Supporting information
Crystallographic Information File (CIF) https://doi.org/10.1107/S0108270102002184/jz1494sup1.cif | |
Structure factor file (CIF format) https://doi.org/10.1107/S0108270102002184/jz1494Isup2.hkl |
CCDC reference: 184469
Data collection: MSC/AFC Diffractometer Control Software (Molecular Structure Corporation, 1993); cell refinement: MSC/AFC Diffractometer Control Software; data reduction: PROCESS in TEXSAN (Molecular Structure Corporation, 1993); program(s) used to solve structure: SHELXS97 (Sheldrick, 1997); program(s) used to refine structure: SHELXL97 (Sheldrick, 1997); molecular graphics: SHELXTL/PC (Sheldrick, 1990); software used to prepare material for publication: SHELXL97.
[PtCl2(C14H38B10P2)]·0.5CH2Cl2 | F(000) = 5360 |
Mr = 684.94 | Dx = 1.688 Mg m−3 |
Monoclinic, C2/c | Mo Kα radiation, λ = 0.71073 Å |
a = 42.785 (12) Å | Cell parameters from 23 reflections |
b = 10.320 (14) Å | θ = 5.9–11.9° |
c = 32.238 (11) Å | µ = 5.63 mm−1 |
β = 130.785 (12)° | T = 193 K |
V = 10778 (15) Å3 | Prismatic, colourless |
Z = 16 | 0.27 × 0.20 × 0.10 mm |
Rigaku AFC-7S diffractometer | 6434 reflections with I > 2σ(I) |
Radiation source: fine-focus sealed tube | Rint = 0.053 |
Graphite monochromator | θmax = 25.3°, θmin = 2.5° |
ω/2θ scans | h = 0→51 |
Absorption correction: ψ (North et al., 1968) | k = 0→12 |
Tmin = 0.295, Tmax = 0.570 | l = −38→29 |
9888 measured reflections | 3 standard reflections every 150 reflections |
9749 independent reflections | intensity decay: <1% |
Refinement on F2 | Primary atom site location: structure-invariant direct methods |
Least-squares matrix: full | Secondary atom site location: difference Fourier map |
R[F2 > 2σ(F2)] = 0.068 | Hydrogen site location: inferred from neighbouring sites |
wR(F2) = 0.146 | H-atom parameters constrained |
S = 1.04 | w = 1/[σ2(Fo2) + (0.0528P)2 + 56.0903P] where P = (Fo2 + 2Fc2)/3 |
9749 reflections | (Δ/σ)max = 0.001 |
324 parameters | Δρmax = 2.12 e Å−3 |
6 restraints | Δρmin = −1.69 e Å−3 |
Experimental. The biggest final residual electron peak and hole found in the vicinity of Pt1A: Fourier peaks appended to. res file x y z Peak Distances to nearest atom (including symmetry equivalents) 0.1864 0.7837 0.0986 2.12 0.99 PT1A 0.2029 0.6408 0.1322 - 1.69 0.94 PT1A The biggest final residual electron peak and hole found in the vicinity of Pt1B: Fourier peaks appended to. res file x y z Peak Distances to nearest atom (including symmetry equivalents) 0.0780 1.4795 0.2181 - 1.66 0.91 PT1B 0.0940 1.4769 0.2506 1.64 0.95 PT1B |
Geometry. All e.s.d.'s (except the e.s.d. in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell e.s.d.'s are taken into account individually in the estimation of e.s.d.'s in distances, angles and torsion angles; correlations between e.s.d.'s in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell e.s.d.'s is used for estimating e.s.d.'s involving l.s. planes. |
