Four new inorganic uranyl chromates were obtained by evaporation and hydrothermal methods: [(CH3)2NH2]2[(UO2)2(CrO4)3(H2O)](H2O) (1), K(Rb0.6K0.4)[(UO2)2(CrO4)3(H2O)](H2O)3 (2) [(CH3)3CNH3]2[(UO2)2(CrO4)3H2O] (3), [(CH3)2NH2]4[(UO2)2(CrO4)3H2O]2(H2O) (4). Their structures are based on two-dimensional chiral or achiral units with the composition [(UO2)2(CrO4)3(H2O)]2- and two types of topologies (A or/and B). The structural architecture of (4) is unique amongst all known uranyl-based structures, and unusual among hybrid organic/inorganic structures in general as it contains layers of identical composition, but of different topology. The unique structural configurations and non-centrosymmetry in (1) and (4) is governed by selective formation of hydrogen bonding rather than by the formation of hydrophobic and hydrophilic zones in the organic interlayer. It is shown that chiral architectures in uranyl systems may form from achiral building units as observed in (3) and (4). This is somewhat analogous to certain organic compounds, where achiral molecules are also able to form chiral layers. Within the concept of such an interpretation the structure of (3) can then be described as a racemate consisting of two A and A' chiral layers. In a similar approach the structure of (4) can be interpreted as being formed by four chiral layers. Layer pairs AA' and BB' can then be considered as racemic pairs and the whole structure is a co-racemate built by a combination of two racemates. Two-stage formation can be suggested for (4).
Supporting information
CCDC references: 1520397; 1520398; 1520399; 1520400
Data collection: APEX2 (Bruker, 20012) for compound_1, compound_3, compound_4; APEX2 (Bruker, 2012) for compound_2. Cell refinement: APEX2 (Bruker, 20012) for compound_1, compound_3, compound_4; APEX2 (Bruker, 2012) for compound_2. For all compounds, data reduction: SAINT (Bruker, 2012); program(s) used to solve structure: WinGX, version 2014.1; program(s) used to refine structure: SHELXL2014/7 (Sheldrick, 2014); molecular graphics: DIAMOND, Version 4.2.2. Software used to prepare material for publication: SHELXL2014/7 (Sheldrick, 2014) for compound_1, compound_3, compound_4.
Crystal data top
C4H20Cr3N2O18U2 | F(000) = 916 |
Mr = 1016.25 | Dx = 3.120 Mg m−3 |
Monoclinic, P21 | Mo Kα radiation, λ = 0.71073 Å |
a = 8.8638 (10) Å | Cell parameters from 1255 reflections |
b = 11.1097 (13) Å | θ = 1.9–27.5° |
c = 11.5441 (13) Å | µ = 16.46 mm−1 |
β = 107.878 (2)° | T = 150 K |
V = 1081.9 (2) Å3 | Plate, red |
Z = 2 | 0.28 × 0.25 × 0.20 mm |
Data collection top
Bruker Kappa APEXII DUO diffractometer | 5129 reflections with I > 2σ(I) |
Radiation source: fine-focus sealed tube | Rint = 0.045 |
π and ω scans | θmax = 28.0°, θmin = 1.9° |
Absorption correction: multi-scane (SADABS; Bruker, 2012) | h = −11→11 |
Tmin = 0.622, Tmax = 0.784 | k = −14→14 |
51165 measured reflections | l = −12→15 |
5160 independent reflections | |
Refinement top
Refinement on F2 | H-atom parameters not refined |
Least-squares matrix: full | w = 1/[σ2(Fo2) + (0.0471P)2 + 3.120P] where P = (Fo2 + 2Fc2)/3 |
R[F2 > 2σ(F2)] = 0.026 | (Δ/σ)max = 0.002 |
wR(F2) = 0.070 | Δρmax = 4.21 e Å−3 |
S = 1.11 | Δρmin = −1.81 e Å−3 |
5160 reflections | Extinction correction: SHELXL-2014/7 (Sheldrick 2014, Fc*=kFc[1+0.001xFc2λ3/sin(2θ)]-1/4 |
264 parameters | Extinction coefficient: 0.0015 (2) |
1 restraint | Absolute structure: Refined as an inversion twin. |
Hydrogen site location: inferred from neighbouring sites | Absolute structure parameter: 0.093 (9) |
Special details top
Geometry. All esds (except the esd in the dihedral angle between two l.s. planes)
are estimated using the full covariance matrix. The cell esds are taken
into account individually in the estimation of esds in distances, angles
and torsion angles; correlations between esds in cell parameters are only
used when they are defined by crystal symmetry. An approximate (isotropic)
treatment of cell esds is used for estimating esds involving l.s. planes. |
Refinement. Refined as a 2-component inversion twin. |
Fractional atomic coordinates and isotropic or equivalent isotropic displacement parameters (Å2) top | x | y | z | Uiso*/Ueq | |
U1 | −0.43346 (4) | 0.50552 (3) | −0.08458 (3) | 0.00721 (10) | |
U2 | −0.51200 (4) | 0.91799 (2) | −0.39075 (3) | 0.00815 (10) | |
Cr1 | −0.27869 (17) | 0.83547 (14) | −0.06668 (13) | 0.0077 (3) | |
Cr2 | −0.29185 (17) | 0.61107 (13) | −0.34566 (14) | 0.0083 (3) | |
Cr3 | −0.58136 (17) | 0.18397 (13) | −0.22129 (14) | 0.0078 (3) | |
O1 | −0.7135 (9) | 1.0366 (6) | −0.5270 (6) | 0.0115 (13) | |
O2 | −0.3095 (9) | 0.8923 (6) | −0.2071 (6) | 0.0136 (14) | |
O3 | −0.6639 (9) | 0.8783 (7) | −0.3240 (7) | 0.0150 (14) | |
O4 | −0.3652 (9) | 0.9569 (7) | −0.4604 (7) | 0.0138 (14) | |
O5 | −0.6088 (8) | 0.5776 (7) | −0.1758 (7) | 0.0145 (14) | |
O6 | −0.2813 (8) | 0.6826 (6) | −0.0706 (6) | 0.0108 (13) | |
O7 | −0.5827 (11) | 0.3862 (7) | 0.0097 (8) | 0.0237 (18) | |
O8 | −0.4869 (8) | 1.1117 (6) | −0.3109 (6) | 0.0120 (13) | |
O9 | −0.3214 (8) | 0.5064 (7) | −0.2495 (6) | 0.0130 (12) | |
O10 | −0.4390 (9) | 0.7105 (6) | −0.3811 (7) | 0.0145 (14) | |
O11 | −0.2544 (9) | 0.4357 (7) | 0.0102 (7) | 0.0176 (15) | |
O12 | −0.1224 (9) | 0.6780 (7) | −0.2886 (7) | 0.0168 (14) | |
O13 | −0.5117 (10) | 0.3241 (7) | −0.2009 (7) | 0.0164 (14) | |
O14 | −0.1039 (10) | 0.8755 (7) | 0.0177 (8) | 0.0242 (19) | |
O15 | −0.4569 (10) | 0.6134 (7) | 0.0882 (7) | 0.0173 (15) | |
O16 | −0.7709 (9) | 0.1838 (7) | −0.2924 (8) | 0.0200 (16) | |
OW17 | −0.6428 (9) | 0.8090 (6) | −0.5892 (6) | 0.0128 (13) | |
HW1A | −0.6632 | 0.7233 | −0.5723 | 0.015* | |
HW1B | −0.5707 | 0.8097 | −0.6410 | 0.015* | |
OW18 | −0.0099 (10) | 0.4226 (9) | 0.2836 (9) | 0.0303 (19) | |
HW1C | −0.0277 | 0.3341 | 0.2885 | 0.036* | |
HW1D | 0.0868 | 0.4346 | 0.2577 | 0.036* | |
C1 | −0.0914 (15) | 0.1732 (13) | −0.1881 (11) | 0.027 (3) | |
H1A | −0.1570 | 0.1148 | −0.2488 | 0.032* | |
H1B | 0.0023 | 0.1984 | −0.2133 | 0.032* | |
H1C | −0.1568 | 0.2455 | −0.1841 | 0.032* | |
N1 | −0.0356 (10) | 0.1147 (8) | −0.0655 (10) | 0.0190 (19) | |
H1D | 0.0502 | 0.0555 | −0.0633 | 0.023* | |
H1E | −0.1253 | 0.0703 | −0.0496 | 0.023* | |
C2 | −0.1380 (14) | 0.1477 (10) | 0.0123 (12) | 0.021 (2) | |
H2A | −0.1177 | 0.2334 | 0.0392 | 0.025* | |
H2B | −0.1122 | 0.0940 | 0.0853 | 0.025* | |
H2C | −0.2522 | 0.1377 | −0.0360 | 0.025* | |
C3 | 0.1321 (13) | 0.6417 (10) | −0.4579 (11) | 0.020 (2) | |
H3A | 0.1196 | 0.6812 | −0.3835 | 0.024* | |
H3B | 0.0953 | 0.6979 | −0.5287 | 0.024* | |
H3C | 0.2463 | 0.6214 | −0.4438 | 0.024* | |
N2 | 0.0360 (10) | 0.5300 (8) | −0.4840 (9) | 0.0167 (17) | |
H2D | 0.0792 | 0.4560 | −0.5118 | 0.020* | |
H2E | −0.0720 | 0.5286 | −0.4738 | 0.020* | |
C4 | 0.0863 (15) | 0.4395 (10) | −0.3833 (12) | 0.027 (3) | |
H4A | 0.1791 | 0.3929 | −0.3912 | 0.032* | |
H4B | −0.0035 | 0.3831 | −0.3883 | 0.032* | |
H4C | 0.1167 | 0.4820 | −0.3030 | 0.032* | |
Atomic displacement parameters (Å2) top | U11 | U22 | U33 | U12 | U13 | U23 |
U1 | 0.00714 (16) | 0.00610 (15) | 0.00807 (16) | −0.00072 (11) | 0.00188 (12) | −0.00048 (11) |
U2 | 0.01005 (17) | 0.00627 (15) | 0.00838 (16) | 0.00012 (12) | 0.00318 (12) | 0.00008 (12) |
Cr1 | 0.0073 (6) | 0.0058 (6) | 0.0087 (7) | 0.0001 (5) | 0.0003 (5) | −0.0002 (5) |
Cr2 | 0.0083 (6) | 0.0066 (6) | 0.0101 (7) | −0.0011 (5) | 0.0028 (5) | −0.0006 (5) |
Cr3 | 0.0076 (6) | 0.0054 (6) | 0.0103 (7) | 0.0000 (5) | 0.0028 (5) | 0.0007 (5) |
O1 | 0.018 (3) | 0.009 (3) | 0.009 (3) | −0.001 (2) | 0.005 (3) | 0.000 (2) |
O2 | 0.018 (3) | 0.012 (3) | 0.009 (3) | 0.004 (3) | 0.002 (3) | 0.004 (2) |
O3 | 0.019 (3) | 0.013 (3) | 0.015 (4) | −0.002 (3) | 0.008 (3) | 0.002 (3) |
O4 | 0.013 (3) | 0.013 (3) | 0.014 (3) | −0.001 (3) | 0.002 (3) | 0.000 (3) |
O5 | 0.009 (3) | 0.014 (3) | 0.018 (4) | −0.001 (3) | 0.001 (3) | −0.003 (3) |
O6 | 0.010 (3) | 0.006 (3) | 0.015 (3) | 0.000 (2) | 0.002 (3) | 0.002 (3) |
O7 | 0.032 (4) | 0.015 (4) | 0.032 (5) | −0.011 (3) | 0.023 (4) | −0.006 (3) |
O8 | 0.013 (3) | 0.012 (3) | 0.012 (3) | −0.003 (3) | 0.004 (3) | −0.003 (3) |
O9 | 0.019 (3) | 0.009 (3) | 0.014 (3) | 0.004 (3) | 0.009 (3) | 0.002 (3) |
O10 | 0.019 (4) | 0.009 (3) | 0.016 (3) | 0.002 (3) | 0.006 (3) | 0.001 (3) |
O11 | 0.023 (4) | 0.014 (4) | 0.013 (3) | 0.002 (3) | 0.001 (3) | 0.006 (3) |
O12 | 0.013 (3) | 0.016 (3) | 0.019 (4) | −0.006 (3) | 0.002 (3) | −0.004 (3) |
O13 | 0.031 (4) | 0.007 (3) | 0.016 (3) | −0.002 (3) | 0.015 (3) | −0.002 (3) |
O14 | 0.025 (4) | 0.012 (3) | 0.024 (4) | −0.007 (3) | −0.009 (3) | 0.001 (3) |
O15 | 0.027 (4) | 0.014 (3) | 0.014 (4) | −0.001 (3) | 0.012 (3) | −0.003 (3) |
O16 | 0.008 (3) | 0.017 (3) | 0.032 (4) | 0.001 (3) | 0.002 (3) | 0.002 (3) |
OW17 | 0.019 (3) | 0.009 (3) | 0.012 (3) | 0.001 (3) | 0.006 (3) | 0.000 (2) |
OW18 | 0.020 (4) | 0.026 (4) | 0.039 (5) | 0.005 (4) | 0.000 (3) | −0.011 (4) |
C1 | 0.022 (5) | 0.037 (6) | 0.023 (6) | −0.010 (5) | 0.008 (5) | −0.003 (5) |
N1 | 0.008 (4) | 0.013 (4) | 0.032 (5) | −0.002 (3) | 0.000 (4) | −0.003 (4) |
C2 | 0.021 (5) | 0.015 (5) | 0.027 (6) | −0.001 (4) | 0.008 (5) | −0.002 (4) |
C3 | 0.019 (5) | 0.016 (5) | 0.026 (6) | −0.002 (4) | 0.007 (5) | 0.000 (4) |
N2 | 0.010 (4) | 0.017 (4) | 0.023 (4) | 0.004 (3) | 0.006 (3) | 0.000 (3) |
C4 | 0.028 (6) | 0.014 (5) | 0.035 (6) | −0.005 (4) | 0.004 (5) | 0.006 (5) |
Geometric parameters (Å, º) top
U1—O5 | 1.778 (7) | O8—O15iii | 2.765 (10) |
U1—O11 | 1.804 (7) | O8—OW17i | 2.875 (10) |
U1—O7 | 2.361 (8) | O8—O10i | 3.584 (10) |
U1—O6 | 2.362 (7) | O8—O7iii | 4.175 (11) |
U1—O15 | 2.390 (7) | O9—O1iv | 2.713 (9) |
U1—O9 | 2.403 (6) | O9—O12 | 2.727 (10) |
U1—O13 | 2.403 (7) | O9—O10 | 2.750 (10) |
U1—O10 | 4.099 (7) | O9—O13 | 2.801 (10) |
U2—O4 | 1.781 (7) | O9—OW17iv | 2.831 (10) |
U2—O3 | 1.799 (7) | O9—O11 | 2.977 (10) |
U2—O8 | 2.325 (7) | O9—O4iv | 3.677 (10) |
U2—O2 | 2.337 (7) | O9—U2iv | 4.078 (7) |
U2—O1 | 2.383 (7) | O10—O12 | 2.703 (11) |
U2—O10 | 2.388 (7) | O10—O1iv | 2.751 (10) |
U2—OW17 | 2.536 (7) | O10—OW17 | 2.751 (10) |
U2—O9i | 4.078 (7) | O10—O4iv | 3.514 (10) |
U2—O16ii | 4.108 (8) | O11—O15 | 2.987 (11) |
U2—O10i | 4.121 (7) | O11—O13 | 3.044 (11) |
U2—O15iii | 4.193 (8) | O11—N1vii | 3.156 (12) |
U2—O7iii | 4.233 (9) | O11—OW18 | 3.237 (12) |
Cr1—O14 | 1.619 (8) | O11—O14ix | 3.356 (12) |
Cr1—O7iii | 1.661 (8) | O11—O3v | 3.958 (10) |
Cr1—O2 | 1.682 (7) | O11—O16iii | 4.220 (11) |
Cr1—O6 | 1.699 (7) | O12—O1iv | 2.686 (10) |
Cr1—O15 | 3.676 (8) | O12—OW18vii | 2.954 (12) |
Cr1—O12 | 3.704 (8) | O12—O14 | 4.121 (12) |
Cr1—O10 | 3.736 (8) | O12—O5x | 4.475 (10) |
Cr2—O12 | 1.623 (7) | O13—O16 | 2.709 (11) |
Cr2—O10 | 1.662 (7) | O13—O8vi | 2.720 (10) |
Cr2—O9 | 1.682 (7) | O13—O15v | 2.734 (11) |
Cr2—O1iv | 1.700 (7) | O13—OW17iv | 3.132 (10) |
Cr2—O6 | 3.247 (7) | O13—O4iv | 4.004 (10) |
Cr2—OW17iv | 3.449 (7) | O13—O6v | 4.381 (10) |
Cr2—O2 | 3.536 (7) | O14—O7iii | 2.701 (13) |
Cr2—O4iv | 3.607 (7) | O14—N1ii | 2.951 (12) |
Cr3—O16 | 1.628 (7) | O14—C2ii | 3.039 (13) |
Cr3—O15v | 1.665 (8) | O14—N1vii | 3.131 (12) |
Cr3—O13 | 1.665 (8) | O14—C1vii | 3.134 (15) |
Cr3—O8vi | 1.717 (7) | O14—O11vii | 3.356 (12) |
Cr3—O7 | 3.490 (8) | O14—OW18vii | 3.943 (13) |
Cr3—O3vi | 3.597 (8) | O14—O9vii | 4.158 (11) |
Cr3—OW17iv | 3.651 (7) | O15—Cr3iii | 1.665 (8) |
Cr3—O1vi | 3.737 (7) | O15—O16iii | 2.706 (11) |
O1—Cr2i | 1.700 (7) | O15—O13iii | 2.734 (11) |
O1—O12i | 2.686 (10) | O15—O8v | 2.765 (10) |
O1—O9i | 2.713 (9) | O15—O7iii | 3.291 (11) |
O1—O10i | 2.751 (10) | O15—O3v | 3.687 (11) |
O1—OW17 | 2.754 (10) | O16—O15v | 2.706 (11) |
O1—O8 | 2.807 (10) | O16—O8vi | 2.712 (10) |
O1—O3 | 2.854 (10) | O16—C4xi | 3.156 (14) |
O1—N2i | 2.900 (11) | O16—O1vi | 3.333 (11) |
O1—O4 | 3.075 (10) | O16—OW18v | 3.511 (12) |
O1—O16ii | 3.333 (11) | O16—O3vi | 3.573 (11) |
O1—Cr3ii | 3.737 (7) | O16—O6v | 4.072 (11) |
O2—O14 | 2.680 (11) | O16—U2vi | 4.108 (8) |
O2—O7iii | 2.729 (11) | O16—O11v | 4.220 (11) |
O2—O6 | 2.781 (10) | OW17—O9i | 2.831 (10) |
O2—O10 | 2.832 (10) | OW17—O8iv | 2.875 (10) |
O2—O4 | 2.903 (10) | OW17—O13i | 3.132 (10) |
O2—O8 | 2.948 (10) | OW17—Cr2i | 3.449 (7) |
O2—O3 | 3.019 (10) | OW17—Cr3i | 3.651 (7) |
O2—O12 | 3.204 (10) | OW17—O4iv | 3.951 (10) |
O2—OW18vii | 3.232 (11) | OW17—O1iv | 4.281 (10) |
O3—O10 | 2.948 (11) | OW17—HW1A | 1.0014 |
O3—O8 | 3.011 (10) | OW17—HW1B | 1.0009 |
O3—OW18iii | 3.106 (12) | OW18—N2xii | 2.849 (13) |
O3—OW17 | 3.217 (10) | OW18—O12ix | 2.954 (12) |
O3—O16ii | 3.573 (11) | OW18—O3v | 3.106 (12) |
O3—O4 | 3.579 (10) | OW18—C1vii | 3.223 (18) |
O3—Cr3ii | 3.597 (8) | OW18—O2ix | 3.232 (11) |
O3—O7iii | 3.617 (13) | OW18—O4ix | 3.346 (11) |
O3—O15iii | 3.687 (11) | OW18—O16iii | 3.511 (12) |
O4—O8 | 2.872 (10) | OW18—O14ix | 3.943 (13) |
O4—OW17 | 2.953 (10) | OW18—O1v | 4.442 (11) |
O4—O10 | 3.022 (10) | OW18—O10ix | 4.462 (11) |
O4—C3viii | 3.251 (13) | OW18—HW1C | 1.0005 |
O4—OW18vii | 3.346 (11) | OW18—HW1D | 1.0024 |
O4—O10i | 3.514 (10) | C1—N1 | 1.497 (16) |
O4—Cr2i | 3.607 (7) | C1—O14ix | 3.135 (15) |
O4—O9i | 3.677 (10) | C1—OW18ix | 3.222 (18) |
O5—O15 | 2.956 (11) | C1—H1A | 0.9998 |
O5—O7 | 2.975 (11) | C1—H1B | 0.9981 |
O5—O13 | 2.984 (10) | C1—H1C | 1.0027 |
O5—O6 | 3.016 (10) | N1—C2 | 1.506 (15) |
O5—O9 | 3.028 (10) | N1—O6ix | 2.867 (11) |
O5—O10 | 3.501 (11) | N1—O14vi | 2.951 (12) |
O5—O11 | 3.581 (10) | N1—O14ix | 3.131 (12) |
O5—O7iii | 4.040 (11) | N1—O11ix | 3.156 (12) |
O5—O14v | 4.209 (12) | N1—H1D | 1.0001 |
O5—O4iv | 4.346 (11) | N1—H1E | 1.0025 |
O6—O14 | 2.668 (10) | C2—O14vi | 3.039 (13) |
O6—O7iii | 2.754 (10) | C2—H2A | 1.0002 |
O6—O9 | 2.788 (10) | C2—H2B | 1.0042 |
O6—O15 | 2.850 (10) | C2—H2C | 0.9989 |
O6—N1vii | 2.867 (11) | C3—N2 | 1.483 (14) |
O6—O11 | 2.884 (10) | C3—O4xiii | 3.251 (13) |
O6—O12 | 3.240 (11) | C3—H3A | 1.0008 |
O7—Cr1v | 1.660 (8) | C3—H3B | 1.0004 |
O7—O14v | 2.701 (13) | C3—H3C | 0.9986 |
O7—O2v | 2.729 (11) | N2—C4 | 1.498 (15) |
O7—O6v | 2.754 (10) | N2—OW18xiv | 2.849 (13) |
O7—O13 | 2.779 (10) | N2—O1iv | 2.900 (11) |
O7—O15 | 2.796 (11) | N2—H2D | 1.0016 |
O7—O11 | 2.960 (11) | N2—H2E | 0.9990 |
O7—O15v | 3.291 (11) | C4—O16x | 3.156 (14) |
O7—O3v | 3.618 (13) | C4—H4A | 1.0004 |
O8—Cr3ii | 1.717 (7) | C4—H4B | 1.0000 |
O8—O16ii | 2.712 (10) | C4—H4C | 0.9985 |
O8—O13ii | 2.720 (10) | | |
| | | |
O5—U1—O11 | 178.6 (4) | O6—O9—O4iv | 131.9 (3) |
O5—U1—O7 | 90.8 (3) | O13—O9—O4iv | 75.0 (3) |
O11—U1—O7 | 89.6 (3) | OW17iv—O9—O4iv | 52.0 (2) |
O5—U1—O6 | 92.4 (3) | O11—O9—O4iv | 137.6 (3) |
O11—U1—O6 | 86.5 (3) | O5—O9—O4iv | 80.2 (2) |
O7—U1—O6 | 145.6 (3) | Cr2—O9—U2iv | 64.9 (2) |
O5—U1—O15 | 89.1 (3) | U1—O9—U2iv | 134.2 (2) |
O11—U1—O15 | 89.7 (3) | O1iv—O9—U2iv | 34.14 (17) |
O7—U1—O15 | 72.1 (3) | O12—O9—U2iv | 92.9 (2) |
O6—U1—O15 | 73.7 (3) | O10—O9—U2iv | 71.2 (2) |
O5—U1—O9 | 91.6 (3) | O6—O9—U2iv | 148.0 (3) |
O11—U1—O9 | 88.9 (3) | O13—O9—U2iv | 88.7 (2) |
O7—U1—O9 | 142.6 (3) | OW17iv—O9—U2iv | 37.92 (17) |
O6—U1—O9 | 71.6 (3) | O11—O9—U2iv | 149.3 (3) |
O15—U1—O9 | 145.3 (3) | O5—O9—U2iv | 106.0 (2) |
O5—U1—O13 | 89.8 (3) | O4iv—O9—U2iv | 25.89 (12) |
O11—U1—O13 | 91.6 (3) | Cr2—O10—U2 | 146.5 (4) |
O7—U1—O13 | 71.4 (3) | Cr2—O10—O12 | 34.2 (2) |
O6—U1—O13 | 142.9 (2) | U2—O10—O12 | 112.4 (3) |
O15—U1—O13 | 143.4 (2) | Cr2—O10—O9 | 34.9 (2) |
O9—U1—O13 | 71.3 (2) | U2—O10—O9 | 150.8 (4) |
O5—U1—O10 | 58.1 (3) | O12—O10—O9 | 60.0 (3) |
O11—U1—O10 | 121.9 (3) | Cr2—O10—O1iv | 35.6 (2) |
O7—U1—O10 | 146.3 (3) | U2—O10—O1iv | 144.9 (4) |
O6—U1—O10 | 57.0 (2) | O12—O10—O1iv | 59.0 (3) |
O15—U1—O10 | 115.9 (2) | O9—O10—O1iv | 59.1 (2) |
O9—U1—O10 | 40.3 (2) | Cr2—O10—OW17 | 137.3 (4) |
O13—U1—O10 | 94.1 (2) | U2—O10—OW17 | 58.6 (2) |
O4—U2—O3 | 178.6 (4) | O12—O10—OW17 | 136.2 (4) |
O4—U2—O8 | 87.7 (3) | O9—O10—OW17 | 147.8 (4) |
O3—U2—O8 | 92.9 (3) | O1iv—O10—OW17 | 102.2 (3) |
O4—U2—O2 | 88.6 (3) | Cr2—O10—O2 | 100.5 (4) |
O3—U2—O2 | 92.8 (3) | U2—O10—O2 | 52.4 (2) |
O8—U2—O2 | 78.4 (2) | O12—O10—O2 | 70.7 (3) |
O4—U2—O1 | 94.1 (3) | O9—O10—O2 | 101.2 (3) |
O3—U2—O1 | 84.8 (3) | O1iv—O10—O2 | 129.4 (4) |
O8—U2—O1 | 73.2 (2) | OW17—O10—O2 | 110.5 (3) |
O2—U2—O1 | 151.4 (2) | Cr2—O10—O3 | 154.0 (4) |
O4—U2—O10 | 91.7 (3) | U2—O10—O3 | 37.59 (18) |
O3—U2—O10 | 88.3 (3) | O12—O10—O3 | 133.4 (4) |
O8—U2—O10 | 152.1 (3) | O9—O10—O3 | 124.4 (3) |
O2—U2—O10 | 73.6 (2) | O1iv—O10—O3 | 167.6 (4) |
O1—U2—O10 | 134.6 (2) | OW17—O10—O3 | 68.6 (3) |
O4—U2—OW17 | 84.4 (3) | O2—O10—O3 | 62.9 (3) |
O3—U2—OW17 | 94.3 (3) | Cr2—O10—O4 | 116.8 (4) |
O8—U2—OW17 | 139.6 (2) | U2—O10—O4 | 36.09 (17) |
O2—U2—OW17 | 140.6 (2) | O12—O10—O4 | 86.9 (3) |
O1—U2—OW17 | 68.0 (2) | O9—O10—O4 | 146.5 (4) |
O10—U2—OW17 | 67.9 (2) | O1iv—O10—O4 | 110.0 (3) |
O4—U2—O9i | 64.4 (3) | OW17—O10—O4 | 61.3 (2) |
O3—U2—O9i | 114.2 (3) | O2—O10—O4 | 59.4 (2) |
O8—U2—O9i | 98.1 (2) | O3—O10—O4 | 73.7 (3) |
O2—U2—O9i | 152.9 (2) | Cr2—O10—O6 | 69.3 (3) |
O1—U2—O9i | 39.71 (19) | U2—O10—O6 | 98.8 (3) |
O10—U2—O9i | 106.8 (2) | O12—O10—O6 | 62.3 (3) |
OW17—U2—O9i | 43.33 (19) | O9—O10—O6 | 52.1 (2) |
O4—U2—O16ii | 119.9 (3) | O1iv—O10—O6 | 104.4 (3) |
O3—U2—O16ii | 60.2 (3) | OW17—O10—O6 | 153.4 (3) |
O8—U2—O16ii | 38.6 (2) | O2—O10—O6 | 51.5 (2) |
O2—U2—O16ii | 100.1 (2) | O3—O10—O6 | 84.8 (3) |
O1—U2—O16ii | 54.2 (2) | O4—O10—O6 | 109.9 (3) |
O10—U2—O16ii | 147.9 (2) | Cr2—O10—O5 | 91.2 (3) |
OW17—U2—O16ii | 117.0 (2) | U2—O10—O5 | 105.8 (3) |
O9i—U2—O16ii | 92.86 (15) | O12—O10—O5 | 106.6 (3) |
O4—U2—O10i | 57.9 (3) | O9—O10—O5 | 56.4 (2) |
O3—U2—O10i | 121.4 (3) | O1iv—O10—O5 | 109.2 (3) |
O8—U2—O10i | 60.1 (2) | OW17—O10—O5 | 117.1 (3) |
O2—U2—O10i | 125.2 (2) | O2—O10—O5 | 89.2 (3) |
O1—U2—O10i | 39.8 (2) | O3—O10—O5 | 69.8 (2) |
O10—U2—O10i | 139.90 (11) | O4—O10—O5 | 140.0 (3) |
OW17—U2—O10i | 82.52 (19) | O6—O10—O5 | 51.5 (2) |
O9i—U2—O10i | 39.19 (15) | Cr2—O10—O4iv | 79.7 (3) |
O16ii—U2—O10i | 69.61 (16) | U2—O10—O4iv | 131.8 (3) |
O4—U2—O15iii | 119.7 (3) | O12—O10—O4iv | 112.7 (3) |
O3—U2—O15iii | 61.4 (3) | O9—O10—O4iv | 70.7 (2) |
O8—U2—O15iii | 38.1 (2) | O1iv—O10—O4iv | 57.2 (2) |
O2—U2—O15iii | 62.4 (2) | OW17—O10—O4iv | 77.1 (3) |
O1—U2—O15iii | 92.0 (2) | O2—O10—O4iv | 165.7 (3) |
O10—U2—O15iii | 123.2 (2) | O3—O10—O4iv | 111.3 (3) |
OW17—U2—O15iii | 150.6 (2) | O4—O10—O4iv | 133.4 (3) |
O9i—U2—O15iii | 128.88 (15) | O6—O10—O4iv | 116.6 (3) |
O16ii—U2—O15iii | 38.03 (16) | O5—O10—O4iv | 76.6 (2) |
O10i—U2—O15iii | 95.92 (15) | U1—O11—O6 | 54.9 (2) |
O4—U2—O7iii | 123.4 (3) | U1—O11—O7 | 52.9 (3) |
O3—U2—O7iii | 58.0 (3) | O6—O11—O7 | 101.1 (3) |
O8—U2—O7iii | 72.6 (2) | U1—O11—O9 | 53.8 (2) |
O2—U2—O7iii | 36.4 (2) | O6—O11—O9 | 56.8 (2) |
O1—U2—O7iii | 127.0 (2) | O7—O11—O9 | 98.9 (3) |
O10—U2—O7iii | 84.6 (2) | U1—O11—O15 | 53.1 (3) |
OW17—U2—O7iii | 142.1 (2) | O6—O11—O15 | 58.1 (2) |
O9i—U2—O7iii | 166.63 (15) | O7—O11—O15 | 56.1 (3) |
O16ii—U2—O7iii | 73.85 (16) | O9—O11—O15 | 100.2 (3) |
O10i—U2—O7iii | 132.71 (15) | U1—O11—O13 | 52.1 (2) |
O15iii—U2—O7iii | 38.75 (14) | O6—O11—O13 | 99.3 (3) |
O14—Cr1—O7iii | 110.9 (5) | O7—O11—O13 | 55.1 (3) |
O14—Cr1—O2 | 108.6 (4) | O9—O11—O13 | 55.4 (2) |
O7iii—Cr1—O2 | 109.5 (4) | O15—O11—O13 | 98.0 (3) |
O14—Cr1—O6 | 107.1 (4) | U1—O11—N1vii | 111.2 (3) |
O7iii—Cr1—O6 | 110.1 (4) | O6—O11—N1vii | 56.5 (2) |
O2—Cr1—O6 | 110.7 (3) | O7—O11—N1vii | 148.9 (4) |
O14—Cr1—O15 | 111.5 (3) | O9—O11—N1vii | 86.3 (3) |
O7iii—Cr1—O15 | 63.5 (3) | O15—O11—N1vii | 92.9 (3) |
O2—Cr1—O15 | 138.9 (3) | O13—O11—N1vii | 141.4 (3) |
O6—Cr1—O15 | 48.5 (3) | U1—O11—OW18 | 144.3 (4) |
O14—Cr1—O12 | 93.1 (4) | O6—O11—OW18 | 108.8 (3) |
O7iii—Cr1—O12 | 156.0 (4) | O7—O11—OW18 | 110.9 (3) |
O2—Cr1—O12 | 59.7 (3) | O9—O11—OW18 | 149.4 (4) |
O6—Cr1—O12 | 61.0 (3) | O15—O11—OW18 | 91.2 (3) |
O15—Cr1—O12 | 109.09 (17) | O13—O11—OW18 | 151.1 (3) |
O14—Cr1—O10 | 134.0 (4) | N1vii—O11—OW18 | 64.6 (3) |
O7iii—Cr1—O10 | 113.8 (4) | U1—O11—O14ix | 135.2 (4) |
O2—Cr1—O10 | 45.8 (3) | O6—O11—O14ix | 98.4 (3) |
O6—Cr1—O10 | 66.7 (3) | O7—O11—O14ix | 157.2 (3) |
O15—Cr1—O10 | 97.53 (17) | O9—O11—O14ix | 81.8 (3) |
O12—Cr1—O10 | 42.61 (16) | O15—O11—O14ix | 146.6 (3) |
O12—Cr2—O10 | 110.8 (4) | O13—O11—O14ix | 109.9 (3) |
O12—Cr2—O9 | 111.1 (4) | N1vii—O11—O14ix | 53.8 (3) |
O10—Cr2—O9 | 110.6 (4) | OW18—O11—O14ix | 73.4 (3) |
O12—Cr2—O1iv | 107.8 (4) | U1—O11—O5 | 0.69 (18) |
O10—Cr2—O1iv | 109.8 (4) | O6—O11—O5 | 54.3 (2) |
O9—Cr2—O1iv | 106.6 (3) | O7—O11—O5 | 53.1 (2) |
O12—Cr2—O6 | 75.3 (3) | O9—O11—O5 | 54.1 (2) |
O10—Cr2—O6 | 82.1 (3) | O15—O11—O5 | 52.6 (2) |
O9—Cr2—O6 | 59.2 (3) | O13—O11—O5 | 52.8 (2) |
O1iv—Cr2—O6 | 164.7 (3) | N1vii—O11—O5 | 110.7 (3) |
O12—Cr2—OW17iv | 127.3 (3) | OW18—O11—O5 | 143.7 (3) |
O10—Cr2—OW17iv | 121.8 (3) | O14ix—O11—O5 | 135.4 (3) |
O9—Cr2—OW17iv | 54.7 (3) | U1—O11—O3v | 104.5 (3) |
O1iv—Cr2—OW17iv | 52.1 (3) | O6—O11—O3v | 115.4 (3) |
O6—Cr2—OW17iv | 113.81 (17) | O7—O11—O3v | 61.0 (3) |
O12—Cr2—O2 | 64.9 (3) | O9—O11—O3v | 158.1 (3) |
O10—Cr2—O2 | 52.0 (3) | O15—O11—O3v | 62.3 (2) |
O9—Cr2—O2 | 105.9 (3) | O13—O11—O3v | 111.4 (3) |
O1iv—Cr2—O2 | 146.9 (3) | N1vii—O11—O3v | 106.4 (3) |
O6—Cr2—O2 | 48.17 (17) | OW18—O11—O3v | 49.9 (2) |
OW17iv—Cr2—O2 | 158.54 (17) | O14ix—O11—O3v | 120.0 (3) |
O12—Cr2—O4iv | 165.5 (3) | O5—O11—O3v | 104.3 (2) |
O10—Cr2—O4iv | 73.4 (3) | U1—O11—O16iii | 90.9 (3) |
O9—Cr2—O4iv | 79.0 (3) | O6—O11—O16iii | 66.9 (2) |
O1iv—Cr2—O4iv | 58.3 (3) | O7—O11—O16iii | 86.7 (3) |
O6—Cr2—O4iv | 119.27 (17) | O9—O11—O16iii | 123.5 (3) |
OW17iv—Cr2—O4iv | 49.42 (17) | O15—O11—O16iii | 39.7 (2) |
O2—Cr2—O4iv | 123.68 (17) | O13—O11—O16iii | 137.2 (3) |
O16—Cr3—O15v | 110.5 (4) | N1vii—O11—O16iii | 65.5 (3) |
O16—Cr3—O13 | 110.7 (4) | OW18—O11—O16iii | 54.2 (2) |
O15v—Cr3—O13 | 110.4 (4) | O14ix—O11—O16iii | 112.1 (3) |
O16—Cr3—O8vi | 108.3 (4) | O5—O11—O16iii | 90.2 (2) |
O15v—Cr3—O8vi | 109.7 (4) | O3v—O11—O16iii | 51.68 (18) |
O13—Cr3—O8vi | 107.1 (3) | Cr2—O12—O1iv | 37.1 (2) |
O16—Cr3—O7 | 98.1 (3) | Cr2—O12—O10 | 35.1 (2) |
O15v—Cr3—O7 | 69.2 (3) | O1iv—O12—O10 | 61.4 (3) |
O13—Cr3—O7 | 51.5 (3) | Cr2—O12—O9 | 35.1 (2) |
O8vi—Cr3—O7 | 151.4 (3) | O1iv—O12—O9 | 60.1 (3) |
O16—Cr3—O3vi | 76.0 (3) | O10—O12—O9 | 60.8 (3) |
O15v—Cr3—O3vi | 79.8 (3) | Cr2—O12—OW18vii | 137.9 (4) |
O13—Cr3—O3vi | 163.4 (3) | O1iv—O12—OW18vii | 131.9 (4) |
O8vi—Cr3—O3vi | 56.5 (3) | O10—O12—OW18vii | 104.0 (3) |
O7—Cr3—O3vi | 144.27 (18) | O9—O12—OW18vii | 155.9 (4) |
O16—Cr3—OW17iv | 111.5 (3) | Cr2—O12—O2 | 87.8 (3) |
O15v—Cr3—OW17iv | 137.6 (3) | O1iv—O12—O2 | 117.7 (3) |
