baxii | 44.7 (3) | Ohx—Ba—W_c | 0 |
Ohiv—Ti_m1(1)—Nb_m1(1) | 0 | Ohx—Ba—Nb_m1(1) | 147.9 (3) |
Ba—Ti_m1(1)—Baxii | 180.0 (5) | Ohx—Ba—Nb_m1(1)xviii | 29.2 (4) |
Ba—Ti_m1(1)—Nb_m1(1) | 0 | Ohx—Ba—Ti_m2 | 84.5 (4) |
Baxii—Ti_m1(1)—Nb_m1(1) | 0 | Ohx—Ba—Mg_m2 | 84.5 (4) |
Na_aiv—Ti_m1(2)—Na_axiv | 174.4 (3) | Baxvi—Ba—Baxiii | 113.86 (17) |
Na_aiv—Ti_m1(2)—Fe_m2 | 92.8 (2) | Baxvi—Ba—W2 | 33.0 (2) |
Na_aiv—Ti_m1(2)—O1 | 58.7 (4) | Baxvi—Ba—W2xvii | 33.0 (2) |
Na_aiv—Ti_m1(2)—O1xiii | 126.5 (4) | Baxvi—Ba—W_c | 0 |
Na_aiv—Ti_m1(2)—O6iv | 44.2 (5) | Baxvi—Ba—Nb_m1(1) | 109.15 (7) |
Na_aiv—Ti_m1(2)—O6xiv | 130.8 (5) | Baxvi—Ba—Nb_m1(1)xviii | 109.15 (7) |
Na_aiv—Ti_m1(2)—Oh | 122.0 (6) | Baxvi—Ba—Ti_m2 | 113.9 (2) |
Na_aiv—Ti_m1(2)—Ohxiii | 58.4 (6) | Baxvi—Ba—Mg_m2 | 113.9 (2) |
Na_aiv—Ti_m1(2)—Ba | 114.0 (3) | Baxiii—Ba—W2 | 109.83 (19) |
Na_aiv—Ti_m1(2)—Baxiii | 70.9 (3) | Baxiii—Ba—W2xvii | 109.83 (19) |
Na_aiv—Ti_m1(2)—Ti_m2 | 92.8 (2) | Baxiii—Ba—W_c | 0 |
Na_aiv—Ti_m1(2)—Mg_m2 | 92.8 (2) | Baxiii—Ba—Nb_m1(1) | 102.18 (8) |
Na_axiv—Ti_m1(2)—Fe_m2 | 92.8 (2) | Baxiii—Ba—Nb_m1(1)xviii | 102.18 (8) |
Na_axiv—Ti_m1(2)—O1 | 126.5 (4) | Baxiii—Ba—Ti_m2 | 0.0 (5) |
Na_axiv—Ti_m1(2)—O1xiii | 58.7 (4) | Baxiii—Ba—Mg_m2 | 0.0 (5) |
Na_axiv—Ti_m1(2)—O6iv | 130.8 (5) | W2—Ba—W2xvii | 66.0 (3) |
Na_axiv—Ti_m1(2)—O6xiv | 44.2 (5) | W2—Ba—W_c | 0 |
Na_axiv—Ti_m1(2)—Oh | 58.4 (6) | W2—Ba—Nb_m1(1) | 78.6 (2) |
Na_axiv—Ti_m1(2)—Ohxiii | 122.0 (6) | W2—Ba—Nb_m1(1)xviii | 138.3 (2) |
Na_axiv—Ti_m1(2)—Ba | 70.9 (3) | W2—Ba—Ti_m2 | 109.8 (2) |
Na_axiv—Ti_m1(2)—Baxiii | 114.0 (3) | W2—Ba—Mg_m2 | 109.8 (2) |
Na_axiv—Ti_m1(2)—Ti_m2 | 92.8 (2) | W2xvii—Ba—W_c | 0 |
Na_axiv—Ti_m1(2)—Mg_m2 | 92.8 (2) | W2xvii—Ba—Nb_m1(1) | 138.3 (2) |
Fe_m2—Ti_m1(2)—O1 | 40.9 (2) | W2xvii—Ba—Nb_m1(1)xviii | 78.6 (2) |
Fe_m2—Ti_m1(2)—O1xiii | 40.9 (2) | W2xvii—Ba—Ti_m2 | 109.8 (2) |
Fe_m2—Ti_m1(2)—O6iv | 130.5 (3) | W2xvii—Ba—Mg_m2 | 109.8 (2) |
Fe_m2—Ti_m1(2)—O6xiv | 130.5 (3) | W_c—Ba—Nb_m1(1) | 0 |
Fe_m2—Ti_m1(2)—Oh | 86.8 (2) | W_c—Ba—Nb_m1(1)xviii | 0 |
Fe_m2—Ti_m1(2)—Ohxiii | 86.8 (2) | W_c—Ba—Ti_m2 | 0 |
Fe_m2—Ti_m1(2)—Ba | 36.49 (8) | W_c—Ba—Mg_m2 | 0 |
Fe_m2—Ti_m1(2)—Baxiii | 36.49 (8) | Nb_m1(1)—Ba—Nb_m1(1)xviii | 120.15 (15) |
Fe_m2—Ti_m1(2)—Ti_m2 | 0.0 (5) | Nb_m1(1)—Ba—Ti_m2 | 102.18 (7) |
Fe_m2—Ti_m1(2)—Mg_m2 | 0.0 (5) | Nb_m1(1)—Ba—Mg_m2 | 102.18 (7) |
O1—Ti_m1(2)—O1xiii | 81.7 (4) | Nb_m1(1)xviii—Ba—Ti_m2 | 102.18 (7) |
O1—Ti_m1(2)—O6iv | 89.8 (4) | Nb_m1(1)xviii—Ba—Mg_m2 | 102.18 (7) |
O1—Ti_m1(2)—O6xiv | 170.4 (4) | Ti_m2—Ba—Mg_m2 | 0.0 (5) |
O1—Ti_m1(2)—Oh | 87.8 (6) | Na_a—W1—Na_ai | 69.1 (11) |
O1—Ti_m1(2)—Ohxiii | 87.3 (6) | Na_a—W1—K_bii | 128.9 (5) |
O1—Ti_m1(2)—Ba | 55.7 (3) | Na_a—W1—K_biii | 125.7 (5) |
O1—Ti_m1(2)—Baxiii | 49.2 (5) | Na_ai—W1—K_bii | 125.7 (5) |
O1—Ti_m1(2)—Ti_m2 | 40.9 (2) | Na_ai—W1—K_biii | 128.9 (5) |
O1—Ti_m1(2)—Mg_m2 | 40.9 (2) | K_bii—W1—K_biii | 85.3 (5) |
O1xiii—Ti_m1(2)—O6iv | 170.4 (4) | Na_av—W2—Na_axiv | 71.3 (11) |
O1xiii—Ti_m1(2)—O6xiv | 89.8 (4) | Na_av—W2—Ba | 114.9 (4) |
O1xiii—Ti_m1(2)—Oh | 87.3 (6) | Na_av—W2—Baxvi | 117.6 (4) |
O1xiii—Ti_m1(2)—Ohxiii | 87.8 (6) | Na_axiv—W2—Ba | 117.6 (4) |
O1xiii—Ti_m1(2)—Ba | 49.2 (5) | Na_axiv—W2—Baxvi | 114.9 (4) |
O1xiii—Ti_m1(2)—Baxiii | 55.7 (3) | Ba—W2—Baxvi | 114.0 (4) |
O1xiii—Ti_m1(2)—Ti_m2 | 40.9 (2) | Fe_m2—W_c—Ba | 0 |
O1xiii—Ti_m1(2)—Mg_m2 | 40.9 (2) | Fe_m2—W_c—Ti_m2 | 0.0 (5) |
O6iv—Ti_m1(2)—O6xiv | 98.9 (4) | Ba—W_c—Ti_m2 | 0 |
O6iv—Ti_m1(2)—Oh | 96.9 (7) | Na_axi—Nb_m1(1)—Na_av | 180.0 (5) |
O6iv—Ti_m1(2)—Ohxiii | 87.2 (7) | Na_axi—Nb_m1(1)—Ti_m1(1) | 0 |
O6iv—Ti_m1(2)—Ba | 128.4 (6) | Na_axi—Nb_m1(1)—O2 | 38.1 (6) |
O6iv—Ti_m1(2)—Baxiii | 115.0 (4) | Na_axi—Nb_m1(1)—O2iv | 141.9 (6) |
O6iv—Ti_m1(2)—Ti_m2 | 130.5 (3) | Na_axi—Nb_m1(1)—O3 | 101.5 (4) |
O6iv—Ti_m1(2)—Mg_m2 | 130.5 (3) | Na_axi—Nb_m1(1)—O3iv | 78.5 (4) |
O6xiv—Ti_m1(2)—Oh | 87.2 (7) | Na_axi—Nb_m1(1)—Oh | 125.4 (6) |
O6xiv—Ti_m1(2)—Ohxiii | 96.9 (7) | Na_axi—Nb_m1(1)—Ohiv | 54.6 (6) |
O6xiv—Ti_m1(2)—Ba | 115.0 (4) | Na_axi—Nb_m1(1)—Ba | 115.1 (3) |
O6xiv—Ti_m1(2)—Baxiii | 128.4 (6) | Na_axi—Nb_m1(1)—Baxii | 64.9 (3) |
O6xiv—Ti_m1(2)—Ti_m2 | 130.5 (3) | Na_av—Nb_m1(1)—Ti_m1(1) | 0 |
O6xiv—Ti_m1(2)—Mg_m2 | 130.5 (3) | Na_av—Nb_m1(1)—O2 | 141.9 (6) |
Oh—Ti_m1(2)—Ohxiii | 173.6 (3) | Na_av—Nb_m1(1)—O2iv | 38.1 (6) |
Oh—Ti_m1(2)—Ba | 50.6 (2) | Na_av—Nb_m1(1)—O3 | 78.5 (4) |
Oh—Ti_m1(2)—Baxiii | 123.0 (2) | Na_av—Nb_m1(1)—O3iv | 101.5 (4) |
Oh—Ti_m1(2)—Ti_m2 | 86.8 (2) | Na_av—Nb_m1(1)—Oh | 54.6 (6) |
Oh—Ti_m1(2)—Mg_m2 | 86.8 (2) | Na_av—Nb_m1(1)—Ohiv | 125.4 (6) |
Ohxiii—Ti_m1(2)—Ba | 123.0 (2) | Na_av—Nb_m1(1)—Ba | 64.9 (3) |
Ohxiii—Ti_m1(2)—Baxiii | 50.6 (2) | Na_av—Nb_m1(1)—Baxii | 115.1 (3) |
Ohxiii—Ti_m1(2)—Ti_m2 | 86.8 (2) | Ti_m1(1)—Nb_m1(1)—O2 | 0 |
Ohxiii—Ti_m1(2)—Mg_m2 | 86.8 (2) | Ti_m1(1)—Nb_m1(1)—O2iv | 0 |
Ba—Ti_m1(2)—Baxiii | 72.97 (12) | Ti_m1(1)—Nb_m1(1)—O3 | 0 |
Ba—Ti_m1(2)—Ti_m2 | 36.49 (8) | Ti_m1(1)—Nb_m1(1)—O3iv | 0 |
Ba—Ti_m1(2)—Mg_m2 | 36.49 (8) | Ti_m1(1)—Nb_m1(1)—Oh | 0 |
Baxiii—Ti_m1(2)—Ti_m2 | 36.49 (8) | Ti_m1(1)—Nb_m1(1)—Ohiv | 0 |
Baxiii—Ti_m1(2)—Mg_m2 | 36.49 (8) | Ti_m1(1)—Nb_m1(1)—Ba | 0 |
Ti_m2—Ti_m1(2)—Mg_m2 | 0.0 (5) | Ti_m1(1)—Nb_m1(1)—Baxii | 0 |
Ti_m1(2)—Fe_m2—Ti_m1(2)xv | 180.0 (5) | O2—Nb_m1(1)—O2iv | 180.0 (5) |
Ti_m1(2)—Fe_m2—O1 | 43.0 (2) | O2—Nb_m1(1)—O3 | 88.2 (4) |
Ti_m1(2)—Fe_m2—O1xiii | 43.0 (2) | O2—Nb_m1(1)—O3iv | 91.8 (4) |
Ti_m1(2)—Fe_m2—O1xv | 137.0 (2) | O2—Nb_m1(1)—Oh | 90.1 (6) |
Ti_m1(2)—Fe_m2—O1x | 137.0 (2) | O2—Nb_m1(1)—Ohiv | 89.9 (6) |
Ti_m1(2)—Fe_m2—Ba | 90 | O2—Nb_m1(1)—Ba | 80.3 (3) |
Ti_m1(2)—Fe_m2—Baxiii | 90 | O2—Nb_m1(1)—Baxii | 99.7 (3) |
Ti_m1(2)—Fe_m2—W_c | 90 | O2iv—Nb_m1(1)—O3 | 91.8 (4) |
Ti_m1(2)—Fe_m2—W_cxiii | 90 | O2iv—Nb_m1(1)—O3iv | 88.2 (4) |
Ti_m1(2)—Fe_m2—Ti_m2 | 0 | O2iv—Nb_m1(1)—Oh | 89.9 (6) |
Ti_m1(2)—Fe_m2—Mg_m2 | 0 | O2iv—Nb_m1(1)—Ohiv | 90.1 (6) |
Ti_m1(2)xv—Fe_m2—O1 | 137.0 (2) | O2iv—Nb_m1(1)—Ba | 99.7 (3) |
Ti_m1(2)xv—Fe_m2—O1xiii | 137.0 (2) | O2iv—Nb_m1(1)—Baxii | 80.3 (3) |
Ti_m1(2)xv—Fe_m2—O1xv | 43.0 (2) | O3—Nb_m1(1)—O3iv | 180.0 (5) |
Ti_m1(2)xv—Fe_m2—O1x | 43.0 (2) | O3—Nb_m1(1)—Oh | 89.2 (6) |
Ti_m1(2)xv—Fe_m2—Ba | 90 | O3—Nb_m1(1)—Ohiv | 90.8 (6) |
Ti_m1(2)xv—Fe_m2—Baxiii | 90 | O3—Nb_m1(1)—Ba | 45.7 (6) |
Ti_m1(2)xv—Fe_m2—W_c | 90 | O3—Nb_m1(1)—Baxii | 134.3 (6) |
Ti_m1(2)xv—Fe_m2—W_cxiii | 90 | O3iv—Nb_m1(1)—Oh | 90.8 (6) |
Ti_m1(2)xv—Fe_m2—Ti_m2 | 0 | O3iv—Nb_m1(1)—Ohiv | 89.2 (6) |
Ti_m1(2)xv—Fe_m2—Mg_m2 | 0 | O3iv—Nb_m1(1)—Ba | 134.3 (6) |
O1—Fe_m2—O1xiii | 86.0 (4) | O3iv—Nb_m1(1)—Baxii | 45.7 (6) |
O1—Fe_m2—O1xv | 180.0 (5) | Oh—Nb_m1(1)—Ohiv | 180.0 (5) |
O1—Fe_m2—O1x | 94.0 (4) | Oh—Nb_m1(1)—Ba | 44.7 (3) |
O1—Fe_m2—Ba | 94.5 (6) | Oh—Nb_m1(1)—Baxii | 135.3 (3) |
O1—Fe_m2—Baxiii | 85.5 (6) | Ohiv—Nb_m1(1)—Ba | 135.3 (3) |
O1—Fe_m2—W_c | 94.5 (6) | Ohiv—Nb_m1(1)—Baxii | 44.7 (3) |
O1—Fe_m2—W_cxiii | 85.5 (6) | Ba—Nb_m1(1)—Baxii | 180.0 (5) |
O1—Fe_m2—Ti_m2 | 0 | Ti_m1(2)—Ti_m2—Ti_m1(2)xv | 180.0 (5) |
O1—Fe_m2—Mg_m2 | 0 | Ti_m1(2)—Ti_m2—Fe_m2 | 0 |
O1xiii—Fe_m2—O1xv | 94.0 (4) | Ti_m1(2)—Ti_m2—O1 | 43.0 (2) |
O1xiii—Fe_m2—O1x | 180.0 (5) | Ti_m1(2)—Ti_m2—O1xiii | 43.0 (2) |
O1xiii—Fe_m2—Ba | 85.5 (6) | Ti_m1(2)—Ti_m2—O1xv | 137.0 (2) |
O1xiii—Fe_m2—Baxiii | 94.5 (6) | Ti_m1(2)—Ti_m2—O1x | 137.0 (2) |
O1xiii—Fe_m2—W_c | 85.5 (6) | Ti_m1(2)—Ti_m2—Ba | 90 |
O1xiii—Fe_m2—W_cxiii | 94.5 (6) | Ti_m1(2)—Ti_m2—Baxiii | 90 |
O1xiii—Fe_m2—Ti_m2 | 0 | Ti_m1(2)—Ti_m2—W_c | 90 |
O1xiii—Fe_m2—Mg_m2 | 0 | Ti_m1(2)—Ti_m2—W_cxiii | 90 |
O1xv—Fe_m2—O1x | 86.0 (4) | Ti_m1(2)—Ti_m2—Mg_m2 | 0 |
O1xv—Fe_m2—Ba | 85.5 (6) | Ti_m1(2)xv—Ti_m2—Fe_m2 | 0 |
O1xv—Fe_m2—Baxiii | 94.5 (6) | Ti_m1(2)xv—Ti_m2—O1 | 137.0 (2) |
O1xv—Fe_m2—W_c | 85.5 (6) | Ti_m1(2)xv—Ti_m2—O1xiii | 137.0 (2) |
O1xv—Fe_m2—W_cxiii | 94.5 (6) | Ti_m1(2)xv—Ti_m2—O1xv | 43.0 (2) |
O1xv—Fe_m2—Ti_m2 | 0 | Ti_m1(2)xv—Ti_m2—O1x | 43.0 (2) |
O1xv—Fe_m2—Mg_m2 | 0 | Ti_m1(2)xv—Ti_m2—Ba | 90 |
O1x—Fe_m2—Ba | 94.5 (6) | Ti_m1(2)xv—Ti_m2—Baxiii | 90 |
O1x—Fe_m2—Baxiii | 85.5 (6) | Ti_m1(2)xv—Ti_m2—W_c | 90 |
O1x—Fe_m2—W_c | 94.5 (6) | Ti_m1(2)xv—Ti_m2—W_cxiii | 90 |
O1x—Fe_m2—W_cxiii | 85.5 (6) | Ti_m1(2)xv—Ti_m2—Mg_m2 | 0 |
O1x—Fe_m2—Ti_m2 | 0 | Fe_m2—Ti_m2—O1 | 0 |
O1x—Fe_m2—Mg_m2 | 0 | Fe_m2—Ti_m2—O1xiii | 0 |
Ba—Fe_m2—Baxiii | 180.0 (5) | Fe_m2—Ti_m2—O1xv | 0 |
Ba—Fe_m2—W_c | 0.0 (5) | Fe_m2—Ti_m2—O1x | 0 |
Ba—Fe_m2—W_cxiii | 180.0 (5) | Fe_m2—Ti_m2—Ba | 0 |
Ba—Fe_m2—Ti_m2 | 0 | Fe_m2—Ti_m2—Baxiii | 0 |
Ba—Fe_m2—Mg_m2 | 0 | Fe_m2—Ti_m2—W_c | 0 |
Baxiii—Fe_m2—W_c | 180.0 (5) | Fe_m2—Ti_m2—W_cxiii | 0 |
Baxiii—Fe_m2—W_cxiii | 0.0 (5) | Fe_m2—Ti_m2—Mg_m2 | 0 |
Baxiii—Fe_m2—Ti_m2 | 0 | O1—Ti_m2—O1xiii | 86.0 (4) |
Baxiii—Fe_m2—Mg_m2 | 0 | O1—Ti_m2—O1xv | 180.0 (5) |
W_c—Fe_m2—W_cxiii | 180.0 (5) | O1—Ti_m2—O1x | 94.0 (4) |
W_c—Fe_m2—Ti_m2 | 0 | O1—Ti_m2—Ba | 94.5 (6) |
W_c—Fe_m2—Mg_m2 | 0 | O1—Ti_m2—Baxiii | 85.5 (6) |
W_cxiii—Fe_m2—Ti_m2 | 0 | O1—Ti_m2—W_c | 94.5 (6) |
W_cxiii—Fe_m2—Mg_m2 | 0 | O1—Ti_m2—W_cxiii | 85.5 (6) |
Ti_m2—Fe_m2—Mg_m2 | 0 | O1—Ti_m2—Mg_m2 | 0 |
K_b—Si1—K_biii | 80.3 (2) | O1xiii—Ti_m2—O1xv | 94.0 (4) |
K_b—Si1—O3 | 52.1 (5) | O1xiii—Ti_m2—O1x | 180.0 (5) |
K_b—Si1—O4 | 62.4 (5) | O1xiii—Ti_m2—Ba | 85.5 (6) |
K_b—Si1—O6 | 103.7 (4) | O1xiii—Ti_m2—Baxiii | 94.5 (6) |
K_b—Si1—O7 | 142.4 (6) | O1xiii—Ti_m2—W_c | 85.5 (6) |
K_biii—Si1—O3 | 132.3 (5) | O1xiii—Ti_m2—W_cxiii | 94.5 (6) |
K_biii—Si1—O4 | 39.8 (9) | O1xiii—Ti_m2—Mg_m2 | 0 |
K_biii—Si1—O6 | 67.0 (7) | O1xv—Ti_m2—O1x | 86.0 (4) |
K_biii—Si1—O7 | 117.6 (6) | O1xv—Ti_m2—Ba | 85.5 (6) |
O3—Si1—O4 | 107.2 (8) | O1xv—Ti_m2—Baxiii | 94.5 (6) |
O3—Si1—O6 | 116.3 (7) | O1xv—Ti_m2—W_c | 85.5 (6) |
O3—Si1—O7 | 104.5 (10) | O1xv—Ti_m2—W_cxiii | 94.5 (6) |
O4—Si1—O6 | 106.0 (11) | O1xv—Ti_m2—Mg_m2 | 0 |
O4—Si1—O7 | 109.0 (5) | O1x—Ti_m2—Ba | 94.5 (6) |
O6—Si1—O7 | 113.6 (6) | O1x—Ti_m2—Baxiii | 85.5 (6) |
Na_aiv—Si2—K_b | 163.2 (4) | O1x—Ti_m2—W_c | 94.5 (6) |
Na_aiv—Si2—O1 | 65.8 (6) | O1x—Ti_m2—W_cxiii | 85.5 (6) |
Na_aiv—Si2—O2 | 98.7 (7) | O1x—Ti_m2—Mg_m2 | 0 |
Na_aiv—Si2—O7xi | 49.8 (6) | Ba—Ti_m2—Baxiii | 180.0 (5) |
Na_aiv—Si2—Ba | 123.4 (4) | Ba—Ti_m2—W_c | 0.0 (5) |
K_b—Si2—O1 | 130.7 (5) | Ba—Ti_m2—W_cxiii | 180.0 (5) |
K_b—Si2—O2 | 72.2 (6) | Ba—Ti_m2—Mg_m2 | 0 |
K_b—Si2—O7xi | 119.9 (6) | Baxiii—Ti_m2—W_c | 180.0 (5) |
K_b—Si2—Ba | 72.59 (17) | Baxiii—Ti_m2—W_cxiii | 0.0 (5) |
O1—Si2—O2 | 114.8 (6) | Baxiii—Ti_m2—Mg_m2 | 0 |
O1—Si2—O7xi | 102.3 (9) | W_c—Ti_m2—W_cxiii | 180.0 (5) |
O1—Si2—Ba | 58.2 (5) | W_c—Ti_m2—Mg_m2 | 0 |
O2—Si2—O7xi | 113.4 (5) | W_cxiii—Ti_m2—Mg_m2 | 0 |
O2—Si2—Ba | 96.7 (3) | Ti_m1(2)—Mg_m2—Ti_m1(2)xv | 180.0 (5) |
O7xi—Si2—Ba | 149.5 (6) | Ti_m1(2)—Mg_m2—Fe_m2 | 0 |
Ti_m1(2)—O1—Fe_m2 | 96.1 (4) | Ti_m1(2)—Mg_m2—O1 | 43.0 (2) |
Ti_m1(2)—O1—Si2 | 121.9 (7) | Ti_m1(2)—Mg_m2—O1xiii | 43.0 (2) |
Ti_m1(2)—O1—Baxiii | 97.6 (7) | Ti_m1(2)—Mg_m2—O1xv | 137.0 (2) |
Ti_m1(2)—O1—Ti_m2 | 96.1 (4) | Ti_m1(2)—Mg_m2—O1x | 137.0 (2) |
Ti_m1(2)—O1—Mg_m2 | 96.1 (4) | Ti_m1(2)—Mg_m2—Ba | 90 |
Fe_m2—O1—Si2 | 127.0 (8) | Ti_m1(2)—Mg_m2—Baxiii | 90 |
Fe_m2—O1—Baxiii | 50.9 (4) | Ti_m1(2)—Mg_m2—Ti_m2 | 0 |