Refinement. Refinement of F2 against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F2, conventional R-factors R are based on F, with F set to zero for negative F2. The threshold expression of F2 > σ(F2) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F2 are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger. |
x | y | z | Uiso*/Ueq | Occ. (<1) | |
Pt1A | 0.184238 (13) | 0.71090 (5) | 0.116498 (18) | 0.03081 (13) | |
Cl1A | 0.17184 (9) | 0.6898 (3) | 0.17729 (12) | 0.0391 (7) | |
Cl2A | 0.18994 (11) | 0.4841 (3) | 0.11847 (14) | 0.0476 (8) | |
P1A | 0.18007 (9) | 0.9262 (3) | 0.11562 (12) | 0.0312 (7) | |
P2A | 0.20067 (9) | 0.7106 (3) | 0.06406 (13) | 0.0352 (7) | |
C1A | 0.1819 (3) | 0.9902 (12) | 0.0626 (4) | 0.033 (3)* | |
C2A | 0.1919 (3) | 0.8748 (11) | 0.0343 (4) | 0.030 (3)* | |
B3A | 0.1428 (4) | 0.9398 (15) | −0.0031 (6) | 0.040 (4)* | |
H3A | 0.1155 | 0.8833 | −0.0155 | 0.048* | |
B4A | 0.1498 (4) | 1.1052 (15) | 0.0159 (6) | 0.039 (3)* | |
H4A | 0.1270 | 1.1596 | 0.0156 | 0.046* | |
B5A | 0.2037 (4) | 1.1338 (16) | 0.0662 (6) | 0.043 (4)* | |
H5A | 0.2168 | 1.2077 | 0.0992 | 0.052* | |
B6A | 0.2296 (4) | 0.9850 (15) | 0.0788 (6) | 0.040 (3)* | |
H6A | 0.2592 | 0.9585 | 0.1203 | 0.048* | |
B7A | 0.1643 (4) | 0.9102 (16) | −0.0333 (6) | 0.042 (3)* | |
H7A | 0.1510 | 0.8355 | −0.0662 | 0.050* | |
B8A | 0.1398 (5) | 1.0574 (16) | −0.0446 (7) | 0.050 (4)* | |
H8A | 0.1098 | 1.0820 | −0.0860 | 0.059* | |
B9A | 0.1767 (5) | 1.1792 (18) | −0.0027 (7) | 0.053 (4)* | |
H9A | 0.1717 | 1.2830 | −0.0158 | 0.064* | |
B10A | 0.2261 (5) | 1.1023 (17) | 0.0373 (6) | 0.052 (4)* | |
H10A | 0.2541 | 1.1564 | 0.0510 | 0.062* | |
B11A | 0.2189 (5) | 0.9409 (16) | 0.0185 (6) | 0.049 (4)* | |
H11A | 0.2422 | 0.8868 | 0.0197 | 0.059* | |
B12A | 0.1857 (5) | 1.0560 (17) | −0.0325 (7) | 0.053 (4)* | |
H12A | 0.1867 | 1.0786 | −0.0656 | 0.064* | |
C13A | 0.2242 (3) | 1.0120 (12) | 0.1776 (4) | 0.036 (3)* | |
H13A | 0.2456 | 1.0202 | 0.1738 | 0.043* | |
C14A | 0.2442 (4) | 0.9316 (14) | 0.2298 (5) | 0.054 (4)* | |
H14A | 0.2693 | 0.9753 | 0.2613 | 0.081* | |
H14B | 0.2513 | 0.8454 | 0.2255 | 0.081* | |
H14C | 0.2247 | 0.9230 | 0.2360 | 0.081* | |
C15A | 0.2158 (4) | 1.1507 (14) | 0.1860 (5) | 0.051 (4)* | |
H15A | 0.2028 | 1.1467 | 0.2021 | 0.077* | |
H15B | 0.1973 | 1.1952 | 0.1506 | 0.077* | |
H15C | 0.2419 | 1.1983 | 0.2106 | 0.077* | |
C16A | 0.1328 (3) | 0.9943 (13) | 0.0978 (5) | 0.039 (3)* | |
H16A | 0.1317 | 1.0879 | 0.0889 | 0.047* | |
C17A | 0.1332 (4) | 0.9883 (14) | 0.1455 (5) | 0.048 (3)* | |
H17A | 0.1105 | 1.0404 | 0.1369 | 0.072* | |
H17B | 0.1596 | 1.0223 | 0.1786 | 0.072* | |