O13—Cr3—OW17iv | 58.8 (3) | O10—O12—O2 | 56.5 (2) |
O8vi—Cr3—OW17iv | 50.3 (3) | O9—O12—O2 | 92.9 (3) |
O7—Cr3—OW17iv | 110.05 (17) | OW18vii—O12—O2 | 63.2 (3) |
O3vi—Cr3—OW17iv | 104.75 (16) | Cr2—O12—O6 | 75.7 (3) |
O16—Cr3—O1vi | 63.1 (3) | O1iv—O12—O6 | 111.5 (3) |
O15v—Cr3—O1vi | 125.5 (3) | O10—O12—O6 | 70.0 (3) |
O13—Cr3—O1vi | 122.6 (3) | O9—O12—O6 | 54.9 (2) |
O8vi—Cr3—O1vi | 45.2 (3) | OW18vii—O12—O6 | 103.6 (3) |
O7—Cr3—O1vi | 158.4 (2) | O2—O12—O6 | 51.1 (2) |
O3vi—Cr3—O1vi | 45.74 (16) | Cr2—O12—Cr1 | 90.1 (3) |
OW17iv—Cr3—O1vi | 70.82 (16) | O1iv—O12—Cr1 | 126.7 (3) |
Cr2i—O1—U2 | 128.7 (4) | O10—O12—Cr1 | 69.3 (2) |
Cr2i—O1—O12i | 35.1 (2) | O9—O12—Cr1 | 79.5 (2) |
U2—O1—O12i | 163.8 (4) | OW18vii—O12—Cr1 | 77.4 (3) |
Cr2i—O1—O9i | 36.5 (2) | O2—O12—Cr1 | 26.95 (14) |
U2—O1—O9i | 106.1 (3) | O6—O12—Cr1 | 27.28 (14) |
O12i—O1—O9i | 60.7 (3) | Cr2—O12—O4 | 82.0 (3) |
Cr2i—O1—O10i | 34.6 (2) | O1iv—O12—O4 | 88.9 (3) |
U2—O1—O10i | 106.6 (3) | O10—O12—O4 | 49.9 (2) |
O12i—O1—O10i | 59.6 (3) | O9—O12—O4 | 110.6 (3) |
O9i—O1—O10i | 60.4 (3) | OW18vii—O12—O4 | 55.9 (2) |
Cr2i—O1—OW17 | 98.7 (3) | O2—O12—O4 | 46.52 (19) |
U2—O1—OW17 | 58.6 (2) | O6—O12—O4 | 94.5 (2) |
O12i—O1—OW17 | 116.2 (3) | Cr1—O12—O4 | 73.41 (18) |
O9i—O1—OW17 | 62.4 (3) | Cr2—O12—O14 | 112.3 (4) |
O10i—O1—OW17 | 111.5 (3) | O1iv—O12—O14 | 149.4 (3) |
Cr2i—O1—O8 | 114.9 (4) | O10—O12—O14 | 91.8 (3) |
U2—O1—O8 | 52.5 (2) | O9—O12—O14 | 95.0 (3) |
O12i—O1—O8 | 126.6 (3) | OW18vii—O12—O14 | 65.3 (3) |
O9i—O1—O8 | 128.5 (3) | O2—O12—O14 | 40.55 (19) |
O10i—O1—O8 | 80.3 (3) | O6—O12—O14 | 40.32 (19) |
OW17—O1—O8 | 110.3 (3) | Cr1—O12—O14 | 23.09 (13) |
Cr2i—O1—O3 | 166.3 (4) | O4—O12—O14 | 83.4 (2) |
U2—O1—O3 | 38.89 (19) | Cr2—O12—U2 | 66.5 (3) |
O12i—O1—O3 | 157.0 (4) | O1iv—O12—U2 | 87.2 (2) |
O9i—O1—O3 | 132.1 (3) | O10—O12—U2 | 31.43 (17) |
O10i—O1—O3 | 141.2 (4) | O9—O12—U2 | 88.4 (2) |
OW17—O1—O3 | 70.0 (3) | OW18vii—O12—U2 | 73.2 (2) |
O8—O1—O3 | 64.3 (3) | O2—O12—U2 | 33.09 (15) |
Cr2i—O1—N2i | 109.9 (4) | O6—O12—U2 | 72.20 (19) |
U2—O1—N2i | 120.4 (3) | Cr1—O12—U2 | 56.56 (11) |
O12i—O1—N2i | 75.4 (3) | O4—O12—U2 | 24.83 (12) |
O9i—O1—N2i | 116.1 (3) | O14—O12—U2 | 73.61 (17) |
O10i—O1—N2i | 130.0 (3) | Cr2—O12—O5x | 137.4 (4) |
OW17—O1—N2i | 107.1 (3) | O1iv—O12—O5x | 109.9 (3) |
O8—O1—N2i | 114.5 (3) | O10—O12—O5x | 171.2 (3) |
O3—O1—N2i | 81.6 (3) | O9—O12—O5x | 115.4 (3) |
Cr2i—O1—O4 | 93.6 (3) | OW18vii—O12—O5x | 82.0 (2) |
U2—O1—O4 | 35.29 (17) | O2—O12—O5x | 132.2 (3) |
O12i—O1—O4 | 128.6 (3) | O6—O12—O5x | 115.1 (3) |
O9i—O1—O4 | 78.6 (3) | Cr1—O12—O5x | 118.7 (2) |
O10i—O1—O4 | 74.0 (3) | O4—O12—O5x | 133.8 (2) |
OW17—O1—O4 | 60.6 (2) | O14—O12—O5x | 96.6 (2) |
O8—O1—O4 | 58.2 (2) | U2—O12—O5x | 155.2 (2) |
O3—O1—O4 | 74.2 (3) | Cr3—O13—U1 | 153.4 (4) |
N2i—O1—O4 | 155.4 (3) | Cr3—O13—O16 | 34.2 (2) |
Cr2i—O1—O16ii | 121.1 (3) | U1—O13—O16 | 139.9 (4) |
U2—O1—O16ii | 90.3 (2) | Cr3—O13—O8vi | 37.1 (2) |
O12i—O1—O16ii | 100.2 (3) | U1—O13—O8vi | 159.7 (4) |
O9i—O1—O16ii | 157.5 (3) | O16—O13—O8vi | 59.9 (3) |
O10i—O1—O16ii | 100.6 (3) | Cr3—O13—O15v | 34.8 (2) |
OW17—O1—O16ii | 140.0 (3) | U1—O13—O15v | 120.4 (3) |
O8—O1—O16ii | 51.6 (2) | O16—O13—O15v | 59.6 (3) |
O3—O1—O16ii | 70.1 (3) | O8vi—O13—O15v | 60.9 (3) |
N2i—O1—O16ii | 65.1 (3) | Cr3—O13—O7 | 100.5 (3) |
O4—O1—O16ii | 109.3 (3) | U1—O13—O7 | 53.6 (2) |
Cr2i—O1—Cr3ii | 121.3 (3) | O16—O13—O7 | 95.2 (3) |
U2—O1—Cr3ii | 70.42 (17) | O8vi—O13—O7 | 134.1 (4) |
O12i—O1—Cr3ii | 115.4 (3) | O15v—O13—O7 | 73.3 (3) |
O9i—O1—Cr3ii | 149.1 (3) | Cr3—O13—O9 | 150.3 (4) |
O10i—O1—Cr3ii | 90.5 (2) | U1—O13—O9 | 54.3 (2) |
OW17—O1—Cr3ii | 128.2 (3) | O16—O13—O9 | 146.0 (4) |
O8—O1—Cr3ii | 25.74 (15) | O8vi—O13—O9 | 113.2 (3) |
O3—O1—Cr3ii | 64.5 (2) | O15v—O13—O9 | 150.5 (4) |
N2i—O1—Cr3ii | 89.9 (3) | O7—O13—O9 | 107.9 (3) |
O4—O1—Cr3ii | 83.7 (2) | Cr3—O13—O5 | 142.2 (4) |
O16ii—O1—Cr3ii | 25.81 (14) | U1—O13—O5 | 36.56 (17) |
Cr1—O2—U2 | 140.6 (4) | O16—O13—O5 | 110.2 (3) |
Cr1—O2—O14 | 34.9 (2) | O8vi—O13—O5 | 158.6 (4) |
U2—O2—O14 | 172.4 (4) | O15v—O13—O5 | 133.4 (3) |
Cr1—O2—O7iii | 35.0 (2) | O7—O13—O5 | 62.0 (3) |
U2—O2—O7iii | 113.1 (3) | O9—O13—O5 | 63.0 (3) |
O14—O2—O7iii | 59.9 (3) | Cr3—O13—O11 | 130.4 (4) |
Cr1—O2—O6 | 34.9 (2) | U1—O13—O11 | 36.32 (18) |
U2—O2—O6 | 121.8 (3) | O16—O13—O11 | 152.1 (4) |
O14—O2—O6 | 58.5 (3) | O8vi—O13—O11 | 125.4 (4) |
O7iii—O2—O6 | 60.0 (3) | O15v—O13—O11 | 97.4 (3) |
Cr1—O2—O10 | 109.0 (3) | O7—O13—O11 | 60.9 (3) |
U2—O2—O10 | 54.0 (2) | O9—O13—O11 | 61.1 (3) |
O14—O2—O10 | 130.1 (3) | O5—O13—O11 | 72.9 (3) |
O7iii—O2—O10 | 113.9 (3) | Cr3—O13—OW17iv | 94.1 (3) |
O6—O2—O10 | 75.6 (3) | U1—O13—OW17iv | 111.0 (3) |
Cr1—O2—O4 | 172.2 (4) | O16—O13—OW17iv | 100.8 (3) |
U2—O2—O4 | 37.82 (18) | O8vi—O13—OW17iv | 58.3 (2) |
O14—O2—O4 | 147.9 (4) | O15v—O13—OW17iv | 117.1 (3) |
O7iii—O2—O4 | 148.5 (4) | O7—O13—OW17iv | 163.8 (4) |
O6—O2—O4 | 137.4 (3) | O9—O13—OW17iv | 56.7 (2) |
O10—O2—O4 | 63.6 (3) | O5—O13—OW17iv | 109.5 (3) |
Cr1—O2—O8 | 127.6 (4) | O11—O13—OW17iv | 104.1 (3) |
U2—O2—O8 | 50.59 (19) | Cr3—O13—O4iv | 103.2 (3) |
O14—O2—O8 | 124.8 (3) | U1—O13—O4iv | 100.5 (2) |
O7iii—O2—O8 | 94.6 (3) | O16—O13—O4iv | 83.5 (3) |
O6—O2—O8 | 150.1 (3) | O8vi—O13—O4iv | 84.3 (3) |
O10—O2—O8 | 104.6 (3) | O15v—O13—O4iv | 138.0 (3) |
O4—O2—O8 | 58.8 (2) | O7—O13—O4iv | 134.1 (3) |
Cr1—O2—O3 | 104.5 (3) | O9—O13—O4iv | 62.5 (2) |
U2—O2—O3 | 36.53 (17) | O5—O13—O4iv | 75.3 (2) |
O14—O2—O3 | 137.3 (4) | O11—O13—O4iv | 123.0 (3) |
O7iii—O2—O3 | 77.8 (3) | OW17iv—O13—O4iv | 46.95 (19) |
O6—O2—O3 | 96.3 (3) | Cr3—O13—O6v | 63.1 (2) |
O10—O2—O3 | 60.4 (3) | U1—O13—O6v | 90.8 (2) |
O4—O2—O3 | 74.4 (3) | O16—O13—O6v | 65.2 (2) |
O8—O2—O3 | 60.6 (2) | O8vi—O13—O6v | 97.7 (3) |
Cr1—O2—O12 | 93.3 (3) | O15v—O13—O6v | 39.3 (2) |
U2—O2—O12 | 98.4 (3) | O7—O13—O6v | 37.5 (2) |
O14—O2—O12 | 88.4 (3) | O9—O13—O6v | 144.4 (3) |
O7iii—O2—O12 | 124.9 (3) | O5—O13—O6v | 94.1 (2) |
O6—O2—O12 | 65.1 (3) | O11—O13—O6v | 87.1 (2) |
O10—O2—O12 | 52.8 (2) | OW17iv—O13—O6v | 155.9 (3) |
O4—O2—O12 | 80.3 (3) | O4iv—O13—O6v | 141.5 (3) |
O8—O2—O12 | 139.0 (3) | Cr1—O14—O6 | 37.5 (2) |
O3—O2—O12 | 113.1 (3) | Cr1—O14—O2 | 36.5 (3) |
Cr1—O2—OW18vii | 114.0 (4) | O6—O14—O2 | 62.6 (3) |
U2—O2—OW18vii | 103.4 (3) | Cr1—O14—O7iii | 35.1 (3) |
O14—O2—OW18vii | 83.1 (3) | O6—O14—O7iii | 61.7 (3) |
O7iii—O2—OW18vii | 142.3 (4) | O2—O14—O7iii | 60.9 (3) |
O6—O2—OW18vii | 108.0 (3) | Cr1—O14—N1ii | 107.8 (4) |
O10—O2—OW18vii | 94.5 (3) | O6—O14—N1ii | 139.0 (4) |
O4—O2—OW18vii | 65.9 (3) | O2—O14—N1ii | 76.6 (3) |
O8—O2—OW18vii | 101.9 (3) | O7iii—O14—N1ii | 103.2 (4) |
O3—O2—OW18vii | 139.6 (3) | Cr1—O14—C2ii | 101.0 (5) |
O12—O2—OW18vii | 54.6 (3) | O6—O14—C2ii | 138.4 (4) |
Cr1—O2—Cr2 | 95.0 (3) | O2—O14—C2ii | 82.9 (4) |
U2—O2—Cr2 | 79.95 (19) | O7iii—O14—C2ii | 82.0 (4) |
O14—O2—Cr2 | 105.4 (3) | N1ii—O14—C2ii | 29.1 (3) |
O7iii—O2—Cr2 | 115.6 (3) | Cr1—O14—N1vii | 96.0 (4) |
O6—O2—Cr2 | 60.5 (2) | O6—O14—N1vii | 58.6 (3) |
O10—O2—Cr2 | 27.52 (17) | O2—O14—N1vii | 110.5 (4) |
O4—O2—Cr2 | 77.3 (2) | O7iii—O14—N1vii | 113.4 (3) |
O8—O2—Cr2 | 129.7 (3) | N1ii—O14—N1vii | 141.4 (3) |
O3—O2—Cr2 | 86.4 (2) | C2ii—O14—N1vii | 162.9 (4) |
O12—O2—Cr2 | 27.31 (14) | Cr1—O14—C1vii | 115.0 (4) |
OW18vii—O2—Cr2 | 78.7 (2) | O6—O14—C1vii | 79.1 (4) |
U2—O3—O1 | 56.3 (2) | O2—O14—C1vii | 137.5 (4) |
U2—O3—O10 | 54.1 (2) | O7iii—O14—C1vii | 117.1 (4) |
O1—O3—O10 | 98.7 (3) | N1ii—O14—C1vii | 136.1 (4) |
U2—O3—O8 | 50.5 (2) | C2ii—O14—C1vii | 139.4 (5) |
O1—O3—O8 | 57.1 (2) | N1vii—O14—C1vii | 27.6 (3) |
O10—O3—O8 | 100.3 (3) | Cr1—O14—O11vii | 139.1 (5) |
U2—O3—O2 | 50.7 (2) | O6—O14—O11vii | 126.0 (4) |
O1—O3—O2 | 102.3 (3) | O2—O14—O11vii | 106.0 (4) |
O10—O3—O2 | 56.7 (2) | O7iii—O14—O11vii | 161.7 (4) |
O8—O3—O2 | 58.6 (2) | N1ii—O14—O11vii | 59.6 (3) |
U2—O3—OW18iii | 151.5 (4) | C2ii—O14—O11vii | 83.7 (3) |
O1—O3—OW18iii | 96.3 (3) | N1vii—O14—O11vii | 82.4 (3) |
O10—O3—OW18iii | 149.1 (4) | C1vii—O14—O11vii | 81.2 (3) |
O8—O3—OW18iii | 110.5 (3) | Cr1—O14—OW18vii | 87.9 (4) |
O2—O3—OW18iii | 144.4 (4) | O6—O14—OW18vii | 92.9 (3) |
U2—O3—OW17 | 51.8 (2) | O2—O14—OW18vii | 54.5 (3) |
O1—O3—OW17 | 53.5 (2) | O7iii—O14—OW18vii | 115.1 (3) |
O10—O3—OW17 | 52.8 (2) | N1ii—O14—OW18vii | 57.3 (3) |
O8—O3—OW17 | 94.2 (3) | C2ii—O14—OW18vii | 84.3 (4) |
O2—O3—OW17 | 94.7 (3) | N1vii—O14—OW18vii | 94.8 (4) |
OW18iii—O3—OW17 | 120.6 (3) | C1vii—O14—OW18vii | 114.0 (4) |
U2—O3—O16ii | 93.9 (3) | O11vii—O14—OW18vii | 51.9 (2) |
O1—O3—O16ii | 61.3 (2) | Cr1—O14—O12 | 63.8 (3) |
O10—O3—O16ii | 147.4 (3) | O6—O14—O12 | 51.8 (2) |
O8—O3—O16ii | 47.7 (2) | O2—O14—O12 | 51.0 (2) |
O2—O3—O16ii | 100.2 (3) | O7iii—O14—O12 | 98.9 (3) |
OW18iii—O3—O16ii | 63.0 (3) | N1ii—O14—O12 | 99.1 (3) |
OW17—O3—O16ii | 114.8 (3) | C2ii—O14—O12 | 122.3 (4) |
U2—O3—O4 | 0.71 (18) | N1vii—O14—O12 | 64.4 (3) |
O1—O3—O4 | 55.7 (2) | C1vii—O14—O12 | 91.5 (3) |
O10—O3—O4 | 54.1 (2) | O11vii—O14—O12 | 79.2 (3) |
O8—O3—O4 | 50.8 (2) | OW18vii—O14—O12 | 42.9 (2) |
O2—O3—O4 | 51.3 (2) | Cr1—O14—O9vii | 173.9 (5) |
OW18iii—O3—O4 | 151.1 (3) | O6—O14—O9vii | 147.0 (3) |
OW17—O3—O4 | 51.2 (2) | O2—O14—O9vii | 144.2 (3) |
O16ii—O3—O4 | 93.9 (2) | O7iii—O14—O9vii | 139.2 (4) |
U2—O3—Cr3ii | 78.8 (2) | N1ii—O14—O9vii | 70.0 (3) |
O1—O3—Cr3ii | 69.7 (2) | C2ii—O14—O9vii | 74.3 (3) |
O10—O3—Cr3ii | 126.0 (3) | N1vii—O14—O9vii | 88.8 (3) |
O8—O3—Cr3ii | 28.38 (15) | C1vii—O14—O9vii | 68.3 (3) |
O2—O3—Cr3ii | 74.1 (2) | O11vii—O14—O9vii | 45.14 (18) |
OW18iii—O3—Cr3ii | 84.6 (3) | OW18vii—O14—O9vii | 95.4 (2) |
OW17—O3—Cr3ii | 118.3 (2) | O12—O14—O9vii | 121.9 (3) |
O16ii—O3—Cr3ii | 26.24 (13) | Cr3iii—O15—U1 | 164.0 (5) |
O4—O3—Cr3ii | 79.15 (18) | Cr3iii—O15—O16iii | 34.3 (2) |
U2—O3—O7iii | 97.0 (3) | U1—O15—O16iii | 129.7 (4) |
O1—O3—O7iii | 134.6 (3) | Cr3iii—O15—O13iii | 34.8 (2) |
O10—O3—O7iii | 89.9 (3) | U1—O15—O13iii | 151.0 (4) |
O8—O3—O7iii | 77.5 (2) | O16iii—O15—O13iii | 59.7 (3) |
O2—O3—O7iii | 47.5 (2) | Cr3iii—O15—O8v | 35.8 (2) |
OW18iii—O3—O7iii | 98.6 (3) | U1—O15—O8v | 149.2 (4) |
OW17—O3—O7iii | 140.1 (3) | O16iii—O15—O8v | 59.4 (3) |
O16ii—O3—O7iii | 88.4 (2) | O13iii—O15—O8v | 59.3 (3) |
O4—O3—O7iii | 97.7 (3) | Cr3iii—O15—O7 | 132.3 (4) |
Cr3ii—O3—O7iii | 69.34 (19) | U1—O15—O7 | 53.5 (2) |
U2—O3—O15iii | 93.2 (3) | O16iii—O15—O7 | 131.3 (4) |
O1—O3—O15iii | 96.1 (3) | O13iii—O15—O7 | 147.0 (4) |
O10—O3—O15iii | 123.4 (3) | O8v—O15—O7 | 97.3 (3) |
O8—O3—O15iii | 47.5 (2) | Cr3iii—O15—O6 | 118.0 (4) |
O2—O3—O15iii | 66.8 (2) | U1—O15—O6 | 52.7 (2) |
OW18iii—O3—O15iii | 81.3 (3) | O16iii—O15—O6 | 94.2 (3) |
OW17—O3—O15iii | 141.6 (3) | O13iii—O15—O6 | 103.3 (3) |
O16ii—O3—O15iii | 43.7 (2) | O8v—O15—O6 | 152.8 (4) |
O4—O3—O15iii | 93.8 (2) | O7—O15—O6 | 106.1 (3) |
Cr3ii—O3—O15iii | 26.38 (13) | Cr3iii—O15—O5 | 156.1 (4) |
O7iii—O3—O15iii | 44.99 (19) | U1—O15—O5 | 36.96 (18) |
U2—O4—O8 | 54.0 (2) | O16iii—O15—O5 | 156.8 (4) |
U2—O4—O2 | 53.6 (2) | O13iii—O15—O5 | 121.7 (4) |
O8—O4—O2 | 61.4 (2) | O8v—O15—O5 | 143.4 (4) |
U2—O4—OW17 | 58.7 (2) | O7—O15—O5 | 62.2 (3) |
O8—O4—OW17 | 103.1 (3) | O6—O15—O5 | 62.6 (2) |
O2—O4—OW17 | 103.2 (3) | Cr3iii—O15—O11 | 128.2 (4) |
U2—O4—O10 | 52.2 (2) | U1—O15—O11 | 37.14 (18) |
O8—O4—O10 | 101.8 (3) | O16iii—O15—O11 | 95.6 (3) |
O2—O4—O10 | 57.1 (2) | O13iii—O15—O11 | 150.2 (4) |
OW17—O4—O10 | 54.8 (2) | O8v—O15—O11 | 124.9 (3) |
U2—O4—O1 | 50.6 (2) | O7—O15—O11 | 61.5 (3) |
O8—O4—O1 | 56.2 (2) | O6—O15—O11 | 59.2 (2) |
O2—O4—O1 | 99.8 (3) | O5—O15—O11 | 74.1 (3) |
OW17—O4—O1 | 54.3 (2) | Cr3iii—O15—O7iii | 82.5 (3) |
O10—O4—O1 | 92.4 (3) | U1—O15—O7iii | 97.5 (3) |
U2—O4—C3viii | 154.4 (4) | O16iii—O15—O7iii | 84.4 (3) |
O8—O4—C3viii | 100.7 (3) | O13iii—O15—O7iii | 54.0 (2) |
O2—O4—C3viii | 121.5 (3) | O8v—O15—O7iii | 113.2 (3) |
OW17—O4—C3viii | 135.3 (4) | O7—O15—O7iii | 142.6 (3) |
O10—O4—C3viii | 151.2 (4) | O6—O15—O7iii | 52.7 (2) |
O1—O4—C3viii | 115.1 (3) | O5—O15—O7iii | 80.4 (3) |
U2—O4—OW18vii | 115.1 (3) | O11—O15—O7iii | 111.6 (3) |
O8—O4—OW18vii | 100.8 (3) | Cr3iii—O15—Cr1 | 97.9 (3) |
O2—O4—OW18vii | 61.8 (3) | U1—O15—Cr1 | 76.72 (19) |
OW17—O4—OW18vii | 139.6 (3) | O16iii—O15—Cr1 | 85.0 (3) |
O10—O4—OW18vii | 88.8 (3) | O13iii—O15—Cr1 | 77.2 (2) |
O1—O4—OW18vii | 156.7 (3) | O8v—O15—Cr1 | 133.1 (3) |
C3viii—O4—OW18vii | 69.4 (3) | O7—O15—Cr1 | 129.5 (3) |
U2—O4—O10i | 96.7 (3) | O6—O15—Cr1 | 26.52 (16) |
O8—O4—O10i | 67.4 (2) | O5—O15—Cr1 | 73.6 (2) |
O2—O4—O10i | 128.8 (3) | O11—O15—Cr1 | 84.8 (2) |
OW17—O4—O10i | 89.0 (3) | O7iii—O15—Cr1 | 26.86 (15) |
O10—O4—O10i | 140.0 (2) | Cr3iii—O15—O3v | 73.8 (3) |
O1—O4—O10i | 48.8 (2) | U1—O15—O3v | 100.4 (3) |
C3viii—O4—O10i | 66.4 (3) | O16iii—O15—O3v | 65.9 (3) |
OW18vii—O4—O10i | 130.4 (3) | O13iii—O15—O3v | 107.7 (3) |
U2—O4—O3 | 0.71 (18) | O8v—O15—O3v | 53.3 (2) |
O8—O4—O3 | 54.3 (2) | O7—O15—O3v | 66.2 (3) |
O2—O4—O3 | 54.3 (2) | O6—O15—O3v | 125.0 (3) |
OW17—O4—O3 | 58.1 (2) | O5—O15—O3v | 127.1 (3) |
O10—O4—O3 | 52.2 (2) | O11—O15—O3v | 71.9 (2) |
O1—O4—O3 | 50.1 (2) | O7iii—O15—O3v | 150.3 (3) |
C3viii—O4—O3 | 154.6 (3) | Cr1—O15—O3v | 139.8 (3) |
OW18vii—O4—O3 | 115.8 (3) | Cr3—O16—O15v | 35.2 (2) |
O10i—O4—O3 | 96.4 (2) | Cr3—O16—O13 | 35.1 (2) |
U2—O4—Cr2i | 78.6 (2) | O15v—O16—O13 | 60.7 (3) |
O8—O4—Cr2i | 71.8 (2) | Cr3—O16—O8vi | 36.9 (2) |
O2—O4—Cr2i | 126.4 (3) | O15v—O16—O8vi | 61.4 (3) |
OW17—O4—Cr2i | 62.51 (19) | O13—O16—O8vi | 60.2 (3) |
O10—O4—Cr2i | 113.5 (3) | Cr3—O16—C4xi | 114.4 (4) |
O1—O4—Cr2i | 28.07 (14) | O15v—O16—C4xi | 131.7 (4) |
C3viii—O4—Cr2i | 90.6 (3) | O13—O16—C4xi | 79.5 (3) |
OW18vii—O4—Cr2i | 157.4 (3) | O8vi—O16—C4xi | 121.8 (4) |
O10i—O4—Cr2i | 26.95 (14) | Cr3—O16—O1vi | 91.1 (4) |
O3—O4—Cr2i | 78.02 (19) | O15v—O16—O1vi | 107.9 (3) |
U2—O4—O9i | 89.7 (3) | O13—O16—O1vi | 106.0 (3) |
O8—O4—O9i | 98.0 (3) | O8vi—O16—O1vi | 54.2 (2) |
O2—O4—O9i | 143.3 (3) | C4xi—O16—O1vi | 108.5 (4) |
OW17—O4—O9i | 49.1 (2) | Cr3—O16—OW18v | 118.8 (4) |
O10—O4—O9i | 103.8 (3) | O15v—O16—OW18v | 90.4 (3) |
O1—O4—O9i | 46.31 (19) | O13—O16—OW18v | 151.1 (4) |
C3viii—O4—O9i | 90.6 (3) | O8vi—O16—OW18v | 107.1 (3) |
OW18vii—O4—O9i | 154.7 (3) | C4xi—O16—OW18v | 125.8 (3) |
O10i—O4—O9i | 44.89 (19) | O1vi—O16—OW18v | 80.9 (3) |
O3—O4—O9i | 89.0 (2) | Cr3—O16—O3vi | 77.7 (3) |
Cr2i—O4—O9i | 26.69 (13) | O15v—O16—O3vi | 70.4 (3) |
U1—O5—O15 | 53.9 (3) | O13—O16—O3vi | 111.5 (3) |
U1—O5—O7 | 52.5 (3) | O8vi—O16—O3vi | 55.2 (2) |
O15—O5—O7 | 56.2 (3) | C4xi—O16—O3vi | 155.9 (4) |
U1—O5—O13 | 53.6 (2) | O1vi—O16—O3vi | 48.7 (2) |
O15—O5—O13 | 100.0 (3) | OW18v—O16—O3vi | 52.0 (2) |
O7—O5—O13 | 55.6 (2) | Cr3—O16—O7 | 58.5 (3) |
U1—O5—O6 | 51.5 (2) | O15v—O16—O7 | 53.9 (2) |
O15—O5—O6 | 57.0 (2) | O13—O16—O7 | 43.1 (2) |
O7—O5—O6 | 97.7 (3) | O8vi—O16—O7 | 94.9 (3) |
O13—O5—O6 | 97.7 (3) | C4xi—O16—O7 | 78.7 (3) |
U1—O5—O9 | 52.5 (2) | O1vi—O16—O7 | 147.8 (3) |
O15—O5—O9 | 99.7 (3) | OW18v—O16—O7 | 121.3 (3) |
O7—O5—O9 | 97.4 (3) | O3vi—O16—O7 | 124.3 (3) |
O13—O5—O9 | 55.5 (2) | Cr3—O16—O6v | 73.0 (3) |
O6—O5—O9 | 54.9 (2) | O15v—O16—O6v | 44.3 (2) |
U1—O5—O10 | 96.4 (3) | O13—O16—O6v | 77.6 (3) |
O15—O5—O10 | 119.1 (3) | O8vi—O16—O6v | 105.4 (3) |
O7—O5—O10 | 146.5 (3) | C4xi—O16—O6v | 104.6 (4) |
O13—O5—O10 | 97.8 (3) | O1vi—O16—O6v | 146.8 (3) |
O6—O5—O10 | 63.2 (2) | OW18v—O16—O6v | 81.8 (3) |
O9—O5—O10 | 49.2 (2) | O3vi—O16—O6v | 98.8 (2) |
U1—O5—O11 | 0.70 (18) | O7—O16—O6v | 39.63 (17) |
O15—O5—O11 | 53.3 (2) | Cr3—O16—U2vi | 64.1 (3) |
O7—O5—O11 | 52.7 (2) | O15v—O16—U2vi | 72.7 (2) |
O13—O5—O11 | 54.3 (2) | O13—O16—U2vi | 92.4 (2) |
O6—O5—O11 | 51.0 (2) | O8vi—O16—U2vi | 32.35 (17) |
O9—O5—O11 | 52.8 (2) | C4xi—O16—U2vi | 139.1 (4) |
O10—O5—O11 | 96.4 (2) | O1vi—O16—U2vi | 35.45 (14) |
U1—O5—O3 | 130.1 (3) | OW18v—O16—U2vi | 77.0 (2) |
O15—O5—O3 | 107.9 (3) | O3vi—O16—U2vi | 25.91 (13) |
O7—O5—O3 | 160.7 (3) | O7—O16—U2vi | 121.3 (2) |
O13—O5—O3 | 143.5 (3) | O6v—O16—U2vi | 112.7 (2) |
O6—O5—O3 | 79.1 (2) | Cr3—O16—O11v | 79.0 (3) |
O9—O5—O3 | 96.2 (3) | O15v—O16—O11v | 44.8 (2) |
O10—O5—O3 | 48.09 (19) | O13—O16—O11v | 103.7 (3) |
O11—O5—O3 | 129.7 (3) | O8vi—O16—O11v | 92.1 (3) |
U1—O5—O7iii | 86.4 (3) | C4xi—O16—O11v | 139.9 (4) |
O15—O5—O7iii | 53.4 (2) | O1vi—O16—O11v | 108.8 (2) |
O7—O5—O7iii | 109.7 (2) | OW18v—O16—O11v | 48.5 (2) |
O13—O5—O7iii | 139.0 (3) | O3vi—O16—O11v | 60.38 (19) |
O6—O5—O7iii | 43.0 (2) | O7—O16—O11v | 77.8 (2) |
O9—O5—O7iii | 95.0 (3) | O6v—O16—O11v | 40.66 (16) |
O10—O5—O7iii | 76.0 (2) | U2vi—O16—O11v | 80.92 (17) |
O11—O5—O7iii | 85.7 (2) | U2—OW17—O10 | 53.5 (2) |
O3—O5—O7iii | 55.4 (2) | U2—OW17—O1 | 53.4 (2) |
U1—O5—O14v | 92.2 (3) | O10—OW17—O1 | 106.2 (3) |
O15—O5—O14v | 76.7 (3) | U2—OW17—O9i | 98.8 (3) |
O7—O5—O14v | 39.7 (2) | O10—OW17—O9i | 142.5 (4) |
O13—O5—O14v | 76.7 (2) | O1—OW17—O9i | 58.1 (2) |
O6—O5—O14v | 131.9 (3) | U2—OW17—O8iv | 126.8 (3) |
O9—O5—O14v | 131.0 (3) | O10—OW17—O8iv | 79.1 (3) |
O10—O5—O14v | 164.1 (3) | O1—OW17—O8iv | 162.9 (3) |
O11—O5—O14v | 92.4 (2) | O9i—OW17—O8iv | 107.8 (3) |
O3—O5—O14v | 131.9 (2) | U2—OW17—O4 | 36.88 (18) |
O7iii—O5—O14v | 118.0 (2) | O10—OW17—O4 | 63.9 (3) |
U1—O5—O4iv | 102.2 (3) | O1—OW17—O4 | 65.1 (3) |
O15—O5—O4iv | 155.5 (3) | O9i—OW17—O4 | 78.9 (3) |
O7—O5—O4iv | 116.4 (3) | O8iv—OW17—O4 | 104.6 (3) |
O13—O5—O4iv | 63.0 (2) | U2—OW17—O13i | 119.1 (3) |
O6—O5—O4iv | 105.5 (3) | O10—OW17—O13i | 111.8 (3) |
O9—O5—O4iv | 56.5 (2) | O1—OW17—O13i | 110.0 (3) |
O10—O5—O4iv | 51.84 (19) | O9i—OW17—O13i | 55.8 (2) |
O11—O5—O4iv | 102.7 (2) | O8iv—OW17—O13i | 53.6 (2) |
O3—O5—O4iv | 82.6 (2) | O4—OW17—O13i | 82.3 (3) |
O7iii—O5—O4iv | 127.6 (2) | U2—OW17—O3 | 33.89 (16) |
O14v—O5—O4iv | 113.3 (2) | O10—OW17—O3 | 58.6 (3) |
Cr1—O6—U1 | 146.8 (4) | O1—OW17—O3 | 56.5 (2) |
Cr1—O6—O14 | 35.5 (2) | O9i—OW17—O3 | 114.4 (3) |
U1—O6—O14 | 162.2 (4) | O8iv—OW17—O3 | 135.3 (3) |
Cr1—O6—O7iii | 34.5 (2) | O4—OW17—O3 | 70.8 (3) |
U1—O6—O7iii | 114.6 (3) | O13i—OW17—O3 | 152.9 (3) |
O14—O6—O7iii | 59.7 (3) | U2—OW17—Cr2i | 74.45 (17) |
Cr1—O6—O2 | 34.5 (2) | O10—OW17—Cr2i | 126.8 (3) |
U1—O6—O2 | 135.1 (3) | O1—OW17—Cr2i | 29.16 (16) |
O14—O6—O2 | 58.9 (3) | O9i—OW17—Cr2i | 29.00 (16) |
O7iii—O6—O2 | 59.1 (3) | O8iv—OW17—Cr2i | 135.7 (3) |
Cr1—O6—O9 | 136.0 (4) | O4—OW17—Cr2i | 68.1 (2) |
U1—O6—O9 | 54.9 (2) | O13i—OW17—Cr2i | 82.1 (2) |
O14—O6—O9 | 140.6 (4) | O3—OW17—Cr2i | 85.4 (2) |
O7iii—O6—O9 | 143.1 (4) | U2—OW17—Cr3i | 122.8 (3) |
O2—O6—O9 | 101.5 (3) | O10—OW17—Cr3i | 92.3 (3) |
Cr1—O6—O15 | 105.0 (3) | O1—OW17—Cr3i | 135.7 (3) |
U1—O6—O15 | 53.6 (2) | O9i—OW17—Cr3i | 82.7 (2) |
O14—O6—O15 | 110.2 (4) | O8iv—OW17—Cr3i | 27.34 (15) |
O7iii—O6—O15 | 71.9 (3) | O4—OW17—Cr3i | 89.5 (2) |
O2—O6—O15 | 128.2 (3) | O13i—OW17—Cr3i | 27.06 (15) |
O9—O6—O15 | 108.5 (3) | O3—OW17—Cr3i | 149.6 (3) |
Cr1—O6—N1vii | 104.2 (3) | Cr2i—OW17—Cr3i | 109.00 (18) |
U1—O6—N1vii | 105.1 (3) | U2—OW17—O4iv | 111.0 (2) |
O14—O6—N1vii | 68.8 (3) | O10—OW17—O4iv | 60.1 (2) |
O7iii—O6—N1vii | 120.5 (4) | O1—OW17—O4iv | 150.1 (3) |
O2—O6—N1vii | 115.7 (3) | O9i—OW17—O4iv | 148.9 (3) |
O9—O6—N1vii | 95.8 (3) | O8iv—OW17—O4iv | 46.5 (2) |
O15—O6—N1vii | 102.3 (3) | O4—OW17—O4iv | 120.2 (2) |
Cr1—O6—O11 | 160.6 (4) | O13i—OW17—O4iv | 100.0 (2) |
U1—O6—O11 | 38.63 (18) | O3—OW17—O4iv | 95.9 (2) |
O14—O6—O11 | 131.3 (3) | Cr2i—OW17—O4iv | 171.6 (3) |
O7iii—O6—O11 | 134.3 (3) | Cr3i—OW17—O4iv | 73.83 (16) |
O2—O6—O11 | 164.7 (4) | U2—OW17—O1iv | 88.0 (2) |
O9—O6—O11 | 63.3 (3) | O10—OW17—O1iv | 38.9 (2) |
O15—O6—O11 | 62.8 (3) | O1—OW17—O1iv | 140.6 (3) |
N1vii—O6—O11 | 66.6 (3) | O9i—OW17—O1iv | 132.6 (3) |
Cr1—O6—O5 | 113.7 (3) | O8iv—OW17—O1iv | 40.51 (19) |
U1—O6—O5 | 36.07 (17) | O4—OW17—O1iv | 79.3 (2) |
O14—O6—O5 | 147.8 (4) | O13i—OW17—O1iv | 79.9 (2) |
O7iii—O6—O5 | 88.7 (3) | O3—OW17—O1iv | 97.1 (2) |
O2—O6—O5 | 100.8 (3) | Cr2i—OW17—O1iv | 144.5 (2) |
O9—O6—O5 | 62.7 (2) | Cr3i—OW17—O1iv | 55.53 (13) |
O15—O6—O5 | 60.4 (3) | O4iv—OW17—O1iv | 43.63 (16) |
N1vii—O6—O5 | 141.1 (3) | U2—OW17—HW1A | 109.7 |
O11—O6—O5 | 74.7 (3) | O10—OW17—HW1A | 150.8 |
Cr1—O6—O12 | 91.8 (3) | O1—OW17—HW1A | 58.4 |
U1—O6—O12 | 108.0 (3) | O9i—OW17—HW1A | 54.2 |
O14—O6—O12 | 87.9 (3) | O8iv—OW17—HW1A | 123.4 |
O7iii—O6—O12 | 122.7 (3) | O4—OW17—HW1A | 119.4 |
O2—O6—O12 | 63.8 (2) | O13i—OW17—HW1A | 97.2 |
O9—O6—O12 | 53.1 (2) | O3—OW17—HW1A | 93.9 |
O15—O6—O12 | 161.6 (3) | Cr2i—OW17—HW1A | 52.1 |
N1vii—O6—O12 | 80.5 (3) | Cr3i—OW17—HW1A | 116.2 |
O11—O6—O12 | 102.9 (3) | O4iv—OW17—HW1A | 119.5 |
O5—O6—O12 | 106.0 (3) | O1iv—OW17—HW1A | 160.7 |
Cr1—O6—Cr2 | 105.5 (3) | U2—OW17—HW1B | 109.7 |
U1—O6—Cr2 | 83.4 (2) | O10—OW17—HW1B | 64.8 |
O14—O6—Cr2 | 114.0 (3) | O1—OW17—HW1B | 137.3 |
O7iii—O6—Cr2 | 124.6 (3) | O9i—OW17—HW1B | 150.8 |
O2—O6—Cr2 | 71.4 (2) | O8iv—OW17—HW1B | 59.8 |
O9—O6—Cr2 | 31.21 (16) | O4—OW17—HW1B | 128.4 |
O15—O6—Cr2 | 134.9 (3) | O13i—OW17—HW1B | 112.0 |
N1vii—O6—Cr2 | 101.6 (3) | O3—OW17—HW1B | 87.6 |
O11—O6—Cr2 | 93.3 (2) | Cr2i—OW17—HW1B | 158.2 |
O5—O6—Cr2 | 77.1 (2) | Cr3i—OW17—HW1B | 87.1 |
O12—O6—Cr2 | 28.99 (14) | O4iv—OW17—HW1B | 14.8 |
Cr1v—O7—U1 | 163.9 (5) | O1iv—OW17—HW1B | 56.9 |
Cr1v—O7—O14v | 34.1 (3) | HW1A—OW17—HW1B | 108.0 |
U1—O7—O14v | 132.3 (4) | N2xii—OW18—O12ix | 115.2 (4) |
Cr1v—O7—O2v | 35.5 (2) | N2xii—OW18—O3v | 78.2 (3) |
U1—O7—O2v | 139.5 (4) | O12ix—OW18—O3v | 103.5 (4) |
O14v—O7—O2v | 59.2 (3) | N2xii—OW18—C1vii | 89.2 (4) |
Cr1v—O7—O6v | 35.4 (2) | O12ix—OW18—C1vii | 130.6 (4) |
U1—O7—O6v | 158.4 (4) | O3v—OW18—C1vii | 123.9 (4) |
O14v—O7—O6v | 58.6 (3) | N2xii—OW18—O2ix | 114.7 (3) |
O2v—O7—O6v | 60.9 (3) | O12ix—OW18—O2ix | 62.2 (2) |
Cr1v—O7—O13 | 131.0 (5) | O3v—OW18—O2ix | 163.4 (4) |
U1—O7—O13 | 55.0 (2) | C1vii—OW18—O2ix | 68.7 (3) |
O14v—O7—O13 | 112.8 (4) | N2xii—OW18—O11 | 139.4 (4) |
O2v—O7—O13 | 165.5 (4) | O12ix—OW18—O11 | 101.7 (3) |
O6v—O7—O13 | 104.7 (3) | O3v—OW18—O11 | 77.2 (3) |
Cr1v—O7—O15 | 116.6 (4) | C1vii—OW18—O11 | 78.5 (3) |
U1—O7—O15 | 54.4 (2) | O2ix—OW18—O11 | 96.8 (3) |
O14v—O7—O15 | 111.8 (4) | N2xii—OW18—O4ix | 63.3 (3) |
O2v—O7—O15 | 85.1 (3) | O12ix—OW18—O4ix | 77.2 (3) |
O6v—O7—O15 | 145.2 (4) | O3v—OW18—O4ix | 136.3 (4) |
O13—O7—O15 | 109.4 (3) | C1vii—OW18—O4ix | 77.4 (3) |
Cr1v—O7—O11 | 155.4 (5) | O2ix—OW18—O4ix | 52.3 (2) |
U1—O7—O11 | 37.54 (18) | O11—OW18—O4ix | 146.3 (4) |
O14v—O7—O11 | 169.7 (4) | N2xii—OW18—O16iii | 63.1 (3) |
O2v—O7—O11 | 126.1 (4) | O12ix—OW18—O16iii | 168.5 (4) |
O6v—O7—O11 | 131.2 (4) | O3v—OW18—O16iii | 65.0 (2) |
O13—O7—O11 | 64.0 (3) | C1vii—OW18—O16iii | 60.7 (3) |
O15—O7—O11 | 62.5 (3) | O2ix—OW18—O16iii | 129.3 (4) |