Fe_m2—O1—Ti_m2 | 0.0 (5) | Ti_m1(2)xv—Mg_m2—Fe_m2 | 0 |
Fe_m2—O1—Mg_m2 | 0.0 (5) | Ti_m1(2)xv—Mg_m2—O1 | 137.0 (2) |
Si2—O1—Baxiii | 138.7 (4) | Ti_m1(2)xv—Mg_m2—O1xiii | 137.0 (2) |
Si2—O1—Ti_m2 | 127.0 (8) | Ti_m1(2)xv—Mg_m2—O1xv | 43.0 (2) |
Si2—O1—Mg_m2 | 127.0 (8) | Ti_m1(2)xv—Mg_m2—O1x | 43.0 (2) |
Baxiii—O1—Ti_m2 | 50.9 (4) | Ti_m1(2)xv—Mg_m2—Ba | 90 |
Baxiii—O1—Mg_m2 | 50.9 (4) | Ti_m1(2)xv—Mg_m2—Baxiii | 90 |
Ti_m2—O1—Mg_m2 | 0.0 (5) | Ti_m1(2)xv—Mg_m2—Ti_m2 | 0 |
Na_axi—O2—Ti_m1(1) | 109.3 (8) | Fe_m2—Mg_m2—O1 | 0 |
Na_axi—O2—Si2 | 120.6 (6) | Fe_m2—Mg_m2—O1xiii | 0 |
Na_axi—O2—Nb_m1(1) | 109.3 (8) | Fe_m2—Mg_m2—O1xv | 0 |
Ti_m1(1)—O2—Si2 | 129.5 (5) | Fe_m2—Mg_m2—O1x | 0 |
Ti_m1(1)—O2—Nb_m1(1) | 0.0 (5) | Fe_m2—Mg_m2—Ba | 0 |
Si2—O2—Nb_m1(1) | 129.5 (5) | Fe_m2—Mg_m2—Baxiii | 0 |
K_b—O3—Ti_m1(1) | 121.6 (3) | Fe_m2—Mg_m2—Ti_m2 | 0 |
K_b—O3—Si1 | 100.2 (8) | O1—Mg_m2—O1xiii | 86.0 (4) |
K_b—O3—Ba | 101.0 (4) | O1—Mg_m2—O1xv | 180.0 (5) |
K_b—O3—Nb_m1(1) | 121.6 (3) | O1—Mg_m2—O1x | 94.0 (4) |
Ti_m1(1)—O3—Si1 | 116.3 (5) | O1—Mg_m2—Ba | 94.5 (6) |
Ti_m1(1)—O3—Ba | 104.6 (8) | O1—Mg_m2—Baxiii | 85.5 (6) |
Ti_m1(1)—O3—Nb_m1(1) | 0.0 (5) | O1—Mg_m2—Ti_m2 | 0 |
Si1—O3—Ba | 112.2 (4) | O1xiii—Mg_m2—O1xv | 94.0 (4) |
Si1—O3—Nb_m1(1) | 116.3 (5) | O1xiii—Mg_m2—O1x | 180.0 (5) |
Ba—O3—Nb_m1(1) | 104.6 (8) | O1xiii—Mg_m2—Ba | 85.5 (6) |
K_biii—O4—Si1 | 115.5 (9) | O1xiii—Mg_m2—Baxiii | 94.5 (6) |
K_biii—O4—Si1x | 115.5 (9) | O1xiii—Mg_m2—Ti_m2 | 0 |
Si1—O4—Si1x | 127.1 (17) | O1xv—Mg_m2—O1x | 86.0 (4) |
Na_a—O6—Ti_m1(2)iv | 99.8 (7) | O1xv—Mg_m2—Ba | 85.5 (6) |
Na_a—O6—Si1 | 123.4 (7) | O1xv—Mg_m2—Baxiii | 94.5 (6) |
Ti_m1(2)iv—O6—Si1 | 131.2 (10) | O1xv—Mg_m2—Ti_m2 | 0 |
Na_av—O7—Si1 | 123.0 (6) | O1x—Mg_m2—Ba | 94.5 (6) |
Na_av—O7—Si2ii | 97.4 (6) | O1x—Mg_m2—Baxiii | 85.5 (6) |
Si1—O7—Si2ii | 128.2 (13) | O1x—Mg_m2—Ti_m2 | 0 |
Ti_m1(1)—Oh—Ti_m1(2) | 128.4 (4) | Ba—Mg_m2—Baxiii | 180.0 (5) |
Ti_m1(1)—Oh—Ba | 106.1 (6) | Ba—Mg_m2—Ti_m2 | 0 |
Ti_m1(1)—Oh—Nb_m1(1) | 0.0 (5) | Baxiii—Mg_m2—Ti_m2 | 0 |
Ti_m1(2)—Oh—Ba | 98.2 (5) | | |
Symmetry codes: (i) −x+1, y, −z; (ii) x, y, z−1; (iii) −x+1, y, −z+1; (iv) −x+1/2, −y+1/2, −z+1; (v) −x+1/2, −y+1/2, −z; (vi) x+1/2, y+1/2, z; (vii) −x+1/2, y+1/2, −z; (viii) −x+1, y, −z+2; (ix) −x+1, −y, −z+1; (x) x, −y, z; (xi) x, y, z+1; (xii) −x+1/2, y+1/2, −z+1; (xiii) −x, y, −z+1; (xiv) x−1/2, −y+1/2, z; (xv) −x, −y, −z+1; (xvi) −x, y, −z; (xvii) −x, −y, −z; (xviii) −x+1/2, y−1/2, −z+1; (xix) x, −y, z+1; (xx) x−1/2, y−1/2, z; (xxi) −x+1/2, y−1/2, −z. |
Crystal data top
Ba0.7Fe0.5K2.1Mg0.05Na2Nb0.1O33Si8Ti4 | Z = 2 |
Mr = 1206.8 | F(000) = 1167 |
Monoclinic, C2/m | Dx = 3.569 Mg m−3 |
Hall symbol: -C 2y | Synchrotron radiation, λ = 0.414 Å |
a = 13.442 (9) Å | Cell parameters from 2573 reflections |
b = 13.0636 (12) Å | θ = 1.9–19.0° |
c = 7.102 (2) Å | µ = 0.94 mm−1 |
β = 115.81 (5)° | T = 293 K |
V = 1122.7 (10) Å3 | Anhedral grain |
Data collection top
ESRF ID 09 diffractometer | θmax = 19.0°, θmin = 1.9° |
2573 measured reflections | h = −8→8 |
757 independent reflections | k = −20→20 |
391 reflections with I > 2σ(I) | l = −9→10 |
Rint = 0.052 | |
Refinement top
Refinement on F | 0 restraints |
R[F2 > 2σ(F2)] = 0.119 | 6 constraints |
wR(F2) = 0.189 | Weighting scheme based on measured s.u.'s w = 1/(σ2(F) + 0.0143999998F2) |
S = 1.06 | (Δ/σ)max = 0.049 |
757 reflections | Δρmax = 1.31 e Å−3 |
57 parameters | Δρmin = −1.43 e Å−3 |
Fractional atomic coordinates and isotropic or equivalent isotropic displacement parameters (Å2) top | x | y | z | Uiso*/Ueq | Occ. (<1) |
Na_a | 0.420 (3) | 0.2724 (13) | 0.012 (3) | 0.049 (5)* | 0.5 |
K_b | 0.4366 (16) | 0 | 0.7391 (13) | 0.059 (2)* | |
Ti_m1(1) | 0.25 | 0.25 | 0.5 | 0.0273 (11)* | 0.95 |
Ti_m1(2) | 0 | 0.2160 (3) | 0.5 | 0.0249 (11)* | |
Fe_m2 | 0 | 0 | 0.5 | 0.040 (2)* | 0.5 |
Si1 | 0.3319 (8) | 0.1094 (3) | 0.2753 (6) | 0.0182 (10)* | |
Si2 | 0.2110 (7) | 0.1086 (3) | 0.8213 (6) | 0.0161 (10)* | |
O1 | 0.0777 (18) | 0.1032 (7) | 0.6867 (15) | 0.017 (2)* | |
O2 | 0.268 (2) | 0.2013 (7) | 0.7695 (16) | 0.022 (2)* | |
O3 | 0.295 (2) | 0.1143 (8) | 0.4513 (17) | 0.024 (3)* | |
O4 | 0.394 (3) | 0 | 0.294 (2) | 0.017 (3)* | |
O5 | 0.267 (3) | 0 | 0.803 (2) | 0.018 (3)* | |
O6 | 0.420 (2) | 0.1899 (9) | 0.2847 (18) | 0.030 (3)* | |
O7 | 0.2190 (19) | 0.1122 (6) | 0.0565 (14) | 0.013 (2)* | |
Oh | 0.0989 (19) | 0.2082 (7) | 0.3806 (15) | 0.016 (2)* | |
Ba | 0.0980 (7) | 0 | 0.3342 (5) | 0.0223 (9)* | 0.35 |
W1 | 0.5 | 0.1468 (16) | 0 | 0.047 (5)* | |
W2 | 0 | 0.1058 (13) | 0 | 0.036 (5)* | |
W_c | 0.0980 (7) | 0 | 0.3342 (5) | 0.0223 (9)* | 0.65 |
Nb_m1(1) | 0.25 | 0.25 | 0.5 | 0.0273 (11)* | 0.05 |
Ti_m2 | 0 | 0 | 0.5 | 0.040 (2)* | 0.1 |
Mg_m2 | 0 | 0 | 0.5 | 0.040 (2)* | 0.05 |
Atomic displacement parameters (Å2) top | U11 | U22 | U33 | U12 | U13 | U23 |
? | ? | ? | ? | ? | ? | ? |
Geometric parameters (Å, º) top
Na_a—Na_ai | 2.23 (6) | Ti_m1(2)—Ohxiii | 1.87 (2) |
Na_a—K_bii | 4.10 (2) | Ti_m1(2)—Ba | 3.526 (6) |
Na_a—K_biii | 4.07 (2) | Ti_m1(2)—Baxiii | 3.526 (6) |
Na_a—Ti_m1(1)ii | 3.359 (18) | Ti_m1(2)—Ti_m2 | 2.821 (4) |
Na_a—Ti_m1(2)iv | 3.156 (19) | Ti_m1(2)—Mg_m2 | 2.821 (4) |
Na_a—Si2iv | 2.96 (4) | Fe_m2—O1 | 1.860 (10) |
Na_a—O2ii | 2.22 (3) | Fe_m2—O1xiii | 1.860 (10) |
Na_a—O6 | 2.22 (3) | Fe_m2—O1xv | 1.860 (10) |
Na_a—O7v | 2.28 (4) | Fe_m2—O1x | 1.860 (10) |
Na_a—Bavi | 3.88 (2) | Fe_m2—Ba | 2.115 (8) |
Na_a—Bavii | 3.80 (2) | Fe_m2—Baxiii | 2.115 (8) |
Na_a—W1 | 1.98 (3) | Fe_m2—W_c | 2.115 (8) |
Na_a—W2v | 1.94 (3) | Fe_m2—W_cxiii | 2.115 (8) |
Na_a—Nb_m1(1)ii | 3.359 (18) | Fe_m2—Ti_m2 | 0 |
K_b—K_biii | 4.41 (3) | Fe_m2—Mg_m2 | 0 |
K_b—K_bviii | 3.337 (12) | Si1—O3 | 1.54 (2) |
K_b—Si1 | 3.292 (9) | Si1—O4 | 1.630 (18) |
K_b—Si1iii | 3.47 (2) | Si1—O6 | 1.57 (3) |
K_b—Si1ix | 3.47 (2) | Si1—O7 | 1.633 (16) |
K_b—Si1x | 3.292 (9) | Si2—O1 | 1.62 (2) |
K_b—Si2 | 3.62 (2) | Si2—O2 | 1.560 (19) |
K_b—Si2x | 3.62 (2) | Si2—O5 | 1.64 (2) |
K_b—O3 | 2.580 (17) | Si2—O7xi | 1.627 (15) |
K_b—O3x | 2.580 (17) | Si2—Ba | 3.422 (6) |
K_b—O4iii | 2.39 (4) | O1—Baxiii | 2.67 (2) |
K_b—O5 | 2.51 (4) | O1—Ti_m2 | 1.860 (10) |
K_b—Ba | 4.19 (2) | O1—Mg_m2 | 1.860 (10) |
K_b—W1xi | 2.542 (17) | O2—Nb_m1(1) | 1.930 (14) |
K_b—W1ix | 2.542 (17) | O3—Ba | 2.83 (3) |
Ti_m1(1)—O2 | 1.930 (14) | O3—Nb_m1(1) | 1.950 (15) |
Ti_m1(1)—O2iv | 1.930 (14) | Oh—Ba | 2.739 (9) |
Ti_m1(1)—O3 | 1.950 (15) | Oh—Nb_m1(1) | 1.91 (2) |
Ti_m1(1)—O3iv | 1.950 (15) | Ba—Baxvi | 4.312 (7) |
Ti_m1(1)—Oh | 1.91 (2) | Ba—Baxiii | 4.229 (12) |
Ti_m1(1)—Ohiv | 1.91 (2) | Ba—W2 | 2.561 (10) |
Ti_m1(1)—Ba | 3.759 (4) | Ba—W2xvii | 2.561 (10) |
Ti_m1(1)—Baxii | 3.759 (4) | Ba—W_c | 0 |
Ti_m1(1)—Nb_m1(1) | 0 | Ba—Nb_m1(1) | 3.759 (4) |
Ti_m1(2)—Fe_m2 | 2.821 (4) | Ba—Nb_m1(1)xviii | 3.759 (4) |
Ti_m1(2)—O1 | 1.953 (11) | Ba—Ti_m2 | 2.115 (8) |
Ti_m1(2)—O1xiii | 1.953 (11) | Ba—Mg_m2 | 2.115 (8) |
Ti_m1(2)—O6iv | 1.889 (13) | W_c—Ti_m2 | 2.115 (8) |
Ti_m1(2)—O6xiv | 1.889 (13) | W_c—Mg_m2 | 2.115 (8) |
Ti_m1(2)—Oh | 1.87 (2) | Ti_m2—Mg_m2 | 0 |
| | | |
Na_ai—Na_a—K_bii | 73.3 (9) | Na_axx—Ba—Ti_m1(1)xviii | 68.3 (4) |
Na_ai—Na_a—K_biii | 75.1 (8) | Na_axx—Ba—Ti_m1(2) | 125.9 (6) |
Na_ai—Na_a—Ti_m1(1)ii | 98.2 (10) | Na_axx—Ba—Ti_m1(2)xv | 50.2 (4) |
Na_ai—Na_a—Ti_m1(2)iv | 101.7 (10) | Na_axx—Ba—Fe_m2 | 87.4 (6) |
Na_ai—Na_a—Si2iv | 142.4 (9) | Na_axx—Ba—Si2 | 143.4 (5) |
Na_ai—Na_a—O2ii | 122.3 (14) | Na_axx—Ba—Si2x | 99.6 (3) |
Na_ai—Na_a—O6 | 115.5 (14) | Na_axx—Ba—O1xiii | 92.9 (6) |
Na_ai—Na_a—O7v | 135.4 (12) | Na_axx—Ba—O1xv | 43.6 (6) |
Na_ai—Na_a—Bavi | 71.1 (8) | Na_axx—Ba—O3 | 146.7 (8) |
Na_ai—Na_a—Bavii | 75.1 (9) | Na_axx—Ba—O3x | 91.5 (6) |
Na_ai—Na_a—W1 | 55.8 (12) | Na_axx—Ba—Oh | 143.3 (6) |
Na_ai—Na_a—W2v | 55.0 (11) | Na_axx—Ba—Ohx | 43.9 (4) |
Na_ai—Na_a—Nb_m1(1)ii | 98.2 (10) | Na_axx—Ba—Baxvi | 54.9 (3) |
K_bii—Na_a—K_biii | 48.2 (3) | Na_axx—Ba—Baxiii | 87.4 (6) |
K_bii—Na_a—Ti_m1(1)ii | 64.2 (3) | Na_axx—Ba—W2 | 86.0 (4) |
K_bii—Na_a—Ti_m1(2)iv | 119.8 (5) | Na_axx—Ba—W2xvii | 26.2 (5) |
K_bii—Na_a—Si2iv | 144.1 (11) | Na_axx—Ba—W_c | 0 |
K_bii—Na_a—O2ii | 59.5 (7) | Na_axx—Ba—Nb_m1(1) | 164.3 (3) |
K_bii—Na_a—O6 | 90.7 (6) | Na_axx—Ba—Nb_m1(1)xviii | 68.3 (4) |
K_bii—Na_a—O7v | 132.9 (9) | Na_axx—Ba—Ti_m2 | 87.4 (6) |
K_bii—Na_a—Bavi | 142.8 (11) | Na_axx—Ba—Mg_m2 | 87.4 (6) |
K_bii—Na_a—Bavii | 112.0 (6) | Na_axxi—Ba—Na_av | 103.1 (5) |
K_bii—Na_a—W1 | 28.5 (4) | Na_axxi—Ba—Na_axiv | 111.7 (4) |
K_bii—Na_a—W2v | 123.0 (15) | Na_axxi—Ba—K_b | 100.8 (6) |
K_bii—Na_a—Nb_m1(1)ii | 64.2 (3) | Na_axxi—Ba—Ti_m1(1) | 139.1 (6) |
K_biii—Na_a—Ti_m1(1)ii | 111.4 (5) | Na_axxi—Ba—Ti_m1(1)xviii | 52.8 (3) |
K_biii—Na_a—Ti_m1(2)iv | 72.2 (4) | Na_axxi—Ba—Ti_m1(2) | 156.2 (5) |
K_biii—Na_a—Si2iv | 122.5 (8) | Na_axxi—Ba—Ti_m1(2)xv | 70.2 (5) |
K_biii—Na_a—O2ii | 94.2 (6) | Na_axxi—Ba—Fe_m2 | 118.7 (6) |
K_biii—Na_a—O6 | 51.2 (8) | Na_axxi—Ba—Si2 | 148.6 (3) |
K_biii—Na_a—O7v | 149.3 (15) | Na_axxi—Ba—Si2x | 101.8 (3) |
K_biii—Na_a—Bavi | 111.1 (6) | Na_axxi—Ba—O1xiii | 123.7 (6) |
K_biii—Na_a—Bavii | 148.3 (12) | Na_axxi—Ba—O1xv | 76.3 (7) |
K_biii—Na_a—W1 | 29.7 (5) | Na_axxi—Ba—O3 | 113.1 (8) |
K_biii—Na_a—W2v | 124.7 (15) | Na_axxi—Ba—O3x | 64.2 (5) |
K_biii—Na_a—Nb_m1(1)ii | 111.4 (5) | Na_axxi—Ba—Oh | 148.3 (5) |
Ti_m1(1)ii—Na_a—Ti_m1(2)iv | 159.9 (14) | Na_axxi—Ba—Ohx | 45.2 (4) |
Ti_m1(1)ii—Na_a—Si2iv | 103.7 (9) | Na_axxi—Ba—Baxvi | 56.7 (3) |
Ti_m1(1)ii—Na_a—O2ii | 33.2 (5) | Na_axxi—Ba—Baxiii | 118.7 (6) |
Ti_m1(1)ii—Na_a—O6 | 130.2 (13) | Na_axxi—Ba—W2 | 87.8 (4) |
Ti_m1(1)ii—Na_a—O7v | 73.7 (6) | Na_axxi—Ba—W2xvii | 27.8 (5) |
Ti_m1(1)ii—Na_a—Bavi | 131.3 (6) | Na_axxi—Ba—W_c | 0 |
Ti_m1(1)ii—Na_a—Bavii | 63.0 (3) | Na_axxi—Ba—Nb_m1(1) | 139.1 (6) |
Ti_m1(1)ii—Na_a—W1 | 90.5 (6) | Na_axxi—Ba—Nb_m1(1)xviii | 52.8 (3) |
Ti_m1(1)ii—Na_a—W2v | 98.8 (7) | Na_axxi—Ba—Ti_m2 | 118.7 (6) |
Ti_m1(1)ii—Na_a—Nb_m1(1)ii | 0.0 (5) | Na_axxi—Ba—Mg_m2 | 118.7 (6) |
Ti_m1(2)iv—Na_a—Si2iv | 60.8 (5) | Na_av—Ba—Na_axiv | 33.8 (9) |
Ti_m1(2)iv—Na_a—O2ii | 129.0 (16) | Na_av—Ba—K_b | 100.8 (6) |
Ti_m1(2)iv—Na_a—O6 | 36.1 (4) | Na_av—Ba—Ti_m1(1) | 52.8 (3) |
Ti_m1(2)iv—Na_a—O7v | 93.3 (10) | Na_av—Ba—Ti_m1(1)xviii | 139.1 (6) |
Ti_m1(2)iv—Na_a—Bavi | 59.1 (3) | Na_av—Ba—Ti_m1(2) | 70.2 (5) |
Ti_m1(2)iv—Na_a—Bavii | 124.6 (5) | Na_av—Ba—Ti_m1(2)xv | 156.2 (5) |
Ti_m1(2)iv—Na_a—W1 | 98.9 (7) | Na_av—Ba—Fe_m2 | 118.7 (6) |
Ti_m1(2)iv—Na_a—W2v | 94.4 (6) | Na_av—Ba—Si2 | 101.8 (3) |
Ti_m1(2)iv—Na_a—Nb_m1(1)ii | 159.9 (14) | Na_av—Ba—Si2x | 148.6 (3) |
Si2iv—Na_a—O2ii | 91.3 (14) | Na_av—Ba—O1xiii | 76.3 (7) |
Si2iv—Na_a—O6 | 71.3 (11) | Na_av—Ba—O1xv | 123.7 (6) |
Si2iv—Na_a—O7v | 33.1 (6) | Na_av—Ba—O3 | 64.2 (5) |
Si2iv—Na_a—Bavi | 71.5 (4) | Na_av—Ba—O3x | 113.1 (8) |
Si2iv—Na_a—Bavii | 88.1 (5) | Na_av—Ba—Oh | 45.2 (4) |
Si2iv—Na_a—W1 | 151.7 (13) | Na_av—Ba—Ohx | 148.3 (5) |
Si2iv—Na_a—W2v | 91.4 (8) | Na_av—Ba—Baxvi | 56.7 (3) |
Si2iv—Na_a—Nb_m1(1)ii | 103.7 (9) | Na_av—Ba—Baxiii | 118.7 (6) |
O2ii—Na_a—O6 | 97.2 (14) | Na_av—Ba—W2 | 27.8 (5) |
O2ii—Na_a—O7v | 73.7 (12) | Na_av—Ba—W2xvii | 87.8 (4) |
O2ii—Na_a—Bavi | 154.3 (10) | Na_av—Ba—W_c | 0 |
