Acta Crystallographica Section E

Structure Reports Online

Volume 60, Part 11 (November 2004)

metal-organic compounds


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lh6279 scheme

Acta Cryst. (2004). E60, m1558-m1561    [ doi:10.1107/S1600536804023943 ]

trans-Bis(1H-benzimidazol-2-ylmethyl-[kappa]N3 diethyl phosphate)dichloropalladium(II) monohydrate

L. Checinska, M. Malecka, J. Ochocki and U. Kalinowska

Abstract: The title compound, trans-[PdCl2(2-bimOpe)2]·H2O, where 2-bimOpe is 1H-benzimidazol-2-ylmethyl diethyl phosphate (C12H17N2O4P), crystallizes as a monohydrate. The most satisfactory structure refinement was obtained by eliminating the solvent contribution from the intensity data and the solvent-free model was employed for the final refinement. The Pd atom possesses a square-planar geometry in a centrosymmetric trans configuration.

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