Cr1v—O7—O5 | 128.6 (5) | O11—OW18—O16iii | 77.3 (3) |
U1—O7—O5 | 36.69 (18) | O4ix—OW18—O16iii | 110.1 (3) |
O14v—O7—O5 | 95.6 (4) | N2xii—OW18—O14ix | 152.3 (4) |
O2v—O7—O5 | 127.8 (4) | O12ix—OW18—O14ix | 71.8 (3) |
O6v—O7—O5 | 145.8 (4) | O3v—OW18—O14ix | 127.8 (3) |
O13—O7—O5 | 62.4 (3) | C1vii—OW18—O14ix | 68.8 (3) |
O15—O7—O5 | 61.5 (3) | O2ix—OW18—O14ix | 42.4 (2) |
O11—O7—O5 | 74.2 (3) | O11—OW18—O14ix | 54.7 (2) |
Cr1v—O7—O15v | 89.6 (3) | O4ix—OW18—O14ix | 94.5 (3) |
U1—O7—O15v | 103.0 (3) | O16iii—OW18—O14ix | 115.4 (3) |
O14v—O7—O15v | 97.7 (3) | N2xii—OW18—O1v | 39.8 (2) |
O2v—O7—O15v | 114.3 (3) | O12ix—OW18—O1v | 122.9 (3) |
O6v—O7—O15v | 55.4 (2) | O3v—OW18—O1v | 39.7 (2) |
O13—O7—O15v | 52.7 (2) | C1vii—OW18—O1v | 103.6 (3) |
O15—O7—O15v | 150.3 (3) | O2ix—OW18—O1v | 154.5 (3) |
O11—O7—O15v | 87.9 (3) | O11—OW18—O1v | 105.6 (3) |
O5—O7—O15v | 113.8 (3) | O4ix—OW18—O1v | 102.7 (3) |
Cr1v—O7—Cr3 | 105.1 (3) | O16iii—OW18—O1v | 47.8 (2) |
U1—O7—Cr3 | 82.9 (2) | O14ix—OW18—O1v | 159.4 (3) |
O14v—O7—Cr3 | 97.3 (3) | N2xii—OW18—O15 | 97.2 (3) |
O2v—O7—Cr3 | 137.6 (3) | O12ix—OW18—O15 | 137.3 (3) |
O6v—O7—Cr3 | 76.7 (2) | O3v—OW18—O15 | 55.0 (2) |
O13—O7—Cr3 | 27.98 (18) | C1vii—OW18—O15 | 73.3 (3) |
O15—O7—Cr3 | 137.3 (3) | O2ix—OW18—O15 | 129.0 (3) |
O11—O7—Cr3 | 83.5 (2) | O11—OW18—O15 | 42.2 (2) |
O5—O7—Cr3 | 85.9 (3) | O4ix—OW18—O15 | 144.9 (3) |
O15v—O7—Cr3 | 28.23 (15) | O16iii—OW18—O15 | 37.46 (18) |
Cr1v—O7—O3v | 83.5 (4) | O14ix—OW18—O15 | 92.6 (2) |
U1—O7—O3v | 103.0 (3) | O1v—OW18—O15 | 66.83 (18) |
O14v—O7—O3v | 113.5 (4) | N2xii—OW18—O10ix | 97.2 (3) |
O2v—O7—O3v | 54.7 (3) | O12ix—OW18—O10ix | 36.0 (2) |
O6v—O7—O3v | 84.3 (3) | O3v—OW18—O10ix | 132.7 (3) |
O13—O7—O3v | 130.0 (4) | C1vii—OW18—O10ix | 102.8 (3) |
O15—O7—O3v | 68.8 (3) | O2ix—OW18—O10ix | 39.26 (18) |
O11—O7—O3v | 73.2 (3) | O11—OW18—O10ix | 123.2 (3) |
O5—O7—O3v | 129.0 (3) | O4ix—OW18—O10ix | 42.62 (18) |
O15v—O7—O3v | 103.1 (3) | O16iii—OW18—O10ix | 152.6 (3) |
Cr3—O7—O3v | 127.5 (3) | O14ix—OW18—O10ix | 72.7 (2) |
Cr3ii—O8—U2 | 131.8 (4) | O1v—OW18—O10ix | 127.9 (3) |
Cr3ii—O8—O16ii | 34.7 (2) | O15—OW18—O10ix | 165.0 (3) |
U2—O8—O16ii | 109.0 (3) | N2xii—OW18—HW1C | 109.6 |
Cr3ii—O8—O13ii | 35.8 (2) | O12ix—OW18—HW1C | 129.5 |
U2—O8—O13ii | 167.5 (3) | O3v—OW18—HW1C | 63.9 |
O16ii—O8—O13ii | 59.8 (3) | C1vii—OW18—HW1C | 70.0 |
Cr3ii—O8—O15iii | 34.5 (2) | O2ix—OW18—HW1C | 117.4 |
U2—O8—O15iii | 110.6 (3) | O11—OW18—HW1C | 29.9 |
O16ii—O8—O15iii | 59.2 (3) | O4ix—OW18—HW1C | 146.8 |
O13ii—O8—O15iii | 59.8 (3) | O16iii—OW18—HW1C | 47.7 |
Cr3ii—O8—O1 | 109.0 (3) | O14ix—OW18—HW1C | 79.5 |
U2—O8—O1 | 54.3 (2) | O1v—OW18—HW1C | 79.9 |
O16ii—O8—O1 | 74.3 (3) | O15—OW18—HW1C | 13.1 |
O13ii—O8—O1 | 122.3 (3) | O10ix—OW18—HW1C | 151.9 |
O15iii—O8—O1 | 123.0 (3) | N2xii—OW18—HW1D | 109.5 |
Cr3ii—O8—O4 | 170.1 (4) | O12ix—OW18—HW1D | 35.3 |
U2—O8—O4 | 38.29 (18) | O3v—OW18—HW1D | 68.3 |
O16ii—O8—O4 | 138.9 (3) | C1vii—OW18—HW1D | 160.2 |
O13ii—O8—O4 | 154.1 (3) | O2ix—OW18—HW1D | 96.6 |
O15iii—O8—O4 | 140.5 (3) | O11—OW18—HW1D | 90.6 |
O1—O8—O4 | 65.6 (3) | O4ix—OW18—HW1D | 104.7 |
Cr3ii—O8—OW17i | 102.4 (3) | O16iii—OW18—HW1D | 133.3 |
U2—O8—OW17i | 123.2 (3) | O14ix—OW18—HW1D | 91.3 |
O16ii—O8—OW17i | 107.6 (3) | O1v—OW18—HW1D | 95.2 |
O13ii—O8—OW17i | 68.0 (3) | O15—OW18—HW1D | 109.4 |
O15iii—O8—OW17i | 125.2 (3) | O10ix—OW18—HW1D | 69.3 |
O1—O8—OW17i | 97.8 (3) | HW1C—OW18—HW1D | 108.0 |
O4—O8—OW17i | 86.9 (3) | N1—C1—O14ix | 76.1 (6) |
Cr3ii—O8—O2 | 116.1 (4) | N1—C1—OW18ix | 84.4 (7) |
U2—O8—O2 | 51.0 (2) | O14ix—C1—OW18ix | 132.5 (5) |
O16ii—O8—O2 | 127.2 (3) | N1—C1—H1A | 109.5 |
O13ii—O8—O2 | 129.6 (3) | O14ix—C1—H1A | 174.4 |
O15iii—O8—O2 | 81.6 (3) | OW18ix—C1—H1A | 50.4 |
O1—O8—O2 | 105.2 (3) | N1—C1—H1B | 109.7 |
O4—O8—O2 | 59.8 (2) | O14ix—C1—H1B | 68.3 |
OW17i—O8—O2 | 124.4 (3) | OW18ix—C1—H1B | 78.8 |
Cr3ii—O8—O3 | 95.2 (3) | H1A—C1—H1B | 109.7 |
U2—O8—O3 | 36.64 (18) | N1—C1—H1C | 109.2 |
O16ii—O8—O3 | 77.1 (3) | O14ix—C1—H1C | 67.3 |
O13ii—O8—O3 | 130.9 (3) | OW18ix—C1—H1C | 159.3 |
O15iii—O8—O3 | 79.2 (3) | H1A—C1—H1C | 109.3 |
O1—O8—O3 | 58.6 (2) | H1B—C1—H1C | 109.4 |
O4—O8—O3 | 74.9 (3) | C1—N1—C2 | 111.9 (9) |
OW17i—O8—O3 | 154.5 (3) | C1—N1—O6ix | 112.8 (6) |
O2—O8—O3 | 60.9 (2) | C2—N1—O6ix | 106.1 (7) |
Cr3ii—O8—O10i | 118.7 (3) | C1—N1—O14vi | 131.1 (7) |
U2—O8—O10i | 85.6 (2) | C2—N1—O14vi | 78.7 (6) |
O16ii—O8—O10i | 95.5 (3) | O6ix—N1—O14vi | 108.8 (4) |
O13ii—O8—O10i | 100.4 (3) | C1—N1—O14ix | 76.3 (6) |
O15iii—O8—O10i | 152.9 (3) | C2—N1—O14ix | 87.0 (6) |
O1—O8—O10i | 49.2 (2) | O6ix—N1—O14ix | 52.6 (2) |
O4—O8—O10i | 64.9 (2) | O14vi—N1—O14ix | 152.3 (4) |
OW17i—O8—O10i | 48.9 (2) | C1—N1—O11ix | 118.5 (7) |
O2—O8—O10i | 124.7 (3) | C2—N1—O11ix | 129.5 (7) |
O3—O8—O10i | 106.2 (3) | O6ix—N1—O11ix | 57.0 (2) |
Cr3ii—O8—O7iii | 75.7 (3) | O14vi—N1—O11ix | 66.6 (3) |
U2—O8—O7iii | 75.3 (2) | O14ix—N1—O11ix | 107.1 (3) |
O16ii—O8—O7iii | 90.8 (3) | C1—N1—H1D | 109.7 |
O13ii—O8—O7iii | 98.3 (3) | C2—N1—H1D | 62.5 |
O15iii—O8—O7iii | 41.6 (2) | O6ix—N1—H1D | 48.5 |
O1—O8—O7iii | 116.4 (3) | O14vi—N1—H1D | 116.8 |
O4—O8—O7iii | 98.9 (3) | O14ix—N1—H1D | 36.0 |
OW17i—O8—O7iii | 144.7 (3) | O11ix—N1—H1D | 101.5 |
O2—O8—O7iii | 40.66 (19) | C1—N1—H1E | 109.4 |
O3—O8—O7iii | 57.8 (2) | C2—N1—H1E | 138.3 |
O10i—O8—O7iii | 161.0 (3) | O6ix—N1—H1E | 61.2 |
Cr2—O9—U1 | 135.4 (4) | O14vi—N1—H1E | 70.2 |
Cr2—O9—O1iv | 36.9 (2) | O14ix—N1—H1E | 108.2 |
U1—O9—O1iv | 161.8 (3) | O11ix—N1—H1E | 9.4 |
Cr2—O9—O12 | 33.7 (2) | H1D—N1—H1E | 108.0 |
U1—O9—O12 | 125.4 (3) | N1—C2—O14vi | 72.2 (6) |
O1iv—O9—O12 | 59.2 (3) | N1—C2—H2A | 109.7 |
Cr2—O9—O10 | 34.4 (2) | O14vi—C2—H2A | 159.0 |
U1—O9—O10 | 105.2 (3) | N1—C2—H2B | 109.5 |
O1iv—O9—O10 | 60.5 (3) | O14vi—C2—H2B | 52.8 |
O12—O9—O10 | 59.2 (3) | H2A—C2—H2B | 109.1 |
Cr2—O9—O6 | 89.6 (3) | N1—C2—H2C | 109.7 |
U1—O9—O6 | 53.5 (2) | O14vi—C2—H2C | 88.5 |
O1iv—O9—O6 | 126.3 (3) | H2A—C2—H2C | 109.6 |
O12—O9—O6 | 72.0 (3) | H2B—C2—H2C | 109.2 |
O10—O9—O6 | 76.8 (3) | N2—C3—O4xiii | 77.8 (6) |
Cr2—O9—O13 | 149.0 (4) | N2—C3—H3A | 109.4 |
U1—O9—O13 | 54.4 (2) | O4xiii—C3—H3A | 140.7 |
O1iv—O9—O13 | 122.1 (3) | N2—C3—H3B | 109.4 |
O12—O9—O13 | 176.9 (4) | O4xiii—C3—H3B | 103.7 |
O10—O9—O13 | 123.9 (3) | H3A—C3—H3B | 109.4 |
O6—O9—O13 | 107.9 (3) | N2—C3—H3C | 109.6 |
Cr2—O9—OW17iv | 96.3 (3) | O4xiii—C3—H3C | 37.2 |
U1—O9—OW17iv | 121.8 (3) | H3A—C3—H3C | 109.5 |
O1iv—O9—OW17iv | 59.5 (2) | H3B—C3—H3C | 109.6 |
O12—O9—OW17iv | 112.4 (3) | C3—N2—C4 | 112.9 (9) |
O10—O9—OW17iv | 109.2 (3) | C3—N2—OW18xiv | 116.7 (7) |
O6—O9—OW17iv | 173.8 (3) | C4—N2—OW18xiv | 111.9 (7) |
O13—O9—OW17iv | 67.6 (3) | C3—N2—O1iv | 118.8 (6) |
Cr2—O9—O11 | 145.4 (4) | C4—N2—O1iv | 92.6 (7) |
U1—O9—O11 | 37.27 (18) | OW18xiv—N2—O1iv | 101.2 (3) |
O1iv—O9—O11 | 160.9 (3) | C3—N2—H2D | 119.9 |
O12—O9—O11 | 114.3 (3) | C4—N2—H2D | 69.2 |
O10—O9—O11 | 134.3 (3) | OW18xiv—N2—H2D | 46.6 |
O6—O9—O11 | 59.9 (2) | O1iv—N2—H2D | 121.1 |
O13—O9—O11 | 63.5 (3) | C3—N2—H2E | 120.2 |
OW17iv—O9—O11 | 113.9 (3) | C4—N2—H2E | 87.9 |
Cr2—O9—O5 | 108.7 (3) | OW18xiv—N2—H2E | 103.8 |
U1—O9—O5 | 35.93 (17) | O1iv—N2—H2E | 4.8 |
O1iv—O9—O5 | 125.9 (3) | H2D—N2—H2E | 119.9 |
O12—O9—O5 | 120.5 (3) | N2—C4—O16x | 148.9 (9) |
O10—O9—O5 | 74.4 (3) | N2—C4—H4A | 109.4 |
O6—O9—O5 | 62.3 (2) | O16x—C4—H4A | 46.2 |
O13—O9—O5 | 61.5 (2) | N2—C4—H4B | 109.4 |
OW17iv—O9—O5 | 116.9 (3) | O16x—C4—H4B | 71.8 |
O11—O9—O5 | 73.2 (3) | H4A—C4—H4B | 109.5 |
Cr2—O9—O4iv | 74.3 (3) | N2—C4—H4C | 109.4 |
U1—O9—O4iv | 109.9 (2) | O16x—C4—H4C | 98.7 |
O1iv—O9—O4iv | 55.1 (2) | H4A—C4—H4C | 109.6 |
O12—O9—O4iv | 107.5 (3) | H4B—C4—H4C | 109.6 |
O10—O9—O4iv | 64.4 (2) | | |
Symmetry codes: (i) −x−1, y+1/2, −z−1; (ii) x, y+1, z; (iii) −x−1, y+1/2, −z; (iv) −x−1, y−1/2, −z−1; (v) −x−1, y−1/2, −z; (vi) x, y−1, z; (vii) −x, y+1/2, −z; (viii) −x, y+1/2, −z−1; (ix) −x, y−1/2, −z; (x) x+1, y, z; (xi) x−1, y, z; (xii) x, y, z+1; (xiii) −x, y−1/2, −z−1; (xiv) x, y, z−1. |
Crystal data top
Cr3H8K1.4O20Rb0.6U2 | F(000) = 1889 |
Mr = 1066.12 | Dx = 3.710 Mg m−3 |
Monoclinic, P21/c | Mo Kα radiation, λ = 0.71073 Å |
a = 11.0898 (7) Å | Cell parameters from 3600 reflections |
b = 10.5667 (7) Å | θ = 2.0–27.8° |
c = 16.2713 (10) Å | µ = 20.44 mm−1 |
β = 90.109 (1)° | T = 150 K |
V = 1906.7 (2) Å3 | Plane, red |
Z = 4 | 0.34 × 0.30 × 0.27 mm |
Data collection top
Bruker Kappa APEXII DUO diffractometer | 3824 reflections with I > 2σ(I) |
Radiation source: fine-focus sealed tube | Rint = 0.112 |
π and ω scans | θmax = 28.0°, θmin = 1.8° |
Absorption correction: multi-scan (SADABS; Bruker, 2012) | h = −14→14 |
Tmin = 0.659, Tmax = 0.822 | k = −13→13 |
21653 measured reflections | l = −21→21 |
4605 independent reflections | |
Refinement top
Refinement on F2 | Hydrogen site location: inferred from neighbouring sites |
Least-squares matrix: full | H-atom parameters not refined |
R[F2 > 2σ(F2)] = 0.046 | w = 1/[σ2(Fo2) + (0.0709P)2] where P = (Fo2 + 2Fc2)/3 |
wR(F2) = 0.115 | (Δ/σ)max = 0.001 |
S = 1.00 | Δρmax = 3.20 e Å−3 |
4605 reflections | Δρmin = −6.60 e Å−3 |
247 parameters | Extinction correction: SHELXL-2014/7 (Sheldrick 2014, Fc*=kFc[1+0.001xFc2λ3/sin(2θ)]-1/4 |
0 restraints | Extinction coefficient: 0.00088 (12) |
Special details top
Geometry. All esds (except the esd in the dihedral angle between two l.s. planes)
are estimated using the full covariance matrix. The cell esds are taken
into account individually in the estimation of esds in distances, angles
and torsion angles; correlations between esds in cell parameters are only
used when they are defined by crystal symmetry. An approximate (isotropic)
treatment of cell esds is used for estimating esds involving l.s. planes. |
Fractional atomic coordinates and isotropic or equivalent isotropic displacement parameters (Å2) top | x | y | z | Uiso*/Ueq | Occ. (<1) |
U1 | 0.08903 (3) | 0.93136 (3) | 0.18101 (2) | 0.01750 (12) | |
U2 | −0.38937 (3) | 1.46721 (3) | −0.26782 (2) | 0.01718 (12) | |
Cr1 | −0.10099 (14) | 1.41887 (13) | −0.15270 (10) | 0.0193 (3) | |
Cr2 | −0.39911 (14) | 1.17970 (13) | −0.12370 (9) | 0.0187 (3) | |
Cr3 | 0.20833 (14) | 1.23378 (13) | 0.26700 (10) | 0.0201 (3) | |
Rb1 | 0.10446 (17) | 1.25464 (16) | 0.00961 (12) | 0.0506 (7) | 0.573 (11) |
K1 | 0.10446 (17) | 1.25464 (16) | 0.00961 (12) | 0.0506 (7) | 0.427 (11) |
K2 | −0.3159 (3) | 1.1020 (3) | −0.40271 (17) | 0.0458 (7) | |
O1 | −0.5165 (6) | 1.0805 (6) | −0.1255 (4) | 0.0239 (14) | |
O2 | −0.2464 (7) | 1.4573 (6) | −0.1628 (4) | 0.0263 (15) | |
O3 | −0.2717 (7) | 1.4363 (7) | −0.3380 (5) | 0.0286 (16) | |
O4 | −0.5091 (6) | 1.4976 (7) | −0.1990 (5) | 0.0286 (15) | |
O5 | 0.0184 (7) | 0.9862 (7) | 0.0894 (5) | 0.0323 (17) | |
O6 | −0.0856 (7) | 1.2706 (6) | −0.1199 (4) | 0.0268 (15) | |
O7 | −0.0328 (7) | 1.4309 (6) | −0.2426 (5) | 0.0283 (16) | |
O8 | 0.3309 (6) | 1.3236 (6) | 0.2458 (5) | 0.0255 (15) | |
O9 | −0.2711 (6) | 1.0953 (6) | −0.1073 (4) | 0.0256 (15) | |
O10 | −0.3906 (7) | 1.2557 (6) | −0.2110 (5) | 0.0309 (17) | |
O11 | 0.1613 (7) | 0.8777 (7) | 0.2719 (5) | 0.0325 (16) | |
O12 | −0.4175 (8) | 1.2772 (7) | −0.0495 (5) | 0.0378 (19) | |
O13 | 0.1893 (7) | 1.1305 (6) | 0.1910 (5) | 0.0320 (17) | |
O14 | −0.0387 (9) | 1.5099 (8) | −0.0878 (5) | 0.044 (2) | |
O15 | 0.0917 (7) | 1.3248 (6) | 0.2745 (6) | 0.040 (2) | |
O16 | 0.2263 (9) | 1.1592 (8) | 0.3499 (5) | 0.046 (2) | |
OW17 | −0.5118 (7) | 1.3127 (6) | −0.3510 (4) | 0.0282 (16) | |
H20A | −0.4754 | 1.2705 | −0.4000 | 0.034* | |
H20B | −0.5969 | 1.2935 | −0.3350 | 0.034* | |
OW18 | −0.1460 (11) | 1.2726 (9) | −0.4481 (7) | 0.066 (3) | |
HW1C | −0.1022 | 1.2620 | −0.5013 | 0.079* | |
HW1D | −0.1272 | 1.3462 | −0.4117 | 0.079* | |
OW19 | −0.3371 (13) | 0.9200 (9) | −0.5190 (7) | 0.073 (4) | |
HW1E | −0.2857 | 0.9233 | −0.5694 | 0.088* | |
HW1F | −0.3963 | 0.8495 | −0.5116 | 0.088* | |
OW20 | 0.3398 (8) | 1.1221 (7) | 0.0178 (5) | 0.0360 (18) | |
HW1A | 0.3452 | 1.0360 | 0.0431 | 0.043* | |
HW1B | 0.4138 | 1.1634 | −0.0048 | 0.043* | |
Atomic displacement parameters (Å2) top | U11 | U22 | U33 | U12 | U13 | U23 |
U1 | 0.0172 (2) | 0.02137 (18) | 0.01391 (19) | −0.00065 (12) | 0.00021 (13) | 0.00055 (11) |
U2 | 0.0164 (2) | 0.01909 (18) | 0.01610 (19) | 0.00097 (11) | 0.00226 (13) | 0.00015 (11) |
Cr1 | 0.0201 (8) | 0.0191 (6) | 0.0187 (8) | 0.0001 (5) | −0.0014 (6) | −0.0005 (5) |
Cr2 | 0.0177 (8) | 0.0209 (6) | 0.0177 (7) | −0.0011 (5) | −0.0001 (6) | −0.0008 (5) |
Cr3 | 0.0181 (8) | 0.0196 (6) | 0.0226 (8) | 0.0001 (5) | 0.0034 (6) | −0.0011 (5) |
Rb1 | 0.0516 (12) | 0.0543 (11) | 0.0457 (11) | 0.0103 (7) | −0.0068 (8) | −0.0055 (7) |
K1 | 0.0516 (12) | 0.0543 (11) | 0.0457 (11) | 0.0103 (7) | −0.0068 (8) | −0.0055 (7) |
K2 | 0.0381 (16) | 0.0679 (17) | 0.0315 (14) | −0.0123 (13) | −0.0055 (11) | 0.0152 (12) |
O1 | 0.022 (4) | 0.029 (3) | 0.021 (4) | −0.005 (3) | −0.003 (3) | −0.001 (3) |
O2 | 0.025 (4) | 0.038 (4) | 0.016 (4) | 0.008 (3) | −0.005 (3) | 0.000 (3) |
O3 | 0.021 (4) | 0.040 (4) | 0.024 (4) | 0.006 (3) | 0.002 (3) | −0.002 (3) |
O4 | 0.019 (4) | 0.035 (3) | 0.032 (4) | 0.002 (3) | 0.007 (3) | 0.002 (3) |
O5 | 0.038 (5) | 0.031 (3) | 0.028 (4) | 0.005 (3) | −0.010 (3) | 0.001 (3) |
O6 | 0.038 (4) | 0.022 (3) | 0.020 (4) | −0.001 (3) | 0.003 (3) | 0.000 (3) |
O7 | 0.030 (4) | 0.026 (3) | 0.029 (4) | 0.003 (3) | 0.011 (3) | 0.007 (3) |
O8 | 0.015 (4) | 0.025 (3) | 0.037 (4) | −0.003 (2) | 0.002 (3) | −0.007 (3) |
O9 | 0.020 (4) | 0.035 (3) | 0.023 (4) | 0.004 (3) | 0.005 (3) | 0.006 (3) |
O10 | 0.035 (5) | 0.021 (3) | 0.036 (4) | −0.001 (3) | −0.008 (3) | 0.009 (3) |
O11 | 0.029 (4) | 0.044 (4) | 0.024 (4) | 0.003 (3) | −0.003 (3) | 0.003 (3) |
O12 | 0.044 (5) | 0.039 (4) | 0.030 (4) | −0.010 (4) | −0.002 (4) | −0.011 (3) |
O13 | 0.031 (4) | 0.031 (3) | 0.033 (4) | −0.013 (3) | 0.008 (3) | −0.007 (3) |
O14 | 0.052 (6) | 0.040 (4) | 0.041 (5) | −0.006 (4) | −0.015 (4) | −0.015 (4) |
O15 | 0.020 (4) | 0.026 (3) | 0.072 (6) | 0.007 (3) | 0.013 (4) | 0.004 (4) |
O16 | 0.060 (6) | 0.042 (4) | 0.036 (5) | −0.002 (4) | −0.001 (4) | 0.015 (4) |
OW17 | 0.036 (4) | 0.029 (3) | 0.019 (4) | −0.013 (3) | −0.001 (3) | 0.002 (3) |
OW18 | 0.083 (8) | 0.056 (5) | 0.058 (7) | −0.010 (5) | 0.038 (6) | −0.013 (5) |
OW19 | 0.115 (11) | 0.056 (6) | 0.048 (7) | −0.023 (6) | 0.000 (7) | 0.015 (5) |
OW20 | 0.041 (5) | 0.040 (4) | 0.027 (4) | 0.001 (3) | 0.007 (3) | 0.002 (3) |
Geometric parameters (Å, º) top
U1—O11 | 1.774 (7) | Rb1—O5ii | 3.305 (8) |
U1—O5 | 1.779 (7) | Rb1—O13 | 3.363 (8) |
U1—O7i | 2.344 (7) | Rb1—O14 | 3.506 (9) |
U1—O6ii | 2.355 (6) | Rb1—Cr3vi | 4.116 (2) |
U1—O9ii | 2.368 (7) | K2—OW19 | 2.708 (12) |
U1—O13 | 2.385 (7) | K2—OW18 | 2.711 (11) |
U1—O15iii | 2.412 (7) | K2—O11ii | 2.740 (8) |
U1—K1ii | 4.2498 (18) | K2—O4viii | 2.781 (8) |
U1—Rb1ii | 4.2498 (18) | K2—O12vi | 2.932 (8) |
U1—Rb1 | 4.4135 (18) | K2—O16ii | 3.056 (9) |
U2—O3 | 1.766 (7) | K2—Rb1ix | 4.692 (4) |
U2—O4 | 1.768 (7) | O1—U2viii | 2.351 (7) |
U2—O8iv | 2.331 (6) | O4—K2v | 2.781 (8) |
U2—O2 | 2.332 (7) | O5—Rb1ii | 3.305 (8) |
U2—O1v | 2.351 (7) | O6—U1ii | 2.354 (6) |
U2—O10 | 2.419 (6) | O7—U1vi | 2.344 (7) |
U2—OW17 | 2.517 (7) | O8—U2iv | 2.331 (6) |
Cr1—O14 | 1.586 (8) | O9—U1ii | 2.368 (7) |
Cr1—O7 | 1.653 (7) | O11—K2ii | 2.740 (8) |
Cr1—O6 | 1.664 (6) | O12—K2i | 2.932 (8) |
Cr1—O2 | 1.670 (7) | O14—K1iv | 2.888 (8) |
Cr1—Rb1 | 3.893 (2) | O14—Rb1iv | 2.888 (8) |
Cr1—Rb1iv | 4.162 (2) | O15—U1x | 2.412 (7) |
Cr2—O12 | 1.601 (8) | O16—K2ii | 3.056 (9) |
Cr2—O10 | 1.634 (7) | O16—Rb1i | 3.069 (9) |
Cr2—O1 | 1.672 (7) | O16—K1i | 3.069 (9) |
Cr2—O9 | 1.697 (7) | OW17—H20A | 1.0000 |
Cr3—O16 | 1.575 (8) | OW17—H20B | 1.0000 |
Cr3—O15 | 1.616 (7) | OW18—K1vi | 2.878 (12) |
Cr3—O13 | 1.662 (7) | OW18—Rb1vi | 2.878 (12) |
Cr3—O8 | 1.694 (7) | OW18—HW1C | 1.0000 |
Cr3—Rb1i | 4.116 (2) | OW18—HW1D | 1.0000 |
Rb1—OW18i | 2.878 (12) | OW19—K1ix | 3.119 (14) |
Rb1—O14iv | 2.888 (8) | OW19—Rb1ix | 3.119 (14) |
Rb1—OW20 | 2.965 (9) | OW19—HW1E | 1.0000 |
Rb1—O6 | 2.982 (8) | OW19—HW1F | 1.0000 |
Rb1—O16vi | 3.069 (9) | OW20—HW1A | 1.0000 |
Rb1—OW19vii | 3.119 (14) | OW20—HW1B | 1.0000 |
Rb1—O5 | 3.263 (8) | | |
| | | |
O11—U1—O5 | 179.2 (4) | O6—Rb1—O5ii | 53.75 (17) |
O11—U1—O7i | 90.9 (3) | O16vi—Rb1—O5ii | 89.9 (2) |
O5—U1—O7i | 89.4 (3) | OW19vii—Rb1—O5ii | 142.7 (3) |
O11—U1—O6ii | 94.0 (3) | O5—Rb1—O5ii | 53.4 (2) |
O5—U1—O6ii | 86.2 (3) | OW18i—Rb1—O13 | 91.1 (3) |
O7i—U1—O6ii | 141.0 (3) | O14iv—Rb1—O13 | 91.2 (2) |
O11—U1—O9ii | 90.0 (3) | OW20—Rb1—O13 | 62.1 (2) |
O5—U1—O9ii | 89.3 (3) | O6—Rb1—O13 | 146.97 (19) |
O7i—U1—O9ii | 146.7 (2) | O16vi—Rb1—O13 | 137.4 (2) |
O6ii—U1—O9ii | 72.0 (3) | OW19vii—Rb1—O13 | 86.9 (2) |
O11—U1—O13 | 90.9 (3) | O5—Rb1—O13 | 52.63 (18) |
O5—U1—O13 | 88.5 (3) | O5ii—Rb1—O13 | 104.00 (17) |
O7i—U1—O13 | 71.7 (2) | OW18i—Rb1—O14 | 75.4 (3) |
O6ii—U1—O13 | 146.7 (3) | O14iv—Rb1—O14 | 54.7 (3) |
O9ii—U1—O13 | 75.0 (2) | OW20—Rb1—O14 | 141.4 (2) |
O11—U1—O15iii | 88.5 (3) | O6—Rb1—O14 | 47.05 (18) |
O5—U1—O15iii | 92.2 (3) | O16vi—Rb1—O14 | 65.7 (2) |
O7i—U1—O15iii | 69.5 (2) | OW19vii—Rb1—O14 | 88.0 (3) |
O6ii—U1—O15iii | 72.0 (3) | O5—Rb1—O14 | 135.7 (2) |
O9ii—U1—O15iii | 143.8 (2) | O5ii—Rb1—O14 | 100.73 (18) |
O13—U1—O15iii | 141.2 (3) | O13—Rb1—O14 | 145.32 (19) |
O11—U1—K1ii | 133.4 (2) | OW18i—Rb1—Cr1 | 69.1 (2) |
O5—U1—K1ii | 47.0 (2) | O14iv—Rb1—Cr1 | 76.51 (18) |
O7i—U1—K1ii | 112.5 (2) | OW20—Rb1—Cr1 | 139.04 (16) |
O6ii—U1—K1ii | 42.68 (18) | O6—Rb1—Cr1 | 23.59 (12) |
O9ii—U1—K1ii | 90.29 (18) | O16vi—Rb1—Cr1 | 63.35 (18) |
O13—U1—K1ii | 133.83 (19) | OW19vii—Rb1—Cr1 | 105.5 (2) |
O15iii—U1—K1ii | 65.5 (2) | O5—Rb1—Cr1 | 119.10 (15) |
O11—U1—Rb1ii | 133.4 (2) | O5ii—Rb1—Cr1 | 76.83 (13) |
O5—U1—Rb1ii | 47.0 (2) | O13—Rb1—Cr1 | 158.72 (15) |
O7i—U1—Rb1ii | 112.5 (2) | O14—Rb1—Cr1 | 24.04 (13) |
O6ii—U1—Rb1ii | 42.68 (18) | OW18i—Rb1—Cr3vi | 120.3 (2) |
O9ii—U1—Rb1ii | 90.29 (18) | O14iv—Rb1—Cr3vi | 117.9 (2) |
O13—U1—Rb1ii | 133.83 (19) | OW20—Rb1—Cr3vi | 79.01 (16) |
O15iii—U1—Rb1ii | 65.5 (2) | O6—Rb1—Cr3vi | 61.28 (15) |
K1ii—U1—Rb1ii | 0.0 | O16vi—Rb1—Cr3vi | 19.05 (15) |
O11—U1—Rb1 | 139.1 (3) | OW19vii—Rb1—Cr3vi | 78.3 (2) |
O5—U1—Rb1 | 40.2 (2) | O5—Rb1—Cr3vi | 119.34 (14) |
O7i—U1—Rb1 | 82.97 (18) | O5ii—Rb1—Cr3vi | 70.80 (14) |
O6ii—U1—Rb1 | 115.79 (17) | O13—Rb1—Cr3vi | 140.81 (14) |
O9ii—U1—Rb1 | 74.80 (16) | O14—Rb1—Cr3vi | 70.80 (16) |
O13—U1—Rb1 | 48.8 (2) | Cr1—Rb1—Cr3vi | 60.04 (4) |
O15iii—U1—Rb1 | 125.8 (2) | OW19—K2—OW18 | 109.9 (3) |
K1ii—U1—Rb1 | 85.2 | OW19—K2—O11ii | 130.7 (3) |
Rb1ii—U1—Rb1 | 85.23 (4) | OW18—K2—O11ii | 74.1 (3) |
O3—U2—O4 | 179.0 (4) | OW19—K2—O4viii | 94.3 (3) |
O3—U2—O8iv | 94.0 (3) | OW18—K2—O4viii | 155.8 (3) |
O4—U2—O8iv | 86.5 (3) | O11ii—K2—O4viii | 90.3 (2) |
O3—U2—O2 | 87.9 (3) | OW19—K2—O12vi | 73.0 (3) |
O4—U2—O2 | 93.1 (3) | OW18—K2—O12vi | 75.8 (3) |
O8iv—U2—O2 | 75.0 (2) | O11ii—K2—O12vi | 146.9 (3) |
O3—U2—O1v | 86.8 (3) | O4viii—K2—O12vi | 112.9 (2) |
O4—U2—O1v | 92.5 (3) | OW19—K2—O16ii | 65.3 (3) |
O8iv—U2—O1v | 75.7 (2) | OW18—K2—O16ii | 116.8 (3) |
O2—U2—O1v | 149.8 (2) | O11ii—K2—O16ii | 69.5 (2) |
O3—U2—O10 | 94.7 (3) | O4viii—K2—O16ii | 72.6 (2) |
O4—U2—O10 | 85.4 (3) | O12vi—K2—O16ii | 138.3 (3) |
O8iv—U2—O10 | 145.0 (3) | OW19—K2—Rb1ix | 39.5 (3) |
O2—U2—O10 | 71.5 (2) | OW18—K2—Rb1ix | 94.1 (2) |
O1v—U2—O10 | 138.6 (2) | O11ii—K2—Rb1ix | 92.11 (18) |
O3—U2—OW17 | 86.0 (3) | O4viii—K2—Rb1ix | 105.07 (16) |
O4—U2—OW17 | 93.1 (3) | O12vi—K2—Rb1ix | 103.30 (18) |
O8iv—U2—OW17 | 147.9 (2) | O16ii—K2—Rb1ix | 40.10 (17) |
O2—U2—OW17 | 136.9 (2) | Cr2—O1—U2viii | 132.6 (4) |
O1v—U2—OW17 | 72.2 (2) | Cr1—O2—U2 | 137.5 (4) |
O10—U2—OW17 | 66.6 (2) | U2—O4—K2v | 167.1 (4) |
O14—Cr1—O7 | 110.1 (4) | U1—O5—Rb1 | 119.2 (3) |
O14—Cr1—O6 | 108.2 (4) | U1—O5—Rb1ii | 109.8 (3) |
O7—Cr1—O6 | 108.1 (3) | Rb1—O5—Rb1ii | 126.6 (2) |
O14—Cr1—O2 | 109.7 (4) | Cr1—O6—U1ii | 135.7 (4) |
O7—Cr1—O2 | 109.7 (4) | Cr1—O6—Rb1 | 110.6 (3) |
O6—Cr1—O2 | 111.0 (4) | U1ii—O6—Rb1 | 105.0 (2) |
O14—Cr1—Rb1 | 64.2 (3) | Cr1—O7—U1vi | 141.5 (4) |
O7—Cr1—Rb1 | 111.5 (3) | Cr3—O8—U2iv | 136.3 (4) |
O6—Cr1—Rb1 | 45.8 (3) | Cr2—O9—U1ii | 134.1 (4) |
O2—Cr1—Rb1 | 137.6 (3) | Cr2—O10—U2 | 141.9 (4) |
O14—Cr1—Rb1iv | 29.5 (3) | U1—O11—K2ii | 154.7 (4) |
O7—Cr1—Rb1iv | 115.8 (2) | Cr2—O12—K2i | 147.7 (5) |
O6—Cr1—Rb1iv | 127.0 (2) | Cr3—O13—U1 | 133.5 (4) |
O2—Cr1—Rb1iv | 81.0 (2) | Cr3—O13—Rb1 | 115.6 (3) |
Rb1—Cr1—Rb1iv | 89.77 (5) | U1—O13—Rb1 | 98.9 (2) |
O12—Cr2—O10 | 110.3 (4) | Cr1—O14—K1iv | 134.9 (5) |
O12—Cr2—O1 | 108.5 (4) | Cr1—O14—Rb1iv | 134.9 (5) |
O10—Cr2—O1 | 109.8 (4) | K1iv—O14—Rb1iv | 0.0 |
O12—Cr2—O9 | 109.1 (4) | Cr1—O14—Rb1 | 91.8 (3) |
O10—Cr2—O9 | 110.2 (4) | K1iv—O14—Rb1 | 125.3 |
O1—Cr2—O9 | 108.9 (3) | Rb1iv—O14—Rb1 | 125.3 (3) |
O16—Cr3—O15 | 109.5 (5) | Cr3—O15—U1x | 165.0 (5) |
O16—Cr3—O13 | 108.9 (4) | Cr3—O16—K2ii | 137.1 (5) |
O15—Cr3—O13 | 110.3 (4) | Cr3—O16—Rb1i | 121.5 (4) |
O16—Cr3—O8 | 110.8 (4) | K2ii—O16—Rb1i | 100.0 (2) |
O15—Cr3—O8 | 108.9 (4) | Cr3—O16—K1i | 121.5 (4) |
O13—Cr3—O8 | 108.5 (3) | K2ii—O16—K1i | 100.0 (2) |
O16—Cr3—Rb1i | 39.5 (3) | Rb1i—O16—K1i | 0.00 (6) |
O15—Cr3—Rb1i | 71.6 (3) | U2—OW17—H20A | 120.0 |
O13—Cr3—Rb1i | 134.2 (3) | U2—OW17—H20B | 120.0 |
O8—Cr3—Rb1i | 113.9 (3) | H20A—OW17—H20B | 120.0 |
OW18i—Rb1—O14iv | 74.7 (3) | K2—OW18—K1vi | 132.1 (4) |
OW18i—Rb1—OW20 | 142.4 (3) | K2—OW18—Rb1vi | 132.1 (4) |
O14iv—Rb1—OW20 | 127.6 (2) | K1vi—OW18—Rb1vi | 0.0 |
OW18i—Rb1—O6 | 59.5 (3) | K2—OW18—HW1C | 120.0 |
O14iv—Rb1—O6 | 94.8 (2) | K1vi—OW18—HW1C | 46.4 |
OW20—Rb1—O6 | 132.8 (2) | Rb1vi—OW18—HW1C | 46.4 |
OW18i—Rb1—O16vi | 131.2 (3) | K2—OW18—HW1D | 120.0 |
O14iv—Rb1—O16vi | 103.2 (2) | K1vi—OW18—HW1D | 91.1 |
OW20—Rb1—O16vi | 77.8 (2) | Rb1vi—OW18—HW1D | 91.1 |
O6—Rb1—O16vi | 72.3 (2) | HW1C—OW18—HW1D | 120.0 |
OW18i—Rb1—OW19vii | 147.5 (3) | K2—OW19—K1ix | 107.0 (4) |
O14iv—Rb1—OW19vii | 72.9 (3) | K2—OW19—Rb1ix | 107.0 (4) |
OW20—Rb1—OW19vii | 62.3 (2) | K1ix—OW19—Rb1ix | 0.0 |
O6—Rb1—OW19vii | 125.9 (3) | K2—OW19—HW1E | 120.0 |
O16vi—Rb1—OW19vii | 60.7 (3) | K1ix—OW19—HW1E | 65.6 |
OW18i—Rb1—O5 | 62.3 (2) | Rb1ix—OW19—HW1E | 65.6 |
O14iv—Rb1—O5 | 120.0 (2) | K2—OW19—HW1F | 120.0 |
OW20—Rb1—O5 | 80.2 (2) | K1ix—OW19—HW1F | 96.9 |
O6—Rb1—O5 | 97.09 (19) | Rb1ix—OW19—HW1F | 96.9 |
O16vi—Rb1—O5 | 136.4 (2) | HW1E—OW19—HW1F | 120.0 |
OW19vii—Rb1—O5 | 135.2 (3) | Rb1—OW20—HW1A | 120.0 |
OW18i—Rb1—O5ii | 69.0 (3) | Rb1—OW20—HW1B | 120.0 |
O14iv—Rb1—O5ii | 140.7 (2) | HW1A—OW20—HW1B | 120.0 |
OW20—Rb1—O5ii | 91.2 (2) | | |