O2ii—Na_a—Bavii | 92.8 (6) | Na_av—Ba—Nb_m1(1) | 52.8 (3) |
O2ii—Na_a—W1 | 87.4 (8) | Na_av—Ba—Nb_m1(1)xviii | 139.1 (6) |
O2ii—Na_a—W2v | 130.5 (9) | Na_av—Ba—Ti_m2 | 118.7 (6) |
O2ii—Na_a—Nb_m1(1)ii | 33.2 (5) | Na_av—Ba—Mg_m2 | 118.7 (6) |
O6—Na_a—O7v | 101.4 (17) | Na_axiv—Ba—K_b | 127.7 (5) |
O6—Na_a—Bavi | 95.2 (6) | Na_axiv—Ba—Ti_m1(1) | 68.3 (4) |
O6—Na_a—Bavii | 157.2 (10) | Na_axiv—Ba—Ti_m1(1)xviii | 164.3 (3) |
O6—Na_a—W1 | 80.8 (8) | Na_axiv—Ba—Ti_m1(2) | 50.2 (4) |
O6—Na_a—W2v | 130.2 (10) | Na_axiv—Ba—Ti_m1(2)xv | 125.9 (6) |
O6—Na_a—Nb_m1(1)ii | 130.2 (13) | Na_axiv—Ba—Fe_m2 | 87.4 (6) |
O7v—Na_a—Bavi | 81.8 (6) | Na_axiv—Ba—Si2 | 99.6 (3) |
O7v—Na_a—Bavii | 62.0 (6) | Na_axiv—Ba—Si2x | 143.4 (5) |
O7v—Na_a—W1 | 161.1 (13) | Na_axiv—Ba—O1xiii | 43.6 (6) |
O7v—Na_a—W2v | 82.4 (8) | Na_axiv—Ba—O1xv | 92.9 (6) |
O7v—Na_a—Nb_m1(1)ii | 73.7 (6) | Na_axiv—Ba—O3 | 91.5 (6) |
Bavi—Na_a—Bavii | 68.3 (4) | Na_axiv—Ba—O3x | 146.7 (8) |
Bavi—Na_a—W1 | 116.9 (13) | Na_axiv—Ba—Oh | 43.9 (4) |
Bavi—Na_a—W2v | 35.6 (3) | Na_axiv—Ba—Ohx | 143.3 (6) |
Bavi—Na_a—Nb_m1(1)ii | 131.3 (6) | Na_axiv—Ba—Baxvi | 54.9 (3) |
Bavii—Na_a—W1 | 120.2 (14) | Na_axiv—Ba—Baxiii | 87.4 (6) |
Bavii—Na_a—W2v | 37.9 (4) | Na_axiv—Ba—W2 | 26.2 (5) |
Bavii—Na_a—Nb_m1(1)ii | 63.0 (3) | Na_axiv—Ba—W2xvii | 86.0 (4) |
W1—Na_a—W2v | 111 (2) | Na_axiv—Ba—W_c | 0 |
W1—Na_a—Nb_m1(1)ii | 90.5 (6) | Na_axiv—Ba—Nb_m1(1) | 68.3 (4) |
W2v—Na_a—Nb_m1(1)ii | 98.8 (7) | Na_axiv—Ba—Nb_m1(1)xviii | 164.3 (3) |
Na_axi—K_b—Na_aiii | 31.7 (8) | Na_axiv—Ba—Ti_m2 | 87.4 (6) |
Na_axi—K_b—Na_aix | 131.8 (4) | Na_axiv—Ba—Mg_m2 | 87.4 (6) |
Na_axi—K_b—Na_axix | 120.3 (6) | K_b—Ba—Ti_m1(1) | 60.37 (10) |
Na_axi—K_b—K_biii | 118.8 (5) | K_b—Ba—Ti_m1(1)xviii | 60.37 (10) |
Na_axi—K_b—K_bviii | 65.3 (3) | K_b—Ba—Ti_m1(2) | 102.88 (15) |
Na_axi—K_b—Si1 | 90.5 (3) | K_b—Ba—Ti_m1(2)xv | 102.88 (15) |
Na_axi—K_b—Si1iii | 83.7 (6) | K_b—Ba—Fe_m2 | 111.8 (3) |
Na_axi—K_b—Si1ix | 127.3 (7) | K_b—Ba—Si2 | 55.6 (3) |
Na_axi—K_b—Si1x | 139.6 (4) | K_b—Ba—Si2x | 55.6 (3) |
Na_axi—K_b—Si2 | 50.4 (6) | K_b—Ba—O1xiii | 135.1 (3) |
Na_axi—K_b—Si2x | 92.4 (7) | K_b—Ba—O1xv | 135.1 (3) |
Na_axi—K_b—O3 | 72.4 (4) | K_b—Ba—O3 | 37.0 (3) |
Na_axi—K_b—O3x | 134.6 (9) | K_b—Ba—O3x | 37.0 (3) |
Na_axi—K_b—O4iii | 107.3 (7) | K_b—Ba—Oh | 88.3 (4) |
Na_axi—K_b—O5 | 71.0 (6) | K_b—Ba—Ohx | 88.3 (4) |
Na_axi—K_b—Ba | 93.3 (6) | K_b—Ba—Baxvi | 135.7 (3) |
Na_axi—K_b—W1xi | 21.8 (5) | K_b—Ba—Baxiii | 111.8 (2) |
Na_axi—K_b—W1ix | 112.3 (5) | K_b—Ba—W2 | 127.0 (3) |
Na_aiii—K_b—Na_aix | 122.1 (6) | K_b—Ba—W2xvii | 127.0 (3) |
Na_aiii—K_b—Na_axix | 131.8 (4) | K_b—Ba—W_c | 0 |
Na_aiii—K_b—K_biii | 93.8 (6) | K_b—Ba—Nb_m1(1) | 60.37 (10) |
Na_aiii—K_b—K_bviii | 66.5 (3) | K_b—Ba—Nb_m1(1)xviii | 60.37 (10) |
Na_aiii—K_b—Si1 | 88.3 (3) | K_b—Ba—Ti_m2 | 111.8 (3) |
Na_aiii—K_b—Si1iii | 52.4 (6) | K_b—Ba—Mg_m2 | 111.8 (3) |
Na_aiii—K_b—Si1ix | 96.4 (7) | Ti_m1(1)—Ba—Ti_m1(1)xviii | 120.6 (2) |
Na_aiii—K_b—Si1x | 136.9 (5) | Ti_m1(1)—Ba—Ti_m1(2) | 55.35 (5) |
Na_aiii—K_b—Si2 | 81.9 (6) | Ti_m1(1)—Ba—Ti_m1(2)xv | 145.26 (12) |
Na_aiii—K_b—Si2x | 123.0 (7) | Ti_m1(1)—Ba—Fe_m2 | 102.18 (10) |
Na_aiii—K_b—O3 | 83.4 (4) | Ti_m1(1)—Ba—Si2 | 51.81 (12) |
Na_aiii—K_b—O3x | 153.9 (4) | Ti_m1(1)—Ba—Si2x | 95.85 (13) |
Na_aiii—K_b—O4iii | 75.6 (7) | Ti_m1(1)—Ba—O1xiii | 85.8 (3) |
Na_aiii—K_b—O5 | 102.6 (7) | Ti_m1(1)—Ba—O1xv | 143.5 (4) |
Na_aiii—K_b—Ba | 117.8 (5) | Ti_m1(1)—Ba—O3 | 30.4 (4) |
Na_aiii—K_b—W1xi | 22.8 (5) | Ti_m1(1)—Ba—O3x | 93.2 (4) |
Na_aiii—K_b—W1ix | 113.4 (5) | Ti_m1(1)—Ba—Oh | 29.1 (5) |
Na_aix—K_b—Na_axix | 31.7 (8) | Ti_m1(1)—Ba—Ohx | 148.4 (4) |
Na_aix—K_b—K_biii | 93.8 (6) | Ti_m1(1)—Ba—Baxvi | 109.46 (9) |
Na_aix—K_b—K_bviii | 66.5 (3) | Ti_m1(1)—Ba—Baxiii | 102.18 (11) |
Na_aix—K_b—Si1 | 136.9 (5) | Ti_m1(1)—Ba—W2 | 79.1 (3) |
Na_aix—K_b—Si1iii | 96.4 (7) | Ti_m1(1)—Ba—W2xvii | 138.5 (3) |
Na_aix—K_b—Si1ix | 52.4 (6) | Ti_m1(1)—Ba—W_c | 0 |
Na_aix—K_b—Si1x | 88.3 (3) | Ti_m1(1)—Ba—Nb_m1(1) | 0.0 (5) |
Na_aix—K_b—Si2 | 123.0 (7) | Ti_m1(1)—Ba—Nb_m1(1)xviii | 120.6 (2) |
Na_aix—K_b—Si2x | 81.9 (6) | Ti_m1(1)—Ba—Ti_m2 | 102.18 (10) |
Na_aix—K_b—O3 | 153.9 (4) | Ti_m1(1)—Ba—Mg_m2 | 102.18 (10) |
Na_aix—K_b—O3x | 83.4 (4) | Ti_m1(1)xviii—Ba—Ti_m1(2) | 145.26 (12) |
Na_aix—K_b—O4iii | 75.6 (7) | Ti_m1(1)xviii—Ba—Ti_m1(2)xv | 55.35 (5) |
Na_aix—K_b—O5 | 102.6 (7) | Ti_m1(1)xviii—Ba—Fe_m2 | 102.18 (10) |
Na_aix—K_b—Ba | 117.8 (5) | Ti_m1(1)xviii—Ba—Si2 | 95.85 (13) |
Na_aix—K_b—W1xi | 113.4 (5) | Ti_m1(1)xviii—Ba—Si2x | 51.81 (12) |
Na_aix—K_b—W1ix | 22.8 (5) | Ti_m1(1)xviii—Ba—O1xiii | 143.5 (4) |
Na_axix—K_b—K_biii | 118.8 (5) | Ti_m1(1)xviii—Ba—O1xv | 85.8 (3) |
Na_axix—K_b—K_bviii | 65.3 (3) | Ti_m1(1)xviii—Ba—O3 | 93.2 (4) |
Na_axix—K_b—Si1 | 139.6 (4) | Ti_m1(1)xviii—Ba—O3x | 30.4 (4) |
Na_axix—K_b—Si1iii | 127.3 (7) | Ti_m1(1)xviii—Ba—Oh | 148.4 (4) |
Na_axix—K_b—Si1ix | 83.7 (6) | Ti_m1(1)xviii—Ba—Ohx | 29.1 (5) |
Na_axix—K_b—Si1x | 90.5 (3) | Ti_m1(1)xviii—Ba—Baxvi | 109.46 (9) |
Na_axix—K_b—Si2 | 92.4 (7) | Ti_m1(1)xviii—Ba—Baxiii | 102.18 (11) |
Na_axix—K_b—Si2x | 50.4 (6) | Ti_m1(1)xviii—Ba—W2 | 138.5 (3) |
Na_axix—K_b—O3 | 134.6 (9) | Ti_m1(1)xviii—Ba—W2xvii | 79.1 (3) |
Na_axix—K_b—O3x | 72.4 (4) | Ti_m1(1)xviii—Ba—W_c | 0 |
Na_axix—K_b—O4iii | 107.3 (7) | Ti_m1(1)xviii—Ba—Nb_m1(1) | 120.6 (2) |
Na_axix—K_b—O5 | 71.0 (6) | Ti_m1(1)xviii—Ba—Nb_m1(1)xviii | 0.0 (5) |
Na_axix—K_b—Ba | 93.3 (6) | Ti_m1(1)xviii—Ba—Ti_m2 | 102.18 (10) |
Na_axix—K_b—W1xi | 112.3 (5) | Ti_m1(1)xviii—Ba—Mg_m2 | 102.18 (10) |
Na_axix—K_b—W1ix | 21.8 (5) | Ti_m1(2)—Ba—Ti_m1(2)xv | 106.3 (2) |
K_biii—K_b—K_bviii | 132.3 (7) | Ti_m1(2)—Ba—Fe_m2 | 53.15 (12) |
K_biii—K_b—Si1 | 51.0 (3) | Ti_m1(2)—Ba—Si2 | 52.90 (14) |
K_biii—K_b—Si1iii | 47.5 (3) | Ti_m1(2)—Ba—Si2x | 93.45 (16) |
K_biii—K_b—Si1ix | 47.5 (3) | Ti_m1(2)—Ba—O1xiii | 33.2 (3) |
K_biii—K_b—Si1x | 51.0 (3) | Ti_m1(2)—Ba—O1xv | 88.4 (4) |
K_biii—K_b—Si2 | 139.1 (3) | Ti_m1(2)—Ba—O3 | 85.2 (4) |
K_biii—K_b—Si2x | 139.1 (3) | Ti_m1(2)—Ba—O3x | 139.6 (3) |
K_biii—K_b—O3 | 77.9 (7) | Ti_m1(2)—Ba—Oh | 31.6 (5) |
K_biii—K_b—O3x | 77.9 (7) | Ti_m1(2)—Ba—Ohx | 137.5 (5) |
K_biii—K_b—O4iii | 38.7 (4) | Ti_m1(2)—Ba—Baxvi | 103.27 (13) |
K_biii—K_b—O5 | 145.5 (5) | Ti_m1(2)—Ba—Baxiii | 53.15 (12) |
K_biii—K_b—Ba | 98.0 (3) | Ti_m1(2)—Ba—W2 | 76.2 (3) |
K_biii—K_b—W1xi | 116.2 (6) | Ti_m1(2)—Ba—W2xvii | 128.7 (3) |
K_biii—K_b—W1ix | 116.2 (6) | Ti_m1(2)—Ba—W_c | 0 |
K_bviii—K_b—Si1 | 154.19 (11) | Ti_m1(2)—Ba—Nb_m1(1) | 55.35 (5) |
K_bviii—K_b—Si1iii | 90.1 (5) | Ti_m1(2)—Ba—Nb_m1(1)xviii | 145.26 (12) |
K_bviii—K_b—Si1ix | 90.1 (5) | Ti_m1(2)—Ba—Ti_m2 | 53.15 (12) |
K_bviii—K_b—Si1x | 154.19 (11) | Ti_m1(2)—Ba—Mg_m2 | 53.15 (12) |
K_bviii—K_b—Si2 | 83.1 (5) | Ti_m1(2)xv—Ba—Fe_m2 | 53.15 (12) |
K_bviii—K_b—Si2x | 83.1 (5) | Ti_m1(2)xv—Ba—Si2 | 93.45 (16) |
K_bviii—K_b—O3 | 136.4 (6) | Ti_m1(2)xv—Ba—Si2x | 52.90 (14) |
K_bviii—K_b—O3x | 136.4 (6) | Ti_m1(2)xv—Ba—O1xiii | 88.4 (4) |
K_bviii—K_b—O4iii | 93.6 (7) | Ti_m1(2)xv—Ba—O1xv | 33.2 (3) |
K_bviii—K_b—O5 | 82.2 (6) | Ti_m1(2)xv—Ba—O3 | 139.6 (3) |
K_bviii—K_b—Ba | 129.7 (7) | Ti_m1(2)xv—Ba—O3x | 85.2 (4) |
K_bviii—K_b—W1xi | 49.0 (3) | Ti_m1(2)xv—Ba—Oh | 137.5 (5) |
K_bviii—K_b—W1ix | 49.0 (3) | Ti_m1(2)xv—Ba—Ohx | 31.6 (5) |
Si1—K_b—Si1iii | 77.9 (4) | Ti_m1(2)xv—Ba—Baxvi | 103.27 (13) |
Si1—K_b—Si1ix | 98.5 (5) | Ti_m1(2)xv—Ba—Baxiii | 53.15 (12) |
Si1—K_b—Si1x | 51.47 (16) | Ti_m1(2)xv—Ba—W2 | 128.7 (3) |
Si1—K_b—Si2 | 88.2 (4) | Ti_m1(2)xv—Ba—W2xvii | 76.2 (3) |
Si1—K_b—Si2x | 108.0 (5) | Ti_m1(2)xv—Ba—W_c | 0 |
Si1—K_b—O3 | 27.1 (6) | Ti_m1(2)xv—Ba—Nb_m1(1) | 145.26 (12) |
Si1—K_b—O3x | 67.2 (3) | Ti_m1(2)xv—Ba—Nb_m1(1)xviii | 55.35 (5) |
Si1—K_b—O4iii | 84.9 (5) | Ti_m1(2)xv—Ba—Ti_m2 | 53.15 (12) |
Si1—K_b—O5 | 98.8 (6) | Ti_m1(2)xv—Ba—Mg_m2 | 53.15 (12) |
Si1—K_b—Ba | 56.7 (3) | Fe_m2—Ba—Si2 | 63.1 (2) |
Si1—K_b—W1xi | 105.3 (3) | Fe_m2—Ba—Si2x | 63.1 (2) |
Si1—K_b—W1ix | 156.7 (4) | Fe_m2—Ba—O1xiii | 43.9 (3) |
Si1iii—K_b—Si1ix | 48.7 (3) | Fe_m2—Ba—O1xv | 43.9 (3) |
Si1iii—K_b—Si1x | 98.5 (5) | Fe_m2—Ba—O3 | 124.4 (4) |
Si1iii—K_b—Si2 | 132.02 (13) | Fe_m2—Ba—O3x | 124.4 (4) |
Si1iii—K_b—Si2x | 173.1 (3) | Fe_m2—Ba—Oh | 84.5 (5) |
Si1iii—K_b—O3 | 95.9 (7) | Fe_m2—Ba—Ohx | 84.5 (5) |
Si1iii—K_b—O3x | 125.4 (8) | Fe_m2—Ba—Baxvi | 112.5 (3) |
Si1iii—K_b—O4iii | 24.58 (18) | Fe_m2—Ba—Baxiii | 0.0 (5) |
Si1iii—K_b—O5 | 154.5 (2) | Fe_m2—Ba—W2 | 108.8 (3) |
Si1iii—K_b—Ba | 134.4 (2) | Fe_m2—Ba—W2xvii | 108.8 (3) |
Si1iii—K_b—W1xi | 72.0 (4) | Fe_m2—Ba—W_c | 0 |
Si1iii—K_b—W1ix | 108.2 (6) | Fe_m2—Ba—Nb_m1(1) | 102.18 (10) |
Si1ix—K_b—Si1x | 77.9 (4) | Fe_m2—Ba—Nb_m1(1)xviii | 102.18 (10) |
Si1ix—K_b—Si2 | 173.1 (3) | Fe_m2—Ba—Ti_m2 | 0.0 (5) |
Si1ix—K_b—Si2x | 132.02 (13) | Fe_m2—Ba—Mg_m2 | 0.0 (5) |
Si1ix—K_b—O3 | 125.4 (8) | Si2—Ba—Si2x | 48.98 (10) |
Si1ix—K_b—O3x | 95.9 (7) | Si2—Ba—O1xiii | 80.8 (3) |
Si1ix—K_b—O4iii | 24.58 (18) | Si2—Ba—O1xv | 105.0 (4) |
Si1ix—K_b—O5 | 154.5 (2) | Si2—Ba—O3 | 62.4 (4) |
Si1ix—K_b—Ba | 134.4 (2) | Si2—Ba—O3x | 88.6 (3) |
Si1ix—K_b—W1xi | 108.2 (6) | Si2—Ba—Oh | 59.3 (2) |
Si1ix—K_b—W1ix | 72.0 (4) | Si2—Ba—Ohx | 108.3 (2) |
Si1x—K_b—Si2 | 108.0 (5) | Si2—Ba—Baxvi | 154.50 (11) |
Si1x—K_b—Si2x | 88.2 (4) | Si2—Ba—Baxiii | 63.1 (2) |
Si1x—K_b—O3 | 67.2 (3) | Si2—Ba—W2 | 122.4 (3) |
Si1x—K_b—O3x | 27.1 (6) | Si2—Ba—W2xvii | 169.6 (3) |
Si1x—K_b—O4iii | 84.9 (5) | Si2—Ba—W_c | 0 |
Si1x—K_b—O5 | 98.8 (6) | Si2—Ba—Nb_m1(1) | 51.81 (12) |
Si1x—K_b—Ba | 56.7 (3) | Si2—Ba—Nb_m1(1)xviii | 95.85 (13) |
Si1x—K_b—W1xi | 156.7 (4) | Si2—Ba—Ti_m2 | 63.1 (2) |
Si1x—K_b—W1ix | 105.3 (3) | Si2—Ba—Mg_m2 | 63.1 (2) |
Si2—K_b—Si2x | 46.2 (3) | Si2x—Ba—O1xiii | 105.0 (4) |
Si2—K_b—O3 | 61.2 (7) | Si2x—Ba—O1xv | 80.8 (3) |
Si2—K_b—O3x | 88.4 (8) | Si2x—Ba—O3 | 88.6 (3) |
Si2—K_b—O4iii | 156.60 (18) | Si2x—Ba—O3x | 62.4 (4) |
Si2—K_b—O5 | 23.09 (16) | Si2x—Ba—Oh | 108.3 (2) |
Si2—K_b—Ba | 51.3 (3) | Si2x—Ba—Ohx | 59.3 (2) |
Si2—K_b—W1xi | 68.0 (4) | Si2x—Ba—Baxvi | 154.50 (11) |
Si2—K_b—W1ix | 102.5 (6) | Si2x—Ba—Baxiii | 63.1 (2) |
Si2x—K_b—O3 | 88.4 (8) | Si2x—Ba—W2 | 169.6 (3) |
Si2x—K_b—O3x | 61.2 (7) | Si2x—Ba—W2xvii | 122.4 (3) |
Si2x—K_b—O4iii | 156.60 (18) | Si2x—Ba—W_c | 0 |
Si2x—K_b—O5 | 23.09 (16) | Si2x—Ba—Nb_m1(1) | 95.85 (13) |
Si2x—K_b—Ba | 51.3 (3) | Si2x—Ba—Nb_m1(1)xviii | 51.81 (12) |
Si2x—K_b—W1xi | 102.5 (6) | Si2x—Ba—Ti_m2 | 63.1 (2) |
Si2x—K_b—W1ix | 68.0 (4) | Si2x—Ba—Mg_m2 | 63.1 (2) |
O3—K_b—O3x | 70.7 (5) | O1xiii—Ba—O1xv | 60.7 (5) |
O3—K_b—O4iii | 109.3 (8) | O1xiii—Ba—O3 | 116.2 (5) |
O3—K_b—O5 | 74.0 (8) | O1xiii—Ba—O3x | 167.2 (4) |
O3—K_b—Ba | 41.3 (6) | O1xiii—Ba—Oh | 57.5 (6) |
O3—K_b—W1xi | 92.2 (4) | O1xiii—Ba—Ohx | 117.8 (7) |
O3—K_b—W1ix | 155.7 (10) | O1xiii—Ba—Baxvi | 80.6 (3) |
O3x—K_b—O4iii | 109.3 (8) | O1xiii—Ba—Baxiii | 43.9 (3) |
O3x—K_b—O5 | 74.0 (8) | O1xiii—Ba—W2 | 65.8 (3) |
O3x—K_b—Ba | 41.3 (6) | O1xiii—Ba—W2xvii | 97.8 (4) |
O3x—K_b—W1xi | 155.7 (10) | O1xiii—Ba—W_c | 0 |
O3x—K_b—W1ix | 92.2 (4) | O1xiii—Ba—Nb_m1(1) | 85.8 (3) |
O4iii—K_b—O5 | 175.8 (6) | O1xiii—Ba—Nb_m1(1)xviii | 143.5 (4) |