H17C | 0.1300 | 0.8981 | 0.1517 | 0.072* | |
C18A | 0.0930 (4) | 0.9314 (14) | 0.0475 (5) | 0.055 (4)* | |
H18A | 0.0955 | 0.8370 | 0.0515 | 0.082* | |
H18B | 0.0885 | 0.9564 | 0.0146 | 0.082* | |
H18C | 0.0697 | 0.9607 | 0.0441 | 0.082* | |
C19A | 0.2568 (4) | 0.6732 (13) | 0.1053 (5) | 0.043 (3)* | |
H19A | 0.2675 | 0.7314 | 0.0922 | 0.052* | |
C20A | 0.2810 (4) | 0.7039 (14) | 0.1661 (5) | 0.051 (4)* | |
H20A | 0.2721 | 0.6453 | 0.1806 | 0.077* | |
H20B | 0.2757 | 0.7937 | 0.1698 | 0.077* | |
H20C | 0.3106 | 0.6922 | 0.1867 | 0.077* | |
C21A | 0.2655 (5) | 0.5350 (15) | 0.0999 (6) | 0.064 (4)* | |
H21A | 0.2952 | 0.5242 | 0.1210 | 0.096* | |
H21B | 0.2505 | 0.5155 | 0.0613 | 0.096* | |
H21C | 0.2565 | 0.4758 | 0.1141 | 0.096* | |
C22A | 0.1720 (4) | 0.5933 (14) | 0.0078 (5) | 0.049 (3)* | |
H22A | 0.1809 | 0.5073 | 0.0266 | 0.058* | |
C23A | 0.1827 (5) | 0.5863 (16) | −0.0289 (6) | 0.066 (4)* | |
H23A | 0.1877 | 0.4959 | −0.0325 | 0.099* | |
H23B | 0.2076 | 0.6376 | −0.0127 | 0.099* | |
H23C | 0.1597 | 0.6210 | −0.0652 | 0.099* | |
C24A | 0.1264 (4) | 0.5963 (15) | −0.0238 (6) | 0.058 (4)* | |
H24A | 0.1152 | 0.6799 | −0.0424 | 0.088* | |
H24B | 0.1213 | 0.5844 | 0.0015 | 0.088* | |
H24C | 0.1130 | 0.5264 | −0.0509 | 0.088* | |
Pt1B | 0.095268 (14) | 1.40974 (5) | 0.231749 (18) | 0.03398 (14) | |
Cl1B | 0.13864 (10) | 1.3774 (4) | 0.32680 (12) | 0.0520 (9) | |
Cl2B | 0.09764 (10) | 1.1843 (3) | 0.22331 (13) | 0.0479 (8) | |
P1B | 0.09413 (9) | 1.6237 (3) | 0.24138 (12) | 0.0341 (8) | |
P2B | 0.05980 (9) | 1.4363 (3) | 0.14269 (12) | 0.0305 (7) | |
C1B | 0.0472 (3) | 1.6889 (12) | 0.1735 (4) | 0.033 (3)* | |
C2B | 0.0282 (3) | 1.5870 (12) | 0.1216 (4) | 0.032 (3)* | |
B3B | 0.0023 (4) | 1.6010 (15) | 0.1456 (6) | 0.038 (3)* | |
H3B | 0.0008 | 1.5225 | 0.1682 | 0.045* | |
B4B | 0.0058 (4) | 1.7640 (14) | 0.1620 (6) | 0.034 (3)* | |
H4B | 0.0061 | 1.7940 | 0.1957 | 0.041* | |
B5B | 0.0364 (4) | 1.8473 (15) | 0.1525 (6) | 0.038 (3)* | |
H5B | 0.0565 | 1.9308 | 0.1792 | 0.046* | |
B6B | 0.0507 (4) | 1.7332 (14) | 0.1256 (5) | 0.033 (3)* | |
H6B | 0.0805 | 1.7422 | 0.1341 | 0.040* | |
B7B | −0.0251 (4) | 1.5921 (15) | 0.0740 (5) | 0.037 (3)* | |
H7B | −0.0455 | 1.5080 | 0.0483 | 0.044* | |
B8B | −0.0389 (4) | 1.7052 (15) | 0.0999 (6) | 0.039 (3)* | |
H8B | −0.0687 | 1.6961 | 0.0915 | 0.047* | |
B9B | −0.0193 (4) | 1.8579 (16) | 0.1030 (6) | 0.044 (4)* | |
H9B | −0.0360 | 1.9498 | 0.0963 | 0.053* | |
B10B | 0.0095 (4) | 1.8383 (16) | 0.0800 (6) | 0.041 (4)* | |
H10B | 0.0120 | 1.9170 | 0.0583 | 0.049* | |
B11B | 0.0055 (4) | 1.6694 (15) | 0.0629 (6) | 0.041 (4)* | |
H11B | 0.0056 | 1.6349 | 0.0302 | 0.049* | |
B12B | −0.0375 (4) | 1.7492 (15) | 0.0482 (6) | 0.041 (4)* | |
H12B | −0.0661 | 1.7705 | 0.0051 | 0.050* | |