Symmetry codes: (i) x, −y+5/2, z+1/2; (ii) −x, −y+2, −z; (iii) −x, y−1/2, −z+1/2; (iv) −x, −y+3, −z; (v) −x−1, y+1/2, −z−1/2; (vi) x, −y+5/2, z−1/2; (vii) −x, y+1/2, −z−1/2; (viii) −x−1, y−1/2, −z−1/2; (ix) −x, y−1/2, −z−1/2; (x) −x, y+1/2, −z+1/2. |
Crystal data top
C8H26Cr3N2O17U2 | F(000) = 1816 |
Mr = 1054.34 | Dx = 2.830 Mg m−3 |
Monoclinic, P21/c | Mo Kα radiation, λ = 0.71073 Å |
a = 11.4334 (17) Å | Cell parameters from 2570 reflections |
b = 11.5250 (13) Å | θ = 1.8–27.8° |
c = 18.790 (3) Å | µ = 14.40 mm−1 |
β = 92.427 (5)° | T = 150 K |
V = 2473.7 (6) Å3 | Plate, red |
Z = 4 | 0.26 × 0.22 × 0.19 mm |
Data collection top
Bruker Kappa APEXII DUO diffractometer | 4991 reflections with I > 2σ(I) |
Radiation source: fine-focus sealed tube | Rint = 0.046 |
π and ω scans | θmax = 28.0°, θmin = 1.8° |
Absorption correction: multi-scane (SADABS; Bruker, 2012) | h = −15→15 |
Tmin = 0.568, Tmax = 0.841 | k = −13→15 |
25245 measured reflections | l = −24→24 |
5969 independent reflections | |
Refinement top
Refinement on F2 | H-atom parameters not defined |
Least-squares matrix: full | w = 1/[σ2(Fo2) + (0.0301P)2 + 23.9724P] where P = (Fo2 + 2Fc2)/3 |
R[F2 > 2σ(F2)] = 0.033 | (Δ/σ)max = 0.001 |
wR(F2) = 0.079 | Δρmax = 4.48 e Å−3 |
S = 1.02 | Δρmin = −3.68 e Å−3 |
5969 reflections | Extinction correction: SHELXL-2014/7 (Sheldrick 2014, Fc*=kFc[1+0.001xFc2λ3/sin(2θ)]-1/4 |
290 parameters | Extinction coefficient: 0.00013 (3) |
0 restraints | |
Special details top
Geometry. All esds (except the esd in the dihedral angle between two l.s. planes)
are estimated using the full covariance matrix. The cell esds are taken
into account individually in the estimation of esds in distances, angles
and torsion angles; correlations between esds in cell parameters are only
used when they are defined by crystal symmetry. An approximate (isotropic)
treatment of cell esds is used for estimating esds involving l.s. planes. |
Fractional atomic coordinates and isotropic or equivalent isotropic displacement parameters (Å2) top | x | y | z | Uiso*/Ueq | |
U1 | 0.09219 (2) | 0.89260 (2) | 0.21220 (2) | 0.01604 (7) | |
U2 | −0.37883 (2) | 1.53968 (2) | −0.22896 (2) | 0.02376 (8) | |
Cr1 | −0.09064 (9) | 1.43573 (9) | −0.15778 (6) | 0.0174 (2) | |
Cr2 | −0.38934 (10) | 1.22594 (11) | −0.17230 (6) | 0.0248 (3) | |
Cr3 | 0.16222 (9) | 1.21500 (9) | 0.20288 (6) | 0.0182 (2) | |
O1 | −0.5130 (5) | 1.1708 (6) | −0.2023 (4) | 0.057 (2) | |
O2 | −0.2205 (4) | 1.5011 (4) | −0.1463 (3) | 0.0241 (11) | |
O3 | −0.2864 (5) | 1.5263 (5) | −0.3034 (3) | 0.0359 (13) | |
O4 | −0.4687 (5) | 1.5540 (6) | −0.1565 (4) | 0.0453 (16) | |
O5 | 0.0309 (4) | 0.9399 (4) | 0.1286 (3) | 0.0252 (11) | |
O6 | −0.1077 (5) | 1.2938 (4) | −0.1619 (3) | 0.0286 (12) | |
O7 | −0.0386 (4) | 1.4812 (5) | −0.2337 (3) | 0.0270 (11) | |
O8 | 0.2928 (4) | 1.2791 (4) | 0.2032 (3) | 0.0257 (11) | |
O9 | −0.2836 (4) | 1.1253 (4) | −0.1720 (3) | 0.0268 (11) | |
O10 | −0.3582 (5) | 1.3373 (5) | −0.2241 (4) | 0.0449 (16) | |
O11 | 0.1492 (5) | 0.8491 (5) | 0.2974 (3) | 0.0288 (12) | |
O12 | −0.4006 (7) | 1.2754 (7) | −0.0946 (4) | 0.063 (2) | |
O13 | 0.1823 (4) | 1.0768 (4) | 0.2257 (3) | 0.0261 (11) | |
O14 | −0.0045 (5) | 1.4702 (5) | −0.0913 (3) | 0.0340 (13) | |
O15 | 0.0771 (5) | 1.2812 (5) | 0.2591 (3) | 0.0300 (12) | |
O16 | 0.1005 (5) | 1.2208 (5) | 0.1242 (3) | 0.0369 (14) | |
OW17 | −0.5512 (5) | 1.4372 (6) | −0.2916 (4) | 0.0506 (18) | |
N1 | −0.1470 (6) | 1.3657 (6) | −0.3763 (3) | 0.0298 (14) | |
N2 | −0.1723 (6) | 1.6213 (6) | −0.0140 (4) | 0.0346 (16) | |
C1 | 0.2198 (7) | 0.6665 (8) | 0.4438 (4) | 0.0314 (17) | |
C2 | −0.1491 (9) | 1.2576 (9) | 0.0167 (5) | 0.047 (2) | |
C3 | 0.3347 (8) | 0.7183 (10) | 0.4181 (5) | 0.050 (3) | |
C4 | −0.2387 (12) | 1.0565 (10) | 0.0122 (6) | 0.063 (3) | |
C5 | 0.2723 (8) | 1.3355 (8) | −0.0300 (4) | 0.0367 (19) | |
C6 | −0.3509 (9) | 1.7395 (11) | −0.0185 (6) | 0.061 (3) | |
C7 | 0.2170 (13) | 1.2638 (13) | −0.0894 (7) | 0.093 (6) | |
C8 | 0.3337 (15) | 1.4440 (14) | −0.0523 (12) | 0.131 (8) | |
Atomic displacement parameters (Å2) top | U11 | U22 | U33 | U12 | U13 | U23 |
U1 | 0.01613 (12) | 0.01403 (12) | 0.01808 (12) | 0.00049 (9) | 0.00198 (8) | 0.00075 (9) |
U2 | 0.01532 (13) | 0.01649 (14) | 0.03937 (17) | 0.00019 (10) | 0.00018 (10) | −0.00334 (11) |
Cr1 | 0.0175 (5) | 0.0151 (5) | 0.0195 (5) | 0.0011 (4) | 0.0018 (4) | −0.0006 (4) |
Cr2 | 0.0196 (6) | 0.0271 (6) | 0.0273 (6) | 0.0054 (5) | −0.0031 (4) | −0.0047 (5) |
Cr3 | 0.0149 (5) | 0.0152 (5) | 0.0244 (6) | −0.0010 (4) | 0.0014 (4) | 0.0012 (4) |
O1 | 0.026 (3) | 0.030 (4) | 0.113 (6) | −0.004 (3) | −0.026 (3) | −0.008 (4) |
O2 | 0.023 (3) | 0.025 (3) | 0.025 (3) | 0.003 (2) | 0.005 (2) | 0.000 (2) |
O3 | 0.035 (3) | 0.035 (3) | 0.037 (3) | 0.005 (3) | 0.004 (2) | −0.009 (3) |
O4 | 0.032 (3) | 0.047 (4) | 0.059 (4) | −0.010 (3) | 0.023 (3) | −0.003 (3) |
O5 | 0.027 (3) | 0.026 (3) | 0.023 (3) | 0.001 (2) | −0.001 (2) | −0.001 (2) |
O6 | 0.029 (3) | 0.019 (3) | 0.038 (3) | 0.002 (2) | 0.011 (2) | −0.003 (2) |
O7 | 0.024 (3) | 0.025 (3) | 0.032 (3) | −0.001 (2) | 0.010 (2) | 0.006 (2) |
O8 | 0.021 (2) | 0.017 (3) | 0.040 (3) | −0.005 (2) | 0.007 (2) | −0.004 (2) |
O9 | 0.021 (3) | 0.022 (3) | 0.038 (3) | 0.006 (2) | 0.005 (2) | 0.002 (2) |
O10 | 0.044 (4) | 0.024 (3) | 0.066 (4) | 0.002 (3) | −0.006 (3) | 0.001 (3) |
O11 | 0.028 (3) | 0.033 (3) | 0.025 (3) | 0.001 (2) | −0.003 (2) | 0.004 (2) |
O12 | 0.072 (5) | 0.080 (6) | 0.036 (4) | 0.027 (4) | 0.000 (3) | −0.012 (4) |
O13 | 0.023 (3) | 0.015 (3) | 0.040 (3) | 0.000 (2) | −0.001 (2) | −0.002 (2) |
O14 | 0.031 (3) | 0.035 (3) | 0.035 (3) | 0.006 (2) | −0.010 (2) | −0.007 (2) |
O15 | 0.025 (3) | 0.026 (3) | 0.040 (3) | 0.008 (2) | 0.013 (2) | 0.004 (2) |
O16 | 0.033 (3) | 0.047 (4) | 0.030 (3) | −0.007 (3) | −0.006 (2) | 0.006 (3) |
OW17 | 0.028 (3) | 0.033 (4) | 0.089 (5) | −0.009 (3) | −0.013 (3) | −0.012 (3) |
N1 | 0.030 (3) | 0.031 (4) | 0.027 (3) | 0.001 (3) | −0.003 (3) | −0.004 (3) |
N2 | 0.033 (4) | 0.043 (4) | 0.028 (4) | 0.011 (3) | 0.009 (3) | −0.003 (3) |
C1 | 0.027 (4) | 0.038 (5) | 0.029 (4) | 0.003 (3) | −0.004 (3) | −0.005 (3) |
C2 | 0.049 (6) | 0.052 (6) | 0.040 (5) | −0.013 (5) | −0.001 (4) | 0.017 (4) |
C3 | 0.035 (5) | 0.068 (7) | 0.045 (5) | −0.007 (5) | −0.007 (4) | −0.015 (5) |
C4 | 0.088 (9) | 0.054 (7) | 0.045 (6) | −0.016 (6) | −0.011 (6) | −0.011 (5) |
C5 | 0.038 (5) | 0.042 (5) | 0.031 (4) | 0.013 (4) | 0.010 (3) | −0.005 (4) |
C6 | 0.041 (6) | 0.084 (9) | 0.057 (7) | 0.031 (6) | −0.010 (5) | −0.008 (6) |
C7 | 0.099 (10) | 0.110 (11) | 0.067 (8) | 0.066 (9) | −0.037 (7) | −0.060 (8) |
C8 | 0.105 (12) | 0.076 (11) | 0.22 (2) | 0.001 (9) | 0.105 (14) | 0.065 (12) |
Geometric parameters (Å, º) top
U1—O11 | 1.775 (5) | N1—O5vii | 3.024 (8) |
U1—O5 | 1.778 (5) | N1—U1vii | 4.197 (7) |
U1—O7i | 2.348 (5) | N2—C5v | 1.523 (10) |
U1—O9ii | 2.354 (5) | N2—C8v | 2.391 (14) |
U1—O6ii | 2.357 (5) | N2—C7v | 2.424 (12) |
U1—O13 | 2.368 (5) | N2—C6 | 2.454 (12) |
U1—O15iii | 2.403 (5) | N2—O16v | 2.901 (9) |
U1—N1i | 4.197 (7) | N2—O14v | 2.962 (9) |
U2—O4 | 1.747 (6) | N2—C2v | 3.933 (12) |
U2—O3 | 1.796 (6) | N2—C2 | 4.237 (12) |
U2—O1iv | 2.312 (6) | C1—C4iii | 1.524 (13) |
U2—O10 | 2.345 (6) | C1—N1ii | 1.532 (10) |
U2—O8v | 2.350 (5) | C1—C2iii | 1.536 (12) |
U2—O2 | 2.377 (5) | C1—C3 | 1.540 (13) |
U2—OW17 | 2.543 (6) | C2—C1viii | 1.536 (12) |
Cr1—O14 | 1.608 (5) | C2—N1i | 2.462 (11) |
Cr1—O6 | 1.649 (5) | C2—C4 | 2.535 (15) |
Cr1—O7 | 1.654 (5) | C2—C3viii | 2.537 (14) |
Cr1—O2 | 1.686 (5) | C2—N2v | 3.933 (12) |
Cr1—N2 | 3.600 (7) | C2—C8v | 4.10 (2) |
Cr2—O12 | 1.577 (7) | C3—N1ii | 2.453 (11) |
Cr2—O1 | 1.629 (6) | C3—C2iii | 2.537 (14) |
Cr2—O10 | 1.659 (6) | C3—C4iii | 2.554 (17) |
Cr2—O9 | 1.675 (5) | C3—C6ix | 3.769 (13) |
Cr3—O16 | 1.612 (6) | C3—C8i | 3.932 (19) |
Cr3—O15 | 1.653 (5) | C4—C1viii | 1.524 (13) |
Cr3—O13 | 1.663 (5) | C4—N1i | 2.471 (12) |
Cr3—O8 | 1.665 (5) | C4—C3viii | 2.554 (17) |
O1—U2vi | 2.312 (6) | C4—C6x | 3.906 (17) |
O2—N2 | 2.879 (9) | C4—C7ii | 3.97 (2) |
O3—N1 | 2.833 (9) | C5—C8 | 1.502 (16) |
O5—N1i | 3.024 (8) | C5—C7 | 1.506 (14) |
O6—U1ii | 2.357 (5) | C5—N2v | 1.523 (10) |
O7—U1vii | 2.348 (5) | C5—C6v | 1.523 (13) |
O8—U2v | 2.350 (5) | C6—C5v | 1.523 (13) |
O9—U1ii | 2.354 (5) | C6—C7v | 2.489 (15) |
O11—N1ii | 2.887 (9) | C6—C8v | 2.502 (19) |
O14—N2v | 2.962 (9) | C6—C3xi | 3.769 (13) |
O14—N2 | 3.009 (9) | C6—C4xii | 3.906 (17) |
O15—U1viii | 2.403 (5) | C7—N2v | 2.424 (12) |
O16—N2v | 2.901 (9) | C7—C6v | 2.489 (15) |
O16—N1i | 3.001 (9) | C7—C8 | 2.55 (2) |
N1—C1ii | 1.533 (10) | C7—C4ii | 3.97 (2) |
N1—C3ii | 2.453 (11) | C8—N2v | 2.391 (14) |
N1—C2vii | 2.462 (11) | C8—C6v | 2.502 (19) |
N1—C4vii | 2.471 (12) | C8—C3vii | 3.932 (19) |
N1—O11ii | 2.887 (9) | C8—C2v | 4.10 (2) |
N1—O16vii | 3.001 (9) | C8—C8xiii | 4.40 (4) |
| | | |
O11—U1—O5 | 177.6 (2) | O2—N2—O14v | 120.4 (3) |
O11—U1—O7i | 90.1 (2) | O16v—N2—O14v | 119.6 (3) |
O5—U1—O7i | 87.6 (2) | C5v—N2—O14 | 163.7 (6) |
O11—U1—O9ii | 87.3 (2) | C8v—N2—O14 | 126.2 (5) |
O5—U1—O9ii | 94.7 (2) | C7v—N2—O14 | 149.7 (4) |
O7i—U1—O9ii | 144.18 (18) | C6—N2—O14 | 148.4 (4) |
O11—U1—O6ii | 94.2 (2) | O2—N2—O14 | 53.67 (18) |
O5—U1—O6ii | 87.6 (2) | O16v—N2—O14 | 79.2 (2) |
O7i—U1—O6ii | 142.98 (18) | O14v—N2—O14 | 71.6 (2) |
O9ii—U1—O6ii | 72.82 (18) | C5v—N2—Cr1 | 145.7 (5) |
O11—U1—O13 | 90.9 (2) | C8v—N2—Cr1 | 115.7 (6) |
O5—U1—O13 | 88.4 (2) | C7v—N2—Cr1 | 175.2 (4) |
O7i—U1—O13 | 71.38 (18) | C6—N2—Cr1 | 123.1 (4) |
O9ii—U1—O13 | 72.95 (18) | O2—N2—Cr1 | 27.40 (11) |
O6ii—U1—O13 | 145.09 (18) | O16v—N2—Cr1 | 75.32 (19) |
O11—U1—O15iii | 85.2 (2) | O14v—N2—Cr1 | 95.6 (2) |
O5—U1—O15iii | 94.0 (2) | O14—N2—Cr1 | 26.27 (12) |
O7i—U1—O15iii | 72.55 (18) | C5v—N2—C2v | 127.9 (5) |
O9ii—U1—O15iii | 142.53 (18) | C8v—N2—C2v | 149.4 (7) |
O6ii—U1—O15iii | 71.21 (18) | C7v—N2—C2v | 92.6 (5) |
O13—U1—O15iii | 143.69 (18) | C6—N2—C2v | 125.4 (4) |
O11—U1—N1i | 138.9 (2) | O2—N2—C2v | 107.7 (3) |
O5—U1—N1i | 38.79 (19) | O16v—N2—C2v | 58.4 (2) |
O7i—U1—N1i | 49.03 (16) | O14v—N2—C2v | 61.5 (2) |
O9ii—U1—N1i | 122.02 (15) | O14—N2—C2v | 65.4 (2) |
O6ii—U1—N1i | 120.31 (16) | Cr1—N2—C2v | 85.9 (2) |
O13—U1—N1i | 73.78 (15) | C5v—N2—C2 | 107.1 (5) |
O15iii—U1—N1i | 85.74 (16) | C8v—N2—C2 | 70.3 (4) |
O4—U2—O3 | 179.5 (3) | C7v—N2—C2 | 116.4 (5) |
O4—U2—O1iv | 93.1 (3) | C6—N2—C2 | 127.0 (4) |
O3—U2—O1iv | 86.5 (3) | O2—N2—C2 | 69.5 (2) |
O4—U2—O10 | 97.2 (3) | O16v—N2—C2 | 134.4 (3) |
O3—U2—O10 | 83.3 (3) | O14v—N2—C2 | 61.3 (2) |
O1iv—U2—O10 | 136.2 (2) | O14—N2—C2 | 57.0 (2) |
O4—U2—O8v | 90.6 (2) | Cr1—N2—C2 | 59.85 (17) |
O3—U2—O8v | 88.9 (2) | C2v—N2—C2 | 107.4 (2) |
O1iv—U2—O8v | 75.1 (2) | C4iii—C1—N1ii | 107.9 (7) |
O10—U2—O8v | 146.6 (2) | C4iii—C1—C2iii | 111.8 (8) |
O4—U2—O2 | 88.0 (3) | N1ii—C1—C2iii | 106.7 (6) |
O3—U2—O2 | 92.1 (2) | C4iii—C1—C3 | 112.9 (8) |
O1iv—U2—O2 | 149.5 (2) | N1ii—C1—C3 | 106.0 (7) |
O10—U2—O2 | 73.5 (2) | C2iii—C1—C3 | 111.1 (8) |
O8v—U2—O2 | 74.42 (18) | C1viii—C2—N1i | 36.6 (4) |
O4—U2—OW17 | 86.3 (3) | C1viii—C2—C4 | 33.9 (5) |
O3—U2—OW17 | 94.0 (3) | N1i—C2—C4 | 59.3 (4) |
O1iv—U2—OW17 | 70.1 (2) | C1viii—C2—C3viii | 34.5 (5) |
O10—U2—OW17 | 68.3 (2) | N1i—C2—C3viii | 58.8 (3) |
O8v—U2—OW17 | 144.8 (2) | C4—C2—C3viii | 60.5 (4) |
O2—U2—OW17 | 140.3 (2) | C1viii—C2—N2v | 139.4 (6) |
O14—Cr1—O6 | 110.4 (3) | N1i—C2—N2v | 103.8 (3) |
O14—Cr1—O7 | 111.2 (3) | C4—C2—N2v | 134.5 (5) |
O6—Cr1—O7 | 108.7 (3) | C3viii—C2—N2v | 150.6 (4) |
O14—Cr1—O2 | 107.7 (3) | C1viii—C2—C8v | 102.1 (6) |
O6—Cr1—O2 | 110.2 (3) | N1i—C2—C8v | 109.8 (4) |
O7—Cr1—O2 | 108.6 (3) | C4—C2—C8v | 124.2 (5) |
O14—Cr1—N2 | 55.9 (2) | C3viii—C2—C8v | 67.9 (4) |
O6—Cr1—N2 | 126.2 (2) | N2v—C2—C8v | 101.1 (3) |
O7—Cr1—N2 | 125.0 (2) | C1viii—C2—N2 | 135.3 (6) |
O2—Cr1—N2 | 51.8 (2) | N1i—C2—N2 | 132.9 (4) |
O12—Cr2—O1 | 111.0 (4) | C4—C2—N2 | 151.3 (5) |
O12—Cr2—O10 | 106.9 (4) | C3viii—C2—N2 | 101.2 (4) |
O1—Cr2—O10 | 107.6 (4) | N2v—C2—N2 | 72.6 (2) |
O12—Cr2—O9 | 109.6 (3) | C8v—C2—N2 | 33.3 (2) |
O1—Cr2—O9 | 110.3 (3) | C1—C3—N1ii | 36.9 (4) |
O10—Cr2—O9 | 111.4 (3) | C1—C3—C2iii | 34.4 (5) |
O16—Cr3—O15 | 108.7 (3) | N1ii—C3—C2iii | 59.1 (3) |
O16—Cr3—O13 | 109.0 (3) | C1—C3—C4iii | 33.4 (5) |
O15—Cr3—O13 | 110.9 (3) | N1ii—C3—C4iii | 59.1 (4) |
O16—Cr3—O8 | 110.0 (3) | C2iii—C3—C4iii | 59.7 (4) |
O15—Cr3—O8 | 110.2 (3) | C1—C3—C6ix | 140.0 (6) |
O13—Cr3—O8 | 108.1 (3) | N1ii—C3—C6ix | 164.1 (5) |
Cr2—O1—U2vi | 152.2 (4) | C2iii—C3—C6ix | 129.1 (4) |
Cr1—O2—U2 | 130.6 (3) | C4iii—C3—C6ix | 110.9 (5) |
Cr1—O2—N2 | 100.8 (3) | C1—C3—C8i | 109.4 (6) |
U2—O2—N2 | 125.9 (2) | N1ii—C3—C8i | 115.3 (5) |
U2—O3—N1 | 142.6 (3) | C2iii—C3—C8i | 75.3 (4) |
U1—O5—N1i | 119.6 (3) | C4iii—C3—C8i | 130.3 (5) |
Cr1—O6—U1ii | 155.8 (3) | C6ix—C3—C8i | 80.6 (4) |
Cr1—O7—U1vii | 146.0 (3) | C1viii—C4—N1i | 36.2 (4) |
Cr3—O8—U2v | 139.7 (3) | C1viii—C4—C2 | 34.2 (5) |
Cr2—O9—U1ii | 137.8 (3) | N1i—C4—C2 | 58.9 (3) |
Cr2—O10—U2 | 140.2 (4) | C1viii—C4—C3viii | 33.7 (5) |
U1—O11—N1ii | 134.0 (3) | N1i—C4—C3viii | 58.4 (4) |
Cr3—O13—U1 | 141.0 (3) | C2—C4—C3viii | 59.8 (4) |
Cr1—O14—N2v | 144.0 (3) | C1viii—C4—C6x | 153.6 (7) |
Cr1—O14—N2 | 97.8 (3) | N1i—C4—C6x | 126.1 (5) |
N2v—O14—N2 | 108.4 (2) | C2—C4—C6x | 171.9 (5) |
Cr3—O15—U1viii | 153.0 (3) | C3viii—C4—C6x | 127.8 (5) |
Cr3—O16—N2v | 123.7 (3) | C1viii—C4—C7ii | 124.7 (6) |
Cr3—O16—N1i | 111.4 (3) | N1i—C4—C7ii | 90.6 (4) |
N2v—O16—N1i | 120.1 (3) | C2—C4—C7ii | 145.0 (5) |
C1ii—N1—C3ii | 37.1 (4) | C3viii—C4—C7ii | 120.9 (5) |
C1ii—N1—C2vii | 36.7 (4) | C6x—C4—C7ii | 36.8 (2) |
C3ii—N1—C2vii | 62.1 (4) | C8—C5—C7 | 115.9 (13) |
C1ii—N1—C4vii | 35.9 (5) | C8—C5—N2v | 104.5 (9) |
C3ii—N1—C4vii | 62.5 (4) | C7—C5—N2v | 106.3 (8) |
C2vii—N1—C4vii | 61.8 (4) | C8—C5—C6v | 111.6 (11) |
C1ii—N1—O3 | 105.2 (5) | C7—C5—C6v | 110.5 (9) |
C3ii—N1—O3 | 84.8 (3) | N2v—C5—C6v | 107.3 (7) |
C2vii—N1—O3 | 141.8 (4) | C5v—C6—N2 | 36.3 (4) |
C4vii—N1—O3 | 86.9 (4) | C5v—C6—C7v | 34.5 (5) |
C1ii—N1—O11ii | 101.6 (5) | N2—C6—C7v | 58.7 (4) |
C3ii—N1—O11ii | 78.4 (3) | C5v—C6—C8v | 33.9 (7) |
C2vii—N1—O11ii | 85.7 (3) | N2—C6—C8v | 57.7 (4) |
C4vii—N1—O11ii | 137.2 (4) | C7v—C6—C8v | 61.4 (7) |
O3—N1—O11ii | 107.1 (3) | C5v—C6—C3xi | 142.5 (8) |
C1ii—N1—O16vii | 113.7 (5) | N2—C6—C3xi | 149.7 (5) |
C3ii—N1—O16vii | 133.0 (4) | C7v—C6—C3xi | 143.6 (5) |
C2vii—N1—O16vii | 77.7 (3) | C8v—C6—C3xi | 109.2 (6) |
C4vii—N1—O16vii | 119.3 (4) | C5v—C6—C4xii | 105.1 (7) |
O3—N1—O16vii | 139.9 (3) | N2—C6—C4xii | 104.3 (5) |
O11ii—N1—O16vii | 75.0 (2) | C7v—C6—C4xii | 73.0 (5) |
C1ii—N1—O5vii | 123.1 (5) | C8v—C6—C4xii | 134.0 (7) |
C3ii—N1—O5vii | 151.7 (4) | C3xi—C6—C4xii | 103.2 (4) |
C2vii—N1—O5vii | 115.8 (4) | C5—C7—N2v | 37.1 (4) |
C4vii—N1—O5vii | 91.0 (4) | C5—C7—C6v | 35.0 (5) |
O3—N1—O5vii | 83.8 (2) | N2v—C7—C6v | 59.9 (4) |
O11ii—N1—O5vii | 129.8 (3) | C5—C7—C8 | 32.0 (7) |
O16vii—N1—O5vii | 67.2 (2) | N2v—C7—C8 | 57.4 (5) |
C1ii—N1—U1vii | 144.1 (5) | C6v—C7—C8 | 59.5 (6) |
C3ii—N1—U1vii | 159.3 (4) | C5—C7—C4ii | 102.8 (8) |
C2vii—N1—U1vii | 133.7 (3) | N2v—C7—C4ii | 103.1 (6) |
C4vii—N1—U1vii | 109.9 (4) | C6v—C7—C4ii | 70.2 (5) |
O3—N1—U1vii | 75.25 (18) | C8—C7—C4ii | 129.3 (6) |
O11ii—N1—U1vii | 112.7 (2) | C5—C8—N2v | 38.1 (5) |
O16vii—N1—U1vii | 67.70 (17) | C5—C8—C6v | 34.5 (6) |
O5vii—N1—U1vii | 21.61 (11) | N2v—C8—C6v | 60.1 (4) |
C5v—N2—C8v | 37.5 (6) | C5—C8—C7 | 32.1 (7) |
C5v—N2—C7v | 36.6 (5) | N2v—C8—C7 | 58.6 (5) |
C8v—N2—C7v | 64.0 (7) | C6v—C8—C7 | 59.0 (5) |
C5v—N2—C6 | 36.3 (5) | C5—C8—C3vii | 150.2 (9) |
C8v—N2—C6 | 62.2 (5) | N2v—C8—C3vii | 113.1 (6) |
C7v—N2—C6 | 61.4 (4) | C6v—C8—C3vii | 155.7 (9) |
C5v—N2—O2 | 120.4 (5) | C7—C8—C3vii | 140.5 (8) |
C8v—N2—O2 | 100.0 (6) | C5—C8—C2v | 113.7 (8) |
C7v—N2—O2 | 156.4 (4) | N2v—C8—C2v | 76.4 (5) |
C6—N2—O2 | 96.3 (4) | C6v—C8—C2v | 130.6 (6) |
C5v—N2—O16v | 115.1 (5) | C7—C8—C2v | 117.4 (6) |
C8v—N2—O16v | 144.8 (5) | C3vii—C8—C2v | 36.7 (2) |
C7v—N2—O16v | 107.8 (5) | C5—C8—C8xiii | 121.7 (12) |
C6—N2—O16v | 83.5 (4) | N2v—C8—C8xiii | 122.1 (10) |
O2—N2—O16v | 74.6 (2) | C6v—C8—C8xiii | 87.9 (8) |
C5v—N2—O14v | 105.1 (5) | C7—C8—C8xiii | 142.5 (8) |
C8v—N2—O14v | 93.4 (6) | C3vii—C8—C8xiii | 76.4 (4) |
C7v—N2—O14v | 79.6 (4) | C2v—C8—C8xiii | 97.0 (6) |
C6—N2—O14v | 139.8 (4) | | |
Symmetry codes: (i) x, −y+5/2, z+1/2; (ii) −x, −y+2, −z; (iii) −x, y−1/2, −z+1/2; (iv) −x−1, y+1/2, −z−1/2; (v) −x, −y+3, −z; (vi) −x−1, y−1/2, −z−1/2; (vii) x, −y+5/2, z−1/2; (viii) −x, y+1/2, −z+1/2; (ix) x+1, −y+5/2, z+1/2; (x) x, y−1, z; (xi) x−1, −y+5/2, z−1/2; (xii) x, y+1, z; (xiii) −x+1, −y+3, −z. |
Crystal data top
C8H38Cr6N4O35U4 | Dx = 3.282 Mg m−3 |
Mr = 2014.54 | Mo Kα radiation, λ = 0.71073 Å |
Orthorhombic, P212121 | Cell parameters from 2540 reflections |
a = 11.1281 (10) Å | θ = 1.2–27.8° |
b = 11.152 (1) Å | µ = 17.47 mm−1 |
c = 32.850 (3) Å | T = 150 K |
V = 4076.7 (6) Å3 | Plate, red |
Z = 4 | 0.25 × 0.20 × 0.17 mm |
F(000) = 3624 | |
Data collection top
Bruker Kappa APEXII DUO diffractometer | 7726 reflections with I > 2σ(I) |
Radiation source: fine-focus sealed tube | Rint = 0.054 |
π and ω scans | θmax = 28.0°, θmin = 1.2° |
Absorption correction: multi-scan (SADABS; Bruker, 2012) | h = −11→14 |
Tmin = 0.640, Tmax = 0.746 | k = −14→6 |
16152 measured reflections | l = −43→33 |
8521 independent reflections | |
Refinement top
Refinement on F2 | H-atom parameters not refined |
Least-squares matrix: full | w = 1/[σ2(Fo2) + 85.643P] where P = (Fo2 + 2Fc2)/3 |
R[F2 > 2σ(F2)] = 0.049 | (Δ/σ)max = 0.005 |
wR(F2) = 0.111 | Δρmax = 2.99 e Å−3 |
S = 1.07 | Δρmin = −2.27 e Å−3 |
8521 reflections | Extinction correction: SHELXL-2014/7 (Sheldrick 2014, Fc*=kFc[1+0.001xFc2λ3/sin(2θ)]-1/4 |
281 parameters | Extinction coefficient: 0.00012 (3) |
0 restraints | Absolute structure: Refined as an inversion twin. |
Hydrogen site location: inferred from neighbouring sites | Absolute structure parameter: 0.395 (13) |
Special details top
Geometry. All esds (except the esd in the dihedral angle between two l.s. planes)
are estimated using the full covariance matrix. The cell esds are taken
into account individually in the estimation of esds in distances, angles
and torsion angles; correlations between esds in cell parameters are only
used when they are defined by crystal symmetry. An approximate (isotropic)
treatment of cell esds is used for estimating esds involving l.s. planes. |
Refinement. Refined as a 2-component inversion twin. |
Fractional atomic coordinates and isotropic or equivalent isotropic displacement parameters (Å2) top | x | y | z | Uiso*/Ueq | |
U1 | 0.79273 (6) | 0.34185 (6) | 0.02681 (2) | 0.00768 (16) | |
U2 | 0.87286 (6) | 0.86690 (6) | −0.00050 (3) | 0.00959 (17) | |
U3 | 0.04887 (6) | −0.11194 (6) | 0.21643 (2) | 0.00715 (16) | |
U4 | 0.46409 (6) | 0.18507 (6) | 0.23093 (3) | 0.00819 (17) | |
Cr1 | 0.9574 (3) | 1.1516 (3) | −0.05072 (11) | 0.0094 (6) | |
Cr2 | 0.6725 (2) | 0.6449 (3) | 0.05160 (11) | 0.0086 (7) | |
Cr3 | 0.6217 (3) | 1.0713 (3) | −0.02092 (12) | 0.0131 (7) | |
Cr4 | 0.3835 (3) | −0.1141 (3) | 0.18602 (11) | 0.0087 (7) | |
Cr5 | 0.2004 (3) | −0.3741 (2) | 0.26527 (11) | 0.0097 (7) | |
Cr6 | 0.1263 (3) | 0.2152 (3) | 0.20220 (11) | 0.0096 (7) | |
O1 | 0.7422 (11) | 0.7758 (12) | 0.0466 (5) | 0.009 (3)* | |
O2 | 0.8997 (12) | 1.0093 (12) | −0.0515 (5) | 0.011 (3)* | |
O3 | 0.8535 (12) | 0.7573 (12) | −0.0382 (5) | 0.014 (3)* | |
O4 | 0.8906 (11) | 0.9734 (11) | 0.0377 (4) | 0.007 (3)* | |
O5 | 0.7385 (12) | 0.3940 (13) | −0.0212 (5) | 0.015 (3)* | |
O6 | 1.1051 (12) | 1.1439 (12) | −0.0589 (5) | 0.013 (3)* | |
O7 | 0.9282 (11) | 1.2133 (11) | −0.0069 (5) | 0.010 (3)* | |
O8 | 0.6775 (12) | 0.9317 (12) | −0.0176 (5) | 0.015 (3)* | |
O9 | 0.7796 (12) | 0.5407 (11) | 0.0536 (5) | 0.008 (3)* | |
O10 | 0.5830 (12) | 0.6251 (13) | 0.0121 (5) | 0.017 (3)* | |
O11 | 0.8521 (13) | 0.2929 (13) | 0.0744 (5) | 0.016 (3)* | |
O12 | 0.5951 (11) | 0.6454 (12) | 0.0931 (5) | 0.010 (3)* | |
O13 | 0.4741 (11) | 1.0584 (11) | −0.0124 (5) | 0.008 (3)* | |
O14 | 0.8961 (13) | 1.2274 (13) | −0.0862 (5) | 0.018 (3)* | |
O15 | 0.6866 (11) | 1.1617 (11) | 0.0123 (5) | 0.010 (3)* | |
O16 | 0.6418 (14) | 1.1201 (15) | −0.0658 (6) | 0.026 (4)* | |
OW17 | 0.9777 (13) | 0.7048 (13) | 0.0396 (5) | 0.017 (3)* | |
HW3C | 0.9805 | 0.7276 | 0.0690 | 0.020* | |
HW3D | 1.0622 | 0.6957 | 0.0297 | 0.020* | |
O18 | 0.0640 (11) | 0.0839 (11) | 0.1894 (5) | 0.008 (3)* | |
O19 | 0.2748 (13) | 0.1974 (13) | 0.2011 (5) | 0.017 (3)* | |
O20 | 0.1294 (12) | −0.5034 (11) | 0.2682 (5) | 0.010 (3)* | |
O21 | 0.1100 (13) | −0.0633 (12) | 0.2632 (5) | 0.016 (3)* | |
O22 | 0.5182 (13) | 0.2724 (13) | 0.1903 (5) | 0.017 (3)* | |
O23 | 0.4093 (12) | 0.0962 (12) | 0.2714 (5) | 0.015 (3)* | |
O24 | 0.1525 (11) | −0.2983 (11) | 0.2255 (5) | 0.008 (3)* | |
O25 | 0.1790 (12) | −0.2987 (12) | 0.3056 (5) | 0.012 (3)* | |
O26 | −0.0140 (13) | −0.1620 (13) | 0.1701 (5) | 0.018 (3)* | |
O27 | 0.2353 (11) | −0.0886 (11) | 0.1829 (5) | 0.008 (3)* | |
O28 | 0.4562 (13) | 0.0171 (12) | 0.1880 (5) | 0.012 (3)* | |
O29 | 0.3482 (11) | −0.4081 (11) | 0.2617 (4) | 0.007 (3)* | |
O30 | 0.4141 (13) | −0.1931 (13) | 0.2262 (6) | 0.021 (4)* | |
O31 | 0.0882 (13) | 0.2569 (13) | 0.2480 (6) | 0.019 (3)* | |
O32 | 0.0851 (13) | 0.3163 (14) | 0.1699 (5) | 0.018 (3)* | |
O33 | 0.4278 (13) | −0.1835 (14) | 0.1463 (5) | 0.021 (4)* | |
OW34 | 0.3449 (12) | 0.3474 (12) | 0.2633 (5) | 0.013 (3)* | |
HW3A | 0.3677 | 0.4265 | 0.2513 | 0.016* | |
HW3B | 0.3622 | 0.3500 | 0.2932 | 0.016* | |
OW35 | 0.439 (3) | 0.968 (3) | 0.0706 (10) | 0.079 (8)* | |
HW3E | 0.4333 | 1.0452 | 0.0555 | 0.094* | |
HW3F | 0.3627 | 0.9563 | 0.0863 | 0.094* | |
C1 | 0.5671 (19) | 0.3733 (19) | −0.0942 (8) | 0.018 (5)* | |
H1A | 0.5050 | 0.4245 | −0.0807 | 0.022* | |
H1B | 0.5907 | 0.3066 | −0.0755 | 0.022* | |
H1C | 0.5334 | 0.3390 | −0.1199 | 0.022* | |
C2 | 0.279 (2) | −0.069 (2) | 0.3483 (8) | 0.022 (5)* | |
H2A | 0.3084 | −0.0561 | 0.3198 | 0.027* | |
H2B | 0.3055 | −0.1496 | 0.3581 | 0.027* | |
H2C | 0.3135 | −0.0054 | 0.3664 | 0.027* | |
C3 | 0.724 (3) | 0.906 (4) | 0.1361 (13) | 0.060 (10)* | |
H3A | 0.7966 | 0.9592 | 0.1381 | 0.072* | |
H3B | 0.7416 | 0.8385 | 0.1169 | 0.072* | |
H3C | 0.7048 | 0.8732 | 0.1636 | 0.072* | |
C4 | 0.709 (2) | 0.889 (2) | −0.1258 (9) | 0.027 (5)* | |
H4A | 0.6698 | 0.9323 | −0.1027 | 0.033* | |
H4B | 0.6976 | 0.8004 | −0.1222 | 0.033* | |
H4C | 0.6723 | 0.9148 | −0.1521 | 0.033* | |
C5 | 0.880 (3) | 1.003 (3) | −0.1577 (10) | 0.037 (7)* | |