O4iii—K_b—Ba | 136.7 (5) | O1xiii—Ba—Ti_m2 | 43.9 (3) |
O4iii—K_b—W1xi | 92.4 (6) | O1xiii—Ba—Mg_m2 | 43.9 (3) |
O4iii—K_b—W1ix | 92.4 (6) | O1xv—Ba—O3 | 167.2 (4) |
O5—K_b—Ba | 47.4 (4) | O1xv—Ba—O3x | 116.2 (5) |
O5—K_b—W1xi | 84.9 (5) | O1xv—Ba—Oh | 117.8 (7) |
O5—K_b—W1ix | 84.9 (5) | O1xv—Ba—Ohx | 57.5 (6) |
Ba—K_b—W1xi | 114.8 (5) | O1xv—Ba—Baxvi | 80.6 (3) |
Ba—K_b—W1ix | 114.8 (5) | O1xv—Ba—Baxiii | 43.9 (3) |
W1xi—K_b—W1ix | 97.9 (5) | O1xv—Ba—W2 | 97.8 (4) |
Na_axi—Ti_m1(1)—Na_av | 180.0 (5) | O1xv—Ba—W2xvii | 65.8 (3) |
Na_axi—Ti_m1(1)—O2 | 39.0 (8) | O1xv—Ba—W_c | 0 |
Na_axi—Ti_m1(1)—O2iv | 141.0 (8) | O1xv—Ba—Nb_m1(1) | 143.5 (4) |
Na_axi—Ti_m1(1)—O3 | 98.9 (5) | O1xv—Ba—Nb_m1(1)xviii | 85.8 (3) |
Na_axi—Ti_m1(1)—O3iv | 81.1 (5) | O1xv—Ba—Ti_m2 | 43.9 (3) |
Na_axi—Ti_m1(1)—Oh | 126.6 (8) | O1xv—Ba—Mg_m2 | 43.9 (3) |
Na_axi—Ti_m1(1)—Ohiv | 53.4 (8) | O3—Ba—O3x | 63.8 (5) |
Na_axi—Ti_m1(1)—Ba | 115.8 (4) | O3—Ba—Oh | 59.0 (6) |
Na_axi—Ti_m1(1)—Baxii | 64.2 (4) | O3—Ba—Ohx | 122.3 (6) |
Na_axi—Ti_m1(1)—Nb_m1(1) | 0 | O3—Ba—Baxvi | 111.6 (3) |
Na_av—Ti_m1(1)—O2 | 141.0 (8) | O3—Ba—Baxiii | 124.4 (4) |
Na_av—Ti_m1(1)—O2iv | 39.0 (8) | O3—Ba—W2 | 91.4 (3) |
Na_av—Ti_m1(1)—O3 | 81.1 (5) | O3—Ba—W2xvii | 126.6 (5) |
Na_av—Ti_m1(1)—O3iv | 98.9 (5) | O3—Ba—W_c | 0 |
Na_av—Ti_m1(1)—Oh | 53.4 (8) | O3—Ba—Nb_m1(1) | 30.4 (4) |
Na_av—Ti_m1(1)—Ohiv | 126.6 (8) | O3—Ba—Nb_m1(1)xviii | 93.2 (4) |
Na_av—Ti_m1(1)—Ba | 64.2 (4) | O3—Ba—Ti_m2 | 124.4 (4) |
Na_av—Ti_m1(1)—Baxii | 115.8 (4) | O3—Ba—Mg_m2 | 124.4 (4) |
Na_av—Ti_m1(1)—Nb_m1(1) | 0 | O3x—Ba—Oh | 122.3 (6) |
O2—Ti_m1(1)—O2iv | 180.0 (5) | O3x—Ba—Ohx | 59.0 (6) |
O2—Ti_m1(1)—O3 | 87.7 (6) | O3x—Ba—Baxvi | 111.6 (3) |
O2—Ti_m1(1)—O3iv | 92.3 (6) | O3x—Ba—Baxiii | 124.4 (4) |
O2—Ti_m1(1)—Oh | 89.8 (8) | O3x—Ba—W2 | 126.6 (5) |
O2—Ti_m1(1)—Ohiv | 90.2 (8) | O3x—Ba—W2xvii | 91.4 (3) |
O2—Ti_m1(1)—Ba | 80.8 (4) | O3x—Ba—W_c | 0 |
O2—Ti_m1(1)—Baxii | 99.2 (4) | O3x—Ba—Nb_m1(1) | 93.2 (4) |
O2—Ti_m1(1)—Nb_m1(1) | 0 | O3x—Ba—Nb_m1(1)xviii | 30.4 (4) |
O2iv—Ti_m1(1)—O3 | 92.3 (6) | O3x—Ba—Ti_m2 | 124.4 (4) |
O2iv—Ti_m1(1)—O3iv | 87.7 (6) | O3x—Ba—Mg_m2 | 124.4 (4) |
O2iv—Ti_m1(1)—Oh | 90.2 (8) | Oh—Ba—Ohx | 166.4 (5) |
O2iv—Ti_m1(1)—Ohiv | 89.8 (8) | Oh—Ba—Baxvi | 95.8 (2) |
O2iv—Ti_m1(1)—Ba | 99.2 (4) | Oh—Ba—Baxiii | 84.5 (5) |
O2iv—Ti_m1(1)—Baxii | 80.8 (4) | Oh—Ba—W2 | 63.2 (4) |
O2iv—Ti_m1(1)—Nb_m1(1) | 0 | Oh—Ba—W2xvii | 128.4 (4) |
O3—Ti_m1(1)—O3iv | 180.0 (5) | Oh—Ba—W_c | 0 |
O3—Ti_m1(1)—Oh | 90.6 (8) | Oh—Ba—Nb_m1(1) | 29.1 (5) |
O3—Ti_m1(1)—Ohiv | 89.4 (8) | Oh—Ba—Nb_m1(1)xviii | 148.4 (4) |
O3—Ti_m1(1)—Ba | 47.3 (8) | Oh—Ba—Ti_m2 | 84.5 (5) |
O3—Ti_m1(1)—Baxii | 132.7 (8) | Oh—Ba—Mg_m2 | 84.5 (5) |
O3—Ti_m1(1)—Nb_m1(1) | 0 | Ohx—Ba—Baxvi | 95.8 (2) |
O3iv—Ti_m1(1)—Oh | 89.4 (8) | Ohx—Ba—Baxiii | 84.5 (5) |
O3iv—Ti_m1(1)—Ohiv | 90.6 (8) | Ohx—Ba—W2 | 128.4 (4) |
O3iv—Ti_m1(1)—Ba | 132.7 (8) | Ohx—Ba—W2xvii | 63.2 (4) |
O3iv—Ti_m1(1)—Baxii | 47.3 (8) | Ohx—Ba—W_c | 0 |
O3iv—Ti_m1(1)—Nb_m1(1) | 0 | Ohx—Ba—Nb_m1(1) | 148.4 (4) |
Oh—Ti_m1(1)—Ohiv | 180.0 (5) | Ohx—Ba—Nb_m1(1)xviii | 29.1 (5) |
Oh—Ti_m1(1)—Ba | 44.3 (4) | Ohx—Ba—Ti_m2 | 84.5 (5) |
Oh—Ti_m1(1)—Baxii | 135.7 (4) | Ohx—Ba—Mg_m2 | 84.5 (5) |
Oh—Ti_m1(1)—Nb_m1(1) | 0 | Baxvi—Ba—Baxiii | 112.5 (2) |
Ohiv—Ti_m1(1)—Ba | 135.7 (4) | Baxvi—Ba—W2 | 32.7 (3) |
Ohiv—Ti_m1(1)—Baxii | 44.3 (4) | Baxvi—Ba—W2xvii | 32.7 (3) |
Ohiv—Ti_m1(1)—Nb_m1(1) | 0 | Baxvi—Ba—W_c | 0 |
Ba—Ti_m1(1)—Baxii | 180.0 (5) | Baxvi—Ba—Nb_m1(1) | 109.46 (9) |
Ba—Ti_m1(1)—Nb_m1(1) | 0 | Baxvi—Ba—Nb_m1(1)xviii | 109.46 (9) |
Baxii—Ti_m1(1)—Nb_m1(1) | 0 | Baxvi—Ba—Ti_m2 | 112.5 (3) |
Na_aiv—Ti_m1(2)—Na_axiv | 174.5 (5) | Baxvi—Ba—Mg_m2 | 112.5 (3) |
Na_aiv—Ti_m1(2)—Fe_m2 | 92.8 (3) | Baxiii—Ba—W2 | 108.8 (3) |
Na_aiv—Ti_m1(2)—O1 | 57.6 (5) | Baxiii—Ba—W2xvii | 108.8 (3) |
Na_aiv—Ti_m1(2)—O1xiii | 127.5 (6) | Baxiii—Ba—W_c | 0 |
Na_aiv—Ti_m1(2)—O6iv | 43.7 (7) | Baxiii—Ba—Nb_m1(1) | 102.18 (11) |
Na_aiv—Ti_m1(2)—O6xiv | 131.3 (7) | Baxiii—Ba—Nb_m1(1)xviii | 102.18 (11) |
Na_aiv—Ti_m1(2)—Oh | 122.2 (8) | Baxiii—Ba—Ti_m2 | 0.0 (5) |
Na_aiv—Ti_m1(2)—Ohxiii | 58.2 (8) | Baxiii—Ba—Mg_m2 | 0.0 (5) |
Na_aiv—Ti_m1(2)—Ba | 114.0 (5) | W2—Ba—W2xvii | 65.3 (4) |
Na_aiv—Ti_m1(2)—Baxiii | 70.7 (5) | W2—Ba—W_c | 0 |
Na_aiv—Ti_m1(2)—Ti_m2 | 92.8 (3) | W2—Ba—Nb_m1(1) | 79.1 (3) |
Na_aiv—Ti_m1(2)—Mg_m2 | 92.8 (3) | W2—Ba—Nb_m1(1)xviii | 138.5 (3) |
Na_axiv—Ti_m1(2)—Fe_m2 | 92.8 (3) | W2—Ba—Ti_m2 | 108.8 (3) |
Na_axiv—Ti_m1(2)—O1 | 127.5 (6) | W2—Ba—Mg_m2 | 108.8 (3) |
Na_axiv—Ti_m1(2)—O1xiii | 57.6 (5) | W2xvii—Ba—W_c | 0 |
Na_axiv—Ti_m1(2)—O6iv | 131.3 (7) | W2xvii—Ba—Nb_m1(1) | 138.5 (3) |
Na_axiv—Ti_m1(2)—O6xiv | 43.7 (7) | W2xvii—Ba—Nb_m1(1)xviii | 79.1 (3) |
Na_axiv—Ti_m1(2)—Oh | 58.2 (8) | W2xvii—Ba—Ti_m2 | 108.8 (3) |
Na_axiv—Ti_m1(2)—Ohxiii | 122.2 (8) | W2xvii—Ba—Mg_m2 | 108.8 (3) |
Na_axiv—Ti_m1(2)—Ba | 70.7 (5) | W_c—Ba—Nb_m1(1) | 0 |
Na_axiv—Ti_m1(2)—Baxiii | 114.0 (5) | W_c—Ba—Nb_m1(1)xviii | 0 |
Na_axiv—Ti_m1(2)—Ti_m2 | 92.8 (3) | W_c—Ba—Ti_m2 | 0 |
Na_axiv—Ti_m1(2)—Mg_m2 | 92.8 (3) | W_c—Ba—Mg_m2 | 0 |
Fe_m2—Ti_m1(2)—O1 | 41.0 (3) | Nb_m1(1)—Ba—Nb_m1(1)xviii | 120.6 (2) |
Fe_m2—Ti_m1(2)—O1xiii | 41.0 (3) | Nb_m1(1)—Ba—Ti_m2 | 102.18 (10) |
Fe_m2—Ti_m1(2)—O6iv | 130.6 (4) | Nb_m1(1)—Ba—Mg_m2 | 102.18 (10) |
Fe_m2—Ti_m1(2)—O6xiv | 130.6 (4) | Nb_m1(1)xviii—Ba—Ti_m2 | 102.18 (10) |
Fe_m2—Ti_m1(2)—Oh | 86.9 (3) | Nb_m1(1)xviii—Ba—Mg_m2 | 102.18 (10) |
Fe_m2—Ti_m1(2)—Ohxiii | 86.9 (3) | Ti_m2—Ba—Mg_m2 | 0.0 (5) |
Fe_m2—Ti_m1(2)—Ba | 36.85 (12) | Na_a—W1—Na_ai | 68.4 (16) |
Fe_m2—Ti_m1(2)—Baxiii | 36.85 (12) | Na_a—W1—K_bii | 129.7 (8) |
Fe_m2—Ti_m1(2)—Ti_m2 | 0.0 (5) | Na_a—W1—K_biii | 127.5 (8) |
Fe_m2—Ti_m1(2)—Mg_m2 | 0.0 (5) | Na_ai—W1—K_bii | 127.5 (8) |
O1—Ti_m1(2)—O1xiii | 82.0 (5) | Na_ai—W1—K_biii | 129.7 (8) |
O1—Ti_m1(2)—O6iv | 89.7 (5) | K_bii—W1—K_biii | 82.1 (7) |
O1—Ti_m1(2)—O6xiv | 170.9 (5) | Na_av—W2—Na_axiv | 70.0 (16) |
O1—Ti_m1(2)—Oh | 89.5 (8) | Na_av—W2—Ba | 114.2 (6) |
O1—Ti_m1(2)—Ohxiii | 85.8 (8) | Na_av—W2—Baxvi | 118.3 (6) |
O1—Ti_m1(2)—Ba | 57.0 (5) | Na_axiv—W2—Ba | 118.3 (6) |
O1—Ti_m1(2)—Baxiii | 48.5 (7) | Na_axiv—W2—Baxvi | 114.2 (6) |
O1—Ti_m1(2)—Ti_m2 | 41.0 (3) | Ba—W2—Baxvi | 114.7 (6) |
O1—Ti_m1(2)—Mg_m2 | 41.0 (3) | Fe_m2—W_c—Ba | 0 |
O1xiii—Ti_m1(2)—O6iv | 170.9 (5) | Fe_m2—W_c—Ti_m2 | 0.0 (5) |
O1xiii—Ti_m1(2)—O6xiv | 89.7 (5) | Fe_m2—W_c—Mg_m2 | 0.0 (5) |
O1xiii—Ti_m1(2)—Oh | 85.8 (8) | Ba—W_c—Ti_m2 | 0 |
O1xiii—Ti_m1(2)—Ohxiii | 89.5 (8) | Ba—W_c—Mg_m2 | 0 |
O1xiii—Ti_m1(2)—Ba | 48.5 (7) | Ti_m2—W_c—Mg_m2 | 0.0 (5) |
O1xiii—Ti_m1(2)—Baxiii | 57.0 (5) | Na_axi—Nb_m1(1)—Na_av | 180.0 (5) |
O1xiii—Ti_m1(2)—Ti_m2 | 41.0 (3) | Na_axi—Nb_m1(1)—Ti_m1(1) | 0 |
O1xiii—Ti_m1(2)—Mg_m2 | 41.0 (3) | Na_axi—Nb_m1(1)—O2 | 39.0 (8) |
O6iv—Ti_m1(2)—O6xiv | 98.8 (6) | Na_axi—Nb_m1(1)—O2iv | 141.0 (8) |
O6iv—Ti_m1(2)—Oh | 98.0 (10) | Na_axi—Nb_m1(1)—O3 | 98.9 (5) |
O6iv—Ti_m1(2)—Ohxiii | 86.1 (9) | Na_axi—Nb_m1(1)—O3iv | 81.1 (5) |
O6iv—Ti_m1(2)—Ba | 129.0 (8) | Na_axi—Nb_m1(1)—Oh | 126.6 (8) |
O6iv—Ti_m1(2)—Baxiii | 114.4 (6) | Na_axi—Nb_m1(1)—Ohiv | 53.4 (8) |
O6iv—Ti_m1(2)—Ti_m2 | 130.6 (4) | Na_axi—Nb_m1(1)—Ba | 115.8 (4) |
O6iv—Ti_m1(2)—Mg_m2 | 130.6 (4) | Na_axi—Nb_m1(1)—Baxii | 64.2 (4) |
O6xiv—Ti_m1(2)—Oh | 86.1 (9) | Na_av—Nb_m1(1)—Ti_m1(1) | 0 |
O6xiv—Ti_m1(2)—Ohxiii | 98.0 (10) | Na_av—Nb_m1(1)—O2 | 141.0 (8) |
O6xiv—Ti_m1(2)—Ba | 114.4 (6) | Na_av—Nb_m1(1)—O2iv | 39.0 (8) |
O6xiv—Ti_m1(2)—Baxiii | 129.0 (8) | Na_av—Nb_m1(1)—O3 | 81.1 (5) |
O6xiv—Ti_m1(2)—Ti_m2 | 130.6 (4) | Na_av—Nb_m1(1)—O3iv | 98.9 (5) |
O6xiv—Ti_m1(2)—Mg_m2 | 130.6 (4) | Na_av—Nb_m1(1)—Oh | 53.4 (8) |
Oh—Ti_m1(2)—Ohxiii | 173.7 (5) | Na_av—Nb_m1(1)—Ohiv | 126.6 (8) |
Oh—Ti_m1(2)—Ba | 50.3 (3) | Na_av—Nb_m1(1)—Ba | 64.2 (4) |
Oh—Ti_m1(2)—Baxiii | 123.5 (3) | Na_av—Nb_m1(1)—Baxii | 115.8 (4) |
Oh—Ti_m1(2)—Ti_m2 | 86.9 (3) | Ti_m1(1)—Nb_m1(1)—O2 | 0 |
Oh—Ti_m1(2)—Mg_m2 | 86.9 (3) | Ti_m1(1)—Nb_m1(1)—O2iv | 0 |
Ohxiii—Ti_m1(2)—Ba | 123.5 (3) | Ti_m1(1)—Nb_m1(1)—O3 | 0 |
Ohxiii—Ti_m1(2)—Baxiii | 50.3 (3) | Ti_m1(1)—Nb_m1(1)—O3iv | 0 |
Ohxiii—Ti_m1(2)—Ti_m2 | 86.9 (3) | Ti_m1(1)—Nb_m1(1)—Oh | 0 |
Ohxiii—Ti_m1(2)—Mg_m2 | 86.9 (3) | Ti_m1(1)—Nb_m1(1)—Ohiv | 0 |
Ba—Ti_m1(2)—Baxiii | 73.71 (17) | Ti_m1(1)—Nb_m1(1)—Ba | 0 |
Ba—Ti_m1(2)—Ti_m2 | 36.85 (12) | Ti_m1(1)—Nb_m1(1)—Baxii | 0 |
Ba—Ti_m1(2)—Mg_m2 | 36.85 (12) | O2—Nb_m1(1)—O2iv | 180.0 (5) |
Baxiii—Ti_m1(2)—Ti_m2 | 36.85 (12) | O2—Nb_m1(1)—O3 | 87.7 (6) |
Baxiii—Ti_m1(2)—Mg_m2 | 36.85 (12) | O2—Nb_m1(1)—O3iv | 92.3 (6) |
Ti_m2—Ti_m1(2)—Mg_m2 | 0.0 (5) | O2—Nb_m1(1)—Oh | 89.8 (8) |
Ti_m1(2)—Fe_m2—Ti_m1(2)xv | 180.0 (5) | O2—Nb_m1(1)—Ohiv | 90.2 (8) |
Ti_m1(2)—Fe_m2—O1 | 43.6 (3) | O2—Nb_m1(1)—Ba | 80.8 (4) |
Ti_m1(2)—Fe_m2—O1xiii | 43.6 (3) | O2—Nb_m1(1)—Baxii | 99.2 (4) |
Ti_m1(2)—Fe_m2—O1xv | 136.4 (3) | O2iv—Nb_m1(1)—O3 | 92.3 (6) |
Ti_m1(2)—Fe_m2—O1x | 136.4 (3) | O2iv—Nb_m1(1)—O3iv | 87.7 (6) |
Ti_m1(2)—Fe_m2—Ba | 90 | O2iv—Nb_m1(1)—Oh | 90.2 (8) |
Ti_m1(2)—Fe_m2—Baxiii | 90 | O2iv—Nb_m1(1)—Ohiv | 89.8 (8) |
Ti_m1(2)—Fe_m2—W_c | 90 | O2iv—Nb_m1(1)—Ba | 99.2 (4) |
Ti_m1(2)—Fe_m2—W_cxiii | 90 | O2iv—Nb_m1(1)—Baxii | 80.8 (4) |
Ti_m1(2)—Fe_m2—Ti_m2 | 0 | O3—Nb_m1(1)—O3iv | 180.0 (5) |
Ti_m1(2)—Fe_m2—Mg_m2 | 0 | O3—Nb_m1(1)—Oh | 90.6 (8) |
Ti_m1(2)xv—Fe_m2—O1 | 136.4 (3) | O3—Nb_m1(1)—Ohiv | 89.4 (8) |
Ti_m1(2)xv—Fe_m2—O1xiii | 136.4 (3) | O3—Nb_m1(1)—Ba | 47.3 (8) |
Ti_m1(2)xv—Fe_m2—O1xv | 43.6 (3) | O3—Nb_m1(1)—Baxii | 132.7 (8) |
Ti_m1(2)xv—Fe_m2—O1x | 43.6 (3) | O3iv—Nb_m1(1)—Oh | 89.4 (8) |
Ti_m1(2)xv—Fe_m2—Ba | 90 | O3iv—Nb_m1(1)—Ohiv | 90.6 (8) |
Ti_m1(2)xv—Fe_m2—Baxiii | 90 | O3iv—Nb_m1(1)—Ba | 132.7 (8) |
Ti_m1(2)xv—Fe_m2—W_c | 90 | O3iv—Nb_m1(1)—Baxii | 47.3 (8) |
Ti_m1(2)xv—Fe_m2—W_cxiii | 90 | Oh—Nb_m1(1)—Ohiv | 180.0 (5) |
Ti_m1(2)xv—Fe_m2—Ti_m2 | 0 | Oh—Nb_m1(1)—Ba | 44.3 (4) |
Ti_m1(2)xv—Fe_m2—Mg_m2 | 0 | Oh—Nb_m1(1)—Baxii | 135.7 (4) |
O1—Fe_m2—O1xiii | 87.1 (4) | Ohiv—Nb_m1(1)—Ba | 135.7 (4) |
O1—Fe_m2—O1xv | 180.0 (5) | Ohiv—Nb_m1(1)—Baxii | 44.3 (4) |
O1—Fe_m2—O1x | 92.9 (4) | Ba—Nb_m1(1)—Baxii | 180.0 (5) |
O1—Fe_m2—Ba | 96.0 (7) | Ti_m1(2)—Ti_m2—Ti_m1(2)xv | 180.0 (5) |
O1—Fe_m2—Baxiii | 84.0 (7) | Ti_m1(2)—Ti_m2—Fe_m2 | 0 |
O1—Fe_m2—W_c | 96.0 (7) | Ti_m1(2)—Ti_m2—O1 | 43.6 (3) |
O1—Fe_m2—W_cxiii | 84.0 (7) | Ti_m1(2)—Ti_m2—O1xiii | 43.6 (3) |
O1—Fe_m2—Ti_m2 | 0 | Ti_m1(2)—Ti_m2—O1xv | 136.4 (3) |
O1—Fe_m2—Mg_m2 | 0 | Ti_m1(2)—Ti_m2—O1x | 136.4 (3) |
O1xiii—Fe_m2—O1xv | 92.9 (4) | Ti_m1(2)—Ti_m2—Ba | 90 |
O1xiii—Fe_m2—O1x | 180.0 (5) | Ti_m1(2)—Ti_m2—Baxiii | 90 |
O1xiii—Fe_m2—Ba | 84.0 (7) | Ti_m1(2)—Ti_m2—W_c | 90 |
O1xiii—Fe_m2—Baxiii | 96.0 (7) | Ti_m1(2)—Ti_m2—W_cxiii | 90 |
O1xiii—Fe_m2—W_c | 84.0 (7) | Ti_m1(2)—Ti_m2—Mg_m2 | 0 |
O1xiii—Fe_m2—W_cxiii | 96.0 (7) | Ti_m1(2)xv—Ti_m2—Fe_m2 | 0 |
O1xiii—Fe_m2—Ti_m2 | 0 | Ti_m1(2)xv—Ti_m2—O1 | 136.4 (3) |
O1xiii—Fe_m2—Mg_m2 | 0 | Ti_m1(2)xv—Ti_m2—O1xiii | 136.4 (3) |
O1xv—Fe_m2—O1x | 87.1 (4) | Ti_m1(2)xv—Ti_m2—O1xv | 43.6 (3) |
O1xv—Fe_m2—Ba | 84.0 (7) | Ti_m1(2)xv—Ti_m2—O1x | 43.6 (3) |
O1xv—Fe_m2—Baxiii | 96.0 (7) | Ti_m1(2)xv—Ti_m2—Ba | 90 |
O1xv—Fe_m2—W_c | 84.0 (7) | Ti_m1(2)xv—Ti_m2—Baxiii | 90 |
O1xv—Fe_m2—W_cxiii | 96.0 (7) | Ti_m1(2)xv—Ti_m2—W_c | 90 |
O1xv—Fe_m2—Ti_m2 | 0 | Ti_m1(2)xv—Ti_m2—W_cxiii | 90 |
O1xv—Fe_m2—Mg_m2 | 0 | Ti_m1(2)xv—Ti_m2—Mg_m2 | 0 |
O1x—Fe_m2—Ba | 96.0 (7) | Fe_m2—Ti_m2—O1 | 0 |
O1x—Fe_m2—Baxiii | 84.0 (7) | Fe_m2—Ti_m2—O1xiii | 0 |
O1x—Fe_m2—W_c | 96.0 (7) | Fe_m2—Ti_m2—O1xv | 0 |
O1x—Fe_m2—W_cxiii | 84.0 (7) | Fe_m2—Ti_m2—O1x | 0 |
O1x—Fe_m2—Ti_m2 | 0 | Fe_m2—Ti_m2—Ba | 0 |
O1x—Fe_m2—Mg_m2 | 0 | Fe_m2—Ti_m2—Baxiii | 0 |
Ba—Fe_m2—Baxiii | 180.0 (5) | Fe_m2—Ti_m2—W_c | 0 |
Ba—Fe_m2—W_c | 0.0 (5) | Fe_m2—Ti_m2—W_cxiii | 0 |
Ba—Fe_m2—W_cxiii | 180.0 (5) | Fe_m2—Ti_m2—Mg_m2 | 0 |
Ba—Fe_m2—Ti_m2 | 0 | O1—Ti_m2—O1xiii | 87.1 (4) |
Ba—Fe_m2—Mg_m2 | 0 | O1—Ti_m2—O1xv | 180.0 (5) |
Baxiii—Fe_m2—W_c | 180.0 (5) | O1—Ti_m2—O1x | 92.9 (4) |
Baxiii—Fe_m2—W_cxiii | 0.0 (5) | O1—Ti_m2—Ba | 96.0 (7) |
Baxiii—Fe_m2—Ti_m2 | 0 | O1—Ti_m2—Baxiii | 84.0 (7) |
Baxiii—Fe_m2—Mg_m2 | 0 | O1—Ti_m2—W_c | 96.0 (7) |
W_c—Fe_m2—W_cxiii | 180.0 (5) | O1—Ti_m2—W_cxiii | 84.0 (7) |
W_c—Fe_m2—Ti_m2 | 0 | O1—Ti_m2—Mg_m2 | 0 |
W_c—Fe_m2—Mg_m2 | 0 | O1xiii—Ti_m2—O1xv | 92.9 (4) |
W_cxiii—Fe_m2—Ti_m2 | 0 | O1xiii—Ti_m2—O1x | 180.0 (5) |
W_cxiii—Fe_m2—Mg_m2 | 0 | O1xiii—Ti_m2—Ba | 84.0 (7) |
Ti_m2—Fe_m2—Mg_m2 | 0 | O1xiii—Ti_m2—Baxiii | 96.0 (7) |
K_b—Si1—K_biii | 81.5 (4) | O1xiii—Ti_m2—W_c | 84.0 (7) |
K_b—Si1—O3 | 49.7 (8) | O1xiii—Ti_m2—W_cxiii | 96.0 (7) |
K_b—Si1—O4 | 63.6 (6) | O1xiii—Ti_m2—Mg_m2 | 0 |
K_b—Si1—O6 | 105.2 (6) | O1xv—Ti_m2—O1x | 87.1 (4) |
K_b—Si1—O7 | 141.0 (8) | O1xv—Ti_m2—Ba | 84.0 (7) |
K_biii—Si1—O3 | 131.0 (8) | O1xv—Ti_m2—Baxiii | 96.0 (7) |
K_biii—Si1—O4 | 37.6 (12) | O1xv—Ti_m2—W_c | 84.0 (7) |
K_biii—Si1—O6 | 66.6 (9) | O1xv—Ti_m2—W_cxiii | 96.0 (7) |
K_biii—Si1—O7 | 117.1 (8) | O1xv—Ti_m2—Mg_m2 | 0 |
O3—Si1—O4 | 107.7 (10) | O1x—Ti_m2—Ba | 96.0 (7) |
O3—Si1—O6 | 116.6 (9) | O1x—Ti_m2—Baxiii | 84.0 (7) |
O3—Si1—O7 | 106.0 (13) | O1x—Ti_m2—W_c | 96.0 (7) |
O4—Si1—O6 | 103.5 (15) | O1x—Ti_m2—W_cxiii | 84.0 (7) |
O4—Si1—O7 | 109.2 (7) | O1x—Ti_m2—Mg_m2 | 0 |
O6—Si1—O7 | 113.5 (8) | Ba—Ti_m2—Baxiii | 180.0 (5) |
Na_aiv—Si2—K_b | 163.4 (6) | Ba—Ti_m2—W_c | 0.0 (5) |
Na_aiv—Si2—O1 | 64.0 (8) | Ba—Ti_m2—W_cxiii | 180.0 (5) |
Na_aiv—Si2—O2 | 97.2 (9) | Ba—Ti_m2—Mg_m2 | 0 |
Na_aiv—Si2—O5 | 149.6 (11) | Baxiii—Ti_m2—W_c | 180.0 (5) |
Na_aiv—Si2—O7xi | 50.0 (8) | Baxiii—Ti_m2—W_cxiii | 0.0 (5) |
Na_aiv—Si2—Ba | 122.9 (5) | Baxiii—Ti_m2—Mg_m2 | 0 |
K_b—Si2—O1 | 132.5 (6) | W_c—Ti_m2—W_cxiii | 180.0 (5) |
K_b—Si2—O2 | 74.6 (9) | W_c—Ti_m2—Mg_m2 | 0 |
K_b—Si2—O5 | 37.0 (12) | W_cxiii—Ti_m2—Mg_m2 | 0 |
K_b—Si2—O7xi | 119.5 (8) | Ti_m1(2)—Mg_m2—Ti_m1(2)xv | 180.0 (5) |
K_b—Si2—Ba | 73.1 (3) | Ti_m1(2)—Mg_m2—Fe_m2 | 0 |
O1—Si2—O2 | 115.1 (8) | Ti_m1(2)—Mg_m2—O1 | 43.6 (3) |
O1—Si2—O5 | 110.0 (10) | Ti_m1(2)—Mg_m2—O1xiii | 43.6 (3) |
O1—Si2—O7xi | 99.7 (11) | Ti_m1(2)—Mg_m2—O1xv | 136.4 (3) |
O1—Si2—Ba | 59.8 (6) | Ti_m1(2)—Mg_m2—O1x | 136.4 (3) |
O2—Si2—O5 | 111.4 (15) | Ti_m1(2)—Mg_m2—Ba | 90 |
O2—Si2—O7xi | 113.6 (7) | Ti_m1(2)—Mg_m2—Baxiii | 90 |
O2—Si2—Ba | 97.5 (5) | Ti_m1(2)—Mg_m2—W_c | 90 |
O5—Si2—O7xi | 106.3 (8) | Ti_m1(2)—Mg_m2—W_cxiii | 90 |
O5—Si2—Ba | 64.9 (5) | Ti_m1(2)—Mg_m2—Ti_m2 | 0 |
O7xi—Si2—Ba | 148.4 (7) | Ti_m1(2)xv—Mg_m2—Fe_m2 | 0 |
Ti_m1(2)—O1—Fe_m2 | 95.4 (5) | Ti_m1(2)xv—Mg_m2—O1 | 136.4 (3) |
Ti_m1(2)—O1—Si2 | 119.6 (9) | Ti_m1(2)xv—Mg_m2—O1xiii | 136.4 (3) |
Ti_m1(2)—O1—Baxiii | 98.3 (8) | Ti_m1(2)xv—Mg_m2—O1xv | 43.6 (3) |
Ti_m1(2)—O1—Ti_m2 | 95.4 (5) | Ti_m1(2)xv—Mg_m2—O1x | 43.6 (3) |
Ti_m1(2)—O1—Mg_m2 | 95.4 (5) | Ti_m1(2)xv—Mg_m2—Ba | 90 |
Fe_m2—O1—Si2 | 125.8 (10) | Ti_m1(2)xv—Mg_m2—Baxiii | 90 |
Fe_m2—O1—Baxiii | 52.1 (5) | Ti_m1(2)xv—Mg_m2—W_c | 90 |
Fe_m2—O1—Ti_m2 | 0.0 (5) | Ti_m1(2)xv—Mg_m2—W_cxiii | 90 |
Fe_m2—O1—Mg_m2 | 0.0 (5) | Ti_m1(2)xv—Mg_m2—Ti_m2 | 0 |
Si2—O1—Baxiii | 141.1 (6) | Fe_m2—Mg_m2—O1 | 0 |
Si2—O1—Ti_m2 | 125.8 (10) | Fe_m2—Mg_m2—O1xiii | 0 |
Si2—O1—Mg_m2 | 125.8 (10) | Fe_m2—Mg_m2—O1xv | 0 |
Baxiii—O1—Ti_m2 | 52.1 (5) | Fe_m2—Mg_m2—O1x | 0 |
Baxiii—O1—Mg_m2 | 52.1 (5) | Fe_m2—Mg_m2—Ba | 0 |
Ti_m2—O1—Mg_m2 | 0.0 (5) | Fe_m2—Mg_m2—Baxiii | 0 |
Na_axi—O2—Ti_m1(1) | 107.8 (12) | Fe_m2—Mg_m2—W_c | 0 |
Na_axi—O2—Si2 | 121.5 (8) | Fe_m2—Mg_m2—W_cxiii | 0 |
Na_axi—O2—Nb_m1(1) | 107.8 (12) | Fe_m2—Mg_m2—Ti_m2 | 0 |
Ti_m1(1)—O2—Si2 | 128.9 (7) | O1—Mg_m2—O1xiii | 87.1 (4) |
Ti_m1(1)—O2—Nb_m1(1) | 0.0 (5) | O1—Mg_m2—O1xv | 180.0 (5) |
Si2—O2—Nb_m1(1) | 128.9 (7) | O1—Mg_m2—O1x | 92.9 (4) |
K_b—O3—Ti_m1(1) | 124.3 (5) | O1—Mg_m2—Ba | 96.0 (7) |
K_b—O3—Si1 | 103.2 (13) | O1—Mg_m2—Baxiii | 84.0 (7) |
K_b—O3—Ba | 101.7 (6) | O1—Mg_m2—W_c | 96.0 (7) |
K_b—O3—Nb_m1(1) | 124.3 (5) | O1—Mg_m2—W_cxiii | 84.0 (7) |
Ti_m1(1)—O3—Si1 | 114.6 (7) | O1—Mg_m2—Ti_m2 | 0 |
Ti_m1(1)—O3—Ba | 102.3 (11) | O1xiii—Mg_m2—O1xv | 92.9 (4) |
Ti_m1(1)—O3—Nb_m1(1) | 0.0 (5) | O1xiii—Mg_m2—O1x | 180.0 (5) |
Si1—O3—Ba | 109.5 (7) | O1xiii—Mg_m2—Ba | 84.0 (7) |
Si1—O3—Nb_m1(1) | 114.6 (7) | O1xiii—Mg_m2—Baxiii | 96.0 (7) |
Ba—O3—Nb_m1(1) | 102.3 (11) | O1xiii—Mg_m2—W_c | 84.0 (7) |
K_biii—O4—Si1 | 117.8 (12) | O1xiii—Mg_m2—W_cxiii | 96.0 (7) |
K_biii—O4—Si1x | 117.8 (12) | O1xiii—Mg_m2—Ti_m2 | 0 |
Si1—O4—Si1x | 123 (2) | O1xv—Mg_m2—O1x | 87.1 (4) |
K_b—O5—Si2 | 119.9 (12) | O1xv—Mg_m2—Ba | 84.0 (7) |
K_b—O5—Si2x | 119.9 (12) | O1xv—Mg_m2—Baxiii | 96.0 (7) |
Si2—O5—Si2x | 120 (2) | O1xv—Mg_m2—W_c | 84.0 (7) |
Na_a—O6—Ti_m1(2)iv | 100.2 (9) | O1xv—Mg_m2—W_cxiii | 96.0 (7) |
Na_a—O6—Si1 | 125.2 (10) | O1xv—Mg_m2—Ti_m2 | 0 |
Ti_m1(2)iv—O6—Si1 | 128.5 (13) | O1x—Mg_m2—Ba | 96.0 (7) |
Na_av—O7—Si1 | 123.5 (8) | O1x—Mg_m2—Baxiii | 84.0 (7) |
Na_av—O7—Si2ii | 96.8 (8) | O1x—Mg_m2—W_c | 96.0 (7) |
Si1—O7—Si2ii | 126.5 (17) | O1x—Mg_m2—W_cxiii | 84.0 (7) |
Ti_m1(1)—Oh—Ti_m1(2) | 127.9 (5) | O1x—Mg_m2—Ti_m2 | 0 |
Ti_m1(1)—Oh—Ba | 106.6 (8) | Ba—Mg_m2—Baxiii | 180.0 (5) |
Ti_m1(1)—Oh—Nb_m1(1) | 0.0 (5) | Ba—Mg_m2—W_c | 0.0 (5) |
Ti_m1(2)—Oh—Ba | 98.2 (7) | Ba—Mg_m2—W_cxiii | 180.0 (5) |
Ti_m1(2)—Oh—Nb_m1(1) | 127.9 (5) | Ba—Mg_m2—Ti_m2 | 0 |
Ba—Oh—Nb_m1(1) | 106.6 (8) | Baxiii—Mg_m2—W_c | 180.0 (5) |
Na_axx—Ba—Na_axxi | 33.8 (9) | Baxiii—Mg_m2—W_cxiii | 0.0 (5) |
Na_axx—Ba—Na_av | 111.7 (4) | Baxiii—Mg_m2—Ti_m2 | 0 |
Na_axx—Ba—Na_axiv | 100.1 (5) | W_c—Mg_m2—W_cxiii | 180.0 (5) |
Na_axx—Ba—K_b | 127.7 (5) | W_c—Mg_m2—Ti_m2 | 0 |
Na_axx—Ba—Ti_m1(1) | 164.3 (3) | W_cxiii—Mg_m2—Ti_m2 | 0 |
Symmetry codes: (i) −x+1, y, −z; (ii) x, y, z−1; (iii) −x+1, y, −z+1; (iv) −x+1/2, −y+1/2, −z+1; (v) −x+1/2, −y+1/2, −z; (vi) x+1/2, y+1/2, z; (vii) −x+1/2, y+1/2, −z; (viii) −x+1, y, −z+2; (ix) −x+1, −y, −z+1; (x) x, −y, z; (xi) x, y, z+1; (xii) −x+1/2, y+1/2, −z+1; (xiii) −x, y, −z+1; (xiv) x−1/2, −y+1/2, z; (xv) −x, −y, −z+1; (xvi) −x, y, −z; (xvii) −x, −y, −z; (xviii) −x+1/2, y−1/2, −z+1; (xix) x, −y, z+1; (xx) x−1/2, y−1/2, z; (xxi) −x+1/2, y−1/2, −z. |
Crystal data top
Ba0.7Fe0.5K2.1Mg0.05Na2Nb0.1O33Si8Ti4 | Z = 2 |
Mr = 1206.8 | F(000) = 1167 |
Monoclinic, C2/m | Dx = 3.632 Mg m−3 |
Hall symbol: -C 2y | Synchrotron radiation, λ = 0.414 Å |
a = 13.342 (6) Å | Cell parameters from 1825 reflections |
b = 13.0162 (6) Å | θ = 1.9–18.9° |
c = 7.0497 (13) Å | µ = 0.96 mm−1 |
β = 115.68 (3)° | T = 293 K |
V = 1103.3 (6) Å3 | Anhedral grain |
Data collection top
ESRF ID 09 diffractometer | θmax = 18.9°, θmin = 1.9° |
1825 measured reflections | h = −8→8 |
666 independent reflections | k = −20→20 |
293 reflections with I > 2σ(I) | l = −9→10 |
Rint = 0.053 | |
Refinement top
Refinement on F | 0 restraints |
R[F2 > 2σ(F2)] = 0.098 | 6 constraints |
wR(F2) = 0.168 | Weighting scheme based on measured s.u.'s w = 1/(σ2(F) + 0.0100000007F2) |
S = 1.01 | (Δ/σ)max = 0.049 |
666 reflections | Δρmax = 0.96 e Å−3 |
57 parameters | Δρmin = −0.96 e Å−3 |
Fractional atomic coordinates and isotropic or equivalent isotropic displacement parameters (Å2) top | x | y | z | Uiso*/Ueq | Occ. (<1) |
Na_a | 0.414 (3) | 0.2741 (13) | 0.018 (3) | 0.053 (5)* | 0.5 |
K_b | 0.4385 (16) | 0 | 0.7443 (13) | 0.067 (3)* | |
Ti_m1(1) | 0.25 | 0.25 | 0.5 | 0.0368 (13)* | 0.95 |
Ti_m1(2) | 0 | 0.2162 (3) | 0.5 | 0.0311 (12)* | |
Fe_m2 | 0 | 0 | 0.5 | 0.050 (3)* | 0.5 |
Si1 | 0.3318 (9) | 0.1098 (3) | 0.2777 (6) | 0.0220 (11)* | |
Si2 | 0.2130 (8) | 0.1087 (3) | 0.8217 (6) | 0.0207 (10)* | |
O1 | 0.0758 (19) | 0.1041 (7) | 0.6874 (16) | 0.022 (2)* | |
O2 | 0.270 (2) | 0.2019 (8) | 0.7708 (16) | 0.027 (3)* | |
O3 | 0.299 (2) | 0.1145 (8) | 0.4537 (16) | 0.026 (3)* | |
O4 | 0.389 (3) | 0 | 0.298 (2) | 0.030 (4)* | |
O5 | 0.271 (3) | 0 | 0.796 (2) | 0.025 (4)* | |
O6 | 0.416 (2) | 0.1904 (10) | 0.2853 (19) | 0.040 (4)* | |
O7 | 0.221 (2) | 0.1117 (7) | 0.0592 (15) | 0.021 (2)* | |
Oh | 0.0988 (19) | 0.2075 (7) | 0.3788 (14) | 0.017 (2)* | |
Ba | 0.0988 (7) | 0 | 0.3345 (6) | 0.0287 (10)* | 0.35 |
W1 | 0.5 | 0.146 (2) | 0 | 0.075 (8)* | |
W2 | 0 | 0.1056 (13) | 0 | 0.038 (5)* | |
W_c | 0.0988 (7) | 0 | 0.3345 (6) | 0.0287 (10)* | 0.65 |
Nb_m1(1) | 0.25 | 0.25 | 0.5 | 0.0368 (13)* | 0.05 |
Ti_m2 | 0 | 0 | 0.5 | 0.050 (3)* | 0.1 |
Mg_m2 | 0 | 0 | 0.5 | 0.050 (3)* | 0.05 |
Atomic displacement parameters (Å2) top | U11 | U22 | U33 | U12 | U13 | U23 |
? | ? | ? | ? | ? | ? | ? |
Geometric parameters (Å, º) top
Na_a—Na_ai | 2.41 (6) | Ti_m1(2)—Ohxiii | 1.86 (2) |
Na_a—K_bii | 4.14 (2) | Ti_m1(2)—Ba | 3.515 (6) |
Na_a—K_biii | 4.07 (2) | Ti_m1(2)—Baxiii | 3.515 (6) |
Na_a—Ti_m1(1)ii | 3.364 (17) | Ti_m1(2)—Ti_m2 | 2.815 (4) |
Na_a—Ti_m1(2)iv | 3.080 (18) | Ti_m1(2)—Mg_m2 | 2.815 (4) |
Na_a—Si2iv | 2.85 (4) | Fe_m2—O1 | 1.856 (11) |
Na_a—O2ii | 2.17 (3) | Fe_m2—O1xiii | 1.856 (11) |
Na_a—O6 | 2.16 (3) | Fe_m2—O1xv | 1.856 (11) |
Na_a—O7v | 2.22 (4) | Fe_m2—O1x | 1.856 (11) |
Na_a—Bavi | 3.86 (2) | Fe_m2—Ba | 2.105 (9) |
Na_a—Bavii | 3.81 (2) | Fe_m2—Baxiii | 2.105 (9) |
Na_a—W1 | 2.06 (4) | Fe_m2—W_c | 2.105 (9) |
Na_a—W2v | 1.98 (3) | Fe_m2—W_cxiii | 2.105 (9) |
Na_a—Nb_m1(1)ii | 3.364 (17) | Fe_m2—Ti_m2 | 0 |
K_b—K_biii | 4.41 (3) | Fe_m2—Mg_m2 | 0 |
K_b—K_bviii | 3.250 (11) | Si1—O3 | 1.48 (2) |
K_b—Si1 | 3.291 (8) | Si1—O4 | 1.60 (2) |
K_b—Si1iii | 3.44 (2) | Si1—O6 | 1.52 (3) |
K_b—Si1ix | 3.44 (2) | Si1—O7 | 1.607 (16) |
K_b—Si1x | 3.291 (8) | Si2—O1 | 1.66 (2) |
K_b—Si2 | 3.57 (2) | Si2—O2 | 1.56 (2) |
K_b—Si2x | 3.57 (2) | Si2—O5 | 1.66 (2) |
K_b—O3 | 2.563 (17) | Si2—O7xi | 1.631 (16) |
K_b—O3x | 2.563 (17) | Si2—Ba | 3.404 (5) |
K_b—O4iii | 2.44 (5) | O1—Baxiii | 2.64 (2) |
K_b—O5 | 2.42 (5) | O1—Ti_m2 | 1.856 (11) |
K_b—Ba | 4.19 (2) | O1—Mg_m2 | 1.856 (11) |
K_b—W1xi | 2.50 (2) | O2—Nb_m1(1) | 1.913 (14) |
K_b—W1ix | 2.50 (2) | O3—Ba | 2.85 (3) |
Ti_m1(1)—O2 | 1.913 (14) | O3—Nb_m1(1) | 1.958 (15) |
Ti_m1(1)—O2iv | 1.913 (14) | Oh—Ba | 2.718 (9) |
Ti_m1(1)—O3 | 1.958 (15) | Oh—Nb_m1(1) | 1.90 (2) |
Ti_m1(1)—O3iv | 1.958 (15) | Ba—Baxvi | 4.291 (6) |
Ti_m1(1)—Oh | 1.90 (2) | Ba—Baxiii | 4.210 (13) |
Ti_m1(1)—Ohiv | 1.90 (2) | Ba—W2 | 2.548 (10) |
Ti_m1(1)—Ba | 3.739 (4) | Ba—W2xvii | 2.548 (10) |
Ti_m1(1)—Baxii | 3.739 (4) | Ba—W_c | 0 |
Ti_m1(1)—Nb_m1(1) | 0 | Ba—Nb_m1(1) | 3.739 (4) |
Ti_m1(2)—Fe_m2 | 2.815 (4) | Ba—Nb_m1(1)xviii | 3.739 (4) |
Ti_m1(2)—O1 | 1.934 (11) | Ba—Ti_m2 | 2.105 (9) |