H5A | 0.8255 | 0.9947 | −0.1817 | 0.044* | |
H5B | 0.9649 | 0.9863 | −0.1664 | 0.044* | |
H5C | 0.8749 | 1.0865 | −0.1467 | 0.044* | |
C6 | 0.663 (2) | 0.580 (3) | −0.0916 (10) | 0.036 (7)* | |
H6A | 0.5769 | 0.6044 | −0.0957 | 0.043* | |
H6B | 0.7159 | 0.6328 | −0.1084 | 0.043* | |
H6C | 0.6842 | 0.5895 | −0.0622 | 0.043* | |
C7 | 0.100 (2) | 0.062 (2) | 0.3460 (9) | 0.023 (5)* | |
H7A | 0.1668 | 0.1192 | 0.3530 | 0.027* | |
H7B | 0.0322 | 0.0741 | 0.3655 | 0.027* | |
H7C | 0.0722 | 0.0780 | 0.3176 | 0.027* | |
C8 | 0.686 (3) | 0.105 (4) | 0.1113 (14) | 0.066 (11)* | |
H8A | 0.7380 | 0.1303 | 0.1346 | 0.079* | |
H8B | 0.6208 | 0.1650 | 0.1071 | 0.079* | |
H8C | 0.7360 | 0.0987 | 0.0861 | 0.079* | |
N1 | 0.679 (2) | 0.450 (2) | −0.1043 (9) | 0.043 (6)* | |
H1D | 0.7499 | 0.4435 | −0.1229 | 0.051* | |
H1E | 0.6063 | 0.4222 | −0.1193 | 0.051* | |
N2 | 0.626 (4) | −0.027 (4) | 0.1215 (13) | 0.087 (12)* | |
H2D | 0.5520 | −0.0486 | 0.1371 | 0.104* | |
H2E | 0.6119 | −0.0461 | 0.0921 | 0.104* | |
N3 | 0.1446 (16) | −0.0617 (16) | 0.3491 (6) | 0.016 (4)* | |
H3D | 0.1034 | −0.1037 | 0.3721 | 0.020* | |
H3E | 0.2329 | −0.0615 | 0.3547 | 0.020* | |
N4 | 0.8450 (17) | 0.9178 (18) | −0.1262 (7) | 0.023 (4)* | |
H4D | 0.8692 | 0.9490 | −0.0988 | 0.028* | |
H4E | 0.8867 | 0.8395 | −0.1307 | 0.028* | |
Atomic displacement parameters (Å2) top | U11 | U22 | U33 | U12 | U13 | U23 |
U1 | 0.0044 (3) | 0.0088 (3) | 0.0099 (4) | 0.0003 (2) | −0.0007 (3) | −0.0012 (3) |
U2 | 0.0056 (3) | 0.0077 (3) | 0.0155 (4) | 0.0002 (2) | 0.0016 (3) | −0.0004 (3) |
U3 | 0.0035 (3) | 0.0076 (3) | 0.0103 (4) | 0.0006 (2) | 0.0002 (3) | 0.0000 (3) |
U4 | 0.0033 (3) | 0.0079 (3) | 0.0134 (4) | 0.0001 (2) | 0.0002 (3) | −0.0011 (3) |
Cr1 | 0.0043 (12) | 0.0117 (14) | 0.0122 (18) | −0.0003 (11) | 0.0004 (15) | −0.0003 (12) |
Cr2 | 0.0030 (12) | 0.0101 (14) | 0.0127 (18) | −0.0003 (10) | 0.0046 (14) | −0.0015 (13) |
Cr3 | 0.0082 (14) | 0.0137 (14) | 0.017 (2) | 0.0008 (12) | −0.0021 (16) | −0.0012 (14) |
Cr4 | 0.0033 (12) | 0.0056 (13) | 0.017 (2) | −0.0009 (11) | 0.0009 (14) | 0.0001 (12) |
Cr5 | 0.0059 (13) | 0.0032 (12) | 0.020 (2) | 0.0010 (11) | 0.0015 (15) | −0.0019 (12) |
Cr6 | 0.0040 (13) | 0.0092 (13) | 0.016 (2) | −0.0003 (11) | 0.0000 (15) | 0.0026 (12) |
Geometric parameters (Å, º) top
U1—O11 | 1.782 (16) | O15—O16 | 2.66 (2) |
U1—O5 | 1.786 (16) | O15—O6viii | 2.80 (2) |
U1—O6i | 2.344 (14) | O15—O5xi | 2.87 (2) |
U1—O13ii | 2.353 (13) | O15—O11xi | 3.11 (2) |
U1—O7iii | 2.357 (13) | O15—O7viii | 3.200 (18) |
U1—O15iii | 2.378 (13) | O15—Cr1viii | 3.526 (13) |
U1—O9 | 2.391 (13) | O16—C1xi | 3.09 (3) |
U1—O10 | 3.957 (14) | O16—O11i | 3.38 (2) |
U1—O14iii | 4.090 (17) | O16—O32ii | 3.55 (3) |
U1—O16ii | 4.113 (16) | O16—O5xi | 3.56 (2) |
U1—O7i | 4.155 (12) | O16—O7viii | 3.85 (2) |
U1—OW35ii | 4.17 (3) | OW17—O8ii | 2.79 (2) |
U2—O4 | 1.739 (13) | OW17—O10ii | 2.80 (2) |
U2—O3 | 1.752 (15) | OW17—O13ii | 3.069 (19) |
U2—O2 | 2.328 (15) | OW17—Cr3ii | 3.525 (15) |
U2—O1 | 2.354 (14) | OW17—O1ii | 4.09 (2) |
U2—O8 | 2.359 (14) | OW17—OW35ii | 4.12 (4) |
U2—O10ii | 2.371 (14) | OW17—HW3C | 1.0022 |
U2—OW17 | 2.523 (15) | OW17—HW3D | 1.0076 |
U2—O15 | 3.910 (13) | O18—O32 | 2.68 (2) |
U2—O7 | 3.918 (12) | O18—O19 | 2.693 (19) |
U2—O12ii | 3.922 (15) | O18—O27 | 2.717 (18) |
U2—O9 | 4.179 (13) | O18—O31 | 2.74 (2) |
U2—O10 | 4.224 (14) | O18—O20iv | 2.743 (19) |
U3—O21 | 1.764 (16) | O18—O26 | 2.95 (2) |
U3—O26 | 1.766 (16) | O18—O21 | 2.97 (2) |
U3—O18 | 2.364 (13) | O18—O25iv | 3.009 (18) |
U3—O27 | 2.364 (13) | O18—N1xii | 3.10 (3) |
U3—O20iv | 2.379 (13) | O18—C1xii | 3.16 (3) |
U3—O24 | 2.395 (12) | O19—O31 | 2.67 (2) |
U3—O31v | 2.415 (16) | O19—O32 | 2.70 (2) |
U3—O25 | 3.875 (15) | O19—OW34 | 2.75 (2) |
U3—O32v | 4.099 (17) | O19—O22 | 2.86 (2) |
U3—O30 | 4.176 (15) | O19—O28 | 2.88 (2) |
U3—O31 | 4.265 (15) | O19—O23 | 2.97 (2) |
U3—O19 | 4.299 (14) | O19—O27 | 3.28 (2) |
U4—O22 | 1.758 (16) | O19—O21 | 4.00 (2) |
U4—O23 | 1.767 (16) | O20—U3v | 2.379 (13) |
U4—O19 | 2.327 (15) | O20—O25 | 2.651 (19) |
U4—O29vi | 2.345 (12) | O20—O29 | 2.665 (18) |
U4—O28 | 2.347 (14) | O20—O24 | 2.695 (19) |
U4—O30vi | 2.381 (16) | O20—O18v | 2.743 (19) |
U4—OW34 | 2.484 (14) | O20—O31iii | 2.79 (2) |
U4—O25vi | 4.154 (14) | O20—OW34iii | 2.923 (18) |
U4—O30 | 4.257 (15) | O20—O21v | 2.93 (2) |
U4—O27 | 4.277 (13) | O20—O26v | 2.98 (2) |
U4—O31 | 4.295 (15) | O20—O31v | 3.818 (19) |
Cr1—O14 | 1.592 (17) | O20—O32iii | 3.84 (2) |
Cr1—O7 | 1.628 (15) | O21—N3 | 2.85 (3) |
Cr1—O6 | 1.668 (14) | O21—O20iv | 2.93 (2) |
Cr1—O2 | 1.712 (13) | O21—O24 | 2.937 (19) |
Cr1—O15vii | 3.526 (13) | O21—O27 | 3.00 (2) |
Cr1—O16 | 3.563 (16) | O21—O31v | 3.00 (2) |
Cr1—O4 | 3.597 (14) | O21—C7 | 3.06 (3) |
Cr1—O10ii | 3.618 (15) | O21—O25 | 3.07 (2) |
Cr1—O15 | 3.658 (14) | O21—O32v | 3.37 (2) |
Cr2—O12 | 1.612 (15) | O21—O26 | 3.53 (2) |
Cr2—O10 | 1.650 (16) | O22—O30vi | 2.87 (2) |
Cr2—O1 | 1.662 (13) | O22—O28 | 2.931 (19) |
Cr2—O9 | 1.666 (13) | O22—O29vi | 2.96 (2) |
Cr2—O6i | 3.315 (14) | O22—C5i | 3.13 (3) |
Cr2—OW17 | 3.485 (14) | O22—C2vi | 3.13 (3) |
Cr2—O2i | 3.489 (13) | O22—OW34 | 3.19 (2) |
Cr2—O3i | 3.739 (14) | O22—O25vi | 3.464 (19) |
Cr3—O16 | 1.588 (19) | O22—O23 | 3.52 (2) |
Cr3—O15 | 1.653 (14) | O22—O14i | 3.68 (2) |
Cr3—O13 | 1.673 (13) | O22—O23vi | 3.91 (2) |
Cr3—O8 | 1.680 (14) | O23—OW34 | 2.903 (19) |
Cr3—O2 | 3.325 (14) | O23—O29vi | 2.910 (19) |
Cr3—O7viii | 3.353 (13) | O23—O28 | 2.93 (2) |
Cr3—OW17i | 3.525 (15) | O23—O30vi | 3.06 (2) |
Cr3—O4 | 3.722 (14) | O23—O30 | 3.55 (2) |
Cr4—O33 | 1.595 (17) | O23—O22ix | 3.91 (2) |
Cr4—O30 | 1.622 (18) | O23—O27 | 4.06 (2) |
Cr4—O28 | 1.672 (14) | O24—O25 | 2.65 (2) |
Cr4—O27 | 1.676 (13) | O24—O29 | 2.768 (18) |
Cr4—OW34ix | 3.477 (14) | O24—O27 | 2.877 (19) |
Cr4—O24 | 3.537 (13) | O24—O31v | 2.88 (2) |
Cr4—O23 | 3.667 (16) | O24—O26 | 3.01 (2) |
Cr4—O19 | 3.711 (15) | O24—O30 | 3.139 (19) |
Cr5—O25 | 1.588 (16) | O24—O18v | 3.918 (19) |
Cr5—O24 | 1.645 (15) | O25—O29 | 2.668 (19) |
Cr5—O20 | 1.647 (13) | O25—O18v | 3.009 (18) |
Cr5—O29 | 1.692 (12) | O25—N3 | 3.03 (2) |
Cr5—O18v | 3.331 (13) | O25—C2 | 3.13 (3) |
Cr5—O30 | 3.373 (16) | O25—O32v | 3.30 (2) |
Cr5—OW34iii | 3.498 (14) | O25—Cr6v | 3.410 (14) |
Cr5—O31v | 3.555 (15) | O25—O22ix | 3.464 (19) |
Cr5—O21 | 3.610 (14) | O25—O31v | 3.51 (2) |
Cr6—O32 | 1.615 (16) | O26—O27 | 2.923 (19) |
Cr6—O31 | 1.632 (18) | O26—O31v | 2.96 (2) |
Cr6—O19 | 1.665 (15) | O26—O20iv | 2.98 (2) |
Cr6—O18 | 1.673 (13) | O26—C3xiii | 3.21 (4) |
Cr6—O25iv | 3.410 (14) | O26—C7v | 3.27 (3) |
Cr6—OW34 | 3.482 (15) | O26—OW34v | 4.28 (2) |
Cr6—O27 | 3.654 (13) | O27—O33 | 2.67 (2) |
Cr6—O21 | 3.699 (15) | O27—O30 | 2.71 (2) |
O1—O9 | 2.665 (18) | O27—O28 | 2.731 (19) |
O1—O12 | 2.669 (19) | O27—N1xii | 3.07 (3) |
O1—O10 | 2.69 (2) | O27—C6xii | 3.11 (4) |
O1—OW17 | 2.748 (19) | O28—O33 | 2.64 (2) |
O1—O4 | 2.769 (18) | O28—O30 | 2.70 (2) |
O1—O8 | 2.83 (2) | O28—O29vi | 2.857 (19) |
O1—O3 | 3.06 (2) | O28—N2 | 2.93 (4) |
O1—OW35 | 4.07 (3) | O28—OW34ix | 3.32 (2) |
O1—OW17i | 4.09 (2) | O28—OW35iii | 3.90 (4) |
O1—O3i | 4.349 (18) | O29—U4ix | 2.345 (12) |
O2—O14 | 2.69 (2) | O29—OW34iii | 2.727 (18) |
O2—N4 | 2.73 (3) | O29—O30 | 2.77 (2) |
O2—O7 | 2.725 (19) | O29—O28ix | 2.857 (19) |
O2—O6 | 2.745 (19) | O29—O23ix | 2.910 (19) |
O2—O10ii | 2.84 (2) | O29—O22ix | 2.96 (2) |
O2—O8 | 2.846 (19) | O29—O30ix | 4.154 (19) |
O2—O3 | 2.890 (19) | O30—U4ix | 2.381 (16) |
O2—O4 | 2.96 (2) | O30—O33 | 2.63 (3) |
O2—O12ii | 3.093 (19) | O30—OW34ix | 2.74 (2) |
O2—O16 | 3.16 (2) | O30—O22ix | 2.87 (2) |
O3—O8 | 2.84 (2) | O30—O23ix | 3.06 (2) |
O3—OW35ii | 2.89 (3) | O31—U3iv | 2.415 (16) |
O3—OW17 | 2.96 (2) | O31—O32 | 2.65 (3) |
O3—O10ii | 3.00 (2) | O31—O20xi | 2.79 (2) |
O3—O12ii | 3.41 (2) | O31—O24iv | 2.88 (2) |
O3—O4 | 3.49 (2) | O31—O26iv | 2.96 (2) |
O3—O10 | 3.74 (2) | O31—O21iv | 3.00 (2) |
O3—Cr2ii | 3.739 (14) | O31—OW34 | 3.07 (2) |
O3—O33x | 3.74 (2) | O31—O25iv | 3.51 (2) |
O4—O10ii | 2.91 (2) | O31—Cr5iv | 3.555 (15) |
O4—O8 | 3.02 (2) | O32—N3iv | 2.96 (2) |
O4—O7 | 3.079 (18) | O32—O25iv | 3.30 (2) |
O4—OW17 | 3.149 (18) | O32—O21iv | 3.37 (2) |
O4—C1ii | 3.20 (3) | O32—O16i | 3.55 (3) |
O4—O15 | 3.203 (18) | O32—O20xi | 3.84 (2) |
O5—O15iii | 2.87 (2) | O32—O11xiv | 4.08 (2) |
O5—N1 | 2.88 (3) | O32—U3iv | 4.099 (17) |
O5—O13ii | 2.893 (19) | O32—OW34 | 4.23 (2) |
O5—O7iii | 2.956 (19) | O33—N4xii | 2.85 (3) |
O5—O9 | 2.99 (2) | O33—N2 | 2.93 (4) |
O5—O6i | 3.05 (2) | O33—OW35iii | 3.01 (4) |
O5—C1 | 3.07 (3) | O33—O12iii | 3.19 (2) |
O5—OW35ii | 3.16 (3) | O33—O3xii | 3.74 (2) |
O5—C6 | 3.22 (3) | O33—OW34ix | 3.91 (2) |
O5—O10 | 3.29 (2) | O33—O23ix | 4.08 (2) |
O5—O14iii | 3.33 (2) | OW34—O29xi | 2.727 (18) |
O6—U1ii | 2.344 (14) | OW34—O30vi | 2.74 (2) |
O6—O14 | 2.66 (2) | OW34—O20xi | 2.923 (18) |
O6—O7 | 2.72 (2) | OW34—O28vi | 3.32 (2) |
O6—O15vii | 2.80 (2) | OW34—Cr4vi | 3.477 (14) |
O6—O9ii | 2.836 (19) | OW34—Cr5xi | 3.498 (14) |
O6—O11ii | 2.883 (19) | OW34—HW3A | 1.0035 |
O6—O5ii | 3.05 (2) | OW34—HW3B | 1.0029 |
O6—Cr2ii | 3.315 (14) | OW35—N2xi | 2.67 (5) |
O6—O10ii | 3.38 (2) | OW35—O3i | 2.89 (3) |
O6—O12ii | 3.418 (19) | OW35—O33xi | 3.01 (4) |
O7—U1xi | 2.357 (13) | OW35—O5i | 3.16 (3) |
O7—O14 | 2.63 (2) | OW35—C6i | 3.19 (4) |
O7—O13vii | 2.672 (18) | OW35—O14viii | 3.47 (3) |
O7—O15 | 2.821 (18) | OW35—O28xi | 3.90 (4) |
O7—O11xi | 2.94 (2) | OW35—HW3E | 1.0094 |
O7—O5xi | 2.956 (19) | OW35—HW3F | 1.0106 |
O7—O15vii | 3.200 (18) | C1—N1 | 1.55 (3) |
O7—Cr3vii | 3.353 (13) | C1—O16iii | 3.09 (3) |
O8—O16 | 2.66 (2) | C1—O11xii | 3.10 (3) |
O8—O13 | 2.675 (18) | C1—O18x | 3.16 (3) |
O8—O15 | 2.75 (2) | C1—O4i | 3.20 (3) |
O8—OW17i | 2.79 (2) | C1—H1A | 1.0038 |
O8—O10 | 3.71 (2) | C1—H1B | 1.0035 |
O8—OW35 | 3.95 (3) | C1—H1C | 0.9984 |
O9—O12 | 2.695 (19) | C2—N3 | 1.50 (3) |
O9—O10 | 2.74 (2) | C2—O22ix | 3.13 (3) |
O9—O13ii | 2.782 (19) | C2—H2A | 1.0090 |
O9—O6i | 2.836 (19) | C2—H2B | 1.0031 |
O9—OW17 | 2.902 (19) | C2—H2C | 1.0021 |
O9—O11 | 2.959 (19) | C3—N2xi | 1.41 (5) |
O10—U2i | 2.371 (13) | C3—O26xv | 3.21 (4) |
O10—O12 | 2.67 (2) | C3—H3A | 0.9990 |
O10—OW17i | 2.80 (2) | C3—H3B | 1.0019 |
O10—O2i | 2.84 (2) | C3—H3C | 0.9958 |
O10—O4i | 2.91 (2) | C4—N4 | 1.55 (3) |
O10—O3i | 3.00 (2) | C4—H4A | 0.9989 |
O10—O6i | 3.38 (2) | C4—H4B | 0.9933 |
O10—Cr1i | 3.618 (15) | C4—H4C | 0.9995 |
O11—O6i | 2.883 (19) | C5—N4 | 1.46 (4) |
O11—O7iii | 2.94 (2) | C5—O22ii | 3.13 (3) |
O11—O13ii | 2.96 (2) | C5—H5A | 1.0009 |
O11—N3vi | 2.99 (3) | C5—H5B | 1.0023 |
O11—C8 | 3.05 (4) | C5—H5C | 0.9983 |
O11—C1x | 3.10 (3) | C6—N1 | 1.52 (4) |
O11—O15iii | 3.11 (2) | C6—O27x | 3.11 (4) |
O11—O16ii | 3.38 (2) | C6—OW35ii | 3.19 (4) |
O11—O4iii | 3.785 (19) | C6—H6A | 1.0032 |
O12—N4i | 3.07 (2) | C6—H6B | 0.9963 |
O12—O2i | 3.093 (19) | C6—H6C | 1.0007 |
O12—O33xi | 3.19 (2) | C7—N3 | 1.47 (3) |
O12—O3i | 3.41 (2) | C7—O26iv | 3.26 (3) |
O12—O6i | 3.418 (19) | C7—H7A | 0.9984 |
O12—U2i | 3.922 (15) | C7—H7B | 1.0002 |
O12—OW35 | 4.06 (3) | C7—H7C | 1.0012 |
O12—O23vi | 4.49 (2) | C8—N2 | 1.65 (6) |
O13—U1i | 2.353 (13) | C8—H8A | 0.9993 |
O13—O16 | 2.65 (2) | C8—H8B | 0.9988 |
O13—O7viii | 2.672 (18) | C8—H8C | 1.0004 |
O13—O15 | 2.753 (18) | N1—O27x | 3.07 (3) |
O13—O9i | 2.782 (19) | N1—O18x | 3.10 (3) |
O13—O5i | 2.893 (19) | N1—H1D | 1.0038 |
O13—OW35 | 2.93 (3) | N1—H1E | 1.0083 |
O13—O11i | 2.96 (2) | N2—C3iii | 1.41 (5) |
O13—OW17i | 3.069 (19) | N2—OW35iii | 2.67 (5) |
O13—O14viii | 4.12 (2) | N2—H2D | 1.0132 |
O14—O16 | 3.14 (2) | N2—H2E | 1.0119 |
O14—O5xi | 3.33 (2) | N3—O32v | 2.96 (2) |
O14—OW35vii | 3.47 (3) | N3—O11ix | 2.99 (3) |
O14—O22ii | 3.68 (2) | N3—H3D | 1.0048 |
O14—O15 | 4.06 (2) | N3—H3E | 1.0032 |
O14—U1xi | 4.090 (17) | N4—O33x | 2.85 (3) |
O14—O19ii | 4.10 (2) | N4—O12ii | 3.07 (2) |
O14—O13vii | 4.12 (2) | N4—H4D | 1.0047 |
O15—U1xi | 2.378 (13) | N4—H4E | 1.0052 |
| | | |
O11—U1—O5 | 177.8 (6) | O10ii—OW17—O9 | 147.2 (7) |
O11—U1—O6i | 87.5 (6) | U2—OW17—O3 | 36.1 (3) |
O5—U1—O6i | 94.2 (6) | O1—OW17—O3 | 64.6 (5) |
O11—U1—O13ii | 90.2 (6) | O8ii—OW17—O3 | 104.9 (7) |
O5—U1—O13ii | 87.6 (6) | O10ii—OW17—O3 | 62.5 (5) |
O6i—U1—O13ii | 145.4 (5) | O9—OW17—O3 | 84.7 (6) |
O11—U1—O7iii | 89.4 (6) | U2—OW17—O13ii | 121.8 (6) |
O5—U1—O7iii | 90.0 (6) | O1—OW17—O13ii | 106.7 (6) |
O6i—U1—O7iii | 145.3 (5) | O8ii—OW17—O13ii | 54.1 (5) |
O13ii—U1—O7iii | 69.1 (4) | O10ii—OW17—O13ii | 118.4 (7) |
O11—U1—O15iii | 95.8 (6) | O9—OW17—O13ii | 55.5 (4) |
O5—U1—O15iii | 86.0 (6) | O3—OW17—O13ii | 86.1 (6) |
O6i—U1—O15iii | 72.8 (5) | U2—OW17—O4 | 33.5 (3) |
O13ii—U1—O15iii | 141.7 (5) | O1—OW17—O4 | 55.5 (4) |
O7iii—U1—O15iii | 73.1 (4) | O8ii—OW17—O4 | 139.4 (6) |
O11—U1—O9 | 89.1 (6) | O10ii—OW17—O4 | 58.2 (5) |
O5—U1—O9 | 90.1 (6) | O9—OW17—O4 | 111.7 (6) |
O6i—U1—O9 | 73.6 (5) | O3—OW17—O4 | 69.6 (5) |
O13ii—U1—O9 | 71.8 (4) | O13ii—OW17—O4 | 154.2 (7) |
O7iii—U1—O9 | 140.9 (4) | U2—OW17—Cr2 | 75.3 (4) |
O15iii—U1—O9 | 145.8 (4) | O1—OW17—Cr2 | 27.9 (3) |
O11—U1—O10 | 124.8 (5) | O8ii—OW17—Cr2 | 134.6 (6) |
O5—U1—O10 | 55.4 (5) | O10ii—OW17—Cr2 | 127.3 (6) |
O6i—U1—O10 | 58.4 (4) | O9—OW17—Cr2 | 28.4 (3) |
O13ii—U1—O10 | 96.0 (4) | O3—OW17—Cr2 | 71.4 (4) |
O7iii—U1—O10 | 143.6 (4) | O13ii—OW17—Cr2 | 80.6 (4) |
O15iii—U1—O10 | 110.9 (4) | O4—OW17—Cr2 | 83.4 (4) |
O9—U1—O10 | 43.0 (4) | U2—OW17—Cr3ii | 138.2 (6) |
O11—U1—O14iii | 126.6 (5) | O1—OW17—Cr3ii | 134.4 (6) |
O5—U1—O14iii | 52.8 (5) | O8ii—OW17—Cr3ii | 27.9 (3) |
O6i—U1—O14iii | 132.8 (4) | O10ii—OW17—Cr3ii | 107.2 (5) |
O13ii—U1—O14iii | 73.9 (4) | O9—OW17—Cr3ii | 79.8 (4) |
O7iii—U1—O14iii | 37.2 (4) | O3—OW17—Cr3ii | 103.6 (5) |
O15iii—U1—O14iii | 72.2 (4) | O13ii—OW17—Cr3ii | 28.3 (3) |
O9—U1—O14iii | 129.8 (4) | O4—OW17—Cr3ii | 165.3 (6) |
O10—U1—O14iii | 107.7 (3) | Cr2—OW17—Cr3ii | 107.2 (4) |
O11—U1—O16ii | 53.7 (5) | U2—OW17—O1ii | 86.2 (5) |
O5—U1—O16ii | 124.1 (5) | O1—OW17—O1ii | 136.8 (6) |
O6i—U1—O16ii | 134.0 (4) | O8ii—OW17—O1ii | 43.6 (4) |
O13ii—U1—O16ii | 37.2 (4) | O10ii—OW17—O1ii | 40.9 (4) |
O7iii—U1—O16ii | 66.7 (4) | O9—OW17—O1ii | 133.6 (6) |
O15iii—U1—O16ii | 128.2 (4) | O3—OW17—O1ii | 74.2 (5) |
O9—U1—O16ii | 81.2 (4) | O13ii—OW17—O1ii | 81.9 (5) |
O10—U1—O16ii | 120.8 (3) | O4—OW17—O1ii | 99.1 (5) |
O14iii—U1—O16ii | 92.8 (3) | Cr2—OW17—O1ii | 142.2 (5) |
O11—U1—O7i | 117.0 (5) | Cr3ii—OW17—O1ii | 66.3 (3) |
O5—U1—O7i | 65.1 (5) | U2—OW17—OW35ii | 80.0 (6) |
O6i—U1—O7i | 37.9 (4) | O1—OW17—OW35ii | 96.2 (6) |
O13ii—U1—O7i | 151.2 (4) | O8ii—OW17—OW35ii | 66.6 (6) |
O7iii—U1—O7i | 117.4 (2) | O10ii—OW17—OW35ii | 80.1 (7) |
O15iii—U1—O7i | 50.1 (4) | O9—OW17—OW35ii | 76.4 (6) |
O9—U1—O7i | 97.8 (4) | O3—OW17—OW35ii | 44.4 (5) |
O10—U1—O7i | 61.5 (3) | O13ii—OW17—OW35ii | 45.3 (5) |
O14iii—U1—O7i | 94.9 (3) | O4—OW17—OW35ii | 113.2 (6) |
O16ii—U1—O7i | 170.6 (3) | Cr2—OW17—OW35ii | 84.7 (5) |
O11—U1—OW35ii | 133.2 (6) | Cr3ii—OW17—OW35ii | 59.2 (5) |
O5—U1—OW35ii | 44.6 (6) | O1ii—OW17—OW35ii | 59.5 (5) |
O6i—U1—OW35ii | 131.1 (5) | U2—OW17—HW3C | 109.9 |
O13ii—U1—OW35ii | 43.1 (5) | O1—OW17—HW3C | 78.1 |
O7iii—U1—OW35ii | 72.5 (5) | O8ii—OW17—HW3C | 83.6 |
O15iii—U1—OW35ii | 118.1 (5) | O10ii—OW17—HW3C | 136.6 |
O9—U1—OW35ii | 80.4 (5) | O9—OW17—HW3C | 25.8 |
O10—U1—OW35ii | 74.3 (5) | O3—OW17—HW3C | 81.6 |
O14iii—U1—OW35ii | 49.7 (5) | O13ii—OW17—HW3C | 30.0 |
O16ii—U1—OW35ii | 79.5 (5) | O4—OW17—HW3C | 132.2 |
O7i—U1—OW35ii | 109.6 (4) | Cr2—OW17—HW3C | 50.9 |
O4—U2—O3 | 178.7 (7) | Cr3ii—OW17—HW3C | 56.4 |
O4—U2—O2 | 92.2 (6) | O1ii—OW17—HW3C | 108.9 |
O3—U2—O2 | 89.0 (6) | OW35ii—OW17—HW3C | 56.8 |
O4—U2—O1 | 83.7 (6) | U2—OW17—HW3D | 109.7 |
O3—U2—O1 | 95.0 (6) | O1—OW17—HW3D | 81.0 |
O2—U2—O1 | 147.9 (5) | O8ii—OW17—HW3D | 112.7 |
O4—U2—O8 | 93.9 (6) | O10ii—OW17—HW3D | 115.8 |
O3—U2—O8 | 86.1 (6) | O9—OW17—HW3D | 89.2 |
O2—U2—O8 | 74.8 (5) | O3—OW17—HW3D | 142.0 |
O1—U2—O8 | 73.7 (5) | O13ii—OW17—HW3D | 120.4 |
O4—U2—O10ii | 88.8 (6) | O4—OW17—HW3D | 78.1 |
O3—U2—O10ii | 91.9 (6) | Cr2—OW17—HW3D | 85.8 |
O2—U2—O10ii | 74.5 (5) | Cr3ii—OW17—HW3D | 112.1 |
O1—U2—O10ii | 137.0 (5) | O1ii—OW17—HW3D | 131.8 |
O8—U2—O10ii | 149.2 (5) | OW35ii—OW17—HW3D | 164.1 |
O4—U2—OW17 | 93.5 (6) | HW3C—OW17—HW3D | 107.5 |
O3—U2—OW17 | 85.7 (6) | Cr6—O18—U3 | 138.0 (8) |
O2—U2—OW17 | 143.6 (5) | Cr6—O18—O32 | 34.7 (5) |
O1—U2—OW17 | 68.5 (5) | U3—O18—O32 | 171.7 (8) |
O8—U2—OW17 | 140.4 (5) | Cr6—O18—O19 | 36.1 (4) |
O10ii—U2—OW17 | 69.8 (5) | U3—O18—O19 | 116.3 (6) |
O4—U2—O15 | 53.7 (5) | O32—O18—O19 | 60.2 (5) |
O3—U2—O15 | 126.7 (5) | Cr6—O18—O27 | 110.4 (6) |
O2—U2—O15 | 64.7 (4) | U3—O18—O27 | 54.9 (4) |
O1—U2—O15 | 88.0 (4) | O32—O18—O27 | 127.2 (6) |
O8—U2—O15 | 43.9 (4) | O19—O18—O27 | 74.5 (5) |
O10ii—U2—O15 | 120.6 (4) | Cr6—O18—O31 | 33.5 (5) |
OW17—U2—O15 | 142.3 (4) | U3—O18—O31 | 113.2 (7) |
O4—U2—O7 | 49.3 (5) | O32—O18—O31 | 58.5 (6) |
O3—U2—O7 | 132.0 (6) | O19—O18—O31 | 58.9 (5) |
O2—U2—O7 | 43.0 (4) | O27—O18—O31 | 119.0 (7) |
O1—U2—O7 | 123.9 (4) | Cr6—O18—O20iv | 120.5 (7) |
O8—U2—O7 | 80.2 (4) | U3—O18—O20iv | 54.9 (4) |
O10ii—U2—O7 | 78.4 (4) | O32—O18—O20iv | 122.2 (6) |
OW17—U2—O7 | 131.5 (4) | O19—O18—O20iv | 141.1 (8) |
O15—U2—O7 | 42.3 (3) | O27—O18—O20iv | 109.8 (6) |
O4—U2—O12ii | 120.8 (5) | O31—O18—O20iv | 88.3 (6) |
O3—U2—O12ii | 60.4 (5) | Cr6—O18—O26 | 172.2 (7) |
O2—U2—O12ii | 52.0 (4) | U3—O18—O26 | 36.8 (4) |
O1—U2—O12ii | 152.1 (4) | O32—O18—O26 | 151.0 (8) |
O8—U2—O12ii | 114.0 (4) | O19—O18—O26 | 136.5 (6) |
O10ii—U2—O12ii | 41.8 (5) | O27—O18—O26 | 62.0 (5) |
OW17—U2—O12ii | 95.0 (4) | O31—O18—O26 | 146.7 (7) |
O15—U2—O12ii | 116.6 (3) | O20iv—O18—O26 | 63.1 (5) |
O7—U2—O12ii | 83.9 (3) | Cr6—O18—O21 | 102.0 (7) |
O4—U2—O9 | 108.4 (5) | U3—O18—O21 | 36.4 (3) |
O3—U2—O9 | 70.3 (5) | O32—O18—O21 | 135.6 (7) |
O2—U2—O9 | 158.7 (4) | O19—O18—O21 | 89.6 (6) |
O1—U2—O9 | 36.1 (4) | O27—O18—O21 | 63.4 (5) |
O8—U2—O9 | 98.0 (4) | O31—O18—O21 | 78.4 (6) |
O10ii—U2—O9 | 110.2 (4) | O20iv—O18—O21 | 61.6 (5) |
OW17—U2—O9 | 43.0 (4) | O26—O18—O21 | 73.3 (5) |
O15—U2—O9 | 123.7 (3) | Cr6—O18—O25iv | 88.7 (6) |
O7—U2—O9 | 157.0 (3) | U3—O18—O25iv | 108.5 (5) |
O12ii—U2—O9 | 117.1 (3) | O32—O18—O25iv | 70.8 (5) |
O4—U2—O10 | 116.9 (5) | O19—O18—O25iv | 124.8 (6) |
O3—U2—O10 | 62.0 (5) | O27—O18—O25iv | 160.6 (6) |
O2—U2—O10 | 127.1 (4) | O31—O18—O25iv | 75.2 (5) |
O1—U2—O10 | 35.8 (4) | O20iv—O18—O25iv | 54.6 (4) |
O8—U2—O10 | 61.0 (4) | O26—O18—O25iv | 98.7 (5) |
O10ii—U2—O10 | 142.4 (2) | O21—O18—O25iv | 110.5 (6) |
OW17—U2—O10 | 81.1 (4) | Cr6—O18—N1xii | 99.4 (8) |
O15—U2—O10 | 97.0 (3) | U3—O18—N1xii | 104.7 (7) |
O7—U2—O10 | 139.0 (3) | O32—O18—N1xii | 82.4 (7) |
O12ii—U2—O10 | 122.3 (3) | O19—O18—N1xii | 80.0 (7) |
O9—U2—O10 | 38.1 (3) | O27—O18—N1xii | 63.3 (7) |
O21—U3—O26 | 179.1 (7) | O31—O18—N1xii | 132.9 (7) |
O21—U3—O18 | 90.9 (6) | O20iv—O18—N1xii | 137.6 (7) |
O26—U3—O18 | 89.8 (6) | O26—O18—N1xii | 79.2 (7) |
O21—U3—O27 | 91.9 (6) | O21—O18—N1xii | 126.6 (7) |
O26—U3—O27 | 88.9 (6) | O25iv—O18—N1xii | 118.3 (7) |
O18—U3—O27 | 70.1 (4) | Cr6—O18—C1xii | 96.4 (7) |
O21—U3—O20iv | 88.9 (6) | U3—O18—C1xii | 120.8 (6) |
O26—U3—O20iv | 90.8 (6) | O32—O18—C1xii | 67.5 (6) |
O18—U3—O20iv | 70.7 (4) | O19—O18—C1xii | 93.5 (7) |
O27—U3—O20iv | 140.8 (5) | O27—O18—C1xii | 91.2 (6) |
O21—U3—O24 | 88.5 (6) | O31—O18—C1xii | 126.0 (7) |
O26—U3—O24 | 91.3 (6) | O20iv—O18—C1xii | 124.3 (7) |
O18—U3—O24 | 144.5 (4) | O26—O18—C1xii | 86.0 (6) |
O27—U3—O24 | 74.4 (4) | O21—O18—C1xii | 152.6 (7) |
O20iv—U3—O24 | 144.8 (5) | O25iv—O18—C1xii | 89.9 (6) |
O21—U3—O31v | 90.5 (6) | N1xii—O18—C1xii | 28.7 (6) |
O26—U3—O31v | 88.6 (6) | Cr6—O19—U4 | 153.7 (10) |
O18—U3—O31v | 141.9 (5) | Cr6—O19—O31 | 35.5 (5) |
O27—U3—O31v | 147.9 (5) | U4—O19—O31 | 118.4 (8) |
O20iv—U3—O31v | 71.3 (5) | Cr6—O19—O18 | 36.3 (4) |
O24—U3—O31v | 73.7 (5) | U4—O19—O18 | 145.1 (7) |
O21—U3—O25 | 50.5 (5) | O31—O19—O18 | 61.4 (5) |
O26—U3—O25 | 129.0 (5) | Cr6—O19—O32 | 34.1 (5) |
O18—U3—O25 | 138.9 (4) | U4—O19—O32 | 153.9 (7) |
O27—U3—O25 | 94.8 (4) | O31—O19—O32 | 59.2 (6) |
O20iv—U3—O25 | 115.1 (4) | O18—O19—O32 | 59.6 (5) |
O24—U3—O25 | 42.3 (4) | Cr6—O19—OW34 | 101.1 (8) |
O31v—U3—O25 | 62.9 (4) | U4—O19—OW34 | 57.8 (4) |
O21—U3—O32v | 53.7 (5) | O31—O19—OW34 | 68.9 (6) |
O26—U3—O32v | 125.4 (5) | O18—O19—OW34 | 129.6 (7) |
O18—U3—O32v | 123.3 (4) | O32—O19—OW34 | 101.8 (7) |
O27—U3—O32v | 139.9 (4) | Cr6—O19—O22 | 155.4 (8) |
O20iv—U3—O32v | 66.6 (4) | U4—O19—O22 | 37.9 (4) |
O24—U3—O32v | 83.8 (4) | O31—O19—O22 | 137.4 (8) |
O31v—U3—O32v | 38.0 (5) | O18—O19—O22 | 161.1 (8) |
O25—U3—O32v | 48.9 (3) | O32—O19—O22 | 123.5 (7) |
O21—U3—O30 | 68.0 (5) | OW34—O19—O22 | 69.3 (5) |
O26—U3—O30 | 112.5 (5) | Cr6—O19—O28 | 141.4 (8) |
O18—U3—O30 | 99.2 (4) | U4—O19—O28 | 52.3 (4) |
O27—U3—O30 | 37.4 (4) | O31—O19—O28 | 143.5 (8) |
O20iv—U3—O30 | 154.9 (4) | O18—O19—O28 | 105.1 (6) |
O24—U3—O30 | 48.2 (4) | O32—O19—O28 | 146.6 (8) |
O31v—U3—O30 | 116.5 (4) | OW34—O19—O28 | 109.7 (7) |
O25—U3—O30 | 57.5 (3) | O22—O19—O28 | 61.4 (5) |
O32v—U3—O30 | 104.0 (3) | Cr6—O19—O23 | 121.8 (8) |
O21—U3—O31 | 56.8 (5) | U4—O19—O23 | 36.4 (4) |
O26—U3—O31 | 123.7 (5) | O31—O19—O23 | 92.1 (7) |
O18—U3—O31 | 36.2 (4) | O18—O19—O23 | 111.7 (6) |
O27—U3—O31 | 85.3 (4) | O32—O19—O23 | 151.1 (8) |
O20iv—U3—O31 | 62.8 (4) | OW34—O19—O23 | 60.8 (5) |
O24—U3—O31 | 139.2 (4) | O22—O19—O23 | 74.3 (6) |
O31v—U3—O31 | 122.1 (3) | O28—O19—O23 | 59.9 (5) |
O25—U3—O31 | 107.2 (3) | Cr6—O19—O27 | 89.2 (6) |
O32v—U3—O31 | 90.2 (3) | U4—O19—O27 | 98.1 (5) |
O30—U3—O31 | 95.2 (3) | O31—O19—O27 | 104.1 (6) |
O21—U3—O19 | 68.3 (5) | O18—O19—O27 | 53.1 (4) |
O26—U3—O19 | 112.6 (5) | O32—O19—O27 | 107.7 (6) |
O18—U3—O19 | 34.2 (4) | OW34—O19—O27 | 139.9 (7) |
O27—U3—O19 | 49.0 (4) | O22—O19—O27 | 112.9 (6) |
O20iv—U3—O19 | 96.0 (4) | O28—O19—O27 | 52.2 (4) |
O24—U3—O19 | 115.4 (3) | O23—O19—O27 | 80.8 (5) |
O31v—U3—O19 | 155.9 (5) | Cr6—O19—Cr4 | 115.9 (6) |
O25—U3—O19 | 107.5 (3) | U4—O19—Cr4 | 72.9 (4) |
O32v—U3—O19 | 118.4 (3) | O31—O19—Cr4 | 124.2 (6) |
O30—U3—O19 | 67.3 (3) | O18—O19—Cr4 | 79.9 (4) |
O31—U3—O19 | 36.3 (3) | O32—O19—Cr4 | 131.7 (6) |
O22—U4—O23 | 179.5 (7) | OW34—O19—Cr4 | 125.1 (6) |
O22—U4—O19 | 87.6 (6) | O22—O19—Cr4 | 87.1 (5) |
O23—U4—O19 | 92.2 (6) | O28—O19—Cr4 | 25.7 (3) |
O22—U4—O29vi | 91.0 (6) | O23—O19—Cr4 | 65.5 (4) |
O23—U4—O29vi | 88.9 (6) | O27—O19—Cr4 | 26.8 (2) |
O19—U4—O29vi | 151.1 (5) | Cr6—O19—O21 | 67.6 (5) |
O22—U4—O28 | 89.9 (6) | U4—O19—O21 | 99.1 (5) |
O23—U4—O28 | 89.5 (6) | O31—O19—O21 | 61.9 (5) |