Ti_m1(2)—O1xiii | 1.934 (11) | Ba—Mg_m2 | 2.105 (9) |
Ti_m1(2)—O6iv | 1.884 (14) | W_c—Ti_m2 | 2.105 (9) |
Ti_m1(2)—O6xiv | 1.884 (14) | W_c—Mg_m2 | 2.105 (9) |
Ti_m1(2)—Oh | 1.86 (2) | Ti_m2—Mg_m2 | 0 |
| | | |
Na_ai—Na_a—K_bii | 71.3 (8) | Na_axx—Ba—Ti_m1(1)xviii | 68.9 (4) |
Na_ai—Na_a—K_biii | 74.5 (8) | Na_axx—Ba—Ti_m1(2) | 124.3 (6) |
Na_ai—Na_a—Ti_m1(1)ii | 94.9 (9) | Na_axx—Ba—Ti_m1(2)xv | 49.1 (4) |
Na_ai—Na_a—Ti_m1(2)iv | 101.7 (10) | Na_axx—Ba—Fe_m2 | 85.6 (6) |
Na_ai—Na_a—Si2iv | 142.9 (9) | Na_axx—Ba—Si2 | 142.5 (5) |
Na_ai—Na_a—O2ii | 117.6 (14) | Na_axx—Ba—Si2x | 99.2 (3) |
Na_ai—Na_a—O6 | 116.0 (15) | Na_axx—Ba—O1xiii | 91.8 (7) |
Na_ai—Na_a—O7v | 133.1 (12) | Na_axx—Ba—O1xv | 41.4 (7) |
Na_ai—Na_a—Bavi | 70.4 (8) | Na_axx—Ba—O3 | 148.2 (8) |
Na_ai—Na_a—Bavii | 72.9 (8) | Na_axx—Ba—O3x | 93.1 (6) |
Na_ai—Na_a—W1 | 54.1 (11) | Na_axx—Ba—Oh | 142.3 (6) |
Na_ai—Na_a—W2v | 52.4 (11) | Na_axx—Ba—Ohx | 43.8 (4) |
Na_ai—Na_a—Nb_m1(1)ii | 94.9 (9) | Na_axx—Ba—Baxvi | 55.4 (3) |
K_bii—Na_a—K_biii | 46.7 (3) | Na_axx—Ba—Baxiii | 85.6 (6) |
K_bii—Na_a—Ti_m1(1)ii | 63.8 (3) | Na_axx—Ba—W2 | 86.1 (4) |
K_bii—Na_a—Ti_m1(2)iv | 118.9 (5) | Na_axx—Ba—W2xvii | 27.2 (5) |
K_bii—Na_a—Si2iv | 145.7 (12) | Na_axx—Ba—W_c | 0 |
K_bii—Na_a—O2ii | 58.1 (8) | Na_axx—Ba—Nb_m1(1) | 164.9 (3) |
K_bii—Na_a—O6 | 89.9 (7) | Na_axx—Ba—Nb_m1(1)xviii | 68.9 (4) |
K_bii—Na_a—O7v | 133.1 (9) | Na_axx—Ba—Ti_m2 | 85.6 (6) |
K_bii—Na_a—Bavi | 140.1 (12) | Na_axx—Ba—Mg_m2 | 85.6 (6) |
K_bii—Na_a—Bavii | 110.6 (7) | Na_axxi—Ba—Na_av | 101.1 (5) |
K_bii—Na_a—W1 | 27.5 (4) | Na_axxi—Ba—Na_axiv | 111.9 (4) |
K_bii—Na_a—W2v | 119.2 (15) | Na_axxi—Ba—K_b | 100.4 (6) |
K_bii—Na_a—Nb_m1(1)ii | 63.8 (3) | Na_axxi—Ba—Ti_m1(1) | 137.9 (6) |
K_biii—Na_a—Ti_m1(1)ii | 109.6 (5) | Na_axxi—Ba—Ti_m1(1)xviii | 52.9 (3) |
K_biii—Na_a—Ti_m1(2)iv | 72.5 (4) | Na_axxi—Ba—Ti_m1(2) | 156.6 (5) |
K_biii—Na_a—Si2iv | 124.8 (8) | Na_axxi—Ba—Ti_m1(2)xv | 71.4 (5) |
K_biii—Na_a—O2ii | 93.0 (6) | Na_axxi—Ba—Fe_m2 | 120.0 (6) |
K_biii—Na_a—O6 | 51.6 (8) | Na_axxi—Ba—Si2 | 148.7 (4) |
K_biii—Na_a—O7v | 152.4 (16) | Na_axxi—Ba—Si2x | 102.3 (3) |
K_biii—Na_a—Bavi | 110.9 (7) | Na_axxi—Ba—O1xiii | 124.7 (6) |
K_biii—Na_a—Bavii | 145.4 (12) | Na_axxi—Ba—O1xv | 77.1 (7) |
K_biii—Na_a—W1 | 29.8 (5) | Na_axxi—Ba—O3 | 111.6 (8) |
K_biii—Na_a—W2v | 122.1 (15) | Na_axxi—Ba—O3x | 63.9 (6) |
K_biii—Na_a—Nb_m1(1)ii | 109.6 (5) | Na_axxi—Ba—Oh | 147.1 (5) |
Ti_m1(1)ii—Na_a—Ti_m1(2)iv | 163.2 (15) | Na_axxi—Ba—Ohx | 46.0 (4) |
Ti_m1(1)ii—Na_a—Si2iv | 105.1 (10) | Na_axxi—Ba—Baxvi | 56.6 (3) |
Ti_m1(1)ii—Na_a—O2ii | 32.1 (5) | Na_axxi—Ba—Baxiii | 120.0 (6) |
Ti_m1(1)ii—Na_a—O6 | 130.9 (13) | Na_axxi—Ba—W2 | 87.3 (4) |
Ti_m1(1)ii—Na_a—O7v | 73.6 (6) | Na_axxi—Ba—W2xvii | 28.3 (5) |
Ti_m1(1)ii—Na_a—Bavi | 130.6 (6) | Na_axxi—Ba—W_c | 0 |
Ti_m1(1)ii—Na_a—Bavii | 62.5 (3) | Na_axxi—Ba—Nb_m1(1) | 137.9 (6) |
Ti_m1(1)ii—Na_a—W1 | 88.5 (6) | Na_axxi—Ba—Nb_m1(1)xviii | 52.9 (3) |
Ti_m1(1)ii—Na_a—W2v | 97.2 (7) | Na_axxi—Ba—Ti_m2 | 120.0 (6) |
Ti_m1(1)ii—Na_a—Nb_m1(1)ii | 0.0 (5) | Na_axxi—Ba—Mg_m2 | 120.0 (6) |
Ti_m1(2)iv—Na_a—Si2iv | 62.8 (6) | Na_av—Ba—Na_axiv | 36.7 (9) |
Ti_m1(2)iv—Na_a—O2ii | 132.9 (16) | Na_av—Ba—K_b | 100.4 (6) |
Ti_m1(2)iv—Na_a—O6 | 37.2 (5) | Na_av—Ba—Ti_m1(1) | 52.9 (3) |
Ti_m1(2)iv—Na_a—O7v | 96.8 (10) | Na_av—Ba—Ti_m1(1)xviii | 137.9 (6) |
Ti_m1(2)iv—Na_a—Bavi | 59.6 (3) | Na_av—Ba—Ti_m1(2) | 71.4 (5) |
Ti_m1(2)iv—Na_a—Bavii | 125.4 (5) | Na_av—Ba—Ti_m1(2)xv | 156.6 (5) |
Ti_m1(2)iv—Na_a—W1 | 98.7 (7) | Na_av—Ba—Fe_m2 | 120.0 (6) |
Ti_m1(2)iv—Na_a—W2v | 95.2 (7) | Na_av—Ba—Si2 | 102.3 (3) |
Ti_m1(2)iv—Na_a—Nb_m1(1)ii | 163.2 (15) | Na_av—Ba—Si2x | 148.7 (4) |
Si2iv—Na_a—O2ii | 94.5 (16) | Na_av—Ba—O1xiii | 77.1 (7) |
Si2iv—Na_a—O6 | 73.2 (12) | Na_av—Ba—O1xv | 124.7 (6) |
Si2iv—Na_a—O7v | 34.7 (6) | Na_av—Ba—O3 | 63.9 (6) |
Si2iv—Na_a—Bavi | 72.8 (4) | Na_av—Ba—O3x | 111.6 (8) |
Si2iv—Na_a—Bavii | 88.8 (5) | Na_av—Ba—Oh | 46.0 (4) |
Si2iv—Na_a—W1 | 154.2 (12) | Na_av—Ba—Ohx | 147.1 (5) |
Si2iv—Na_a—W2v | 93.6 (8) | Na_av—Ba—Baxvi | 56.6 (3) |
Si2iv—Na_a—Nb_m1(1)ii | 105.1 (10) | Na_av—Ba—Baxiii | 120.0 (6) |
O2ii—Na_a—O6 | 98.9 (15) | Na_av—Ba—W2 | 28.3 (5) |
O2ii—Na_a—O7v | 75.5 (12) | Na_av—Ba—W2xvii | 87.3 (4) |
O2ii—Na_a—Bavi | 156.1 (9) | Na_av—Ba—W_c | 0 |
O2ii—Na_a—Bavii | 92.0 (6) | Na_av—Ba—Nb_m1(1) | 52.9 (3) |
O2ii—Na_a—W1 | 85.4 (8) | Na_av—Ba—Nb_m1(1)xviii | 137.9 (6) |
O2ii—Na_a—W2v | 128.7 (9) | Na_av—Ba—Ti_m2 | 120.0 (6) |
O2ii—Na_a—Nb_m1(1)ii | 32.1 (5) | Na_av—Ba—Mg_m2 | 120.0 (6) |
O6—Na_a—O7v | 104.7 (19) | Na_axiv—Ba—K_b | 128.8 (5) |
O6—Na_a—Bavi | 96.7 (7) | Na_axiv—Ba—Ti_m1(1) | 68.9 (4) |
O6—Na_a—Bavii | 159.6 (10) | Na_axiv—Ba—Ti_m1(1)xviii | 164.9 (3) |
O6—Na_a—W1 | 81.3 (9) | Na_axiv—Ba—Ti_m1(2) | 49.1 (4) |
O6—Na_a—W2v | 131.8 (11) | Na_axiv—Ba—Ti_m1(2)xv | 124.3 (6) |
O6—Na_a—Nb_m1(1)ii | 130.9 (13) | Na_axiv—Ba—Fe_m2 | 85.6 (6) |
O7v—Na_a—Bavi | 83.1 (6) | Na_axiv—Ba—Si2 | 99.2 (3) |
O7v—Na_a—Bavii | 61.3 (7) | Na_axiv—Ba—Si2x | 142.5 (5) |
O7v—Na_a—W1 | 160.6 (11) | Na_axiv—Ba—O1xiii | 41.4 (7) |
O7v—Na_a—W2v | 83.4 (9) | Na_axiv—Ba—O1xv | 91.8 (7) |
O7v—Na_a—Nb_m1(1)ii | 73.6 (6) | Na_axiv—Ba—O3 | 93.1 (6) |
Bavi—Na_a—Bavii | 68.1 (4) | Na_axiv—Ba—O3x | 148.2 (8) |
Bavi—Na_a—W1 | 114.9 (14) | Na_axiv—Ba—Oh | 43.8 (4) |
Bavi—Na_a—W2v | 36.1 (3) | Na_axiv—Ba—Ohx | 142.3 (6) |
Bavi—Na_a—Nb_m1(1)ii | 130.6 (6) | Na_axiv—Ba—Baxvi | 55.4 (3) |
Bavii—Na_a—W1 | 117.0 (14) | Na_axiv—Ba—Baxiii | 85.6 (6) |
Bavii—Na_a—W2v | 37.7 (4) | Na_axiv—Ba—W2 | 27.2 (5) |
Bavii—Na_a—Nb_m1(1)ii | 62.5 (3) | Na_axiv—Ba—W2xvii | 86.1 (4) |
W1—Na_a—W2v | 107 (2) | Na_axiv—Ba—W_c | 0 |
W1—Na_a—Nb_m1(1)ii | 88.5 (6) | Na_axiv—Ba—Nb_m1(1) | 68.9 (4) |
W2v—Na_a—Nb_m1(1)ii | 97.2 (7) | Na_axiv—Ba—Nb_m1(1)xviii | 164.9 (3) |
Na_axi—K_b—Na_aiii | 34.2 (8) | Na_axiv—Ba—Ti_m2 | 85.6 (6) |
Na_axi—K_b—Na_aix | 133.3 (4) | Na_axiv—Ba—Mg_m2 | 85.6 (6) |
Na_axi—K_b—Na_axix | 119.2 (6) | K_b—Ba—Ti_m1(1) | 60.55 (10) |
Na_axi—K_b—K_biii | 119.7 (5) | K_b—Ba—Ti_m1(1)xviii | 60.55 (10) |
Na_axi—K_b—K_bviii | 65.5 (3) | K_b—Ba—Ti_m1(2) | 102.73 (15) |
Na_axi—K_b—Si1 | 90.3 (3) | K_b—Ba—Ti_m1(2)xv | 102.73 (15) |
Na_axi—K_b—Si1iii | 85.1 (6) | K_b—Ba—Fe_m2 | 111.6 (3) |
Na_axi—K_b—Si1ix | 129.1 (7) | K_b—Ba—Si2 | 55.0 (3) |
Na_axi—K_b—Si1x | 138.9 (4) | K_b—Ba—Si2x | 55.0 (3) |
Na_axi—K_b—Si2 | 49.1 (6) | K_b—Ba—O1xiii | 134.7 (3) |
Na_axi—K_b—Si2x | 91.6 (7) | K_b—Ba—O1xv | 134.7 (3) |
Na_axi—K_b—O3 | 72.3 (4) | K_b—Ba—O3 | 36.9 (3) |
Na_axi—K_b—O3x | 134.3 (9) | K_b—Ba—O3x | 36.9 (3) |
Na_axi—K_b—O4iii | 109.0 (7) | K_b—Ba—Oh | 88.5 (5) |
Na_axi—K_b—O5 | 70.4 (7) | K_b—Ba—Ohx | 88.5 (5) |
Na_axi—K_b—Ba | 92.4 (6) | K_b—Ba—Baxvi | 136.4 (3) |
Na_axi—K_b—W1xi | 22.4 (5) | K_b—Ba—Baxiii | 111.6 (2) |
Na_axi—K_b—W1ix | 112.7 (6) | K_b—Ba—W2 | 127.5 (3) |
Na_aiii—K_b—Na_aix | 122.6 (6) | K_b—Ba—W2xvii | 127.5 (3) |
Na_aiii—K_b—Na_axix | 133.3 (4) | K_b—Ba—W_c | 0 |
Na_aiii—K_b—K_biii | 92.5 (6) | K_b—Ba—Nb_m1(1) | 60.55 (10) |
Na_aiii—K_b—K_bviii | 67.8 (3) | K_b—Ba—Nb_m1(1)xviii | 60.55 (10) |
Na_aiii—K_b—Si1 | 87.3 (3) | K_b—Ba—Ti_m2 | 111.6 (3) |
Na_aiii—K_b—Si1iii | 51.2 (6) | K_b—Ba—Mg_m2 | 111.6 (3) |
Na_aiii—K_b—Si1ix | 95.8 (7) | Ti_m1(1)—Ba—Ti_m1(1)xviii | 121.0 (2) |
Na_aiii—K_b—Si1x | 135.6 (5) | Ti_m1(1)—Ba—Ti_m1(2) | 55.16 (4) |
Na_aiii—K_b—Si2 | 83.0 (6) | Ti_m1(1)—Ba—Ti_m1(2)xv | 145.34 (13) |
Na_aiii—K_b—Si2x | 125.0 (7) | Ti_m1(1)—Ba—Fe_m2 | 102.11 (10) |
Na_aiii—K_b—O3 | 82.6 (4) | Ti_m1(1)—Ba—Si2 | 51.56 (12) |
Na_aiii—K_b—O3x | 153.2 (4) | Ti_m1(1)—Ba—Si2x | 95.83 (13) |
Na_aiii—K_b—O4iii | 74.8 (7) | Ti_m1(1)—Ba—O1xiii | 85.1 (3) |
Na_aiii—K_b—O5 | 104.6 (7) | Ti_m1(1)—Ba—O1xv | 143.9 (4) |
Na_aiii—K_b—Ba | 118.0 (5) | Ti_m1(1)—Ba—O3 | 31.0 (4) |
Na_aiii—K_b—W1xi | 24.2 (6) | Ti_m1(1)—Ba—O3x | 93.0 (4) |
Na_aiii—K_b—W1ix | 114.9 (5) | Ti_m1(1)—Ba—Oh | 29.1 (5) |
Na_aix—K_b—Na_axix | 34.2 (8) | Ti_m1(1)—Ba—Ohx | 148.8 (4) |
Na_aix—K_b—K_biii | 92.5 (6) | Ti_m1(1)—Ba—Baxvi | 109.53 (10) |
Na_aix—K_b—K_bviii | 67.8 (3) | Ti_m1(1)—Ba—Baxiii | 102.11 (12) |
Na_aix—K_b—Si1 | 135.6 (5) | Ti_m1(1)—Ba—W2 | 79.2 (3) |
Na_aix—K_b—Si1iii | 95.8 (7) | Ti_m1(1)—Ba—W2xvii | 138.7 (3) |
Na_aix—K_b—Si1ix | 51.2 (6) | Ti_m1(1)—Ba—W_c | 0 |
Na_aix—K_b—Si1x | 87.3 (3) | Ti_m1(1)—Ba—Nb_m1(1) | 0.0 (5) |
Na_aix—K_b—Si2 | 125.0 (7) | Ti_m1(1)—Ba—Nb_m1(1)xviii | 121.0 (2) |
Na_aix—K_b—Si2x | 83.0 (6) | Ti_m1(1)—Ba—Ti_m2 | 102.11 (10) |
Na_aix—K_b—O3 | 153.2 (4) | Ti_m1(1)—Ba—Mg_m2 | 102.11 (10) |
Na_aix—K_b—O3x | 82.6 (4) | Ti_m1(1)xviii—Ba—Ti_m1(2) | 145.34 (13) |
Na_aix—K_b—O4iii | 74.8 (7) | Ti_m1(1)xviii—Ba—Ti_m1(2)xv | 55.16 (4) |
Na_aix—K_b—O5 | 104.6 (7) | Ti_m1(1)xviii—Ba—Fe_m2 | 102.11 (10) |
Na_aix—K_b—Ba | 118.0 (5) | Ti_m1(1)xviii—Ba—Si2 | 95.83 (13) |
Na_aix—K_b—W1xi | 114.9 (5) | Ti_m1(1)xviii—Ba—Si2x | 51.56 (12) |
Na_aix—K_b—W1ix | 24.2 (6) | Ti_m1(1)xviii—Ba—O1xiii | 143.9 (4) |
Na_axix—K_b—K_biii | 119.7 (5) | Ti_m1(1)xviii—Ba—O1xv | 85.1 (3) |
Na_axix—K_b—K_bviii | 65.5 (3) | Ti_m1(1)xviii—Ba—O3 | 93.0 (4) |
Na_axix—K_b—Si1 | 138.9 (4) | Ti_m1(1)xviii—Ba—O3x | 31.0 (4) |
Na_axix—K_b—Si1iii | 129.1 (7) | Ti_m1(1)xviii—Ba—Oh | 148.8 (4) |
Na_axix—K_b—Si1ix | 85.1 (6) | Ti_m1(1)xviii—Ba—Ohx | 29.1 (5) |
Na_axix—K_b—Si1x | 90.3 (3) | Ti_m1(1)xviii—Ba—Baxvi | 109.53 (10) |
Na_axix—K_b—Si2 | 91.6 (7) | Ti_m1(1)xviii—Ba—Baxiii | 102.11 (12) |
Na_axix—K_b—Si2x | 49.1 (6) | Ti_m1(1)xviii—Ba—W2 | 138.7 (3) |
Na_axix—K_b—O3 | 134.3 (9) | Ti_m1(1)xviii—Ba—W2xvii | 79.2 (3) |
Na_axix—K_b—O3x | 72.3 (4) | Ti_m1(1)xviii—Ba—W_c | 0 |
Na_axix—K_b—O4iii | 109.0 (7) | Ti_m1(1)xviii—Ba—Nb_m1(1) | 121.0 (2) |
Na_axix—K_b—O5 | 70.4 (7) | Ti_m1(1)xviii—Ba—Nb_m1(1)xviii | 0.0 (5) |
Na_axix—K_b—Ba | 92.4 (6) | Ti_m1(1)xviii—Ba—Ti_m2 | 102.11 (10) |
Na_axix—K_b—W1xi | 112.7 (6) | Ti_m1(1)xviii—Ba—Mg_m2 | 102.11 (10) |
Na_axix—K_b—W1ix | 22.4 (5) | Ti_m1(2)—Ba—Ti_m1(2)xv | 106.4 (2) |
K_biii—K_b—K_bviii | 133.3 (7) | Ti_m1(2)—Ba—Fe_m2 | 53.21 (13) |
K_biii—K_b—Si1 | 50.6 (3) | Ti_m1(2)—Ba—Si2 | 53.17 (14) |
K_biii—K_b—Si1iii | 47.6 (3) | Ti_m1(2)—Ba—Si2x | 93.79 (17) |
K_biii—K_b—Si1ix | 47.6 (3) | Ti_m1(2)—Ba—O1xiii | 32.9 (3) |
K_biii—K_b—Si1x | 50.6 (3) | Ti_m1(2)—Ba—O1xv | 89.0 (4) |
K_biii—K_b—Si2 | 137.9 (3) | Ti_m1(2)—Ba—O3 | 85.5 (4) |
K_biii—K_b—Si2x | 137.9 (3) | Ti_m1(2)—Ba—O3x | 139.4 (3) |
K_biii—K_b—O3 | 76.2 (7) | Ti_m1(2)—Ba—Oh | 31.5 (5) |
K_biii—K_b—O3x | 76.2 (7) | Ti_m1(2)—Ba—Ohx | 137.6 (6) |
K_biii—K_b—O4iii | 38.4 (5) | Ti_m1(2)—Ba—Baxvi | 102.99 (14) |
K_biii—K_b—O5 | 143.1 (5) | Ti_m1(2)—Ba—Baxiii | 53.21 (13) |
K_biii—K_b—Ba | 96.8 (3) | Ti_m1(2)—Ba—W2 | 75.9 (3) |
K_biii—K_b—W1xi | 116.5 (6) | Ti_m1(2)—Ba—W2xvii | 128.4 (3) |
K_biii—K_b—W1ix | 116.5 (6) | Ti_m1(2)—Ba—W_c | 0 |
K_bviii—K_b—Si1 | 154.23 (10) | Ti_m1(2)—Ba—Nb_m1(1) | 55.16 (4) |
K_bviii—K_b—Si1iii | 91.1 (5) | Ti_m1(2)—Ba—Nb_m1(1)xviii | 145.34 (13) |
K_bviii—K_b—Si1ix | 91.1 (5) | Ti_m1(2)—Ba—Ti_m2 | 53.21 (13) |
K_bviii—K_b—Si1x | 154.23 (10) | Ti_m1(2)—Ba—Mg_m2 | 53.21 (13) |
K_bviii—K_b—Si2 | 83.4 (5) | Ti_m1(2)xv—Ba—Fe_m2 | 53.21 (13) |