O19—U4—O28 | 76.1 (5) | O18—O19—O21 | 48.0 (4) |
O29vi—U4—O28 | 75.0 (5) | O32—O19—O21 | 101.1 (6) |
O22—U4—O30vi | 86.4 (7) | OW34—O19—O21 | 101.1 (6) |
O23—U4—O30vi | 94.1 (6) | O22—O19—O21 | 135.3 (6) |
O19—U4—O30vi | 137.0 (5) | O28—O19—O21 | 83.7 (5) |
O29vi—U4—O30vi | 71.6 (5) | O23—O19—O21 | 63.8 (4) |
O28—U4—O30vi | 146.4 (5) | O27—O19—O21 | 47.4 (4) |
O22—U4—OW34 | 96.0 (6) | Cr4—O19—O21 | 62.4 (3) |
O23—U4—OW34 | 84.4 (6) | Cr5—O20—U3v | 149.1 (8) |
O19—U4—OW34 | 69.8 (5) | Cr5—O20—O25 | 34.2 (5) |
O29vi—U4—OW34 | 139.0 (5) | U3v—O20—O25 | 120.9 (6) |
O28—U4—OW34 | 145.0 (5) | Cr5—O20—O29 | 37.6 (4) |
O30vi—U4—OW34 | 68.6 (5) | U3v—O20—O29 | 169.1 (7) |
O22—U4—O25vi | 55.2 (5) | O25—O20—O29 | 60.3 (5) |
O23—U4—O25vi | 124.9 (5) | Cr5—O20—O24 | 35.0 (4) |
O19—U4—O25vi | 137.8 (4) | U3v—O20—O24 | 128.5 (6) |
O29vi—U4—O25vi | 36.6 (4) | O25—O20—O24 | 59.4 (5) |
O28—U4—O25vi | 84.1 (4) | O29—O20—O24 | 62.2 (5) |
O30vi—U4—O25vi | 66.5 (4) | Cr5—O20—O18v | 95.5 (6) |
OW34—U4—O25vi | 127.1 (4) | U3v—O20—O18v | 54.4 (4) |
O22—U4—O30 | 124.5 (6) | O25—O20—O18v | 67.8 (5) |
O23—U4—O30 | 55.0 (5) | O29—O20—O18v | 128.0 (6) |
O19—U4—O30 | 85.7 (4) | O24—O20—O18v | 92.2 (5) |
O29vi—U4—O30 | 71.4 (4) | Cr5—O20—O31iii | 154.6 (9) |
O28—U4—O30 | 35.1 (4) | U3v—O20—O31iii | 55.0 (4) |
O30vi—U4—O30 | 131.4 (3) | O25—O20—O31iii | 165.6 (8) |
OW34—U4—O30 | 131.9 (4) | O29—O20—O31iii | 120.8 (6) |
O25vi—U4—O30 | 99.1 (3) | O24—O20—O31iii | 134.8 (8) |
O22—U4—O27 | 108.6 (5) | O18v—O20—O31iii | 109.3 (6) |
O23—U4—O27 | 70.9 (5) | Cr5—O20—OW34iii | 95.9 (6) |
O19—U4—O27 | 49.3 (4) | U3v—O20—OW34iii | 113.9 (5) |
O29vi—U4—O27 | 104.6 (3) | O25—O20—OW34iii | 110.2 (6) |
O28—U4—O27 | 35.5 (4) | O29—O20—OW34iii | 58.2 (5) |
O30vi—U4—O27 | 164.7 (5) | O24—O20—OW34iii | 112.1 (6) |
OW34—U4—O27 | 111.1 (4) | O18v—O20—OW34iii | 150.9 (7) |
O25vi—U4—O27 | 119.6 (3) | O31iii—O20—OW34iii | 64.9 (5) |
O30—U4—O27 | 37.0 (3) | Cr5—O20—O21v | 127.9 (7) |
O22—U4—O31 | 109.2 (5) | U3v—O20—O21v | 37.0 (4) |
O23—U4—O31 | 70.7 (5) | O25—O20—O21v | 123.2 (6) |
O19—U4—O31 | 33.2 (5) | O29—O20—O21v | 153.2 (7) |
O29vi—U4—O31 | 159.4 (4) | O24—O20—O21v | 95.6 (6) |
O28—U4—O31 | 101.0 (4) | O18v—O20—O21v | 63.0 (5) |
O30vi—U4—O31 | 111.8 (4) | O31iii—O20—O21v | 63.2 (5) |
OW34—U4—O31 | 44.6 (4) | OW34iii—O20—O21v | 126.6 (6) |
O25vi—U4—O31 | 163.9 (3) | Cr5—O20—O26v | 140.0 (8) |
O30—U4—O31 | 93.6 (3) | U3v—O20—O26v | 36.3 (4) |
O27—U4—O31 | 66.5 (3) | O25—O20—O26v | 106.6 (7) |
O14—Cr1—O7 | 109.7 (8) | O29—O20—O26v | 133.2 (7) |
O14—Cr1—O6 | 109.3 (8) | O24—O20—O26v | 154.0 (7) |
O7—Cr1—O6 | 111.1 (7) | O18v—O20—O26v | 61.8 (5) |
O14—Cr1—O2 | 108.7 (8) | O31iii—O20—O26v | 61.5 (5) |
O7—Cr1—O2 | 109.3 (7) | OW34iii—O20—O26v | 93.0 (5) |
O6—Cr1—O2 | 108.6 (7) | O21v—O20—O26v | 73.3 (5) |
O14—Cr1—O15vii | 104.9 (6) | Cr5—O20—O31v | 68.3 (5) |
O7—Cr1—O15vii | 65.1 (5) | U3v—O20—O31v | 83.5 (4) |
O6—Cr1—O15vii | 51.3 (6) | O25—O20—O31v | 62.7 (5) |
O2—Cr1—O15vii | 145.5 (5) | O29—O20—O31v | 105.4 (5) |
O14—Cr1—O16 | 61.9 (6) | O24—O20—O31v | 48.9 (4) |
O7—Cr1—O16 | 88.2 (5) | O18v—O20—O31v | 45.8 (4) |
O6—Cr1—O16 | 160.7 (6) | O31iii—O20—O31v | 126.2 (5) |
O2—Cr1—O16 | 62.4 (5) | OW34iii—O20—O31v | 161.0 (6) |
O15vii—Cr1—O16 | 145.2 (4) | O21v—O20—O31v | 63.1 (4) |
O14—Cr1—O4 | 142.7 (6) | O26v—O20—O31v | 105.8 (5) |
O7—Cr1—O4 | 58.6 (5) | Cr5—O20—O32iii | 118.2 (7) |
O6—Cr1—O4 | 107.8 (6) | U3v—O20—O32iii | 78.7 (4) |
O2—Cr1—O4 | 54.7 (6) | O25—O20—O32iii | 150.3 (7) |
O15vii—Cr1—O4 | 100.8 (3) | O29—O20—O32iii | 105.0 (6) |
O16—Cr1—O4 | 81.6 (4) | O24—O20—O32iii | 91.1 (6) |
O14—Cr1—O10ii | 151.0 (6) | O18v—O20—O32iii | 120.8 (6) |
O7—Cr1—O10ii | 97.4 (5) | O31iii—O20—O32iii | 43.7 (5) |
O6—Cr1—O10ii | 68.4 (5) | OW34iii—O20—O32iii | 76.2 (5) |
O2—Cr1—O10ii | 50.2 (5) | O21v—O20—O32iii | 57.9 (4) |
O15vii—Cr1—O10ii | 95.7 (3) | O26v—O20—O32iii | 101.9 (5) |
O16—Cr1—O10ii | 110.2 (4) | O31v—O20—O32iii | 101.5 (5) |
O4—Cr1—O10ii | 47.6 (3) | U3—O21—N3 | 156.3 (8) |
O14—Cr1—O15 | 92.6 (6) | U3—O21—O20iv | 54.2 (5) |
O7—Cr1—O15 | 47.3 (5) | N3—O21—O20iv | 118.0 (7) |
O6—Cr1—O15 | 154.8 (6) | U3—O21—O24 | 54.6 (5) |
O2—Cr1—O15 | 74.2 (5) | N3—O21—O24 | 113.7 (7) |
O15vii—Cr1—O15 | 112.04 (13) | O20iv—O21—O24 | 101.6 (6) |
O16—Cr1—O15 | 43.1 (4) | U3—O21—O18 | 52.7 (5) |
O4—Cr1—O15 | 52.4 (3) | N3—O21—O18 | 145.9 (7) |
O10ii—Cr1—O15 | 98.4 (3) | O20iv—O21—O18 | 55.4 (5) |
O12—Cr2—O10 | 110.0 (7) | O24—O21—O18 | 100.2 (6) |
O12—Cr2—O1 | 109.2 (7) | U3—O21—O27 | 52.0 (5) |
O10—Cr2—O1 | 108.7 (8) | N3—O21—O27 | 144.1 (7) |
O12—Cr2—O9 | 110.6 (7) | O20iv—O21—O27 | 97.8 (6) |
O10—Cr2—O9 | 111.7 (7) | O24—O21—O27 | 58.0 (5) |
O1—Cr2—O9 | 106.4 (6) | O18—O21—O27 | 54.2 (5) |
O12—Cr2—O6i | 79.7 (5) | U3—O21—O31v | 53.5 (5) |
O10—Cr2—O6i | 77.9 (6) | N3—O21—O31v | 103.0 (7) |
O1—Cr2—O6i | 165.1 (5) | O20iv—O21—O31v | 56.1 (4) |
O9—Cr2—O6i | 58.8 (5) | O24—O21—O31v | 58.1 (5) |
O12—Cr2—OW17 | 128.0 (6) | O18—O21—O31v | 98.2 (6) |
O10—Cr2—OW17 | 121.7 (6) | O27—O21—O31v | 99.9 (6) |
O1—Cr2—OW17 | 50.6 (5) | U3—O21—C7 | 154.2 (9) |
O9—Cr2—OW17 | 56.0 (5) | N3—O21—C7 | 28.5 (6) |
O6i—Cr2—OW17 | 114.5 (3) | O20iv—O21—C7 | 100.1 (7) |
O12—Cr2—O2i | 62.5 (6) | O24—O21—C7 | 142.0 (8) |
O10—Cr2—O2i | 53.8 (6) | O18—O21—C7 | 117.8 (7) |
O1—Cr2—O2i | 147.1 (5) | O27—O21—C7 | 147.3 (7) |
O9—Cr2—O2i | 106.2 (5) | O31v—O21—C7 | 112.9 (7) |
O6i—Cr2—O2i | 47.5 (3) | U3—O21—O25 | 103.2 (6) |
OW17—Cr2—O2i | 160.5 (3) | N3—O21—O25 | 61.4 (6) |
O12—Cr2—O3i | 65.9 (6) | O20iv—O21—O25 | 125.5 (6) |
O10—Cr2—O3i | 51.2 (6) | O24—O21—O25 | 52.3 (5) |
O1—Cr2—O3i | 100.1 (5) | O18—O21—O25 | 152.4 (7) |
O9—Cr2—O3i | 152.6 (5) | O27—O21—O25 | 101.7 (6) |
O6i—Cr2—O3i | 94.4 (3) | O31v—O21—O25 | 70.6 (5) |
OW17—Cr2—O3i | 148.9 (3) | C7—O21—O25 | 89.8 (7) |
O2i—Cr2—O3i | 47.0 (3) | U3—O21—O32v | 101.4 (6) |
O16—Cr3—O15 | 110.1 (8) | N3—O21—O32v | 56.1 (5) |
O16—Cr3—O13 | 108.9 (8) | O20iv—O21—O32v | 74.6 (5) |
O15—Cr3—O13 | 111.7 (7) | O24—O21—O32v | 91.3 (5) |
O16—Cr3—O8 | 109.0 (9) | O18—O21—O32v | 129.9 (6) |
O15—Cr3—O8 | 111.2 (7) | O27—O21—O32v | 146.8 (6) |
O13—Cr3—O8 | 105.8 (7) | O31v—O21—O32v | 48.7 (5) |
O16—Cr3—O2 | 70.1 (7) | C7—O21—O32v | 65.2 (6) |
O15—Cr3—O2 | 85.4 (5) | O25—O21—O32v | 61.6 (5) |
O13—Cr3—O2 | 161.2 (5) | U3—O21—O26 | 0.4 (4) |
O8—Cr3—O2 | 58.9 (5) | N3—O21—O26 | 155.9 (7) |
O16—Cr3—O7viii | 95.6 (7) | O20iv—O21—O26 | 54.0 (5) |
O15—Cr3—O7viii | 70.3 (5) | O24—O21—O26 | 54.5 (4) |
O13—Cr3—O7viii | 52.0 (5) | O18—O21—O26 | 53.0 (4) |
O8—Cr3—O7viii | 152.1 (6) | O27—O21—O26 | 52.4 (4) |
O2—Cr3—O7viii | 146.0 (3) | O31v—O21—O26 | 53.1 (5) |
O16—Cr3—OW17i | 101.6 (7) | C7—O21—O26 | 154.0 (7) |
O15—Cr3—OW17i | 147.8 (6) | O25—O21—O26 | 103.0 (5) |
O13—Cr3—OW17i | 60.5 (5) | O32v—O21—O26 | 100.9 (5) |
O8—Cr3—OW17i | 50.9 (5) | U3—O21—Cr5 | 80.2 (5) |
O2—Cr3—OW17i | 100.9 (3) | N3—O21—Cr5 | 87.1 (5) |
O7viii—Cr3—OW17i | 112.4 (3) | O20iv—O21—Cr5 | 118.6 (5) |
O16—Cr3—O4 | 117.9 (6) | O24—O21—Cr5 | 26.7 (3) |
O15—Cr3—O4 | 59.1 (5) | O18—O21—Cr5 | 126.5 (6) |
O13—Cr3—O4 | 132.7 (6) | O27—O21—Cr5 | 78.3 (4) |
O8—Cr3—O4 | 53.0 (6) | O31v—O21—Cr5 | 64.3 (4) |
O2—Cr3—O4 | 49.3 (3) | C7—O21—Cr5 | 115.6 (6) |
O7viii—Cr3—O4 | 125.8 (3) | O25—O21—Cr5 | 25.9 (3) |
OW17i—Cr3—O4 | 101.5 (3) | O32v—O21—Cr5 | 77.5 (4) |
O33—Cr4—O30 | 109.6 (8) | O26—O21—Cr5 | 80.0 (4) |
O33—Cr4—O28 | 107.8 (8) | U4—O22—O19 | 54.5 (5) |
O30—Cr4—O28 | 110.0 (8) | U4—O22—O30vi | 55.9 (5) |
O33—Cr4—O27 | 109.6 (8) | O19—O22—O30vi | 99.8 (7) |
O30—Cr4—O27 | 110.4 (8) | U4—O22—O28 | 53.2 (5) |
O28—Cr4—O27 | 109.3 (7) | O19—O22—O28 | 59.7 (5) |
O33—Cr4—OW34ix | 93.6 (6) | O30vi—O22—O28 | 102.5 (7) |
O30—Cr4—OW34ix | 50.3 (6) | U4—O22—O29vi | 52.5 (5) |
O28—Cr4—OW34ix | 70.7 (5) | O19—O22—O29vi | 102.2 (6) |
O27—Cr4—OW34ix | 154.9 (6) | O30vi—O22—O29vi | 56.7 (5) |
O33—Cr4—O24 | 104.0 (6) | O28—O22—O29vi | 58.1 (5) |
O30—Cr4—O24 | 62.5 (6) | U4—O22—C5i | 122.4 (9) |
O28—Cr4—O24 | 147.7 (6) | O19—O22—C5i | 79.1 (7) |
O27—Cr4—O24 | 53.6 (5) | O30vi—O22—C5i | 110.4 (8) |
OW34ix—Cr4—O24 | 112.6 (3) | O28—O22—C5i | 130.8 (8) |
O33—Cr4—O23 | 155.7 (6) | O29vi—O22—C5i | 167.1 (9) |
O30—Cr4—O23 | 73.1 (6) | U4—O22—C2vi | 150.1 (9) |
O28—Cr4—O23 | 51.2 (6) | O19—O22—C2vi | 153.8 (8) |
O27—Cr4—O23 | 90.9 (5) | O30vi—O22—C2vi | 97.0 (7) |
OW34ix—Cr4—O23 | 69.2 (3) | O28—O22—C2vi | 135.0 (8) |
O24—Cr4—O23 | 98.5 (3) | O29vi—O22—C2vi | 103.8 (7) |
O33—Cr4—O19 | 131.6 (7) | C5i—O22—C2vi | 76.2 (8) |
O30—Cr4—O19 | 117.9 (6) | U4—O22—OW34 | 50.8 (5) |
O28—Cr4—O19 | 48.3 (5) | O19—O22—OW34 | 53.9 (5) |
O27—Cr4—O19 | 61.9 (5) | O30vi—O22—OW34 | 53.5 (5) |
OW34ix—Cr4—O19 | 109.6 (3) | O28—O22—OW34 | 97.6 (6) |
O24—Cr4—O19 | 105.0 (3) | O29vi—O22—OW34 | 94.7 (6) |
O23—Cr4—O19 | 47.5 (3) | C5i—O22—OW34 | 75.6 (7) |
O25—Cr5—O24 | 110.0 (7) | C2vi—O22—OW34 | 126.2 (7) |
O25—Cr5—O20 | 110.1 (8) | U4—O22—O25vi | 100.2 (6) |
O24—Cr5—O20 | 109.9 (7) | O19—O22—O25vi | 148.3 (6) |
O25—Cr5—O29 | 108.8 (7) | O30vi—O22—O25vi | 74.9 (5) |
O24—Cr5—O29 | 112.1 (7) | O28—O22—O25vi | 90.4 (5) |
O20—Cr5—O29 | 105.9 (6) | O29vi—O22—O25vi | 48.3 (4) |
O25—Cr5—O18v | 64.4 (5) | C5i—O22—O25vi | 132.4 (8) |
O24—Cr5—O18v | 98.1 (5) | C2vi—O22—O25vi | 56.3 (6) |
O20—Cr5—O18v | 55.0 (5) | OW34—O22—O25vi | 128.3 (6) |
O29—Cr5—O18v | 149.1 (5) | U4—O22—O23 | 0.3 (4) |
O25—Cr5—O30 | 96.2 (6) | O19—O22—O23 | 54.4 (5) |
O24—Cr5—O30 | 67.6 (5) | O30vi—O22—O23 | 56.1 (5) |
O20—Cr5—O30 | 152.1 (6) | O28—O22—O23 | 52.9 (5) |
O29—Cr5—O30 | 54.7 (5) | O29vi—O22—O23 | 52.5 (4) |
O18v—Cr5—O30 | 151.3 (3) | C5i—O22—O23 | 122.5 (8) |
O25—Cr5—OW34iii | 123.7 (6) | C2vi—O22—O23 | 150.2 (8) |
O24—Cr5—OW34iii | 126.2 (6) | OW34—O22—O23 | 50.9 (4) |
O20—Cr5—OW34iii | 56.2 (5) | O25vi—O22—O23 | 100.3 (5) |
O29—Cr5—OW34iii | 49.7 (5) | U4—O22—O14i | 125.4 (7) |
O18v—Cr5—OW34iii | 106.8 (3) | O19—O22—O14i | 76.4 (5) |
O30—Cr5—OW34iii | 101.6 (3) | O30vi—O22—O14i | 170.0 (6) |
O25—Cr5—O31v | 75.5 (6) | O28—O22—O14i | 83.6 (5) |
O24—Cr5—O31v | 53.0 (5) | O29vi—O22—O14i | 132.9 (6) |
O20—Cr5—O31v | 86.2 (5) | C5i—O22—O14i | 60.0 (7) |
O29—Cr5—O31v | 164.1 (6) | C2vi—O22—O14i | 83.6 (7) |
O18v—Cr5—O31v | 46.7 (4) | OW34—O22—O14i | 118.4 (5) |
O30—Cr5—O31v | 110.1 (4) | O25vi—O22—O14i | 113.2 (6) |
OW34iii—Cr5—O31v | 141.1 (3) | O23—O22—O14i | 125.1 (5) |
O25—Cr5—O21 | 57.7 (6) | U4—O22—O23vi | 109.8 (7) |
O24—Cr5—O21 | 53.2 (5) | O19—O22—O23vi | 115.2 (6) |
O20—Cr5—O21 | 135.1 (5) | O30vi—O22—O23vi | 61.0 (5) |
O29—Cr5—O21 | 119.0 (5) | O28—O22—O23vi | 162.7 (7) |
O18v—Cr5—O21 | 84.1 (3) | O29vi—O22—O23vi | 110.7 (6) |
O30—Cr5—O21 | 67.3 (3) | C5i—O22—O23vi | 58.1 (6) |
OW34iii—Cr5—O21 | 168.6 (3) | C2vi—O22—O23vi | 57.3 (6) |
O31v—Cr5—O21 | 49.6 (3) | OW34—O22—O23vi | 68.9 (4) |
O32—Cr6—O31 | 109.4 (8) | O25vi—O22—O23vi | 89.9 (4) |
O32—Cr6—O19 | 110.5 (8) | O23—O22—O23vi | 110.1 (5) |
O31—Cr6—O19 | 108.2 (8) | O14i—O22—O23vi | 112.0 (5) |
O32—Cr6—O18 | 109.2 (7) | U4—O23—OW34 | 58.4 (5) |
O31—Cr6—O18 | 111.9 (7) | U4—O23—O29vi | 53.7 (4) |
O19—Cr6—O18 | 107.6 (7) | OW34—O23—O29vi | 102.2 (6) |
O32—Cr6—O25iv | 72.5 (6) | U4—O23—O28 | 53.3 (5) |
O31—Cr6—O25iv | 79.9 (6) | OW34—O23—O28 | 104.5 (7) |
O19—Cr6—O25iv | 169.1 (6) | O29vi—O23—O28 | 58.6 (5) |
O18—Cr6—O25iv | 61.9 (5) | U4—O23—O19 | 51.4 (5) |
O32—Cr6—OW34 | 106.4 (6) | OW34—O23—O19 | 55.9 (5) |
O31—Cr6—OW34 | 61.9 (6) | O29vi—O23—O19 | 100.5 (6) |
O19—Cr6—OW34 | 50.9 (6) | O28—O23—O19 | 58.5 (5) |
O18—Cr6—OW34 | 143.6 (5) | U4—O23—O30vi | 50.8 (5) |
O25iv—Cr6—OW34 | 139.3 (4) | OW34—O23—O30vi | 54.6 (5) |
O32—Cr6—O27 | 128.9 (7) | O29vi—O23—O30vi | 55.1 (5) |
O31—Cr6—O27 | 120.7 (6) | O28—O23—O30vi | 98.1 (6) |
O19—Cr6—O27 | 63.7 (6) | O19—O23—O30vi | 93.0 (6) |
O18—Cr6—O27 | 44.2 (5) | U4—O23—O22 | 0.3 (4) |
O25iv—Cr6—O27 | 106.0 (3) | OW34—O23—O22 | 58.5 (5) |
OW34—Cr6—O27 | 105.1 (3) | O29vi—O23—O22 | 53.7 (4) |
O32—Cr6—O21 | 158.1 (6) | O28—O23—O22 | 53.1 (4) |
O31—Cr6—O21 | 74.2 (6) | O19—O23—O22 | 51.3 (4) |
O19—Cr6—O21 | 87.8 (6) | O30vi—O23—O22 | 51.1 (5) |
O18—Cr6—O21 | 51.8 (6) | U4—O23—O30 | 100.9 (7) |
O25iv—Cr6—O21 | 87.4 (3) | OW34—O23—O30 | 147.3 (7) |
OW34—Cr6—O21 | 94.4 (3) | O29vi—O23—O30 | 79.3 (5) |
O27—Cr6—O21 | 48.1 (3) | O28—O23—O30 | 48.0 (4) |
Cr2—O1—U2 | 137.1 (8) | O19—O23—O30 | 91.6 (6) |
Cr2—O1—O9 | 36.9 (4) | O30vi—O23—O30 | 134.2 (5) |
U2—O1—O9 | 112.6 (6) | O22—O23—O30 | 100.7 (5) |
Cr2—O1—O12 | 34.8 (4) | U4—O23—Cr4 | 79.0 (6) |
U2—O1—O12 | 171.8 (7) | OW34—O23—Cr4 | 121.8 (6) |
O9—O1—O12 | 60.7 (5) | O29vi—O23—Cr4 | 77.1 (4) |
Cr2—O1—O10 | 35.5 (5) | O28—O23—Cr4 | 26.5 (3) |
U2—O1—O10 | 113.5 (7) | O19—O23—Cr4 | 67.0 (4) |
O9—O1—O10 | 61.6 (5) | O30vi—O23—Cr4 | 124.1 (6) |
O12—O1—O10 | 59.8 (5) | O22—O23—Cr4 | 78.8 (4) |
Cr2—O1—OW17 | 101.6 (6) | O30—O23—Cr4 | 25.9 (3) |
U2—O1—OW17 | 58.7 (4) | U4—O23—O21 | 120.9 (7) |
O9—O1—OW17 | 64.8 (5) | OW34—O23—O21 | 103.3 (5) |
O12—O1—OW17 | 118.4 (6) | O29vi—O23—O21 | 141.4 (6) |
O10—O1—OW17 | 114.3 (6) | O28—O23—O21 | 87.0 (5) |
Cr2—O1—O4 | 171.2 (8) | O19—O23—O21 | 71.3 (5) |
U2—O1—O4 | 38.6 (4) | O30vi—O23—O21 | 157.9 (6) |
O9—O1—O4 | 134.3 (6) | O22—O23—O21 | 120.7 (6) |
O12—O1—O4 | 149.3 (7) | O30—O23—O21 | 63.7 (4) |
O10—O1—O4 | 147.6 (8) | Cr4—O23—O21 | 64.9 (3) |
OW17—O1—O4 | 69.6 (5) | U4—O23—O22ix | 133.6 (7) |
Cr2—O1—O8 | 119.7 (7) | OW34—O23—O22ix | 166.4 (7) |
U2—O1—O8 | 53.2 (4) | O29vi—O23—O22ix | 85.0 (5) |
O9—O1—O8 | 135.2 (7) | O28—O23—O22ix | 89.2 (5) |
O12—O1—O8 | 127.3 (6) | O19—O23—O22ix | 134.8 (6) |
O10—O1—O8 | 84.4 (6) | O30vi—O23—O22ix | 124.6 (6) |
OW17—O1—O8 | 110.9 (7) | O22—O23—O22ix | 133.4 (5) |
O4—O1—O8 | 65.4 (5) | O30—O23—O22ix | 44.9 (4) |
Cr2—O1—O3 | 102.7 (7) | Cr4—O23—O22ix | 70.8 (4) |
U2—O1—O3 | 34.8 (3) | O21—O23—O22ix | 76.7 (4) |
O9—O1—O3 | 87.1 (6) | U4—O23—O27 | 84.8 (6) |
O12—O1—O3 | 137.2 (7) | OW34—O23—O27 | 107.9 (5) |
O10—O1—O3 | 80.8 (6) | O29vi—O23—O27 | 99.6 (5) |
OW17—O1—O3 | 61.1 (5) | O28—O23—O27 | 42.3 (4) |
O4—O1—O3 | 73.5 (5) | O19—O23—O27 | 52.8 (4) |
O8—O1—O3 | 57.6 (5) | O30vi—O23—O27 | 135.6 (7) |
Cr2—O1—OW35 | 93.2 (6) | O22—O23—O27 | 84.6 (5) |
U2—O1—OW35 | 114.4 (6) | O30—O23—O27 | 41.0 (4) |
O9—O1—OW35 | 129.0 (7) | Cr4—O23—O27 | 24.4 (2) |
O12—O1—OW35 | 70.6 (6) | O21—O23—O27 | 44.8 (3) |
O10—O1—OW35 | 82.2 (6) | O22ix—O23—O27 | 81.9 (4) |
OW17—O1—OW35 | 163.4 (7) | Cr5—O24—U3 | 134.4 (8) |
O4—O1—OW35 | 95.6 (6) | Cr5—O24—O25 | 34.3 (4) |
O8—O1—OW35 | 67.1 (6) | U3—O24—O25 | 100.3 (6) |
O3—O1—OW35 | 123.2 (7) | Cr5—O24—O20 | 35.1 (4) |
Cr2—O1—OW17i | 77.2 (5) | U3—O24—O20 | 139.0 (6) |
U2—O1—OW17i | 88.1 (5) | O25—O24—O20 | 59.5 (5) |
O9—O1—OW17i | 103.0 (5) | Cr5—O24—O29 | 34.5 (4) |
O12—O1—OW17i | 89.0 (5) | U3—O24—O29 | 144.7 (6) |
O10—O1—OW17i | 42.9 (4) | O25—O24—O29 | 59.0 (5) |
OW17—O1—OW17i | 130.1 (5) | O20—O24—O29 | 58.4 (5) |
O4—O1—OW17i | 108.3 (5) | Cr5—O24—O27 | 134.4 (7) |
O8—O1—OW17i | 42.9 (4) | U3—O24—O27 | 52.3 (4) |
O3—O1—OW17i | 70.4 (4) | O25—O24—O27 | 116.7 (6) |
OW35—O1—OW17i | 60.6 (5) | O20—O24—O27 | 166.8 (6) |
Cr2—O1—O3i | 57.8 (4) | O29—O24—O27 | 108.5 (5) |
U2—O1—O3i | 127.5 (5) | Cr5—O24—O31v | 99.8 (7) |
O9—O1—O3i | 94.4 (5) | U3—O24—O31v | 53.5 (4) |
O12—O1—O3i | 51.7 (4) | O25—O24—O31v | 78.7 (6) |
O10—O1—O3i | 42.8 (4) | O20—O24—O31v | 86.3 (6) |
OW17—O1—O3i | 156.7 (6) | O29—O24—O31v | 134.1 (7) |
O4—O1—O3i | 130.8 (5) | O27—O24—O31v | 105.7 (6) |
O8—O1—O3i | 75.6 (4) | Cr5—O24—O21 | 100.1 (7) |
O3—O1—O3i | 109.8 (4) | U3—O24—O21 | 36.9 (4) |
OW35—O1—O3i | 39.9 (5) | O25—O24—O21 | 66.5 (5) |
OW17i—O1—O3i | 41.0 (3) | O20—O24—O21 | 121.5 (7) |
Cr1—O2—U2 | 132.0 (8) | O29—O24—O21 | 109.9 (6) |
Cr1—O2—O14 | 34.2 (5) | O27—O24—O21 | 62.0 (5) |
U2—O2—O14 | 157.1 (8) | O31v—O24—O21 | 62.1 (5) |
Cr1—O2—N4 | 116.4 (9) | Cr5—O24—O26 | 160.0 (8) |
U2—O2—N4 | 111.3 (7) | U3—O24—O26 | 35.9 (4) |
O14—O2—N4 | 87.4 (7) | O25—O24—O26 | 132.1 (6) |
Cr1—O2—O7 | 34.3 (4) | O20—O24—O26 | 133.2 (6) |
U2—O2—O7 | 101.4 (6) | O29—O24—O26 | 165.5 (7) |
O14—O2—O7 | 58.2 (5) | O27—O24—O26 | 59.5 (5) |
N4—O2—O7 | 145.3 (8) | O31v—O24—O26 | 60.2 (5) |
Cr1—O2—O6 | 35.1 (4) | O21—O24—O26 | 72.8 (5) |
U2—O2—O6 | 122.9 (7) | Cr5—O24—O30 | 83.4 (6) |
O14—O2—O6 | 58.6 (5) | U3—O24—O30 | 97.1 (5) |
N4—O2—O6 | 108.1 (7) | O25—O24—O30 | 83.7 (6) |
O7—O2—O6 | 59.6 (5) | O20—O24—O30 | 113.7 (6) |
Cr1—O2—O10ii | 102.3 (7) | O29—O24—O30 | 55.4 (5) |
U2—O2—O10ii | 53.5 (4) | O27—O24—O30 | 53.3 (5) |
O14—O2—O10ii | 132.9 (7) | O31v—O24—O30 | 141.2 (6) |
N4—O2—O10ii | 111.9 (7) | O21—O24—O30 | 79.2 (5) |
O7—O2—O10ii | 96.4 (6) | O26—O24—O30 | 112.7 (6) |
O6—O2—O10ii | 74.4 (5) | Cr5—O24—Cr4 | 110.7 (5) |
Cr1—O2—O8 | 127.0 (7) | U3—O24—Cr4 | 78.5 (3) |
U2—O2—O8 | 53.1 (4) | O25—O24—Cr4 | 106.5 (5) |
O14—O2—O8 | 115.4 (6) | O20—O24—Cr4 | 138.8 (5) |
N4—O2—O8 | 92.5 (7) | O29—O24—Cr4 | 81.0 (4) |
O7—O2—O8 | 98.3 (6) | O27—O24—Cr4 | 28.0 (3) |
O6—O2—O8 | 157.5 (7) | O31v—O24—Cr4 | 131.4 (5) |
O10ii—O2—O8 | 106.6 (6) | O21—O24—Cr4 | 75.7 (4) |
Cr1—O2—O3 | 164.9 (8) | O26—O24—Cr4 | 86.1 (4) |
U2—O2—O3 | 37.3 (4) | O30—O24—Cr4 | 27.3 (3) |
O14—O2—O3 | 160.4 (8) | Cr5—O24—O18v | 57.3 (5) |
N4—O2—O3 | 74.5 (6) | U3—O24—O18v | 94.8 (4) |
O7—O2—O3 | 138.7 (8) | O25—O24—O18v | 50.1 (4) |
O6—O2—O3 | 133.9 (6) | O20—O24—O18v | 44.4 (4) |
O10ii—O2—O3 | 63.0 (5) | O29—O24—O18v | 91.6 (5) |
O8—O2—O3 | 59.4 (5) | O27—O24—O18v | 144.8 (5) |
Cr1—O2—O4 | 97.1 (7) | O31v—O24—O18v | 44.3 (4) |
U2—O2—O4 | 36.0 (3) | O21—O24—O18v | 84.2 (5) |
O14—O2—O4 | 122.8 (7) | O26—O24—O18v | 102.8 (5) |
N4—O2—O4 | 146.4 (7) | O30—O24—O18v | 133.7 (6) |
O7—O2—O4 | 65.4 (5) | Cr4—O24—O18v | 154.6 (5) |
O6—O2—O4 | 100.9 (6) | Cr5—O25—O24 | 35.7 (5) |
O10ii—O2—O4 | 60.2 (5) | Cr5—O25—O20 | 35.7 (5) |
O8—O2—O4 | 62.7 (5) | O24—O25—O20 | 61.1 (5) |
O3—O2—O4 | 73.3 (5) | Cr5—O25—O29 | 36.9 (4) |
Cr1—O2—O12ii | 105.1 (6) | O24—O25—O29 | 62.7 (5) |
U2—O2—O12ii | 91.6 (5) | O20—O25—O29 | 60.1 (5) |
O14—O2—O12ii | 109.2 (6) | Cr5—O25—O18v | 87.1 (6) |
N4—O2—O12ii | 63.3 (6) | O24—O25—O18v | 87.4 (6) |
O7—O2—O12ii | 128.4 (6) | O20—O25—O18v | 57.6 (5) |
O6—O2—O12ii | 71.4 (5) | O29—O25—O18v | 117.7 (6) |
O10ii—O2—O12ii | 53.3 (5) | Cr5—O25—N3 | 151.0 (9) |
O8—O2—O12ii | 127.8 (6) | O24—O25—N3 | 117.0 (7) |
O3—O2—O12ii | 69.5 (5) | O20—O25—N3 | 160.7 (7) |
O4—O2—O12ii | 112.7 (6) | O29—O25—N3 | 138.0 (7) |
Cr1—O2—O16 | 88.9 (6) | O18v—O25—N3 | 103.9 (6) |
U2—O2—O16 | 104.9 (6) | Cr5—O25—O21 | 96.4 (7) |
O14—O2—O16 | 64.5 (5) | O24—O25—O21 | 61.3 (5) |
N4—O2—O16 | 79.0 (6) | O20—O25—O21 | 118.3 (7) |
O7—O2—O16 | 81.9 (5) | O29—O25—O21 | 108.8 (6) |
O6—O2—O16 | 122.0 (6) | O18v—O25—O21 | 99.9 (5) |
O10ii—O2—O16 | 157.8 (7) | N3—O25—O21 | 55.7 (5) |
O8—O2—O16 | 52.3 (5) | Cr5—O25—C2 | 139.0 (9) |
O3—O2—O16 | 104.0 (6) | O24—O25—C2 | 118.9 (8) |
O4—O2—O16 | 99.7 (6) | O20—O25—C2 | 171.1 (8) |
O12ii—O2—O16 | 142.3 (7) | O29—O25—C2 | 111.4 (7) |
U2—O3—O8 | 55.9 (5) | O18v—O25—C2 | 130.8 (7) |
U2—O3—OW35ii | 145.7 (9) | N3—O25—C2 | 28.2 (5) |
O8—O3—OW35ii | 155.4 (8) | O21—O25—C2 | 65.9 (6) |
U2—O3—O2 | 53.7 (5) | Cr5—O25—O32v | 122.8 (7) |
O8—O3—O2 | 59.5 (5) | O24—O25—O32v | 98.2 (6) |
OW35ii—O3—O2 | 137.0 (9) | O20—O25—O32v | 105.2 (6) |
U2—O3—OW17 | 58.1 (5) | O29—O25—O32v | 159.5 (7) |
O8—O3—OW17 | 104.6 (7) | O18v—O25—O32v | 50.0 (4) |
OW35ii—O3—OW17 | 89.6 (8) | N3—O25—O32v | 55.6 (5) |
O2—O3—OW17 | 103.9 (6) | O21—O25—O32v | 63.7 (5) |
U2—O3—O10ii | 52.3 (5) | C2—O25—O32v | 83.7 (6) |
O8—O3—O10ii | 102.7 (6) | Cr5—O25—Cr6v | 96.4 (6) |
OW35ii—O3—O10ii | 101.9 (7) | O24—O25—Cr6v | 79.3 (5) |
O2—O3—O10ii | 57.8 (5) | O20—O25—Cr6v | 78.3 (4) |
OW17—O3—O10ii | 56.1 (5) | O29—O25—Cr6v | 133.1 (6) |
U2—O3—O1 | 50.1 (5) | O18v—O25—Cr6v | 29.4 (3) |
O8—O3—O1 | 57.2 (5) | N3—O25—Cr6v | 82.5 (5) |
OW35ii—O3—O1 | 121.9 (8) | O21—O25—Cr6v | 71.2 (4) |
O2—O3—O1 | 98.3 (6) | C2—O25—Cr6v | 110.6 (6) |
OW17—O3—O1 | 54.3 (5) | O32v—O25—Cr6v | 27.8 (3) |
O10ii—O3—O1 | 93.2 (6) | Cr5—O25—O22ix | 90.4 (6) |
U2—O3—O12ii | 93.2 (6) | O24—O25—O22ix | 98.4 (6) |
O8—O3—O12ii | 116.8 (6) | O20—O25—O22ix | 114.7 (6) |
OW35ii—O3—O12ii | 79.8 (7) | O29—O25—O22ix | 55.8 (4) |
O2—O3—O12ii | 58.1 (4) | O18v—O25—O22ix | 166.3 (6) |
OW17—O3—O12ii | 98.7 (5) | N3—O25—O22ix | 84.6 (5) |
O10ii—O3—O12ii | 48.8 (5) | O21—O25—O22ix | 93.7 (5) |
O1—O3—O12ii | 141.2 (6) | C2—O25—O22ix | 56.5 (6) |
U2—O3—O4 | 0.7 (3) | O32v—O25—O22ix | 140.1 (6) |
O8—O3—O4 | 55.9 (5) | Cr6v—O25—O22ix | 164.0 (5) |
OW35ii—O3—O4 | 145.5 (8) | Cr5—O25—O31v | 78.6 (6) |
O2—O3—O4 | 54.3 (4) | O24—O25—O31v | 53.6 (5) |
OW17—O3—O4 | 57.7 (4) | O20—O25—O31v | 75.1 (5) |
O10ii—O3—O4 | 52.6 (4) | O29—O25—O31v | 114.0 (6) |
O1—O3—O4 | 49.5 (4) | O18v—O25—O31v | 48.9 (4) |
O12ii—O3—O4 | 93.7 (5) | N3—O25—O31v | 88.6 (5) |
U2—O3—O10 | 93.5 (6) | O21—O25—O31v | 53.8 (4) |
O8—O3—O10 | 67.0 (5) | C2—O25—O31v | 112.5 (6) |
OW35ii—O3—O10 | 94.9 (7) | O32v—O25—O31v | 45.6 (4) |
O2—O3—O10 | 126.4 (6) | Cr6v—O25—O31v | 27.2 (3) |
OW17—O3—O10 | 85.2 (5) | O22ix—O25—O31v | 143.4 (6) |
O10ii—O3—O10 | 137.1 (5) | U3—O26—O27 | 54.0 (5) |
O1—O3—O10 | 45.3 (4) | U3—O26—O18 | 53.4 (5) |
O12ii—O3—O10 | 173.3 (6) | O27—O26—O18 | 55.2 (4) |
O4—O3—O10 | 93.0 (5) | U3—O26—O31v | 54.8 (5) |
U2—O3—Cr2ii | 76.3 (5) | O27—O26—O31v | 102.7 (6) |
O8—O3—Cr2ii | 118.9 (5) | O18—O26—O31v | 99.9 (6) |
OW35ii—O3—Cr2ii | 84.1 (7) | U3—O26—O20iv | 52.9 (5) |
O2—O3—Cr2ii | 62.0 (4) | O27—O26—O20iv | 98.4 (6) |
OW17—O3—Cr2ii | 73.5 (4) | O18—O26—O20iv | 55.1 (5) |
O10ii—O3—Cr2ii | 25.4 (3) | O31v—O26—O20iv | 56.1 (5) |
O1—O3—Cr2ii | 118.2 (5) | U3—O26—O24 | 52.7 (5) |
O12ii—O3—Cr2ii | 25.5 (3) | O27—O26—O24 | 58.0 (4) |
O4—O3—Cr2ii | 76.7 (3) | O18—O26—O24 | 99.1 (6) |
O10—O3—Cr2ii | 158.7 (5) | O31v—O26—O24 | 57.8 (5) |
U2—O3—O33x | 142.9 (7) | O20iv—O26—O24 | 98.9 (6) |
O8—O3—O33x | 121.9 (6) | U3—O26—C3xiii | 125.8 (10) |
OW35ii—O3—O33x | 52.1 (7) | O27—O26—C3xiii | 147.7 (9) |
O2—O3—O33x | 91.8 (6) | O18—O26—C3xiii | 97.0 (8) |
OW17—O3—O33x | 132.3 (6) | O31v—O26—C3xiii | 97.8 (9) |
O10ii—O3—O33x | 100.3 (6) | O20iv—O26—C3xiii | 72.9 (8) |
O1—O3—O33x | 166.1 (6) | O24—O26—C3xiii | 152.7 (9) |
O12ii—O3—O33x | 52.7 (4) | U3—O26—C7v | 123.7 (8) |
O4—O3—O33x | 143.5 (5) | O27—O26—C7v | 124.5 (7) |
O10—O3—O33x | 120.7 (5) | O18—O26—C7v | 176.9 (8) |
Cr2ii—O3—O33x | 75.1 (4) | O31v—O26—C7v | 77.1 (7) |
U2—O4—O1 | 57.7 (5) | O20iv—O26—C7v | 122.8 (7) |
U2—O4—O10ii | 54.5 (5) | O24—O26—C7v | 78.7 (6) |
O1—O4—O10ii | 101.4 (6) | C3xiii—O26—C7v | 84.2 (9) |
U2—O4—O2 | 51.8 (5) | U3—O26—O21 | 0.4 (4) |
O1—O4—O2 | 103.4 (6) | O27—O26—O21 | 54.4 (5) |
O10ii—O4—O2 | 57.9 (5) | O18—O26—O21 | 53.7 (4) |
U2—O4—O8 | 51.1 (4) | O31v—O26—O21 | 54.3 (5) |