K_bviii—K_b—Si2x | 83.4 (5) | Ti_m1(2)xv—Ba—Si2 | 93.79 (17) |
K_bviii—K_b—O3 | 136.8 (6) | Ti_m1(2)xv—Ba—Si2x | 53.17 (14) |
K_bviii—K_b—O3x | 136.8 (6) | Ti_m1(2)xv—Ba—O1xiii | 89.0 (4) |
K_bviii—K_b—O4iii | 95.0 (7) | Ti_m1(2)xv—Ba—O1xv | 32.9 (3) |
K_bviii—K_b—O5 | 83.6 (7) | Ti_m1(2)xv—Ba—O3 | 139.4 (3) |
K_bviii—K_b—Ba | 129.8 (7) | Ti_m1(2)xv—Ba—O3x | 85.5 (4) |
K_bviii—K_b—W1xi | 49.5 (4) | Ti_m1(2)xv—Ba—Oh | 137.6 (6) |
K_bviii—K_b—W1ix | 49.5 (4) | Ti_m1(2)xv—Ba—Ohx | 31.5 (5) |
Si1—K_b—Si1iii | 77.4 (4) | Ti_m1(2)xv—Ba—Baxvi | 102.99 (14) |
Si1—K_b—Si1ix | 98.2 (5) | Ti_m1(2)xv—Ba—Baxiii | 53.21 (13) |
Si1—K_b—Si1x | 51.47 (16) | Ti_m1(2)xv—Ba—W2 | 128.4 (3) |
Si1—K_b—Si2 | 87.3 (4) | Ti_m1(2)xv—Ba—W2xvii | 75.9 (3) |
Si1—K_b—Si2x | 107.2 (5) | Ti_m1(2)xv—Ba—W_c | 0 |
Si1—K_b—O3 | 25.7 (6) | Ti_m1(2)xv—Ba—Nb_m1(1) | 145.34 (13) |
Si1—K_b—O3x | 66.7 (3) | Ti_m1(2)xv—Ba—Nb_m1(1)xviii | 55.16 (4) |
Si1—K_b—O4iii | 84.2 (5) | Ti_m1(2)xv—Ba—Ti_m2 | 53.21 (13) |
Si1—K_b—O5 | 97.1 (6) | Ti_m1(2)xv—Ba—Mg_m2 | 53.21 (13) |
Si1—K_b—Ba | 56.0 (3) | Fe_m2—Ba—Si2 | 63.6 (2) |
Si1—K_b—W1xi | 104.8 (4) | Fe_m2—Ba—Si2x | 63.6 (2) |
Si1—K_b—W1ix | 156.2 (5) | Fe_m2—Ba—O1xiii | 44.3 (3) |
Si1iii—K_b—Si1ix | 49.0 (3) | Fe_m2—Ba—O1xv | 44.3 (3) |
Si1iii—K_b—Si1x | 98.2 (5) | Fe_m2—Ba—O3 | 124.7 (4) |
Si1iii—K_b—Si2 | 131.81 (14) | Fe_m2—Ba—O3x | 124.7 (4) |
Si1iii—K_b—Si2x | 174.3 (3) | Fe_m2—Ba—Oh | 84.6 (5) |
Si1iii—K_b—O3 | 94.2 (7) | Fe_m2—Ba—Ohx | 84.6 (5) |
Si1iii—K_b—O3x | 123.7 (8) | Fe_m2—Ba—Baxvi | 112.0 (3) |
Si1iii—K_b—O4iii | 24.79 (19) | Fe_m2—Ba—Baxiii | 0.0 (5) |
Si1iii—K_b—O5 | 155.0 (2) | Fe_m2—Ba—W2 | 108.4 (3) |
Si1iii—K_b—Ba | 133.4 (2) | Fe_m2—Ba—W2xvii | 108.4 (3) |
Si1iii—K_b—W1xi | 72.4 (4) | Fe_m2—Ba—W_c | 0 |
Si1iii—K_b—W1ix | 109.1 (6) | Fe_m2—Ba—Nb_m1(1) | 102.11 (10) |
Si1ix—K_b—Si1x | 77.4 (4) | Fe_m2—Ba—Nb_m1(1)xviii | 102.11 (10) |
Si1ix—K_b—Si2 | 174.3 (3) | Fe_m2—Ba—Ti_m2 | 0.0 (5) |
Si1ix—K_b—Si2x | 131.81 (14) | Fe_m2—Ba—Mg_m2 | 0.0 (5) |
Si1ix—K_b—O3 | 123.7 (8) | Si2—Ba—Si2x | 49.11 (10) |
Si1ix—K_b—O3x | 94.2 (7) | Si2—Ba—O1xiii | 81.0 (3) |
Si1ix—K_b—O4iii | 24.79 (19) | Si2—Ba—O1xv | 105.7 (4) |
Si1ix—K_b—O5 | 155.0 (2) | Si2—Ba—O3 | 62.1 (4) |
Si1ix—K_b—Ba | 133.4 (2) | Si2—Ba—O3x | 88.1 (3) |
Si1ix—K_b—W1xi | 109.1 (6) | Si2—Ba—Oh | 59.6 (2) |
Si1ix—K_b—W1ix | 72.4 (4) | Si2—Ba—Ohx | 108.6 (2) |
Si1x—K_b—Si2 | 107.2 (5) | Si2—Ba—Baxvi | 154.46 (12) |
Si1x—K_b—Si2x | 87.3 (4) | Si2—Ba—Baxiii | 63.6 (2) |
Si1x—K_b—O3 | 66.7 (3) | Si2—Ba—W2 | 122.4 (3) |
Si1x—K_b—O3x | 25.7 (6) | Si2—Ba—W2xvii | 169.7 (4) |
Si1x—K_b—O4iii | 84.2 (5) | Si2—Ba—W_c | 0 |
Si1x—K_b—O5 | 97.1 (6) | Si2—Ba—Nb_m1(1) | 51.56 (12) |
Si1x—K_b—Ba | 56.0 (3) | Si2—Ba—Nb_m1(1)xviii | 95.83 (13) |
Si1x—K_b—W1xi | 156.2 (5) | Si2—Ba—Ti_m2 | 63.6 (2) |
Si1x—K_b—W1ix | 104.8 (4) | Si2—Ba—Mg_m2 | 63.6 (2) |
Si2—K_b—Si2x | 46.6 (3) | Si2x—Ba—O1xiii | 105.7 (4) |
Si2—K_b—O3 | 61.7 (7) | Si2x—Ba—O1xv | 81.0 (3) |
Si2—K_b—O3x | 89.2 (8) | Si2x—Ba—O3 | 88.1 (3) |
Si2—K_b—O4iii | 156.58 (18) | Si2x—Ba—O3x | 62.1 (4) |
Si2—K_b—O5 | 23.33 (17) | Si2x—Ba—Oh | 108.6 (2) |
Si2—K_b—Ba | 51.3 (3) | Si2x—Ba—Ohx | 59.6 (2) |
Si2—K_b—W1xi | 67.9 (4) | Si2x—Ba—Baxvi | 154.46 (12) |
Si2—K_b—W1ix | 103.0 (6) | Si2x—Ba—Baxiii | 63.6 (2) |
Si2x—K_b—O3 | 89.2 (8) | Si2x—Ba—W2 | 169.7 (4) |
Si2x—K_b—O3x | 61.7 (7) | Si2x—Ba—W2xvii | 122.4 (3) |
Si2x—K_b—O4iii | 156.58 (18) | Si2x—Ba—W_c | 0 |
Si2x—K_b—O5 | 23.33 (17) | Si2x—Ba—Nb_m1(1) | 95.83 (13) |
Si2x—K_b—Ba | 51.3 (3) | Si2x—Ba—Nb_m1(1)xviii | 51.56 (12) |
Si2x—K_b—W1xi | 103.0 (6) | Si2x—Ba—Ti_m2 | 63.6 (2) |
Si2x—K_b—W1ix | 67.9 (4) | Si2x—Ba—Mg_m2 | 63.6 (2) |
O3—K_b—O3x | 71.1 (5) | O1xiii—Ba—O1xv | 61.7 (5) |
O3—K_b—O4iii | 107.2 (8) | O1xiii—Ba—O3 | 116.1 (5) |
O3—K_b—O5 | 73.9 (8) | O1xiii—Ba—O3x | 167.5 (4) |
O3—K_b—Ba | 41.9 (6) | O1xiii—Ba—Oh | 56.9 (6) |
O3—K_b—W1xi | 91.8 (5) | O1xiii—Ba—Ohx | 118.2 (7) |
O3—K_b—W1ix | 156.4 (10) | O1xiii—Ba—Baxvi | 80.2 (3) |
O3x—K_b—O4iii | 107.2 (8) | O1xiii—Ba—Baxiii | 44.3 (3) |
O3x—K_b—O5 | 73.9 (8) | O1xiii—Ba—W2 | 65.2 (3) |
O3x—K_b—Ba | 41.9 (6) | O1xiii—Ba—W2xvii | 97.7 (4) |
O3x—K_b—W1xi | 156.4 (10) | O1xiii—Ba—W_c | 0 |
O3x—K_b—W1ix | 91.8 (5) | O1xiii—Ba—Nb_m1(1) | 85.1 (3) |
O4iii—K_b—O5 | 178.6 (6) | O1xiii—Ba—Nb_m1(1)xviii | 143.9 (4) |
O4iii—K_b—Ba | 135.2 (5) | O1xiii—Ba—Ti_m2 | 44.3 (3) |
O4iii—K_b—W1xi | 93.2 (6) | O1xiii—Ba—Mg_m2 | 44.3 (3) |
O4iii—K_b—W1ix | 93.2 (6) | O1xv—Ba—O3 | 167.5 (4) |
O5—K_b—Ba | 46.2 (4) | O1xv—Ba—O3x | 116.1 (5) |
O5—K_b—W1xi | 85.8 (6) | O1xv—Ba—Oh | 118.2 (7) |
O5—K_b—W1ix | 85.8 (6) | O1xv—Ba—Ohx | 56.9 (6) |
Ba—K_b—W1xi | 114.6 (6) | O1xv—Ba—Baxvi | 80.2 (3) |
Ba—K_b—W1ix | 114.6 (6) | O1xv—Ba—Baxiii | 44.3 (3) |
W1xi—K_b—W1ix | 98.9 (6) | O1xv—Ba—W2 | 97.7 (4) |
Na_axi—Ti_m1(1)—Na_av | 180.0 (5) | O1xv—Ba—W2xvii | 65.2 (3) |
Na_axi—Ti_m1(1)—O2 | 37.1 (8) | O1xv—Ba—W_c | 0 |
Na_axi—Ti_m1(1)—O2iv | 142.9 (8) | O1xv—Ba—Nb_m1(1) | 143.9 (4) |
Na_axi—Ti_m1(1)—O3 | 99.1 (5) | O1xv—Ba—Nb_m1(1)xviii | 85.1 (3) |
Na_axi—Ti_m1(1)—O3iv | 80.9 (5) | O1xv—Ba—Ti_m2 | 44.3 (3) |
Na_axi—Ti_m1(1)—Oh | 125.5 (8) | O1xv—Ba—Mg_m2 | 44.3 (3) |
Na_axi—Ti_m1(1)—Ohiv | 54.5 (8) | O3—Ba—O3x | 63.0 (5) |
Na_axi—Ti_m1(1)—Ba | 115.5 (4) | O3—Ba—Oh | 59.6 (6) |
Na_axi—Ti_m1(1)—Baxii | 64.5 (4) | O3—Ba—Ohx | 122.1 (6) |
Na_axi—Ti_m1(1)—Nb_m1(1) | 0 | O3—Ba—Baxvi | 112.0 (3) |
Na_av—Ti_m1(1)—O2 | 142.9 (8) | O3—Ba—Baxiii | 124.7 (4) |
Na_av—Ti_m1(1)—O2iv | 37.1 (8) | O3—Ba—W2 | 91.9 (3) |
Na_av—Ti_m1(1)—O3 | 80.9 (5) | O3—Ba—W2xvii | 126.7 (5) |
Na_av—Ti_m1(1)—O3iv | 99.1 (5) | O3—Ba—W_c | 0 |
Na_av—Ti_m1(1)—Oh | 54.5 (8) | O3—Ba—Nb_m1(1) | 31.0 (4) |
Na_av—Ti_m1(1)—Ohiv | 125.5 (8) | O3—Ba—Nb_m1(1)xviii | 93.0 (4) |
Na_av—Ti_m1(1)—Ba | 64.5 (4) | O3—Ba—Ti_m2 | 124.7 (4) |
Na_av—Ti_m1(1)—Baxii | 115.5 (4) | O3—Ba—Mg_m2 | 124.7 (4) |
Na_av—Ti_m1(1)—Nb_m1(1) | 0 | O3x—Ba—Oh | 122.1 (6) |
O2—Ti_m1(1)—O2iv | 180.0 (5) | O3x—Ba—Ohx | 59.6 (6) |
O2—Ti_m1(1)—O3 | 87.7 (6) | O3x—Ba—Baxvi | 112.0 (3) |
O2—Ti_m1(1)—O3iv | 92.3 (6) | O3x—Ba—Baxiii | 124.7 (4) |
O2—Ti_m1(1)—Oh | 91.0 (8) | O3x—Ba—W2 | 126.7 (5) |
O2—Ti_m1(1)—Ohiv | 89.0 (8) | O3x—Ba—W2xvii | 91.9 (3) |
O2—Ti_m1(1)—Ba | 81.4 (4) | O3x—Ba—W_c | 0 |
O2—Ti_m1(1)—Baxii | 98.6 (4) | O3x—Ba—Nb_m1(1) | 93.0 (4) |
O2—Ti_m1(1)—Nb_m1(1) | 0 | O3x—Ba—Nb_m1(1)xviii | 31.0 (4) |
O2iv—Ti_m1(1)—O3 | 92.3 (6) | O3x—Ba—Ti_m2 | 124.7 (4) |
O2iv—Ti_m1(1)—O3iv | 87.7 (6) | O3x—Ba—Mg_m2 | 124.7 (4) |
O2iv—Ti_m1(1)—Oh | 89.0 (8) | Oh—Ba—Ohx | 166.8 (5) |
O2iv—Ti_m1(1)—Ohiv | 91.0 (8) | Oh—Ba—Baxvi | 95.5 (2) |
O2iv—Ti_m1(1)—Ba | 98.6 (4) | Oh—Ba—Baxiii | 84.6 (5) |
O2iv—Ti_m1(1)—Baxii | 81.4 (4) | Oh—Ba—W2 | 62.9 (4) |
O2iv—Ti_m1(1)—Nb_m1(1) | 0 | Oh—Ba—W2xvii | 128.1 (4) |
O3—Ti_m1(1)—O3iv | 180.0 (5) | Oh—Ba—W_c | 0 |
O3—Ti_m1(1)—Oh | 91.8 (8) | Oh—Ba—Nb_m1(1) | 29.1 (5) |
O3—Ti_m1(1)—Ohiv | 88.2 (8) | Oh—Ba—Nb_m1(1)xviii | 148.8 (4) |
O3—Ti_m1(1)—Ba | 48.6 (8) | Oh—Ba—Ti_m2 | 84.6 (5) |
O3—Ti_m1(1)—Baxii | 131.4 (8) | Oh—Ba—Mg_m2 | 84.6 (5) |
O3—Ti_m1(1)—Nb_m1(1) | 0 | Ohx—Ba—Baxvi | 95.5 (2) |
O3iv—Ti_m1(1)—Oh | 88.2 (8) | Ohx—Ba—Baxiii | 84.6 (5) |
O3iv—Ti_m1(1)—Ohiv | 91.8 (8) | Ohx—Ba—W2 | 128.1 (4) |
O3iv—Ti_m1(1)—Ba | 131.4 (8) | Ohx—Ba—W2xvii | 62.9 (4) |
O3iv—Ti_m1(1)—Baxii | 48.6 (8) | Ohx—Ba—W_c | 0 |
O3iv—Ti_m1(1)—Nb_m1(1) | 0 | Ohx—Ba—Nb_m1(1) | 148.8 (4) |
Oh—Ti_m1(1)—Ohiv | 180.0 (5) | Ohx—Ba—Nb_m1(1)xviii | 29.1 (5) |
Oh—Ti_m1(1)—Ba | 44.1 (4) | Ohx—Ba—Ti_m2 | 84.6 (5) |
Oh—Ti_m1(1)—Baxii | 135.9 (4) | Ohx—Ba—Mg_m2 | 84.6 (5) |
Oh—Ti_m1(1)—Nb_m1(1) | 0 | Baxvi—Ba—Baxiii | 112.0 (2) |
Ohiv—Ti_m1(1)—Ba | 135.9 (4) | Baxvi—Ba—W2 | 32.7 (3) |
Ohiv—Ti_m1(1)—Baxii | 44.1 (4) | Baxvi—Ba—W2xvii | 32.7 (3) |
Ohiv—Ti_m1(1)—Nb_m1(1) | 0 | Baxvi—Ba—W_c | 0 |
Ba—Ti_m1(1)—Baxii | 180.0 (5) | Baxvi—Ba—Nb_m1(1) | 109.53 (10) |
Ba—Ti_m1(1)—Nb_m1(1) | 0 | Baxvi—Ba—Nb_m1(1)xviii | 109.53 (10) |
Baxii—Ti_m1(1)—Nb_m1(1) | 0 | Baxvi—Ba—Ti_m2 | 112.0 (3) |
Na_aiv—Ti_m1(2)—Na_axiv | 175.3 (5) | Baxvi—Ba—Mg_m2 | 112.0 (3) |
Na_aiv—Ti_m1(2)—Fe_m2 | 92.3 (3) | Baxiii—Ba—W2 | 108.4 (3) |
Na_aiv—Ti_m1(2)—O1 | 56.2 (5) | Baxiii—Ba—W2xvii | 108.4 (3) |
Na_aiv—Ti_m1(2)—O1xiii | 128.2 (6) | Baxiii—Ba—W_c | 0 |
Na_aiv—Ti_m1(2)—O6iv | 44.0 (7) | Baxiii—Ba—Nb_m1(1) | 102.11 (12) |
Na_aiv—Ti_m1(2)—O6xiv | 131.8 (7) | Baxiii—Ba—Nb_m1(1)xviii | 102.11 (12) |
Na_aiv—Ti_m1(2)—Oh | 120.7 (9) | Baxiii—Ba—Ti_m2 | 0.0 (5) |
Na_aiv—Ti_m1(2)—Ohxiii | 59.6 (9) | Baxiii—Ba—Mg_m2 | 0.0 (5) |
Na_aiv—Ti_m1(2)—Ba | 112.6 (5) | W2—Ba—W2xvii | 65.3 (5) |
Na_aiv—Ti_m1(2)—Baxiii | 71.3 (5) | W2—Ba—W_c | 0 |
Na_aiv—Ti_m1(2)—Ti_m2 | 92.3 (3) | W2—Ba—Nb_m1(1) | 79.2 (3) |
Na_aiv—Ti_m1(2)—Mg_m2 | 92.3 (3) | W2—Ba—Nb_m1(1)xviii | 138.7 (3) |
Na_axiv—Ti_m1(2)—Fe_m2 | 92.3 (3) | W2—Ba—Ti_m2 | 108.4 (3) |
Na_axiv—Ti_m1(2)—O1 | 128.2 (6) | W2—Ba—Mg_m2 | 108.4 (3) |
Na_axiv—Ti_m1(2)—O1xiii | 56.2 (5) | W2xvii—Ba—W_c | 0 |
Na_axiv—Ti_m1(2)—O6iv | 131.8 (7) | W2xvii—Ba—Nb_m1(1) | 138.7 (3) |
Na_axiv—Ti_m1(2)—O6xiv | 44.0 (7) | W2xvii—Ba—Nb_m1(1)xviii | 79.2 (3) |
Na_axiv—Ti_m1(2)—Oh | 59.6 (9) | W2xvii—Ba—Ti_m2 | 108.4 (3) |
Na_axiv—Ti_m1(2)—Ohxiii | 120.7 (9) | W2xvii—Ba—Mg_m2 | 108.4 (3) |
Na_axiv—Ti_m1(2)—Ba | 71.3 (5) | W_c—Ba—Nb_m1(1) | 0 |
Na_axiv—Ti_m1(2)—Baxiii | 112.6 (5) | W_c—Ba—Nb_m1(1)xviii | 0 |
Na_axiv—Ti_m1(2)—Ti_m2 | 92.3 (3) | W_c—Ba—Ti_m2 | 0 |
Na_axiv—Ti_m1(2)—Mg_m2 | 92.3 (3) | W_c—Ba—Mg_m2 | 0 |
Fe_m2—Ti_m1(2)—O1 | 41.0 (3) | Nb_m1(1)—Ba—Nb_m1(1)xviii | 121.0 (2) |
Fe_m2—Ti_m1(2)—O1xiii | 41.0 (3) | Nb_m1(1)—Ba—Ti_m2 | 102.11 (10) |
Fe_m2—Ti_m1(2)—O6iv | 130.2 (4) | Nb_m1(1)—Ba—Mg_m2 | 102.11 (10) |
Fe_m2—Ti_m1(2)—O6xiv | 130.2 (4) | Nb_m1(1)xviii—Ba—Ti_m2 | 102.11 (10) |
Fe_m2—Ti_m1(2)—Oh | 86.5 (3) | Nb_m1(1)xviii—Ba—Mg_m2 | 102.11 (10) |
Fe_m2—Ti_m1(2)—Ohxiii | 86.5 (3) | Ti_m2—Ba—Mg_m2 | 0.0 (5) |
Fe_m2—Ti_m1(2)—Ba | 36.79 (13) | Na_a—W1—Na_ai | 71.7 (17) |
Fe_m2—Ti_m1(2)—Baxiii | 36.79 (13) | Na_a—W1—K_bii | 130.1 (8) |
Fe_m2—Ti_m1(2)—Ti_m2 | 0.0 (5) | Na_a—W1—K_biii | 126.0 (8) |
Fe_m2—Ti_m1(2)—Mg_m2 | 0.0 (5) | Na_ai—W1—K_bii | 126.0 (8) |
O1—Ti_m1(2)—O1xiii | 82.0 (5) | Na_ai—W1—K_biii | 130.1 (8) |
O1—Ti_m1(2)—O6iv | 89.2 (5) | K_bii—W1—K_biii | 81.1 (8) |
O1—Ti_m1(2)—O6xiv | 171.1 (5) | Na_av—W2—Na_axiv | 75.2 (16) |
O1—Ti_m1(2)—Oh | 90.2 (8) | Na_av—W2—Ba | 114.0 (6) |
O1—Ti_m1(2)—Ohxiii | 84.5 (8) | Na_av—W2—Baxvi | 116.6 (6) |
O1—Ti_m1(2)—Ba | 57.5 (5) | Na_axiv—W2—Ba | 116.6 (6) |
O1—Ti_m1(2)—Baxiii | 47.8 (7) | Na_axiv—W2—Baxvi | 114.0 (6) |
O1—Ti_m1(2)—Ti_m2 | 41.0 (3) | Ba—W2—Baxvi | 114.7 (6) |
O1—Ti_m1(2)—Mg_m2 | 41.0 (3) | Fe_m2—W_c—Ba | 0 |
O1xiii—Ti_m1(2)—O6iv | 171.1 (5) | Fe_m2—W_c—Ti_m2 | 0.0 (5) |
O1xiii—Ti_m1(2)—O6xiv | 89.2 (5) | Fe_m2—W_c—Mg_m2 | 0.0 (5) |
O1xiii—Ti_m1(2)—Oh | 84.5 (8) | Ba—W_c—Ti_m2 | 0 |
O1xiii—Ti_m1(2)—Ohxiii | 90.2 (8) | Ba—W_c—Mg_m2 | 0 |
O1xiii—Ti_m1(2)—Ba | 47.8 (7) | Ti_m2—W_c—Mg_m2 | 0.0 (5) |
O1xiii—Ti_m1(2)—Baxiii | 57.5 (5) | Na_axi—Nb_m1(1)—Na_av | 180.0 (5) |
O1xiii—Ti_m1(2)—Ti_m2 | 41.0 (3) | Na_axi—Nb_m1(1)—Ti_m1(1) | 0 |
O1xiii—Ti_m1(2)—Mg_m2 | 41.0 (3) | Na_axi—Nb_m1(1)—O2 | 37.1 (8) |
O6iv—Ti_m1(2)—O6xiv | 99.7 (6) | Na_axi—Nb_m1(1)—O2iv | 142.9 (8) |