O1—O4—O8 | 58.2 (5) | O20iv—O26—O21 | 52.7 (4) |
O10ii—O4—O8 | 100.4 (6) | O24—O26—O21 | 52.6 (4) |
O2—O4—O8 | 56.8 (5) | C3xiii—O26—O21 | 125.6 (9) |
U2—O4—O7 | 105.4 (7) | C7v—O26—O21 | 123.3 (7) |
O1—O4—O7 | 145.4 (6) | U3—O26—OW34v | 83.8 (6) |
O10ii—O4—O7 | 87.7 (5) | O27—O26—OW34v | 137.4 (6) |
O2—O4—O7 | 53.6 (4) | O18—O26—OW34v | 96.9 (5) |
O8—O4—O7 | 87.4 (5) | O31v—O26—OW34v | 45.8 (4) |
U2—O4—OW17 | 53.1 (4) | O20iv—O26—OW34v | 43.0 (4) |
O1—O4—OW17 | 54.9 (4) | O24—O26—OW34v | 103.5 (5) |
O10ii—O4—OW17 | 54.9 (5) | C3xiii—O26—OW34v | 52.6 (8) |
O2—O4—OW17 | 97.9 (5) | C7v—O26—OW34v | 81.5 (6) |
O8—O4—OW17 | 96.1 (5) | O21—O26—OW34v | 83.5 (5) |
O7—O4—OW17 | 142.6 (6) | Cr4—O27—U3 | 144.7 (8) |
U2—O4—C1ii | 148.6 (7) | Cr4—O27—O33 | 34.2 (5) |
O1—O4—C1ii | 136.9 (7) | U3—O27—O33 | 150.4 (6) |
O10ii—O4—C1ii | 94.4 (6) | Cr4—O27—O30 | 34.2 (5) |
O2—O4—C1ii | 118.8 (6) | U3—O27—O30 | 110.6 (6) |
O8—O4—C1ii | 155.9 (7) | O33—O27—O30 | 58.5 (6) |
O7—O4—C1ii | 74.2 (6) | Cr4—O27—O18 | 143.6 (7) |
OW17—O4—C1ii | 107.9 (6) | U3—O27—O18 | 54.9 (4) |
U2—O4—O15 | 100.4 (6) | O33—O27—O18 | 151.4 (7) |
O1—O4—O15 | 97.3 (5) | O30—O27—O18 | 141.1 (8) |
O10ii—O4—O15 | 128.5 (6) | Cr4—O27—O28 | 35.3 (4) |
O2—O4—O15 | 71.2 (5) | U3—O27—O28 | 144.0 (7) |
O8—O4—O15 | 52.3 (4) | O33—O27—O28 | 58.5 (5) |
O7—O4—O15 | 53.3 (4) | O30—O27—O28 | 59.5 (5) |
OW17—O4—O15 | 147.9 (6) | O18—O27—O28 | 108.7 (6) |
C1ii—O4—O15 | 103.6 (6) | Cr4—O27—O24 | 98.5 (6) |
U2—O4—O3 | 0.7 (3) | U3—O27—O24 | 53.3 (4) |
O1—O4—O3 | 57.0 (5) | O33—O27—O24 | 98.8 (6) |
O10ii—O4—O3 | 54.9 (4) | O30—O27—O24 | 68.3 (5) |
O2—O4—O3 | 52.4 (4) | O18—O27—O24 | 108.2 (6) |
O8—O4—O3 | 51.1 (4) | O28—O27—O24 | 127.5 (6) |
O7—O4—O3 | 106.0 (6) | Cr4—O27—O26 | 153.5 (7) |
OW17—O4—O3 | 52.7 (4) | U3—O27—O26 | 37.2 (4) |
C1ii—O4—O3 | 148.9 (6) | O33—O27—O26 | 125.8 (7) |
O15—O4—O3 | 100.6 (5) | O30—O27—O26 | 130.7 (7) |
U2—O4—Cr1 | 79.5 (5) | O18—O27—O26 | 62.8 (5) |
O1—O4—Cr1 | 130.4 (6) | O28—O27—O26 | 169.7 (7) |
O10ii—O4—Cr1 | 66.6 (4) | O24—O27—O26 | 62.5 (5) |
O2—O4—Cr1 | 28.2 (3) | Cr4—O27—O21 | 114.8 (8) |
O8—O4—Cr1 | 76.2 (4) | U3—O27—O21 | 36.0 (4) |
O7—O4—Cr1 | 26.8 (3) | O33—O27—O21 | 143.7 (7) |
OW17—O4—Cr1 | 118.5 (5) | O30—O27—O21 | 85.4 (6) |
C1ii—O4—Cr1 | 92.7 (5) | O18—O27—O21 | 62.4 (5) |
O15—O4—Cr1 | 64.8 (3) | O28—O27—O21 | 108.9 (6) |
O3—O4—Cr1 | 80.2 (4) | O24—O27—O21 | 60.0 (5) |
U2—O4—Cr3 | 74.7 (4) | O26—O27—O21 | 73.2 (5) |
O1—O4—Cr3 | 79.0 (4) | Cr4—O27—N1xii | 109.7 (8) |
O10ii—O4—Cr3 | 114.3 (5) | U3—O27—N1xii | 105.6 (6) |
O2—O4—Cr3 | 58.4 (4) | O33—O27—N1xii | 89.1 (7) |
O8—O4—Cr3 | 26.3 (3) | O30—O27—N1xii | 143.8 (8) |
O7—O4—Cr3 | 66.9 (3) | O18—O27—N1xii | 64.4 (7) |
OW17—O4—Cr3 | 122.5 (5) | O28—O27—N1xii | 91.0 (7) |
C1ii—O4—Cr3 | 129.6 (5) | O24—O27—N1xii | 138.7 (7) |
O15—O4—Cr3 | 26.3 (3) | O26—O27—N1xii | 80.0 (7) |
O3—O4—Cr3 | 74.8 (4) | O21—O27—N1xii | 126.7 (7) |
Cr1—O4—Cr3 | 65.6 (2) | Cr4—O27—C6xii | 108.7 (8) |
U1—O5—O15iii | 55.7 (5) | U3—O27—C6xii | 103.0 (7) |
U1—O5—N1 | 170.5 (9) | O33—O27—C6xii | 77.7 (7) |
O15iii—O5—N1 | 121.0 (8) | O30—O27—C6xii | 135.3 (8) |
U1—O5—O13ii | 54.3 (5) | O18—O27—C6xii | 82.7 (7) |
O15iii—O5—O13ii | 101.6 (6) | O28—O27—C6xii | 106.3 (8) |
N1—O5—O13ii | 121.9 (8) | O24—O27—C6xii | 114.2 (7) |
U1—O5—O7iii | 52.9 (5) | O26—O27—C6xii | 67.8 (7) |
O15iii—O5—O7iii | 57.9 (4) | O21—O27—C6xii | 136.5 (7) |
N1—O5—O7iii | 117.6 (8) | N1xii—O27—C6xii | 28.5 (7) |
O13ii—O5—O7iii | 54.4 (4) | Cr4—O27—O19 | 91.2 (6) |
U1—O5—O9 | 53.2 (5) | U3—O27—O19 | 98.0 (5) |
O15iii—O5—O9 | 102.1 (6) | O33—O27—O19 | 111.1 (6) |
N1—O5—O9 | 134.1 (8) | O30—O27—O19 | 103.0 (6) |
O13ii—O5—O9 | 56.5 (5) | O18—O27—O19 | 52.4 (4) |
O7iii—O5—O9 | 97.7 (6) | O28—O27—O19 | 56.5 (4) |
U1—O5—O6i | 50.1 (5) | O24—O27—O19 | 138.2 (7) |
O15iii—O5—O6i | 56.4 (5) | O26—O27—O19 | 115.2 (5) |
N1—O5—O6i | 137.4 (7) | O21—O27—O19 | 79.0 (5) |
O13ii—O5—O6i | 97.9 (6) | N1xii—O27—O19 | 72.1 (6) |
O7iii—O5—O6i | 96.7 (6) | C6xii—O27—O19 | 100.5 (7) |
O9—O5—O6i | 56.0 (5) | Cr4—O28—U4 | 137.7 (8) |
U1—O5—C1 | 151.0 (8) | Cr4—O28—O33 | 35.1 (5) |
O15iii—O5—C1 | 96.1 (6) | U4—O28—O33 | 172.7 (8) |
N1—O5—C1 | 30.0 (7) | Cr4—O28—O30 | 34.4 (5) |
O13ii—O5—C1 | 150.9 (8) | U4—O28—O30 | 114.9 (7) |
O7iii—O5—C1 | 121.0 (7) | O33—O28—O30 | 59.0 (6) |
O9—O5—C1 | 141.1 (7) | Cr4—O28—O27 | 35.4 (4) |
O6i—O5—C1 | 111.1 (6) | U4—O28—O27 | 114.5 (6) |
U1—O5—OW35ii | 112.0 (8) | O33—O28—O27 | 59.7 (5) |
O15iii—O5—OW35ii | 141.2 (8) | O30—O28—O27 | 59.8 (5) |
N1—O5—OW35ii | 64.4 (8) | Cr4—O28—O29vi | 130.3 (8) |
O13ii—O5—OW35ii | 57.8 (7) | U4—O28—O29vi | 52.5 (4) |
O7iii—O5—OW35ii | 84.9 (7) | O33—O28—O29vi | 129.7 (7) |
O9—O5—OW35ii | 92.7 (7) | O30—O28—O29vi | 96.7 (6) |
O6i—O5—OW35ii | 148.7 (8) | O27—O28—O29vi | 147.9 (7) |
C1—O5—OW35ii | 94.2 (8) | Cr4—O28—O19 | 106.1 (7) |
U1—O5—C6 | 158.8 (9) | U4—O28—O19 | 51.6 (4) |
O15iii—O5—C6 | 143.5 (8) | O33—O28—O19 | 125.8 (7) |
N1—O5—C6 | 28.1 (8) | O30—O28—O19 | 114.5 (7) |
O13ii—O5—C6 | 113.1 (7) | O27—O28—O19 | 71.3 (5) |
O7iii—O5—C6 | 137.8 (8) | O29vi—O28—O19 | 104.1 (6) |
O9—O5—C6 | 106.1 (7) | Cr4—O28—O23 | 102.3 (7) |
O6i—O5—C6 | 125.5 (7) | U4—O28—O23 | 37.1 (4) |
C1—O5—C6 | 47.6 (7) | O33—O28—O23 | 136.0 (7) |
OW35ii—O5—C6 | 60.1 (8) | O30—O28—O23 | 78.2 (6) |
U1—O5—O10 | 98.0 (7) | O27—O28—O23 | 91.6 (6) |
O15iii—O5—O10 | 118.2 (6) | O29vi—O28—O23 | 60.4 (5) |
N1—O5—O10 | 91.3 (7) | O19—O28—O23 | 61.6 (5) |
O13ii—O5—O10 | 101.9 (6) | Cr4—O28—N2 | 97.9 (10) |
O7iii—O5—O10 | 148.9 (7) | U4—O28—N2 | 123.9 (10) |
O9—O5—O10 | 51.6 (4) | O33—O28—N2 | 63.2 (9) |
O6i—O5—O10 | 64.3 (5) | O30—O28—N2 | 108.2 (10) |
C1—O5—O10 | 89.5 (6) | O27—O28—N2 | 117.5 (10) |
OW35ii—O5—O10 | 99.1 (7) | O29vi—O28—N2 | 89.4 (9) |
C6—O5—O10 | 66.1 (7) | O19—O28—N2 | 132.9 (10) |
U1—O5—O14iii | 101.9 (6) | O23—O28—N2 | 149.7 (10) |
O15iii—O5—O14iii | 81.3 (5) | Cr4—O28—O22 | 164.7 (8) |
N1—O5—O14iii | 68.6 (7) | U4—O28—O22 | 36.8 (4) |
O13ii—O5—O14iii | 82.5 (5) | O33—O28—O22 | 149.8 (8) |
O7iii—O5—O14iii | 49.1 (5) | O30—O28—O22 | 150.7 (8) |
O9—O5—O14iii | 138.8 (6) | O27—O28—O22 | 129.3 (6) |
O6i—O5—O14iii | 137.1 (6) | O29vi—O28—O22 | 61.4 (5) |
C1—O5—O14iii | 77.6 (6) | O19—O28—O22 | 58.9 (5) |
OW35ii—O5—O14iii | 64.6 (7) | O23—O28—O22 | 74.0 (5) |
C6—O5—O14iii | 92.2 (7) | N2—O28—O22 | 91.8 (9) |
O10—O5—O14iii | 158.0 (7) | Cr4—O28—OW34ix | 81.0 (5) |
Cr1—O6—U1ii | 143.3 (9) | U4—O28—OW34ix | 98.1 (5) |
Cr1—O6—O14 | 34.4 (5) | O33—O28—OW34ix | 81.2 (5) |
U1ii—O6—O14 | 155.0 (7) | O30—O28—OW34ix | 53.0 (5) |
Cr1—O6—O7 | 34.0 (4) | O27—O28—OW34ix | 112.5 (6) |
U1ii—O6—O7 | 110.1 (7) | O29vi—O28—OW34ix | 51.7 (4) |
O14—O6—O7 | 58.6 (5) | O19—O28—OW34ix | 142.4 (7) |
Cr1—O6—O2 | 36.2 (4) | O23—O28—OW34ix | 80.8 (5) |
U1ii—O6—O2 | 137.7 (7) | N2—O28—OW34ix | 80.4 (9) |
O14—O6—O2 | 59.6 (5) | O22—O28—OW34ix | 112.6 (6) |
O7—O6—O2 | 59.8 (5) | Cr4—O28—OW35iii | 79.3 (7) |
Cr1—O6—O15vii | 101.0 (7) | U4—O28—OW35iii | 135.2 (7) |
U1ii—O6—O15vii | 54.1 (4) | O33—O28—OW35iii | 50.3 (6) |
O14—O6—O15vii | 101.3 (6) | O30—O28—OW35iii | 109.1 (7) |
O7—O6—O15vii | 70.8 (5) | O27—O28—OW35iii | 80.4 (6) |
O2—O6—O15vii | 130.1 (7) | O29vi—O28—OW35iii | 130.6 (7) |
Cr1—O6—O9ii | 134.6 (8) | O19—O28—OW35iii | 102.2 (7) |
U1ii—O6—O9ii | 54.0 (4) | O23—O28—OW35iii | 163.7 (7) |
O14—O6—O9ii | 150.9 (7) | N2—O28—OW35iii | 43.2 (10) |
O7—O6—O9ii | 131.6 (7) | O22—O28—OW35iii | 100.1 (7) |
O2—O6—O9ii | 99.7 (6) | OW34ix—O28—OW35iii | 115.4 (6) |
O15vii—O6—O9ii | 107.8 (6) | Cr5—O29—U4ix | 139.4 (7) |
Cr1—O6—O11ii | 162.8 (8) | Cr5—O29—O20 | 36.5 (4) |
U1ii—O6—O11ii | 38.1 (4) | U4ix—O29—O20 | 169.1 (7) |
O14—O6—O11ii | 133.5 (7) | Cr5—O29—O25 | 34.3 (4) |
O7—O6—O11ii | 137.0 (7) | U4ix—O29—O25 | 111.7 (6) |
O2—O6—O11ii | 160.6 (7) | O20—O29—O25 | 59.6 (5) |
O15vii—O6—O11ii | 66.3 (5) | Cr5—O29—OW34iii | 102.1 (6) |
O9ii—O6—O11ii | 62.3 (5) | U4ix—O29—OW34iii | 117.0 (6) |
Cr1—O6—O5ii | 110.4 (8) | O20—O29—OW34iii | 65.6 (5) |
U1ii—O6—O5ii | 35.7 (3) | O25—O29—OW34iii | 115.9 (6) |
O14—O6—O5ii | 139.9 (7) | Cr5—O29—O30 | 95.3 (6) |
O7—O6—O5ii | 81.4 (6) | U4ix—O29—O30 | 54.8 (4) |
O2—O6—O5ii | 104.7 (6) | O20—O29—O30 | 128.4 (6) |
O15vii—O6—O5ii | 58.6 (5) | O25—O29—O30 | 91.1 (6) |
O9ii—O6—O5ii | 60.9 (5) | OW34iii—O29—O30 | 151.5 (7) |
O11ii—O6—O5ii | 73.9 (5) | Cr5—O29—O24 | 33.4 (4) |
Cr1—O6—Cr2ii | 105.2 (6) | U4ix—O29—O24 | 123.3 (6) |
U1ii—O6—Cr2ii | 80.3 (4) | O20—O29—O24 | 59.4 (5) |
O14—O6—Cr2ii | 124.2 (6) | O25—O29—O24 | 58.3 (5) |
O7—O6—Cr2ii | 113.3 (5) | OW34iii—O29—O24 | 116.1 (6) |
O2—O6—Cr2ii | 69.6 (4) | O30—O29—O24 | 69.1 (5) |
O15vii—O6—Cr2ii | 129.7 (6) | Cr5—O29—O28ix | 140.0 (8) |
O9ii—O6—Cr2ii | 30.2 (3) | U4ix—O29—O28ix | 52.5 (4) |
O11ii—O6—Cr2ii | 92.0 (5) | O20—O29—O28ix | 122.2 (6) |
O5ii—O6—Cr2ii | 72.1 (4) | O25—O29—O28ix | 111.0 (7) |
Cr1—O6—O10ii | 84.3 (6) | OW34iii—O29—O28ix | 73.0 (5) |
U1ii—O6—O10ii | 85.4 (5) | O30—O29—O28ix | 107.2 (6) |
O14—O6—O10ii | 113.6 (6) | O24—O29—O28ix | 167.8 (7) |
O7—O6—O10ii | 85.1 (5) | Cr5—O29—O23ix | 157.4 (8) |
O2—O6—O10ii | 54.1 (4) | U4ix—O29—O23ix | 37.4 (4) |
O15vii—O6—O10ii | 117.5 (7) | O20—O29—O23ix | 152.1 (7) |
O9ii—O6—O10ii | 51.5 (4) | O25—O29—O23ix | 148.1 (6) |
O11ii—O6—O10ii | 111.5 (6) | OW34iii—O29—O23ix | 92.1 (5) |
O5ii—O6—O10ii | 61.3 (5) | O30—O29—O23ix | 65.3 (5) |
Cr2ii—O6—O10ii | 28.5 (3) | O24—O29—O23ix | 124.1 (7) |
Cr1—O6—O12ii | 94.0 (6) | O28ix—O29—O23ix | 61.0 (5) |
U1ii—O6—O12ii | 103.9 (5) | Cr5—O29—O22ix | 107.4 (6) |
O14—O6—O12ii | 101.0 (6) | U4ix—O29—O22ix | 36.5 (3) |
O7—O6—O12ii | 116.8 (6) | O20—O29—O22ix | 133.5 (7) |
O2—O6—O12ii | 59.1 (4) | O25—O29—O22ix | 75.8 (5) |
O15vii—O6—O12ii | 156.9 (6) | OW34iii—O29—O22ix | 132.6 (7) |
O9ii—O6—O12ii | 50.0 (4) | O30—O29—O22ix | 60.1 (5) |
O11ii—O6—O12ii | 101.8 (5) | O24—O29—O22ix | 108.9 (6) |
O5ii—O6—O12ii | 99.7 (5) | O28ix—O29—O22ix | 60.5 (5) |
Cr2ii—O6—O12ii | 27.6 (3) | O23ix—O29—O22ix | 73.8 (5) |
O10ii—O6—O12ii | 46.3 (4) | Cr5—O29—O30ix | 141.6 (6) |
Cr1—O7—U1xi | 143.2 (8) | U4ix—O29—O30ix | 76.2 (4) |
Cr1—O7—O14 | 34.7 (5) | O20—O29—O30ix | 105.6 (5) |
U1xi—O7—O14 | 110.0 (6) | O25—O29—O30ix | 138.4 (6) |
Cr1—O7—O13vii | 125.1 (8) | OW34iii—O29—O30ix | 40.7 (4) |
U1xi—O7—O13vii | 55.4 (4) | O30—O29—O30ix | 122.3 (4) |
O14—O7—O13vii | 101.8 (6) | O24—O29—O30ix | 151.7 (6) |
Cr1—O7—O6 | 34.9 (4) | O28ix—O29—O30ix | 40.2 (4) |
U1xi—O7—O6 | 158.7 (7) | O23ix—O29—O30ix | 57.2 (4) |
O14—O7—O6 | 59.6 (6) | O22ix—O29—O30ix | 98.6 (5) |
O13vii—O7—O6 | 106.4 (6) | Cr4—O30—U4ix | 155.6 (9) |
Cr1—O7—O2 | 36.4 (4) | Cr4—O30—O33 | 34.8 (5) |
U1xi—O7—O2 | 133.3 (6) | U4ix—O30—O33 | 125.5 (7) |
O14—O7—O2 | 60.2 (6) | Cr4—O30—O28 | 35.6 (5) |
O13vii—O7—O2 | 160.9 (8) | U4ix—O30—O28 | 132.2 (7) |
O6—O7—O2 | 60.6 (5) | O33—O30—O28 | 59.4 (6) |
Cr1—O7—O15 | 107.6 (7) | Cr4—O30—O27 | 35.5 (4) |
U1xi—O7—O15 | 53.8 (4) | U4ix—O30—O27 | 167.0 (7) |
O14—O7—O15 | 96.0 (6) | O33—O30—O27 | 60.1 (6) |
O13vii—O7—O15 | 108.9 (6) | O28—O30—O27 | 60.7 (5) |
O6—O7—O15 | 140.6 (7) | Cr4—O30—OW34ix | 102.6 (8) |
O2—O7—O15 | 80.7 (5) | U4ix—O30—OW34ix | 57.5 (4) |
Cr1—O7—O11xi | 171.3 (7) | O33—O30—OW34ix | 93.5 (7) |
U1xi—O7—O11xi | 37.3 (4) | O28—O30—OW34ix | 75.3 (6) |
O14—O7—O11xi | 147.3 (7) | O27—O30—OW34ix | 135.5 (7) |
O13vii—O7—O11xi | 63.4 (5) | Cr4—O30—O29 | 139.4 (9) |
O6—O7—O11xi | 149.9 (7) | U4ix—O30—O29 | 53.6 (4) |
O2—O7—O11xi | 135.0 (7) | O33—O30—O29 | 118.2 (7) |
O15—O7—O11xi | 65.4 (5) | O28—O30—O29 | 174.2 (8) |
Cr1—O7—O5xi | 106.9 (7) | O27—O30—O29 | 113.6 (6) |
U1xi—O7—O5xi | 37.2 (4) | OW34ix—O30—O29 | 110.4 (7) |
O14—O7—O5xi | 72.9 (6) | Cr4—O30—O22ix | 154.8 (9) |
O13vii—O7—O5xi | 61.6 (5) | U4ix—O30—O22ix | 37.7 (4) |
O6—O7—O5xi | 127.7 (7) | O33—O30—O22ix | 160.6 (7) |
O2—O7—O5xi | 113.6 (6) | O28—O30—O22ix | 121.0 (7) |
O15—O7—O5xi | 59.6 (5) | O27—O30—O22ix | 138.8 (8) |
O11xi—O7—O5xi | 74.5 (5) | OW34ix—O30—O22ix | 69.2 (6) |
Cr1—O7—O4 | 94.6 (6) | O29—O30—O22ix | 63.2 (6) |
U1xi—O7—O4 | 102.6 (5) | Cr4—O30—O23ix | 124.9 (9) |
O14—O7—O4 | 120.3 (6) | U4ix—O30—O23ix | 35.1 (4) |
O13vii—O7—O4 | 137.8 (7) | O33—O30—O23ix | 91.1 (7) |
O6—O7—O4 | 98.6 (5) | O28—O30—O23ix | 124.5 (7) |
O2—O7—O4 | 61.0 (5) | O27—O30—O23ix | 144.6 (8) |
O15—O7—O4 | 65.6 (4) | OW34ix—O30—O23ix | 59.7 (5) |
O11xi—O7—O4 | 77.9 (5) | O29—O30—O23ix | 59.6 (5) |
O5xi—O7—O4 | 124.8 (6) | O22ix—O30—O23ix | 72.8 (6) |
Cr1—O7—O15vii | 87.5 (6) | Cr4—O30—O24 | 90.2 (7) |
U1xi—O7—O15vii | 109.6 (5) | U4ix—O30—O24 | 108.6 (6) |
O14—O7—O15vii | 92.3 (6) | O33—O30—O24 | 93.6 (6) |
O13vii—O7—O15vii | 55.0 (4) | O28—O30—O24 | 118.8 (7) |
O6—O7—O15vii | 55.8 (4) | O27—O30—O24 | 58.4 (5) |
O2—O7—O15vii | 116.0 (6) | OW34ix—O30—O24 | 165.9 (7) |
O15—O7—O15vii | 163.2 (5) | O29—O30—O24 | 55.5 (4) |
O11xi—O7—O15vii | 100.3 (5) | O22ix—O30—O24 | 101.5 (7) |
O5xi—O7—O15vii | 109.6 (5) | O23ix—O30—O24 | 108.0 (6) |
O4—O7—O15vii | 121.8 (5) | Cr4—O30—Cr5 | 119.1 (7) |
Cr1—O7—Cr3vii | 114.6 (6) | U4ix—O30—Cr5 | 80.5 (4) |
U1xi—O7—Cr3vii | 81.2 (4) | O33—O30—Cr5 | 116.5 (6) |
O14—O7—Cr3vii | 108.3 (5) | O28—O30—Cr5 | 145.0 (6) |
O13vii—O7—Cr3vii | 29.6 (3) | O27—O30—Cr5 | 86.5 (5) |
O6—O7—Cr3vii | 84.9 (4) | OW34ix—O30—Cr5 | 137.8 (7) |
O2—O7—Cr3vii | 145.1 (6) | O29—O30—Cr5 | 30.0 (3) |
O15—O7—Cr3vii | 134.2 (6) | O22ix—O30—Cr5 | 75.0 (5) |
O11xi—O7—Cr3vii | 73.8 (4) | O23ix—O30—Cr5 | 89.1 (5) |
O5xi—O7—Cr3vii | 90.8 (4) | O24—O30—Cr5 | 29.0 (3) |
O4—O7—Cr3vii | 125.4 (5) | Cr4—O30—O23 | 81.0 (6) |
O15vii—O7—Cr3vii | 29.1 (3) | U4ix—O30—O23 | 106.2 (6) |
Cr3—O8—U2 | 129.8 (7) | O33—O30—O23 | 112.4 (7) |
Cr3—O8—O16 | 34.4 (5) | O28—O30—O23 | 53.7 (5) |
U2—O8—O16 | 121.4 (7) | O27—O30—O23 | 79.5 (5) |
Cr3—O8—O13 | 37.0 (4) | OW34ix—O30—O23 | 79.2 (5) |
U2—O8—O13 | 157.9 (8) | O29—O30—O23 | 127.3 (7) |
O16—O8—O13 | 59.6 (5) | O22ix—O30—O23 | 74.1 (5) |
Cr3—O8—O15 | 34.1 (4) | O23ix—O30—O23 | 134.0 (5) |
U2—O8—O15 | 99.6 (6) | O24—O30—O23 | 109.2 (5) |
O16—O8—O15 | 58.8 (6) | Cr5—O30—O23 | 111.9 (5) |
O13—O8—O15 | 61.0 (5) | Cr6—O31—U3iv | 141.5 (9) |
Cr3—O8—OW17i | 101.2 (7) | Cr6—O31—O32 | 35.1 (5) |
U2—O8—OW17i | 129.0 (6) | U3iv—O31—O32 | 107.9 (6) |
O16—O8—OW17i | 99.1 (7) | Cr6—O31—O19 | 36.3 (5) |
O13—O8—OW17i | 68.3 (5) | U3iv—O31—O19 | 157.1 (7) |
O15—O8—OW17i | 129.1 (6) | O32—O31—O19 | 60.9 (6) |
Cr3—O8—O1 | 135.4 (9) | Cr6—O31—O18 | 34.5 (4) |
U2—O8—O1 | 53.1 (4) | U3iv—O31—O18 | 134.8 (7) |
O16—O8—O1 | 165.4 (8) | O32—O31—O18 | 59.6 (6) |
O13—O8—O1 | 119.5 (7) | O19—O31—O18 | 59.7 (5) |
O15—O8—O1 | 107.3 (7) | Cr6—O31—O20xi | 116.7 (8) |
OW17i—O8—O1 | 93.5 (6) | U3iv—O31—O20xi | 53.8 (4) |
Cr3—O8—O3 | 150.9 (9) | O32—O31—O20xi | 89.6 (7) |
U2—O8—O3 | 38.0 (4) | O19—O31—O20xi | 104.3 (7) |
O16—O8—O3 | 120.1 (7) | O18—O31—O20xi | 149.0 (8) |
O13—O8—O3 | 163.9 (7) | Cr6—O31—O24iv | 117.3 (8) |
O15—O8—O3 | 134.3 (6) | U3iv—O31—O24iv | 52.9 (4) |
OW17i—O8—O3 | 96.6 (6) | O32—O31—O24iv | 109.5 (7) |
O1—O8—O3 | 65.2 (5) | O19—O31—O24iv | 147.6 (8) |
Cr3—O8—O2 | 90.8 (6) | O18—O31—O24iv | 88.3 (6) |
U2—O8—O2 | 52.1 (4) | O20xi—O31—O24iv | 106.6 (6) |
O16—O8—O2 | 69.9 (6) | Cr6—O31—O26iv | 178.2 (9) |
O13—O8—O2 | 126.8 (7) | U3iv—O31—O26iv | 36.7 (4) |
O15—O8—O2 | 79.9 (5) | O32—O31—O26iv | 143.2 (7) |
OW17i—O8—O2 | 139.2 (8) | O19—O31—O26iv | 145.0 (8) |
O1—O8—O2 | 104.9 (6) | O18—O31—O26iv | 145.9 (7) |
O3—O8—O2 | 61.1 (5) | O20xi—O31—O26iv | 62.4 (5) |
Cr3—O8—O4 | 100.7 (7) | O24iv—O31—O26iv | 62.0 (5) |
U2—O8—O4 | 35.0 (3) | Cr6—O31—O21iv | 105.6 (8) |
O16—O8—O4 | 110.7 (6) | U3iv—O31—O21iv | 36.0 (4) |
O13—O8—O4 | 122.9 (7) | O32—O31—O21iv | 72.8 (6) |
O15—O8—O4 | 67.2 (5) | O19—O31—O21iv | 131.8 (8) |
OW17i—O8—O4 | 149.8 (7) | O18—O31—O21iv | 108.2 (7) |
O1—O8—O4 | 56.4 (5) | O20xi—O31—O21iv | 60.7 (5) |
O3—O8—O4 | 73.0 (5) | O24iv—O31—O21iv | 59.8 (5) |
O2—O8—O4 | 60.5 (5) | O26iv—O31—O21iv | 72.6 (6) |
Cr3—O8—O10 | 140.1 (7) | Cr6—O31—OW34 | 90.2 (7) |
U2—O8—O10 | 85.2 (4) | U3iv—O31—OW34 | 108.0 (6) |
O16—O8—O10 | 147.4 (7) | O32—O31—OW34 | 95.1 (6) |
O13—O8—O10 | 103.3 (5) | O19—O31—OW34 | 56.8 (5) |
O15—O8—O10 | 140.9 (7) | O18—O31—OW34 | 116.0 (6) |
OW17i—O8—O10 | 48.6 (4) | O20xi—O31—OW34 | 59.6 (5) |
O1—O8—O10 | 46.3 (4) | O24iv—O31—OW34 | 152.2 (8) |
O3—O8—O10 | 68.1 (5) | O26iv—O31—OW34 | 90.6 (6) |
O2—O8—O10 | 129.0 (6) | O21iv—O31—OW34 | 118.9 (6) |
O4—O8—O10 | 101.9 (5) | Cr6—O31—O25iv | 72.9 (6) |
Cr3—O8—OW35 | 72.8 (7) | U3iv—O31—O25iv | 79.3 (4) |
U2—O8—OW35 | 118.4 (7) | O32—O31—O25iv | 63.1 (5) |
O16—O8—OW35 | 104.8 (7) | O19—O31—O25iv | 109.0 (7) |
O13—O8—OW35 | 47.9 (6) | O18—O31—O25iv | 55.9 (4) |
O15—O8—OW35 | 70.6 (6) | O20xi—O31—O25iv | 115.3 (6) |
OW17i—O8—OW35 | 73.1 (6) | O24iv—O31—O25iv | 47.7 (5) |
O1—O8—OW35 | 71.7 (6) | O26iv—O31—O25iv | 105.9 (6) |
O3—O8—OW35 | 135.0 (7) | O21iv—O31—O25iv | 55.6 (4) |
O2—O8—OW35 | 147.1 (7) | OW34—O31—O25iv | 158.1 (7) |
O4—O8—OW35 | 94.0 (7) | Cr6—O31—Cr5iv | 90.2 (6) |
O10—O8—OW35 | 73.1 (6) | U3iv—O31—Cr5iv | 74.8 (4) |
Cr2—O9—U1 | 132.5 (7) | O32—O31—Cr5iv | 88.4 (5) |
Cr2—O9—O1 | 36.7 (4) | O19—O31—Cr5iv | 122.0 (6) |
U1—O9—O1 | 152.9 (7) | O18—O31—Cr5iv | 62.3 (4) |
Cr2—O9—O12 | 34.0 (4) | O20xi—O31—Cr5iv | 124.8 (5) |
U1—O9—O12 | 128.7 (6) | O24iv—O31—Cr5iv | 27.1 (3) |
O1—O9—O12 | 59.7 (5) | O26iv—O31—Cr5iv | 89.1 (5) |
Cr2—O9—O10 | 33.9 (5) | O21iv—O31—Cr5iv | 66.2 (4) |
U1—O9—O10 | 100.6 (6) | OW34—O31—Cr5iv | 174.5 (6) |
O1—O9—O10 | 59.7 (5) | O25iv—O31—Cr5iv | 26.0 (3) |
O12—O9—O10 | 58.8 (5) | Cr6—O32—O31 | 35.5 (5) |
Cr2—O9—O13ii | 144.6 (8) | Cr6—O32—O18 | 36.1 (5) |
U1—O9—O13ii | 53.5 (4) | O31—O32—O18 | 61.8 (6) |
O1—O9—O13ii | 118.1 (6) | Cr6—O32—O19 | 35.3 (5) |
O12—O9—O13ii | 177.7 (6) | O31—O32—O19 | 59.9 (6) |
O10—O9—O13ii | 121.0 (7) | O18—O32—O19 | 60.1 (5) |
Cr2—O9—O6i | 91.0 (6) | Cr6—O32—N3iv | 134.8 (9) |
U1—O9—O6i | 52.5 (4) | O31—O32—N3iv | 109.3 (7) |
O1—O9—O6i | 127.8 (6) | O18—O32—N3iv | 114.8 (7) |
O12—O9—O6i | 76.3 (5) | O19—O32—N3iv | 169.1 (9) |
O10—O9—O6i | 74.5 (5) | Cr6—O32—O25iv | 79.7 (6) |
O13ii—O9—O6i | 105.9 (6) | O31—O32—O25iv | 71.3 (6) |
Cr2—O9—OW17 | 95.6 (6) | O18—O32—O25iv | 59.3 (5) |
U1—O9—OW17 | 118.7 (6) | O19—O32—O25iv | 114.4 (6) |
O1—O9—OW17 | 59.0 (5) | N3iv—O32—O25iv | 57.5 (5) |
O12—O9—OW17 | 112.5 (6) | Cr6—O32—O21iv | 91.9 (7) |
O10—O9—OW17 | 108.1 (6) | O31—O32—O21iv | 58.4 (5) |
O13ii—O9—OW17 | 65.3 (5) | O18—O32—O21iv | 100.0 (6) |
O6i—O9—OW17 | 171.1 (7) | O19—O32—O21iv | 116.9 (7) |
Cr2—O9—O11 | 148.8 (7) | N3iv—O32—O21iv | 53.0 (5) |
U1—O9—O11 | 37.0 (4) | O25iv—O32—O21iv | 54.8 (4) |
O1—O9—O11 | 169.0 (7) | Cr6—O32—O16i | 136.2 (8) |
O12—O9—O11 | 120.1 (6) | O31—O32—O16i | 168.6 (7) |
O10—O9—O11 | 130.7 (6) | O18—O32—O16i | 116.0 (7) |
O13ii—O9—O11 | 61.9 (5) | O19—O32—O16i | 109.0 (6) |
O6i—O9—O11 | 59.6 (5) | N3iv—O32—O16i | 81.9 (6) |
OW17—O9—O11 | 114.8 (6) | O25iv—O32—O16i | 118.0 (6) |
Cr2—O9—O5 | 103.8 (7) | O21iv—O32—O16i | 131.6 (6) |
U1—O9—O5 | 36.7 (3) | Cr6—O32—O20xi | 77.1 (6) |
O1—O9—O5 | 116.4 (7) | O31—O32—O20xi | 46.7 (5) |
O12—O9—O5 | 121.1 (6) | O18—O32—O20xi | 108.5 (6) |
O10—O9—O5 | 69.9 (5) | O19—O32—O20xi | 80.6 (6) |
O13ii—O9—O5 | 60.1 (5) | N3iv—O32—O20xi | 92.7 (6) |
O6i—O9—O5 | 63.1 (5) | O25iv—O32—O20xi | 96.5 (5) |
OW17—O9—O5 | 109.4 (6) | O21iv—O32—O20xi | 47.5 (4) |
O11—O9—O5 | 73.7 (5) | O16i—O32—O20xi | 133.1 (5) |
Cr2—O9—O3 | 72.1 (5) | Cr6—O32—O11xiv | 129.9 (7) |
U1—O9—O3 | 105.9 (5) | O31—O32—O11xiv | 137.5 (6) |
O1—O9—O3 | 50.6 (5) | O18—O32—O11xiv | 93.8 (6) |
O12—O9—O3 | 105.1 (5) | O19—O32—O11xiv | 139.4 (7) |
O10—O9—O3 | 65.0 (5) | N3iv—O32—O11xiv | 47.0 (5) |
O13ii—O9—O3 | 73.1 (5) | O25iv—O32—O11xiv | 66.2 (4) |
O6i—O9—O3 | 129.3 (6) | O21iv—O32—O11xiv | 96.8 (5) |
OW17—O9—O3 | 48.3 (4) | O16i—O32—O11xiv | 52.0 (4) |
O11—O9—O3 | 133.7 (6) | O20xi—O32—O11xiv | 139.7 (5) |
O5—O9—O3 | 74.9 (5) | Cr6—O32—U3iv | 69.0 (6) |
Cr2—O9—U2 | 63.5 (4) | O31—O32—U3iv | 34.1 (4) |
U1—O9—U2 | 129.5 (5) | O18—O32—U3iv | 86.5 (5) |
O1—O9—U2 | 31.3 (3) | O19—O32—U3iv | 92.0 (6) |
O12—O9—U2 | 91.0 (4) | N3iv—O32—U3iv | 77.8 (5) |
O10—O9—U2 | 71.8 (4) | O25iv—O32—U3iv | 62.0 (4) |
O13ii—O9—U2 | 86.9 (4) | O21iv—O32—U3iv | 25.0 (3) |
O6i—O9—U2 | 145.9 (5) | O16i—O32—U3iv | 154.6 (5) |
OW17—O9—U2 | 36.4 (3) | O20xi—O32—U3iv | 34.7 (3) |
O11—O9—U2 | 147.5 (5) | O11xiv—O32—U3iv | 118.8 (4) |
O5—O9—U2 | 99.5 (5) | Cr6—O32—OW34 | 52.2 (5) |
O3—O9—U2 | 24.7 (2) | O31—O32—OW34 | 46.3 (4) |
Cr2—O10—U2i | 135.8 (9) | O18—O32—OW34 | 88.0 (5) |
Cr2—O10—O12 | 34.5 (5) | O19—O32—OW34 | 39.6 (4) |
U2i—O10—O12 | 101.9 (6) | N3iv—O32—OW34 | 134.8 (7) |
Cr2—O10—O1 | 35.8 (4) | O25iv—O32—OW34 | 117.6 (6) |
U2i—O10—O1 | 133.9 (7) | O21iv—O32—OW34 | 86.2 (5) |
O12—O10—O1 | 59.7 (5) | O16i—O32—OW34 | 124.1 (5) |
Cr2—O10—O9 | 34.3 (4) | O20xi—O32—OW34 | 42.1 (3) |
U2i—O10—O9 | 151.5 (7) | O11xiv—O32—OW34 | 176.1 (5) |
O12—O10—O9 | 59.7 (5) | U3iv—O32—OW34 | 64.6 (3) |
O1—O10—O9 | 58.7 (5) | Cr4—O33—O30 | 35.5 (5) |
Cr2—O10—OW17i | 129.7 (8) | Cr4—O33—O28 | 37.1 (5) |
U2i—O10—OW17i | 57.6 (4) | O30—O33—O28 | 61.6 (6) |
O12—O10—OW17i | 124.5 (7) | Cr4—O33—O27 | 36.2 (5) |
O1—O10—OW17i | 96.2 (6) | O30—O33—O27 | 61.4 (6) |
O9—O10—OW17i | 150.0 (7) | O28—O33—O27 | 61.8 (5) |
Cr2—O10—O2i | 98.4 (8) | Cr4—O33—N4xii | 122.4 (9) |
U2i—O10—O2i | 52.1 (4) | O30—O33—N4xii | 100.1 (8) |
O12—O10—O2i | 68.1 (6) | O28—O33—N4xii | 159.4 (9) |
O1—O10—O2i | 127.6 (8) | O27—O33—N4xii | 102.0 (7) |
O9—O10—O2i | 99.5 (6) | Cr4—O33—N2 | 99.9 (11) |
OW17i—O10—O2i | 109.4 (6) | O30—O33—N2 | 110.3 (11) |
Cr2—O10—O4i | 159.4 (9) | O28—O33—N2 | 63.3 (9) |
U2i—O10—O4i | 36.7 (3) | O27—O33—N2 | 119.6 (10) |
O12—O10—O4i | 128.9 (7) | N4xii—O33—N2 | 136.5 (11) |
O1—O10—O4i | 163.0 (7) | Cr4—O33—OW35iii | 114.7 (10) |
O9—O10—O4i | 137.4 (6) | O30—O33—OW35iii | 148.3 (9) |
OW17i—O10—O4i | 66.9 (5) | O28—O33—OW35iii | 87.1 (8) |
O2i—O10—O4i | 61.9 (5) | O27—O33—OW35iii | 100.5 (8) |
Cr2—O10—O3i | 103.4 (8) | N4xii—O33—OW35iii | 109.6 (9) |
U2i—O10—O3i | 35.8 (4) | N2—O33—OW35iii | 53.5 (11) |
O12—O10—O3i | 73.8 (6) | Cr4—O33—O12iii | 156.9 (9) |
O1—O10—O3i | 99.6 (6) | O30—O33—O12iii | 123.8 (7) |
O9—O10—O3i | 133.5 (8) | O28—O33—O12iii | 136.2 (7) |
OW17i—O10—O3i | 61.4 (5) | O27—O33—O12iii | 162.0 (7) |
O2i—O10—O3i | 59.3 (5) | N4xii—O33—O12iii | 60.8 (6) |
O4i—O10—O3i | 72.5 (5) | N2—O33—O12iii | 76.3 (9) |
Cr2—O10—O5 | 92.8 (6) | OW35iii—O33—O12iii | 81.8 (8) |
U2i—O10—O5 | 119.6 (6) | Cr4—O33—O3xii | 144.6 (8) |
O12—O10—O5 | 111.8 (6) | O30—O33—O3xii | 157.8 (7) |
O1—O10—O5 | 106.4 (6) | O28—O33—O3xii | 134.9 (7) |
O9—O10—O5 | 58.5 (5) | O27—O33—O3xii | 109.7 (6) |
OW17i—O10—O5 | 123.3 (7) | N4xii—O33—O3xii | 60.4 (6) |
O2i—O10—O5 | 96.6 (5) | N2—O33—O3xii | 91.9 (10) |
O4i—O10—O5 | 84.5 (5) | OW35iii—O33—O3xii | 49.2 (7) |
O3i—O10—O5 | 152.4 (6) | O12iii—O33—O3xii | 58.4 (4) |
Cr2—O10—O6i | 73.6 (6) | Cr4—O33—OW34ix | 62.4 (6) |
U2i—O10—O6i | 100.3 (5) | O30—O33—OW34ix | 44.4 (5) |
O12—O10—O6i | 67.6 (5) | O28—O33—OW34ix | 57.0 (5) |
O1—O10—O6i | 108.4 (6) | O27—O33—OW34ix | 98.2 (6) |
O9—O10—O6i | 54.0 (4) | N4xii—O33—OW34ix | 117.8 (7) |
OW17i—O10—O6i | 155.0 (6) | N2—O33—OW34ix | 70.9 (9) |
O2i—O10—O6i | 51.5 (4) | OW35iii—O33—OW34ix | 123.5 (7) |
O4i—O10—O6i | 88.5 (5) | O12iii—O33—OW34ix | 95.2 (5) |
O3i—O10—O6i | 108.7 (6) | O3xii—O33—OW34ix | 151.9 (5) |
O5—O10—O6i | 54.4 (4) | Cr4—O33—O23ix | 83.6 (7) |
Cr2—O10—Cr1i | 94.1 (6) | O30—O33—O23ix | 48.7 (5) |
U2i—O10—Cr1i | 73.0 (4) | O28—O33—O23ix | 96.5 (6) |
O12—O10—Cr1i | 75.1 (5) | O27—O33—O23ix | 107.3 (6) |
O1—O10—Cr1i | 129.7 (6) | N4xii—O33—O23ix | 75.2 (6) |
O9—O10—Cr1i | 80.9 (4) | N2—O33—O23ix | 102.0 (9) |
OW17i—O10—Cr1i | 128.9 (5) | OW35iii—O33—O23ix | 150.2 (8) |
O2i—O10—Cr1i | 27.5 (3) | O12iii—O33—O23ix | 75.1 (5) |
O4i—O10—Cr1i | 65.8 (4) | O3xii—O33—O23ix | 126.5 (5) |
O3i—O10—Cr1i | 86.8 (4) | OW34ix—O33—O23ix | 42.5 (3) |
O5—O10—Cr1i | 69.6 (4) | Cr4—O33—O24 | 54.4 (5) |
O6i—O10—Cr1i | 27.3 (3) | O30—O33—O24 | 48.0 (5) |
U1—O11—O6i | 54.3 (5) | O28—O33—O24 | 91.4 (6) |
U1—O11—O7iii | 53.3 (5) | O27—O33—O24 | 42.4 (4) |
O6i—O11—O7iii | 100.8 (6) | N4xii—O33—O24 | 68.3 (6) |
U1—O11—O13ii | 52.7 (5) | N2—O33—O24 | 154.2 (10) |
O6i—O11—O13ii | 100.3 (6) | OW35iii—O33—O24 | 135.2 (7) |
O7iii—O11—O13ii | 53.9 (5) | O12iii—O33—O24 | 125.5 (5) |
U1—O11—O9 | 53.9 (5) | O3xii—O33—O24 | 111.0 (5) |
O6i—O11—O9 | 58.1 (5) | OW34ix—O33—O24 | 91.6 (5) |
O7iii—O11—O9 | 98.7 (6) | O23ix—O33—O24 | 74.4 (4) |
O13ii—O11—O9 | 56.1 (5) | U4—OW34—O29xi | 135.5 (7) |
U1—O11—N3vi | 125.1 (8) | U4—OW34—O30vi | 53.9 (4) |
O6i—O11—N3vi | 91.6 (6) | O29xi—OW34—O30vi | 98.8 (6) |
O7iii—O11—N3vi | 157.5 (7) | U4—OW34—O19 | 52.4 (4) |
O13ii—O11—N3vi | 105.6 (6) | O29xi—OW34—O19 | 126.6 (7) |
O9—O11—N3vi | 72.0 (6) | O30vi—OW34—O19 | 105.7 (7) |
U1—O11—C8 | 109.6 (10) | U4—OW34—O23 | 37.3 (4) |
O6i—O11—C8 | 70.2 (9) | O29xi—OW34—O23 | 164.3 (7) |
O7iii—O11—C8 | 109.2 (10) | O30vi—OW34—O23 | 65.7 (5) |
O13ii—O11—C8 | 159.9 (10) | O19—OW34—O23 | 63.4 (5) |
O9—O11—C8 | 124.8 (9) | U4—OW34—O20xi | 151.2 (7) |
N3vi—O11—C8 | 92.7 (10) | O29xi—OW34—O20xi | 56.2 (4) |
U1—O11—C1x | 130.9 (9) | O30vi—OW34—O20xi | 152.8 (7) |
O6i—O11—C1x | 157.0 (7) | O19—OW34—O20xi | 98.9 (6) |
O7iii—O11—C1x | 77.7 (6) | O23—OW34—O20xi | 138.3 (6) |
O13ii—O11—C1x | 97.2 (6) | U4—OW34—O31 | 100.8 (5) |
O9—O11—C1x | 144.9 (7) | O29xi—OW34—O31 | 109.8 (6) |
N3vi—O11—C1x | 97.9 (7) | O30vi—OW34—O31 | 151.2 (7) |
C8—O11—C1x | 88.4 (9) | O19—OW34—O31 | 54.2 (5) |
U1—O11—O15iii | 49.5 (4) | O23—OW34—O31 | 85.9 (5) |
O6i—O11—O15iii | 55.6 (5) | O20xi—OW34—O31 | 55.5 (4) |
O7iii—O11—O15iii | 55.5 (5) | U4—OW34—O22 | 33.2 (3) |
O13ii—O11—O15iii | 94.8 (6) | O29xi—OW34—O22 | 103.8 (6) |
O9—O11—O15iii | 97.3 (6) | O30vi—OW34—O22 | 57.3 (5) |
N3vi—O11—O15iii | 144.3 (7) | O19—OW34—O22 | 56.9 (5) |
C8—O11—O15iii | 65.1 (9) | O23—OW34—O22 | 70.5 (5) |
C1x—O11—O15iii | 108.3 (6) | O20xi—OW34—O22 | 133.3 (7) |
U1—O11—O16ii | 101.1 (7) | O31—OW34—O22 | 110.7 (6) |
O6i—O11—O16ii | 145.6 (6) | U4—OW34—O28vi | 105.4 (5) |
O7iii—O11—O16ii | 74.7 (5) | O29xi—OW34—O28vi | 55.3 (4) |
O13ii—O11—O16ii | 49.0 (5) | O30vi—OW34—O28vi | 51.8 (5) |
O9—O11—O16ii | 88.4 (5) | O19—OW34—O28vi | 153.1 (7) |
N3vi—O11—O16ii | 84.4 (6) | O23—OW34—O28vi | 109.9 (6) |
C8—O11—O16ii | 144.0 (10) | O20xi—OW34—O28vi | 101.3 (5) |
C1x—O11—O16ii | 56.8 (5) | O31—OW34—O28vi | 152.3 (6) |
O15iii—O11—O16ii | 130.2 (7) | O22—OW34—O28vi | 96.2 (5) |
U1—O11—O5 | 1.1 (3) | U4—OW34—Cr4vi | 80.3 (3) |
O6i—O11—O5 | 55.2 (5) | O29xi—OW34—Cr4vi | 82.7 (4) |
O7iii—O11—O5 | 53.0 (4) | O30vi—OW34—Cr4vi | 27.1 (4) |
O13ii—O11—O5 | 51.6 (4) | O19—OW34—Cr4vi | 132.6 (6) |
O9—O11—O5 | 53.5 (4) | O23—OW34—Cr4vi | 82.0 (4) |
N3vi—O11—O5 | 124.9 (6) | O20xi—OW34—Cr4vi | 128.1 (5) |
C8—O11—O5 | 110.7 (9) | O31—OW34—Cr4vi | 158.1 (6) |
C1x—O11—O5 | 130.4 (7) | O22—OW34—Cr4vi | 82.3 (4) |
O15iii—O11—O5 | 50.4 (4) | O28vi—OW34—Cr4vi | 28.4 (3) |
O16ii—O11—O5 | 100.0 (6) | U4—OW34—Cr6 | 79.5 (4) |
U1—O11—O4iii | 92.9 (6) | O29xi—OW34—Cr6 | 114.9 (5) |
O6i—O11—O4iii | 106.4 (5) | O30vi—OW34—Cr6 | 133.3 (6) |
O7iii—O11—O4iii | 52.7 (4) | O19—OW34—Cr6 | 28.0 (3) |
O13ii—O11—O4iii | 104.9 (5) | O23—OW34—Cr6 | 79.4 (4) |
O9—O11—O4iii | 146.8 (7) | O20xi—OW34—Cr6 | 72.5 (4) |
N3vi—O11—O4iii | 140.9 (7) | O31—OW34—Cr6 | 27.9 (4) |
C8—O11—O4iii | 63.1 (9) | O22—OW34—Cr6 | 83.0 (4) |
C1x—O11—O4iii | 54.3 (5) | O28vi—OW34—Cr6 | 169.8 (5) |
O15iii—O11—O4iii | 54.3 (4) | Cr4vi—OW34—Cr6 | 159.3 (4) |
O16ii—O11—O4iii | 97.8 (5) | U4—OW34—Cr5xi | 154.2 (6) |
O5—O11—O4iii | 93.3 (5) | O29xi—OW34—Cr5xi | 28.2 (3) |
Cr2—O12—O1 | 36.0 (4) | O30vi—OW34—Cr5xi | 126.4 (5) |
Cr2—O12—O10 | 35.4 (5) | O19—OW34—Cr5xi | 115.0 (5) |
O1—O12—O10 | 60.5 (5) | O23—OW34—Cr5xi | 165.6 (6) |
Cr2—O12—O9 | 35.4 (4) | O20xi—OW34—Cr5xi | 27.9 (3) |
O1—O12—O9 | 59.6 (5) | O31—OW34—Cr5xi | 82.4 (4) |
O10—O12—O9 | 61.5 (5) | O22—OW34—Cr5xi | 121.6 (5) |
Cr2—O12—N4i | 141.5 (9) | O28vi—OW34—Cr5xi | 78.0 (4) |
O1—O12—N4i | 152.1 (7) | Cr4vi—OW34—Cr5xi | 106.3 (4) |
O10—O12—N4i | 106.7 (7) | Cr6—OW34—Cr5xi | 93.8 (3) |
O9—O12—N4i | 139.6 (7) | U4—OW34—HW3A | 109.5 |
Cr2—O12—O2i | 90.0 (7) | O29xi—OW34—HW3A | 100.3 |
O1—O12—O2i | 118.9 (7) | O30vi—OW34—HW3A | 160.8 |
O10—O12—O2i | 58.6 (5) | O19—OW34—HW3A | 60.8 |
O9—O12—O2i | 94.7 (6) | O23—OW34—HW3A | 95.2 |
N4i—O12—O2i | 52.5 (5) | O20xi—OW34—HW3A | 46.0 |
Cr2—O12—O33xi | 141.1 (8) | O31—OW34—HW3A | 9.6 |
O1—O12—O33xi | 110.2 (6) | O22—OW34—HW3A | 115.7 |
O10—O12—O33xi | 124.6 (6) | O28vi—OW34—HW3A | 144.7 |
O9—O12—O33xi | 165.5 (6) | Cr4vi—OW34—HW3A | 159.8 |
N4i—O12—O33xi | 54.1 (5) | Cr6—OW34—HW3A | 33.1 |
O2i—O12—O33xi | 99.5 (5) | Cr5xi—OW34—HW3A | 72.8 |
Cr2—O12—O3i | 88.6 (6) | U4—OW34—HW3B | 109.6 |
O1—O12—O3i | 90.4 (5) | O29xi—OW34—HW3B | 27.5 |
O10—O12—O3i | 57.4 (5) | O30vi—OW34—HW3B | 88.7 |
O9—O12—O3i | 118.9 (6) | O19—OW34—HW3B | 106.1 |
N4i—O12—O3i | 63.0 (5) | O23—OW34—HW3B | 145.9 |
O2i—O12—O3i | 52.5 (4) | O20xi—OW34—HW3B | 73.1 |
O33xi—O12—O3i | 68.9 (5) | O31—OW34—HW3B | 115.3 |
Cr2—O12—O6i | 72.6 (5) | O22—OW34—HW3B | 76.8 |
O1—O12—O6i | 107.8 (6) | O28vi—OW34—HW3B | 63.7 |
O10—O12—O6i | 66.1 (5) | Cr4vi—OW34—HW3B | 84.3 |
O9—O12—O6i | 53.7 (4) | Cr6—OW34—HW3B | 106.4 |
N4i—O12—O6i | 85.9 (5) | Cr5xi—OW34—HW3B | 48.2 |
O2i—O12—O6i | 49.6 (4) | HW3A—OW34—HW3B | 107.7 |
O33xi—O12—O6i | 139.8 (6) | N2xi—OW35—O3i | 120.4 (14) |
O3i—O12—O6i | 98.7 (5) | N2xi—OW35—O13 | 118.0 (14) |
Cr2—O12—U2i | 71.4 (5) | O3i—OW35—O13 | 90.1 (10) |
O1—O12—U2i | 87.8 (5) | N2xi—OW35—O33xi | 61.7 (12) |
O10—O12—U2i | 36.3 (3) | O3i—OW35—O33xi | 78.7 (9) |
O9—O12—U2i | 95.3 (5) | O13—OW35—O33xi | 165.3 (12) |
N4i—O12—U2i | 72.3 (5) | N2xi—OW35—O5i | 149.4 (15) |
O2i—O12—U2i | 36.4 (3) | O3i—OW35—O5i | 90.2 (9) |
O33xi—O12—U2i | 94.5 (4) | O13—OW35—O5i | 56.5 (7) |
O3i—O12—U2i | 26.5 (3) | O33xi—OW35—O5i | 132.1 (11) |
O6i—O12—U2i | 74.5 (4) | N2xi—OW35—C6i | 128.2 (16) |
Cr2—O12—OW35 | 94.5 (7) | O3i—OW35—C6i | 67.5 (9) |
O1—O12—OW35 | 71.1 (6) | O13—OW35—C6i | 112.8 (11) |
O10—O12—OW35 | 82.7 (6) | O33xi—OW35—C6i | 71.9 (9) |
O9—O12—OW35 | 128.5 (7) | O5i—OW35—C6i | 60.9 (8) |
N4i—O12—OW35 | 83.1 (6) | N2xi—OW35—O14viii | 89.6 (12) |
O2i—O12—OW35 | 96.4 (6) | O3i—OW35—O14viii | 149.4 (11) |
O33xi—O12—OW35 | 47.2 (6) | O13—OW35—O14viii | 79.5 (8) |
O3i—O12—OW35 | 44.4 (5) | O33xi—OW35—O14viii | 114.9 (10) |
O6i—O12—OW35 | 142.1 (7) | O5i—OW35—O14viii | 60.1 (6) |
U2i—O12—OW35 | 67.6 (5) | C6i—OW35—O14viii | 90.0 (9) |
Cr2—O12—O23vi | 147.6 (7) | N2xi—OW35—O28xi | 48.7 (11) |
O1—O12—O23vi | 129.8 (6) | O3i—OW35—O28xi | 120.3 (10) |
O10—O12—O23vi | 167.6 (6) | O13—OW35—O28xi | 149.6 (10) |
O9—O12—O23vi | 115.6 (5) | O33xi—OW35—O28xi | 42.5 (6) |
N4i—O12—O23vi | 67.1 (5) | O5i—OW35—O28xi | 118.3 (9) |
O2i—O12—O23vi | 111.2 (5) | C6i—OW35—O28xi | 81.8 (9) |
O33xi—O12—O23vi | 61.5 (4) | O14viii—OW35—O28xi | 73.9 (7) |
O3i—O12—O23vi | 123.7 (5) | N2xi—OW35—O8 | 86.4 (12) |
O6i—O12—O23vi | 102.2 (5) | O3i—OW35—O8 | 82.1 (8) |
U2i—O12—O23vi | 139.3 (4) | O13—OW35—O8 | 42.6 (5) |
OW35—O12—O23vi | 106.5 (6) | O33xi—OW35—O8 | 125.3 (9) |
Cr3—O13—U1i | 140.2 (7) | O5i—OW35—O8 | 98.5 (9) |
Cr3—O13—O16 | 34.5 (5) | C6i—OW35—O8 | 142.0 (11) |
U1i—O13—O16 | 110.4 (6) | O14viii—OW35—O8 | 107.4 (8) |
Cr3—O13—O7viii | 98.4 (6) | O28xi—OW35—O8 | 134.9 (8) |
U1i—O13—O7viii | 55.5 (4) | N2xi—OW35—O15 | 75.5 (11) |
O16—O13—O7viii | 92.6 (6) | O3i—OW35—O15 | 121.4 (10) |
Cr3—O13—O8 | 37.2 (4) | O13—OW35—O15 | 43.6 (5) |
U1i—O13—O8 | 164.4 (8) | O33xi—OW35—O15 | 136.7 (10) |
O16—O13—O8 | 59.9 (6) | O5i—OW35—O15 | 88.6 (8) |
O7viii—O13—O8 | 132.9 (6) | C6i—OW35—O15 | 149.1 (11) |
Cr3—O13—O15 | 33.9 (4) | O14viii—OW35—O15 | 68.5 (6) |
U1i—O13—O15 | 126.8 (6) | O28xi—OW35—O15 | 111.3 (8) |
O16—O13—O15 | 58.8 (6) | O8—OW35—O15 | 40.5 (4) |
O7viii—O13—O15 | 72.3 (5) | N2xi—OW35—O12 | 64.6 (11) |
O8—O13—O15 | 60.9 (5) | O3i—OW35—O12 | 55.8 (6) |
Cr3—O13—O9i | 135.8 (8) | O13—OW35—O12 | 114.7 (9) |
U1i—O13—O9i | 54.7 (4) | O33xi—OW35—O12 | 51.0 (6) |
O16—O13—O9i | 109.2 (7) | O5i—OW35—O12 | 145.9 (10) |
O7viii—O13—O9i | 110.2 (6) | C6i—OW35—O12 | 103.0 (9) |
O8—O13—O9i | 114.6 (6) | O14viii—OW35—O12 | 154.0 (10) |
O15—O13—O9i | 168.0 (7) | O28xi—OW35—O12 | 85.6 (7) |
Cr3—O13—O5i | 159.8 (8) | O8—OW35—O12 | 75.9 (6) |
U1i—O13—O5i | 38.1 (4) | O15—OW35—O12 | 105.7 (7) |
O16—O13—O5i | 147.4 (7) | N2xi—OW35—O1 | 59.1 (11) |
O7viii—O13—O5i | 64.0 (5) | O3i—OW35—O1 | 75.2 (7) |
O8—O13—O5i | 152.7 (7) | O13—OW35—O1 | 83.7 (8) |
O15—O13—O5i | 126.1 (6) | O33xi—OW35—O1 | 84.2 (8) |
O9i—O13—O5i | 63.5 (5) | O5i—OW35—O1 | 137.9 (10) |
Cr3—O13—OW35 | 108.5 (9) | C6i—OW35—O1 | 138.7 (10) |
U1i—O13—OW35 | 103.6 (7) | O14viii—OW35—O1 | 131.0 (8) |
O16—O13—OW35 | 143.0 (9) | O28xi—OW35—O1 | 103.0 (7) |
O7viii—O13—OW35 | 94.8 (8) | O8—OW35—O1 | 41.2 (4) |
O8—O13—OW35 | 89.5 (8) | O15—OW35—O1 | 67.7 (5) |
O15—O13—OW35 | 89.2 (8) | O12—OW35—O1 | 38.3 (4) |
O9i—O13—OW35 | 102.2 (7) | N2xi—OW35—HW3E | 109.2 |
O5i—O13—OW35 | 65.7 (7) | O3i—OW35—HW3E | 31.2 |
Cr3—O13—O11i | 106.7 (7) | O13—OW35—HW3E | 69.2 |
U1i—O13—O11i | 37.1 (4) | O33xi—OW35—HW3E | 96.7 |
O16—O13—O11i | 73.9 (6) | O5i—OW35—HW3E | 96.9 |
O7viii—O13—O11i | 62.7 (5) | C6i—OW35—HW3E | 97.3 |
O8—O13—O11i | 129.8 (7) | O14viii—OW35—HW3E | 148.2 |
O15—O13—O11i | 111.3 (6) | O28xi—OW35—HW3E | 137.7 |
O9i—O13—O11i | 62.0 (5) | O8—OW35—HW3E | 51.0 |
O5i—O13—O11i | 75.1 (5) | O15—OW35—HW3E | 91.0 |
OW35—O13—O11i | 140.5 (8) | O12—OW35—HW3E | 53.1 |
Cr3—O13—OW17i | 91.2 (6) | O1—OW35—HW3E | 51.8 |
U1i—O13—OW17i | 113.9 (5) | N2xi—OW35—HW3F | 109.7 |
O16—O13—OW17i | 92.6 (6) | O3i—OW35—HW3F | 121.7 |
O7viii—O13—OW17i | 169.3 (6) | O13—OW35—HW3F | 37.9 |
O8—O13—OW17i | 57.6 (5) | O33xi—OW35—HW3F | 156.5 |
O15—O13—OW17i | 118.3 (6) | O5i—OW35—HW3F | 45.2 |
O9i—O13—OW17i | 59.2 (4) | C6i—OW35—HW3F | 103.6 |
O5i—O13—OW17i | 107.3 (5) | O14viii—OW35—HW3F | 41.6 |
OW35—O13—OW17i | 86.7 (7) | O28xi—OW35—HW3F | 114.6 |
O11i—O13—OW17i | 110.0 (6) | O8—OW35—HW3F | 72.8 |
Cr3—O13—O14viii | 106.8 (6) | O15—OW35—HW3F | 45.6 |
U1i—O13—O14viii | 72.8 (4) | O12—OW35—HW3F | 148.5 |
O16—O13—O14viii | 121.2 (6) | O1—OW35—HW3F | 110.9 |
O7viii—O13—O14viii | 38.8 (4) | HW3E—OW35—HW3F | 106.8 |
O8—O13—O14viii | 122.4 (6) | N1—C1—O5 | 68.1 (14) |
O15—O13—O14viii | 72.9 (5) | N1—C1—O16iii | 110.8 (14) |
O9i—O13—O14viii | 116.7 (5) | O5—C1—O16iii | 70.5 (6) |
O5i—O13—O14viii | 53.3 (4) | N1—C1—O11xii | 176.9 (15) |
OW35—O13—O14viii | 56.0 (7) | O5—C1—O11xii | 111.2 (9) |
O11i—O13—O14viii | 96.9 (5) | O16iii—C1—O11xii | 66.3 (6) |
OW17i—O13—O14viii | 141.9 (6) | N1—C1—O18x | 73.3 (14) |
Cr1—O14—O7 | 35.6 (5) | O5—C1—O18x | 140.1 (8) |
Cr1—O14—O6 | 36.3 (5) | O16iii—C1—O18x | 116.1 (8) |
O7—O14—O6 | 61.8 (6) | O11xii—C1—O18x | 106.8 (8) |
Cr1—O14—O2 | 37.1 (5) | N1—C1—O4i | 108.8 (14) |
O7—O14—O2 | 61.6 (6) | O5—C1—O4i | 83.6 (7) |
O6—O14—O2 | 61.8 (5) | O16iii—C1—O4i | 118.6 (9) |
Cr1—O14—O16 | 91.6 (7) | O11xii—C1—O4i | 73.9 (6) |
O7—O14—O16 | 83.6 (6) | O18x—C1—O4i | 119.1 (8) |
O6—O14—O16 | 125.6 (7) | N1—C1—H1A | 109.5 |
O2—O14—O16 | 65.1 (5) | O5—C1—H1A | 92.3 |
Cr1—O14—O5xi | 93.0 (8) | O16iii—C1—H1A | 125.1 |
O7—O14—O5xi | 58.0 (5) | O11xii—C1—H1A | 73.4 |
O6—O14—O5xi | 116.1 (7) | O18x—C1—H1A | 110.2 |
O2—O14—O5xi | 104.0 (7) | O4i—C1—H1A | 9.3 |
O16—O14—O5xi | 66.5 (5) | N1—C1—H1B | 110.0 |
Cr1—O14—OW35vii | 110.7 (9) | O5—C1—H1B | 54.2 |
O7—O14—OW35vii | 83.9 (7) | O16iii—C1—H1B | 20.9 |
O6—O14—OW35vii | 100.0 (7) | O11xii—C1—H1B | 67.7 |
O2—O14—OW35vii | 145.3 (9) | O18x—C1—H1B | 136.7 |
O16—O14—OW35vii | 117.7 (7) | O4i—C1—H1B | 101.1 |
O5xi—O14—OW35vii | 55.3 (6) | H1A—C1—H1B | 108.9 |
Cr1—O14—O22ii | 121.5 (7) | N1—C1—H1C | 109.8 |
O7—O14—O22ii | 150.4 (6) | O5—C1—H1C | 157.1 |
O6—O14—O22ii | 89.5 (6) | O16iii—C1—H1C | 90.2 |
O2—O14—O22ii | 112.9 (6) | O11xii—C1—H1C | 69.7 |
O16—O14—O22ii | 122.0 (6) | O18x—C1—H1C | 39.0 |
O5xi—O14—O22ii | 142.2 (6) | O4i—C1—H1C | 117.5 |
OW35vii—O14—O22ii | 95.0 (7) | H1A—C1—H1C | 109.3 |
Cr1—O14—O15 | 64.3 (6) | H1B—C1—H1C | 109.3 |
O7—O14—O15 | 43.8 (4) | N3—C2—O25 | 72.2 (12) |
O6—O14—O15 | 99.8 (6) | N3—C2—O22ix | 139.0 (16) |
O2—O14—O15 | 60.4 (5) | O25—C2—O22ix | 67.2 (6) |
O16—O14—O15 | 40.9 (4) | N3—C2—H2A | 110.0 |
O5xi—O14—O15 | 44.5 (4) | O25—C2—H2A | 79.4 |
OW35vii—O14—O15 | 97.9 (7) | O22ix—C2—H2A | 57.4 |
O22ii—O14—O15 | 162.5 (5) | N3—C2—H2B | 110.4 |
Cr1—O14—U1xi | 67.8 (6) | O25—C2—H2B | 61.0 |
O7—O14—U1xi | 32.8 (3) | O22ix—C2—H2B | 53.1 |
O6—O14—U1xi | 92.8 (6) | H2A—C2—H2B | 108.5 |
O2—O14—U1xi | 84.4 (5) | N3—C2—H2C | 110.2 |
O16—O14—U1xi | 70.9 (5) | O25—C2—H2C | 169.4 |
O5xi—O14—U1xi | 25.3 (3) | O22ix—C2—H2C | 110.7 |
OW35vii—O14—U1xi | 66.4 (6) | H2A—C2—H2C | 108.6 |
O22ii—O14—U1xi | 161.3 (5) | H2B—C2—H2C | 109.1 |
O15—O14—U1xi | 33.9 (2) | N2xi—C3—O26xv | 162 (3) |
Cr1—O14—O19ii | 157.5 (8) | N2xi—C3—H3A | 109.6 |
O7—O14—O19ii | 165.6 (6) | O26xv—C3—H3A | 52.2 |
O6—O14—O19ii | 132.1 (7) | N2xi—C3—H3B | 108.1 |
O2—O14—O19ii | 125.5 (6) | O26xv—C3—H3B | 83.5 |
O16—O14—O19ii | 88.7 (5) | H3A—C3—H3B | 109.4 |
O5xi—O14—O19ii | 107.7 (5) | N2xi—C3—H3C | 110.1 |
OW35vii—O14—O19ii | 88.9 (6) | O26xv—C3—H3C | 77.9 |
O22ii—O14—O19ii | 42.7 (4) | H3A—C3—H3C | 109.9 |
O15—O14—O19ii | 125.7 (5) | H3B—C3—H3C | 109.7 |
U1xi—O14—O19ii | 132.8 (4) | N4—C4—H4A | 109.2 |
Cr1—O14—O13vii | 69.1 (6) | N4—C4—H4B | 109.0 |
O7—O14—O13vii | 39.5 (4) | H4A—C4—H4B | 110.1 |
O6—O14—O13vii | 75.8 (5) | N4—C4—H4C | 108.8 |
O2—O14—O13vii | 100.9 (6) | H4A—C4—H4C | 109.6 |
O16—O14—O13vii | 104.1 (6) | H4B—C4—H4C | 110.1 |
O5xi—O14—O13vii | 44.2 (4) | N4—C5—O22ii | 154 (2) |
OW35vii—O14—O13vii | 44.5 (6) | N4—C5—H5A | 109.5 |
O22ii—O14—O13vii | 130.8 (5) | O22ii—C5—H5A | 96.0 |
O15—O14—O13vii | 66.3 (4) | N4—C5—H5B | 109.1 |
U1xi—O14—O13vii | 33.3 (2) | O22ii—C5—H5B | 66.4 |
O19ii—O14—O13vii | 132.5 (5) | H5A—C5—H5B | 109.2 |
Cr3—O15—U1xi | 149.8 (8) | N4—C5—H5C | 110.0 |
Cr3—O15—O16 | 34.2 (5) | O22ii—C5—H5C | 53.0 |
U1xi—O15—O16 | 115.7 (7) | H5A—C5—H5C | 109.6 |
Cr3—O15—O8 | 34.7 (4) | H5B—C5—H5C | 109.4 |
U1xi—O15—O8 | 151.4 (6) | N1—C6—O27x | 74.4 (17) |
O16—O15—O8 | 58.9 (6) | N1—C6—OW35ii | 77.5 (15) |
Cr3—O15—O13 | 34.4 (4) | O27x—C6—OW35ii | 87.9 (9) |
U1xi—O15—O13 | 147.0 (6) | N1—C6—O5 | 63.3 (16) |
O16—O15—O13 | 58.7 (6) | O27x—C6—O5 | 130.1 (10) |
O8—O15—O13 | 58.2 (5) | OW35ii—C6—O5 | 59.0 (8) |
Cr3—O15—O6viii | 133.7 (7) | N1—C6—H6A | 108.8 |
U1xi—O15—O6viii | 53.0 (4) | O27x—C6—H6A | 96.1 |
O16—O15—O6viii | 127.0 (7) | OW35ii—C6—H6A | 173.3 |
O8—O15—O6viii | 154.8 (7) | O5—C6—H6A | 121.1 |
O13—O15—O6viii | 101.9 (6) | N1—C6—H6B | 109.9 |
Cr3—O15—O7 | 113.1 (7) | O27x—C6—H6B | 45.4 |
U1xi—O15—O7 | 53.1 (4) | OW35ii—C6—H6B | 69.6 |
O16—O15—O7 | 89.9 (6) | O5—C6—H6B | 128.5 |
O8—O15—O7 | 98.3 (6) | H6A—C6—H6B | 109.5 |
O13—O15—O7 | 146.9 (7) | N1—C6—H6C | 109.7 |
O6viii—O15—O7 | 105.8 (6) | O27x—C6—H6C | 150.7 |
Cr3—O15—O5xi | 112.6 (8) | OW35ii—C6—H6C | 65.7 |
U1xi—O15—O5xi | 38.3 (4) | O5—C6—H6C | 46.5 |
O16—O15—O5xi | 79.9 (6) | H6A—C6—H6C | 109.2 |
O8—O15—O5xi | 135.3 (7) | H6B—C6—H6C | 109.7 |
O13—O15—O5xi | 115.9 (6) | N3—C7—O21 | 67.6 (13) |
O6viii—O15—O5xi | 65.0 (5) | N3—C7—O26iv | 174.2 (18) |
O7—O15—O5xi | 62.5 (5) | O21—C7—O26iv | 107.2 (9) |
Cr3—O15—O11xi | 168.0 (7) | N3—C7—H7A | 109.2 |
U1xi—O15—O11xi | 34.7 (3) | O21—C7—H7A | 117.7 |
O16—O15—O11xi | 145.7 (7) | O26iv—C7—H7A | 70.2 |
O8—O15—O11xi | 134.0 (6) | N3—C7—H7B | 109.6 |
O13—O15—O11xi | 153.9 (7) | O21—C7—H7B | 130.7 |
O6viii—O15—O11xi | 58.1 (5) | O26iv—C7—H7B | 75.8 |
O7—O15—O11xi | 59.1 (5) | H7A—C7—H7B | 109.6 |
O5xi—O15—O11xi | 73.0 (5) | N3—C7—H7C | 109.5 |
Cr3—O15—O7viii | 80.6 (5) | O21—C7—H7C | 42.5 |
U1xi—O15—O7viii | 95.1 (5) | O26iv—C7—H7C | 65.8 |
O16—O15—O7viii | 81.6 (6) | H7A—C7—H7C | 109.5 |
O8—O15—O7viii | 110.7 (5) | H7B—C7—H7C | 109.4 |
O13—O15—O7viii | 52.7 (4) | N2—C8—O11 | 160 (3) |
O6viii—O15—O7viii | 53.3 (4) | N2—C8—H8A | 110.0 |
O7—O15—O7viii | 139.0 (5) | O11—C8—H8A | 75.5 |
O5xi—O15—O7viii | 76.5 (5) | N2—C8—H8B | 109.6 |
O11xi—O15—O7viii | 111.3 (5) | O11—C8—H8B | 85.3 |
Cr3—O15—O4 | 94.7 (6) | H8A—C8—H8B | 109.6 |
U1xi—O15—O4 | 98.6 (5) | N2—C8—H8C | 108.5 |
O16—O15—O4 | 105.7 (6) | O11—C8—H8C | 52.6 |
O8—O15—O4 | 60.5 (5) | H8A—C8—H8C | 109.5 |
O13—O15—O4 | 114.3 (5) | H8B—C8—H8C | 109.6 |
O6viii—O15—O4 | 126.5 (6) | C6—N1—C1 | 112 (2) |
O7—O15—O4 | 61.1 (4) | C6—N1—O5 | 88.6 (18) |
O5xi—O15—O4 | 123.3 (5) | C1—N1—O5 | 82.0 (15) |
O11xi—O15—O4 | 73.6 (5) | C6—N1—O27x | 77.1 (17) |
O7viii—O15—O4 | 159.5 (6) | C1—N1—O27x | 128.5 (17) |
Cr3—O15—Cr1viii | 106.3 (5) | O5—N1—O27x | 149.4 (10) |
U1xi—O15—Cr1viii | 77.8 (3) | C6—N1—O18x | 108.4 (18) |
O16—O15—Cr1viii | 108.3 (5) | C1—N1—O18x | 78.0 (14) |
O8—O15—Cr1viii | 130.7 (5) | O5—N1—O18x | 157.4 (10) |
O13—O15—Cr1viii | 74.4 (4) | O27x—N1—O18x | 52.3 (6) |
O6viii—O15—Cr1viii | 27.7 (3) | C6—N1—H1D | 109.6 |
O7—O15—Cr1viii | 130.5 (5) | C1—N1—H1D | 68.2 |
O5xi—O15—Cr1viii | 75.5 (4) | O5—N1—H1D | 22.1 |
O11xi—O15—Cr1viii | 85.2 (4) | O27x—N1—H1D | 159.5 |
O7viii—O15—Cr1viii | 27.5 (3) | O18x—N1—H1D | 136.2 |
O4—O15—Cr1viii | 143.8 (5) | C6—N1—H1E | 109.1 |
Cr3—O16—O13 | 36.6 (5) | C1—N1—H1E | 137.7 |
Cr3—O16—O15 | 35.8 (5) | O5—N1—H1E | 109.4 |
O13—O16—O15 | 62.5 (6) | O27x—N1—H1E | 52.8 |
Cr3—O16—O8 | 36.7 (5) | O18x—N1—H1E | 79.6 |
O13—O16—O8 | 60.4 (6) | H1D—N1—H1E | 107.3 |
O15—O16—O8 | 62.3 (6) | C3iii—N2—C8 | 103 (3) |
Cr3—O16—C1xi | 123.8 (10) | C3iii—N2—OW35iii | 144 (3) |
O13—O16—C1xi | 104.3 (7) | C8—N2—OW35iii | 102 (3) |
O15—O16—C1xi | 100.5 (8) | C3iii—N2—O33 | 100 (3) |
O8—O16—C1xi | 160.4 (9) | C8—N2—O33 | 153 (3) |
Cr3—O16—O14 | 117.1 (9) | OW35iii—N2—O33 | 64.8 (12) |
O13—O16—O14 | 150.8 (8) | C3iii—N2—O28 | 110 (3) |
O15—O16—O14 | 88.3 (6) | C8—N2—O28 | 105 (2) |
O8—O16—O14 | 107.0 (7) | OW35iii—N2—O28 | 88.1 (14) |
C1xi—O16—O14 | 80.2 (6) | O33—N2—O28 | 53.6 (8) |
Cr3—O16—O2 | 81.7 (7) | C3iii—N2—H2D | 109.2 |
O13—O16—O2 | 116.1 (7) | C8—N2—H2D | 22.0 |
O15—O16—O2 | 75.8 (6) | OW35iii—N2—H2D | 103.9 |
O8—O16—O2 | 57.8 (5) | O33—N2—H2D | 134.3 |
C1xi—O16—O2 | 130.3 (7) | O28—N2—H2D | 83.3 |
O14—O16—O2 | 50.4 (4) | C3iii—N2—H2E | 109.2 |
Cr3—O16—O11i | 92.4 (7) | C8—N2—H2E | 127.6 |
O13—O16—O11i | 57.2 (5) | OW35iii—N2—H2E | 74.0 |
O15—O16—O11i | 102.1 (7) | O33—N2—H2E | 28.9 |
O8—O16—O11i | 114.8 (7) | O28—N2—H2E | 24.9 |
C1xi—O16—O11i | 57.0 (5) | H2D—N2—H2E | 106.4 |
O14—O16—O11i | 137.0 (7) | C7—N3—C2 | 112.4 (18) |
O2—O16—O11i | 172.5 (7) | C7—N3—O21 | 83.8 (14) |
Cr3—O16—O32ii | 159.8 (9) | C2—N3—O21 | 96.7 (15) |
O13—O16—O32ii | 124.3 (7) | C7—N3—O32v | 97.4 (13) |
O15—O16—O32ii | 158.4 (7) | C2—N3—O32v | 146.5 (15) |
O8—O16—O32ii | 139.3 (7) | O21—N3—O32v | 70.8 (6) |
C1xi—O16—O32ii | 58.6 (6) | C7—N3—O11ix | 124.8 (16) |
O14—O16—O32ii | 83.1 (6) | C2—N3—O11ix | 88.5 (14) |
O2—O16—O32ii | 112.5 (6) | O21—N3—O11ix | 146.2 (8) |
O11i—O16—O32ii | 72.1 (5) | O32v—N3—O11ix | 86.5 (6) |
Cr3—O16—O5xi | 87.4 (7) | C7—N3—O25 | 146.1 (16) |
O13—O16—O5xi | 99.4 (6) | C2—N3—O25 | 79.6 (13) |
O15—O16—O5xi | 52.7 (5) | O21—N3—O25 | 62.9 (6) |
O8—O16—O5xi | 112.8 (7) | O32v—N3—O25 | 67.0 (6) |
C1xi—O16—O5xi | 54.6 (6) | O11ix—N3—O25 | 85.5 (6) |
O14—O16—O5xi | 59.2 (5) | C7—N3—H3D | 109.5 |
O2—O16—O5xi | 90.0 (5) | C2—N3—H3D | 98.2 |
O11i—O16—O5xi | 94.4 (5) | O21—N3—H3D | 28.8 |
O32ii—O16—O5xi | 106.2 (6) | O32v—N3—H3D | 55.9 |
Cr3—O16—Cr1 | 92.5 (7) | O11ix—N3—H3D | 117.4 |
O13—O16—Cr1 | 128.8 (7) | O25—N3—H3D | 36.7 |
O15—O16—Cr1 | 70.3 (5) | C7—N3—H3E | 109.6 |
O8—O16—Cr1 | 81.3 (5) | C2—N3—H3E | 118.6 |
C1xi—O16—Cr1 | 102.6 (6) | O21—N3—H3E | 130.6 |
O14—O16—Cr1 | 26.5 (3) | O32v—N3—H3E | 60.6 |
O2—O16—Cr1 | 28.7 (3) | O11ix—N3—H3E | 30.2 |
O11i—O16—Cr1 | 157.4 (6) | O25—N3—H3E | 89.3 |
O32ii—O16—Cr1 | 106.9 (5) | H3D—N3—H3E | 107.6 |
O5xi—O16—Cr1 | 63.9 (4) | C5—N4—C4 | 114 (2) |
Cr3—O16—O7viii | 60.1 (6) | C5—N4—O2 | 109.6 (16) |
O13—O16—O7viii | 43.9 (4) | C4—N4—O2 | 106.8 (15) |
O15—O16—O7viii | 55.3 (5) | C5—N4—O33x | 110.2 (16) |
O8—O16—O7viii | 96.0 (6) | C4—N4—O33x | 97.2 (13) |
C1xi—O16—O7viii | 65.1 (6) | O2—N4—O33x | 118.7 (9) |
O14—O16—O7viii | 120.3 (6) | C5—N4—O12ii | 99.0 (15) |
O2—O16—O7viii | 131.1 (7) | C4—N4—O12ii | 146.6 (16) |
O11i—O16—O7viii | 47.4 (4) | O2—N4—O12ii | 64.2 (6) |
O32ii—O16—O7viii | 113.1 (5) | O33x—N4—O12ii | 65.1 (6) |
O5xi—O16—O7viii | 61.1 (4) | C5—N4—H4D | 109.5 |
Cr1—O16—O7viii | 118.3 (5) | C4—N4—H4D | 4.9 |
U2—OW17—O1 | 52.8 (4) | O2—N4—H4D | 107.2 |
U2—OW17—O8ii | 128.7 (7) | O33x—N4—H4D | 101.0 |
O1—OW17—O8ii | 159.9 (7) | O12ii—N4—H4D | 151.3 |
U2—OW17—O10ii | 52.6 (4) | C5—N4—H4E | 109.5 |
O1—OW17—O10ii | 104.8 (6) | C4—N4—H4E | 107.0 |
O8ii—OW17—O10ii | 83.1 (6) | O2—N4—H4E | 0.2 |
U2—OW17—O9 | 100.6 (5) | O33x—N4—H4E | 118.6 |
O1—OW17—O9 | 56.2 (5) | O12ii—N4—H4E | 64.0 |
O8ii—OW17—O9 | 107.6 (6) | H4D—N4—H4E | 107.5 |
Symmetry codes: (i) x−1/2, −y+3/2, −z; (ii) x+1/2, −y+3/2, −z; (iii) x, y−1, z; (iv) −x, y+1/2, −z+1/2; (v) −x, y−1/2, −z+1/2; (vi) −x+1, y+1/2, −z+1/2; (vii) x+1/2, −y+5/2, −z; (viii) x−1/2, −y+5/2, −z; (ix) −x+1, y−1/2, −z+1/2; (x) x+1/2, −y+1/2, −z; (xi) x, y+1, z; (xii) x−1/2, −y+1/2, −z; (xiii) x−1, y−1, z; (xiv) x−1, y, z; (xv) x+1, y+1, z. |