O6iv—Ti_m1(2)—Oh | 96.7 (11) | Na_axi—Nb_m1(1)—O3 | 99.1 (5) |
O6iv—Ti_m1(2)—Ohxiii | 87.8 (10) | Na_axi—Nb_m1(1)—O3iv | 80.9 (5) |
O6iv—Ti_m1(2)—Ba | 127.3 (9) | Na_axi—Nb_m1(1)—Oh | 125.5 (8) |
O6iv—Ti_m1(2)—Baxiii | 115.3 (6) | Na_axi—Nb_m1(1)—Ohiv | 54.5 (8) |
O6iv—Ti_m1(2)—Ti_m2 | 130.2 (4) | Na_axi—Nb_m1(1)—Ba | 115.5 (4) |
O6iv—Ti_m1(2)—Mg_m2 | 130.2 (4) | Na_axi—Nb_m1(1)—Baxii | 64.5 (4) |
O6xiv—Ti_m1(2)—Oh | 87.8 (10) | Na_av—Nb_m1(1)—Ti_m1(1) | 0 |
O6xiv—Ti_m1(2)—Ohxiii | 96.7 (11) | Na_av—Nb_m1(1)—O2 | 142.9 (8) |
O6xiv—Ti_m1(2)—Ba | 115.3 (6) | Na_av—Nb_m1(1)—O2iv | 37.1 (8) |
O6xiv—Ti_m1(2)—Baxiii | 127.3 (9) | Na_av—Nb_m1(1)—O3 | 80.9 (5) |
O6xiv—Ti_m1(2)—Ti_m2 | 130.2 (4) | Na_av—Nb_m1(1)—O3iv | 99.1 (5) |
O6xiv—Ti_m1(2)—Mg_m2 | 130.2 (4) | Na_av—Nb_m1(1)—Oh | 54.5 (8) |
Oh—Ti_m1(2)—Ohxiii | 173.0 (5) | Na_av—Nb_m1(1)—Ohiv | 125.5 (8) |
Oh—Ti_m1(2)—Ba | 49.9 (3) | Na_av—Nb_m1(1)—Ba | 64.5 (4) |
Oh—Ti_m1(2)—Baxiii | 123.1 (3) | Na_av—Nb_m1(1)—Baxii | 115.5 (4) |
Oh—Ti_m1(2)—Ti_m2 | 86.5 (3) | Ti_m1(1)—Nb_m1(1)—O2 | 0 |
Oh—Ti_m1(2)—Mg_m2 | 86.5 (3) | Ti_m1(1)—Nb_m1(1)—O2iv | 0 |
Ohxiii—Ti_m1(2)—Ba | 123.1 (3) | Ti_m1(1)—Nb_m1(1)—O3 | 0 |
Ohxiii—Ti_m1(2)—Baxiii | 49.9 (3) | Ti_m1(1)—Nb_m1(1)—O3iv | 0 |
Ohxiii—Ti_m1(2)—Ti_m2 | 86.5 (3) | Ti_m1(1)—Nb_m1(1)—Oh | 0 |
Ohxiii—Ti_m1(2)—Mg_m2 | 86.5 (3) | Ti_m1(1)—Nb_m1(1)—Ohiv | 0 |
Ba—Ti_m1(2)—Baxiii | 73.59 (19) | Ti_m1(1)—Nb_m1(1)—Ba | 0 |
Ba—Ti_m1(2)—Ti_m2 | 36.79 (13) | Ti_m1(1)—Nb_m1(1)—Baxii | 0 |
Ba—Ti_m1(2)—Mg_m2 | 36.79 (13) | O2—Nb_m1(1)—O2iv | 180.0 (5) |
Baxiii—Ti_m1(2)—Ti_m2 | 36.79 (13) | O2—Nb_m1(1)—O3 | 87.7 (6) |
Baxiii—Ti_m1(2)—Mg_m2 | 36.79 (13) | O2—Nb_m1(1)—O3iv | 92.3 (6) |
Ti_m2—Ti_m1(2)—Mg_m2 | 0.0 (5) | O2—Nb_m1(1)—Oh | 91.0 (8) |
Ti_m1(2)—Fe_m2—Ti_m1(2)xv | 180.0 (5) | O2—Nb_m1(1)—Ohiv | 89.0 (8) |
Ti_m1(2)—Fe_m2—O1 | 43.1 (3) | O2—Nb_m1(1)—Ba | 81.4 (4) |
Ti_m1(2)—Fe_m2—O1xiii | 43.1 (3) | O2—Nb_m1(1)—Baxii | 98.6 (4) |
Ti_m1(2)—Fe_m2—O1xv | 136.9 (3) | O2iv—Nb_m1(1)—O3 | 92.3 (6) |
Ti_m1(2)—Fe_m2—O1x | 136.9 (3) | O2iv—Nb_m1(1)—O3iv | 87.7 (6) |
Ti_m1(2)—Fe_m2—Ba | 90 | O2iv—Nb_m1(1)—Oh | 89.0 (8) |
Ti_m1(2)—Fe_m2—Baxiii | 90 | O2iv—Nb_m1(1)—Ohiv | 91.0 (8) |
Ti_m1(2)—Fe_m2—W_c | 90 | O2iv—Nb_m1(1)—Ba | 98.6 (4) |
Ti_m1(2)—Fe_m2—W_cxiii | 90 | O2iv—Nb_m1(1)—Baxii | 81.4 (4) |
Ti_m1(2)—Fe_m2—Ti_m2 | 0 | O3—Nb_m1(1)—O3iv | 180.0 (5) |
Ti_m1(2)—Fe_m2—Mg_m2 | 0 | O3—Nb_m1(1)—Oh | 91.8 (8) |
Ti_m1(2)xv—Fe_m2—O1 | 136.9 (3) | O3—Nb_m1(1)—Ohiv | 88.2 (8) |
Ti_m1(2)xv—Fe_m2—O1xiii | 136.9 (3) | O3—Nb_m1(1)—Ba | 48.6 (8) |
Ti_m1(2)xv—Fe_m2—O1xv | 43.1 (3) | O3—Nb_m1(1)—Baxii | 131.4 (8) |
Ti_m1(2)xv—Fe_m2—O1x | 43.1 (3) | O3iv—Nb_m1(1)—Oh | 88.2 (8) |
Ti_m1(2)xv—Fe_m2—Ba | 90 | O3iv—Nb_m1(1)—Ohiv | 91.8 (8) |
Ti_m1(2)xv—Fe_m2—Baxiii | 90 | O3iv—Nb_m1(1)—Ba | 131.4 (8) |
Ti_m1(2)xv—Fe_m2—W_c | 90 | O3iv—Nb_m1(1)—Baxii | 48.6 (8) |
Ti_m1(2)xv—Fe_m2—W_cxiii | 90 | Oh—Nb_m1(1)—Ohiv | 180.0 (5) |
Ti_m1(2)xv—Fe_m2—Ti_m2 | 0 | Oh—Nb_m1(1)—Ba | 44.1 (4) |
Ti_m1(2)xv—Fe_m2—Mg_m2 | 0 | Oh—Nb_m1(1)—Baxii | 135.9 (4) |
O1—Fe_m2—O1xiii | 86.3 (5) | Ohiv—Nb_m1(1)—Ba | 135.9 (4) |
O1—Fe_m2—O1xv | 180.0 (5) | Ohiv—Nb_m1(1)—Baxii | 44.1 (4) |
O1—Fe_m2—O1x | 93.7 (5) | Ba—Nb_m1(1)—Baxii | 180.0 (5) |
O1—Fe_m2—Ba | 96.7 (7) | Ti_m1(2)—Ti_m2—Ti_m1(2)xv | 180.0 (5) |
O1—Fe_m2—Baxiii | 83.3 (7) | Ti_m1(2)—Ti_m2—Fe_m2 | 0 |
O1—Fe_m2—W_c | 96.7 (7) | Ti_m1(2)—Ti_m2—O1 | 43.1 (3) |
O1—Fe_m2—W_cxiii | 83.3 (7) | Ti_m1(2)—Ti_m2—O1xiii | 43.1 (3) |
O1—Fe_m2—Ti_m2 | 0 | Ti_m1(2)—Ti_m2—O1xv | 136.9 (3) |
O1—Fe_m2—Mg_m2 | 0 | Ti_m1(2)—Ti_m2—O1x | 136.9 (3) |
O1xiii—Fe_m2—O1xv | 93.7 (5) | Ti_m1(2)—Ti_m2—Ba | 90 |
O1xiii—Fe_m2—O1x | 180.0 (5) | Ti_m1(2)—Ti_m2—Baxiii | 90 |
O1xiii—Fe_m2—Ba | 83.3 (7) | Ti_m1(2)—Ti_m2—W_c | 90 |
O1xiii—Fe_m2—Baxiii | 96.7 (7) | Ti_m1(2)—Ti_m2—W_cxiii | 90 |
O1xiii—Fe_m2—W_c | 83.3 (7) | Ti_m1(2)—Ti_m2—Mg_m2 | 0 |
O1xiii—Fe_m2—W_cxiii | 96.7 (7) | Ti_m1(2)xv—Ti_m2—Fe_m2 | 0 |
O1xiii—Fe_m2—Ti_m2 | 0 | Ti_m1(2)xv—Ti_m2—O1 | 136.9 (3) |
O1xiii—Fe_m2—Mg_m2 | 0 | Ti_m1(2)xv—Ti_m2—O1xiii | 136.9 (3) |
O1xv—Fe_m2—O1x | 86.3 (5) | Ti_m1(2)xv—Ti_m2—O1xv | 43.1 (3) |
O1xv—Fe_m2—Ba | 83.3 (7) | Ti_m1(2)xv—Ti_m2—O1x | 43.1 (3) |
O1xv—Fe_m2—Baxiii | 96.7 (7) | Ti_m1(2)xv—Ti_m2—Ba | 90 |
O1xv—Fe_m2—W_c | 83.3 (7) | Ti_m1(2)xv—Ti_m2—Baxiii | 90 |
O1xv—Fe_m2—W_cxiii | 96.7 (7) | Ti_m1(2)xv—Ti_m2—W_c | 90 |
O1xv—Fe_m2—Ti_m2 | 0 | Ti_m1(2)xv—Ti_m2—W_cxiii | 90 |
O1xv—Fe_m2—Mg_m2 | 0 | Ti_m1(2)xv—Ti_m2—Mg_m2 | 0 |
O1x—Fe_m2—Ba | 96.7 (7) | Fe_m2—Ti_m2—O1 | 0 |
O1x—Fe_m2—Baxiii | 83.3 (7) | Fe_m2—Ti_m2—O1xiii | 0 |
O1x—Fe_m2—W_c | 96.7 (7) | Fe_m2—Ti_m2—O1xv | 0 |
O1x—Fe_m2—W_cxiii | 83.3 (7) | Fe_m2—Ti_m2—O1x | 0 |
O1x—Fe_m2—Ti_m2 | 0 | Fe_m2—Ti_m2—Ba | 0 |
O1x—Fe_m2—Mg_m2 | 0 | Fe_m2—Ti_m2—Baxiii | 0 |
Ba—Fe_m2—Baxiii | 180.0 (5) | Fe_m2—Ti_m2—W_c | 0 |
Ba—Fe_m2—W_c | 0.0 (5) | Fe_m2—Ti_m2—W_cxiii | 0 |
Ba—Fe_m2—W_cxiii | 180.0 (5) | Fe_m2—Ti_m2—Mg_m2 | 0 |
Ba—Fe_m2—Ti_m2 | 0 | O1—Ti_m2—O1xiii | 86.3 (5) |
Ba—Fe_m2—Mg_m2 | 0 | O1—Ti_m2—O1xv | 180.0 (5) |
Baxiii—Fe_m2—W_c | 180.0 (5) | O1—Ti_m2—O1x | 93.7 (5) |
Baxiii—Fe_m2—W_cxiii | 0.0 (5) | O1—Ti_m2—Ba | 96.7 (7) |
Baxiii—Fe_m2—Ti_m2 | 0 | O1—Ti_m2—Baxiii | 83.3 (7) |
Baxiii—Fe_m2—Mg_m2 | 0 | O1—Ti_m2—W_c | 96.7 (7) |
W_c—Fe_m2—W_cxiii | 180.0 (5) | O1—Ti_m2—W_cxiii | 83.3 (7) |
W_c—Fe_m2—Ti_m2 | 0 | O1—Ti_m2—Mg_m2 | 0 |
W_c—Fe_m2—Mg_m2 | 0 | O1xiii—Ti_m2—O1xv | 93.7 (5) |
W_cxiii—Fe_m2—Ti_m2 | 0 | O1xiii—Ti_m2—O1x | 180.0 (5) |
W_cxiii—Fe_m2—Mg_m2 | 0 | O1xiii—Ti_m2—Ba | 83.3 (7) |
Ti_m2—Fe_m2—Mg_m2 | 0 | O1xiii—Ti_m2—Baxiii | 96.7 (7) |
K_b—Si1—K_biii | 81.8 (4) | O1xiii—Ti_m2—W_c | 83.3 (7) |
K_b—Si1—O3 | 48.6 (8) | O1xiii—Ti_m2—W_cxiii | 96.7 (7) |
K_b—Si1—O4 | 62.5 (7) | O1xiii—Ti_m2—Mg_m2 | 0 |
K_b—Si1—O6 | 105.7 (6) | O1xv—Ti_m2—O1x | 86.3 (5) |
K_b—Si1—O7 | 141.7 (9) | O1xv—Ti_m2—Ba | 83.3 (7) |
K_biii—Si1—O3 | 130.1 (8) | O1xv—Ti_m2—Baxiii | 96.7 (7) |
K_biii—Si1—O4 | 39.8 (15) | O1xv—Ti_m2—W_c | 83.3 (7) |
K_biii—Si1—O6 | 68.2 (10) | O1xv—Ti_m2—W_cxiii | 96.7 (7) |
K_biii—Si1—O7 | 115.4 (9) | O1xv—Ti_m2—Mg_m2 | 0 |
O3—Si1—O4 | 105.3 (12) | O1x—Ti_m2—Ba | 96.7 (7) |
O3—Si1—O6 | 114.9 (10) | O1x—Ti_m2—Baxiii | 83.3 (7) |
O3—Si1—O7 | 108.7 (14) | O1x—Ti_m2—W_c | 96.7 (7) |
O4—Si1—O6 | 107.1 (18) | O1x—Ti_m2—W_cxiii | 83.3 (7) |
O4—Si1—O7 | 107.9 (9) | O1x—Ti_m2—Mg_m2 | 0 |
O6—Si1—O7 | 112.4 (9) | Ba—Ti_m2—Baxiii | 180.0 (5) |
Na_aiv—Si2—K_b | 163.0 (6) | Ba—Ti_m2—W_c | 0.0 (5) |
Na_aiv—Si2—O1 | 63.0 (8) | Ba—Ti_m2—W_cxiii | 180.0 (5) |
Na_aiv—Si2—O2 | 96.3 (10) | Ba—Ti_m2—Mg_m2 | 0 |
Na_aiv—Si2—O5 | 152.2 (12) | Baxiii—Ti_m2—W_c | 180.0 (5) |
Na_aiv—Si2—O7xi | 50.8 (8) | Baxiii—Ti_m2—W_cxiii | 0.0 (5) |
Na_aiv—Si2—Ba | 122.5 (6) | Baxiii—Ti_m2—Mg_m2 | 0 |
K_b—Si2—O1 | 133.9 (6) | W_c—Ti_m2—W_cxiii | 180.0 (5) |
K_b—Si2—O2 | 75.2 (9) | W_c—Ti_m2—Mg_m2 | 0 |
K_b—Si2—O5 | 35.2 (12) | W_cxiii—Ti_m2—Mg_m2 | 0 |
K_b—Si2—O7xi | 118.7 (9) | Ti_m1(2)—Mg_m2—Ti_m1(2)xv | 180.0 (5) |
K_b—Si2—Ba | 73.7 (3) | Ti_m1(2)—Mg_m2—Fe_m2 | 0 |
O1—Si2—O2 | 115.3 (9) | Ti_m1(2)—Mg_m2—O1 | 43.1 (3) |
O1—Si2—O5 | 111.0 (11) | Ti_m1(2)—Mg_m2—O1xiii | 43.1 (3) |
O1—Si2—O7xi | 98.8 (12) | Ti_m1(2)—Mg_m2—O1xv | 136.9 (3) |
O1—Si2—Ba | 60.5 (6) | Ti_m1(2)—Mg_m2—O1x | 136.9 (3) |
O2—Si2—O5 | 109.9 (16) | Ti_m1(2)—Mg_m2—Ba | 90 |
O2—Si2—O7xi | 113.4 (7) | Ti_m1(2)—Mg_m2—Baxiii | 90 |
O2—Si2—Ba | 98.1 (5) | Ti_m1(2)—Mg_m2—W_c | 90 |
O5—Si2—O7xi | 107.8 (8) | Ti_m1(2)—Mg_m2—W_cxiii | 90 |
O5—Si2—Ba | 64.0 (6) | Ti_m1(2)—Mg_m2—Ti_m2 | 0 |
O7xi—Si2—Ba | 147.9 (8) | Ti_m1(2)xv—Mg_m2—Fe_m2 | 0 |
Ti_m1(2)—O1—Fe_m2 | 95.9 (5) | Ti_m1(2)xv—Mg_m2—O1 | 136.9 (3) |
Ti_m1(2)—O1—Si2 | 118.9 (10) | Ti_m1(2)xv—Mg_m2—O1xiii | 136.9 (3) |
Ti_m1(2)—O1—Baxiii | 99.2 (9) | Ti_m1(2)xv—Mg_m2—O1xv | 43.1 (3) |
Ti_m1(2)—O1—Ti_m2 | 95.9 (5) | Ti_m1(2)xv—Mg_m2—O1x | 43.1 (3) |
Ti_m1(2)—O1—Mg_m2 | 95.9 (5) | Ti_m1(2)xv—Mg_m2—Ba | 90 |
Fe_m2—O1—Si2 | 124.0 (11) | Ti_m1(2)xv—Mg_m2—Baxiii | 90 |
Fe_m2—O1—Baxiii | 52.4 (5) | Ti_m1(2)xv—Mg_m2—W_c | 90 |
Fe_m2—O1—Ti_m2 | 0.0 (5) | Ti_m1(2)xv—Mg_m2—W_cxiii | 90 |
Fe_m2—O1—Mg_m2 | 0.0 (5) | Ti_m1(2)xv—Mg_m2—Ti_m2 | 0 |
Si2—O1—Baxiii | 141.2 (6) | Fe_m2—Mg_m2—O1 | 0 |
Si2—O1—Ti_m2 | 124.0 (11) | Fe_m2—Mg_m2—O1xiii | 0 |
Si2—O1—Mg_m2 | 124.0 (11) | Fe_m2—Mg_m2—O1xv | 0 |
Baxiii—O1—Ti_m2 | 52.4 (5) | Fe_m2—Mg_m2—O1x | 0 |
Baxiii—O1—Mg_m2 | 52.4 (5) | Fe_m2—Mg_m2—Ba | 0 |
Ti_m2—O1—Mg_m2 | 0.0 (5) | Fe_m2—Mg_m2—Baxiii | 0 |
Na_axi—O2—Ti_m1(1) | 110.7 (13) | Fe_m2—Mg_m2—W_c | 0 |
Na_axi—O2—Si2 | 120.2 (9) | Fe_m2—Mg_m2—W_cxiii | 0 |
Na_axi—O2—Nb_m1(1) | 110.7 (13) | Fe_m2—Mg_m2—Ti_m2 | 0 |
Ti_m1(1)—O2—Si2 | 127.8 (7) | O1—Mg_m2—O1xiii | 86.3 (5) |
Ti_m1(1)—O2—Nb_m1(1) | 0.0 (5) | O1—Mg_m2—O1xv | 180.0 (5) |
Si2—O2—Nb_m1(1) | 127.8 (7) | O1—Mg_m2—O1x | 93.7 (5) |
K_b—O3—Ti_m1(1) | 124.7 (5) | O1—Mg_m2—Ba | 96.7 (7) |
K_b—O3—Si1 | 105.7 (13) | O1—Mg_m2—Baxiii | 83.3 (7) |
K_b—O3—Ba | 101.2 (6) | O1—Mg_m2—W_c | 96.7 (7) |
K_b—O3—Nb_m1(1) | 124.7 (5) | O1—Mg_m2—W_cxiii | 83.3 (7) |
Ti_m1(1)—O3—Si1 | 114.7 (7) | O1—Mg_m2—Ti_m2 | 0 |
Ti_m1(1)—O3—Ba | 100.3 (11) | O1xiii—Mg_m2—O1xv | 93.7 (5) |
Ti_m1(1)—O3—Nb_m1(1) | 0.0 (5) | O1xiii—Mg_m2—O1x | 180.0 (5) |
Si1—O3—Ba | 108.0 (7) | O1xiii—Mg_m2—Ba | 83.3 (7) |
Si1—O3—Nb_m1(1) | 114.7 (7) | O1xiii—Mg_m2—Baxiii | 96.7 (7) |
Ba—O3—Nb_m1(1) | 100.3 (11) | O1xiii—Mg_m2—W_c | 83.3 (7) |
K_biii—O4—Si1 | 115.4 (15) | O1xiii—Mg_m2—W_cxiii | 96.7 (7) |
K_biii—O4—Si1x | 115.4 (15) | O1xiii—Mg_m2—Ti_m2 | 0 |
Si1—O4—Si1x | 127 (3) | O1xv—Mg_m2—O1x | 86.3 (5) |
K_b—O5—Si2 | 121.5 (12) | O1xv—Mg_m2—Ba | 83.3 (7) |
K_b—O5—Si2x | 121.5 (12) | O1xv—Mg_m2—Baxiii | 96.7 (7) |
Si2—O5—Si2x | 117 (2) | O1xv—Mg_m2—W_c | 83.3 (7) |
Na_a—O6—Ti_m1(2)iv | 98.8 (10) | O1xv—Mg_m2—W_cxiii | 96.7 (7) |
Na_a—O6—Si1 | 125.9 (11) | O1xv—Mg_m2—Ti_m2 | 0 |
Ti_m1(2)iv—O6—Si1 | 130.1 (14) | O1x—Mg_m2—Ba | 96.7 (7) |
Na_av—O7—Si1 | 124.0 (8) | O1x—Mg_m2—Baxiii | 83.3 (7) |
Na_av—O7—Si2ii | 94.5 (8) | O1x—Mg_m2—W_c | 96.7 (7) |
Si1—O7—Si2ii | 127.5 (18) | O1x—Mg_m2—W_cxiii | 83.3 (7) |
Ti_m1(1)—Oh—Ti_m1(2) | 126.9 (5) | O1x—Mg_m2—Ti_m2 | 0 |
Ti_m1(1)—Oh—Ba | 106.8 (8) | Ba—Mg_m2—Baxiii | 180.0 (5) |
Ti_m1(1)—Oh—Nb_m1(1) | 0.0 (5) | Ba—Mg_m2—W_c | 0.0 (5) |
Ti_m1(2)—Oh—Ba | 98.6 (7) | Ba—Mg_m2—W_cxiii | 180.0 (5) |
Ti_m1(2)—Oh—Nb_m1(1) | 126.9 (5) | Ba—Mg_m2—Ti_m2 | 0 |
Ba—Oh—Nb_m1(1) | 106.8 (8) | Baxiii—Mg_m2—W_c | 180.0 (5) |
Na_axx—Ba—Na_axxi | 36.7 (9) | Baxiii—Mg_m2—W_cxiii | 0.0 (5) |
Na_axx—Ba—Na_av | 111.9 (4) | Baxiii—Mg_m2—Ti_m2 | 0 |
Na_axx—Ba—Na_axiv | 99.2 (5) | W_c—Mg_m2—W_cxiii | 180.0 (5) |
Na_axx—Ba—K_b | 128.8 (5) | W_c—Mg_m2—Ti_m2 | 0 |
Na_axx—Ba—Ti_m1(1) | 164.9 (3) | W_cxiii—Mg_m2—Ti_m2 | 0 |
Symmetry codes: (i) −x+1, y, −z; (ii) x, y, z−1; (iii) −x+1, y, −z+1; (iv) −x+1/2, −y+1/2, −z+1; (v) −x+1/2, −y+1/2, −z; (vi) x+1/2, y+1/2, z; (vii) −x+1/2, y+1/2, −z; (viii) −x+1, y, −z+2; (ix) −x+1, −y, −z+1; (x) x, −y, z; (xi) x, y, z+1; (xii) −x+1/2, y+1/2, −z+1; (xiii) −x, y, −z+1; (xiv) x−1/2, −y+1/2, z; (xv) −x, −y, −z+1; (xvi) −x, y, −z; (xvii) −x, −y, −z; (xviii) −x+1/2, y−1/2, −z+1; (xix) x, −y, z+1; (xx) x−1/2, y−1/2, z; (xxi) −x+1/2, y−1/2, −z. |