C13B | 0.1381 (3) | 1.7056 (12) | 0.2537 (5) | 0.035 (3)* | |
H13B | 0.1330 | 1.6966 | 0.2188 | 0.042* | |
C14B | 0.1785 (4) | 1.6337 (14) | 0.2971 (5) | 0.052 (4)* | |
H14D | 0.2004 | 1.6695 | 0.2986 | 0.077* | |
H14E | 0.1749 | 1.5415 | 0.2878 | 0.077* | |
H14F | 0.1860 | 1.6440 | 0.3329 | 0.077* | |
C15B | 0.1428 (4) | 1.8494 (15) | 0.2655 (6) | 0.059 (4)* | |
H15D | 0.1472 | 1.8645 | 0.2990 | 0.089* | |
H15E | 0.1177 | 1.8945 | 0.2348 | 0.089* | |
H15F | 0.1665 | 1.8825 | 0.2705 | 0.089* | |
C16B | 0.0887 (4) | 1.6867 (14) | 0.2899 (5) | 0.049 (3)* | |
H16B | 0.0765 | 1.7755 | 0.2773 | 0.058* | |
C17B | 0.1288 (4) | 1.6984 (14) | 0.3482 (5) | 0.055 (4)* | |
H17D | 0.1232 | 1.7300 | 0.3715 | 0.082* | |
H17E | 0.1470 | 1.7594 | 0.3498 | 0.082* | |
H17F | 0.1421 | 1.6132 | 0.3613 | 0.082* | |
C18B | 0.0588 (4) | 1.6031 (14) | 0.2899 (5) | 0.049 (3)* | |
H18D | 0.0643 | 1.5112 | 0.2895 | 0.073* | |
H18E | 0.0303 | 1.6231 | 0.2573 | 0.073* | |
H18F | 0.0627 | 1.6218 | 0.3228 | 0.073* | |
C19B | 0.0972 (3) | 1.4656 (12) | 0.1328 (4) | 0.033 (3)* | |
H19B | 0.1116 | 1.5480 | 0.1528 | 0.040* | |
C20B | 0.1309 (4) | 1.3604 (13) | 0.1622 (5) | 0.046 (3)* | |
H20D | 0.1196 | 1.2793 | 0.1413 | 0.069* | |
H20E | 0.1407 | 1.3464 | 0.1991 | 0.069* | |
H20F | 0.1541 | 1.3885 | 0.1648 | 0.069* | |
C21B | 0.0801 (4) | 1.4873 (13) | 0.0746 (5) | 0.044 (3)* | |
H21D | 0.1019 | 1.5230 | 0.0756 | 0.066* | |
H21E | 0.0570 | 1.5483 | 0.0558 | 0.066* | |
H21F | 0.0706 | 1.4046 | 0.0548 | 0.066* | |
C22B | 0.0205 (4) | 1.3192 (13) | 0.0919 (5) | 0.041 (3)* | |
H22B | 0.0010 | 1.3675 | 0.0566 | 0.049* | |
C23B | 0.0370 (4) | 1.2046 (12) | 0.0806 (5) | 0.042 (3)* | |
H23D | 0.0545 | 1.1499 | 0.1134 | 0.062* | |
H23E | 0.0533 | 1.2374 | 0.0714 | 0.062* | |
H23F | 0.0138 | 1.1534 | 0.0500 | 0.062* | |
C24B | −0.0054 (4) | 1.2656 (13) | 0.1059 (5) | 0.044 (3)* | |
H24D | −0.0279 | 1.2119 | 0.0755 | 0.067* | |
H24E | −0.0170 | 1.3379 | 0.1117 | 0.067* | |
H24F | 0.0122 | 1.2131 | 0.1393 | 0.067* | |
C25A | 0.0661 (11) | 1.149 (2) | 0.3045 (15) | 0.071 (10)* | 0.525 (18) |
H25A | 0.0965 | 1.1417 | 0.3283 | 0.086* | 0.525 (18) |
H25B | 0.0557 | 1.1998 | 0.2716 | 0.086* | 0.525 (18) |
Cl3A | 0.0444 (4) | 0.9966 (10) | 0.2853 (5) | 0.101 (5)* | 0.525 (18) |
Cl4A | 0.0534 (3) | 1.2231 (11) | 0.3392 (5) | 0.078 (3)* | 0.525 (18) |
C25B | 0.0581 (12) | 1.177 (2) | 0.2881 (14) | 0.077 (14)* | 0.475 (18) |
H25C | 0.0346 | 1.1751 | 0.2481 | 0.092* | 0.475 (18) |
H25D | 0.0805 | 1.2276 | 0.2944 | 0.092* | 0.475 (18) |
Cl3B | 0.0752 (6) | 1.0207 (14) | 0.3101 (7) | 0.128 (7)* | 0.475 (18) |
Cl4B | 0.0427 (5) | 1.2557 (14) | 0.3191 (7) | 0.109 (5)* | 0.475 (18) |
U11 | U22 | U33 | U12 | U13 | U23 | |
Pt1A | 0.0305 (2) | 0.0342 (3) | 0.0321 (2) | 0.0005 (2) | 0.0224 (2) | 0.0007 (2) |
Cl1A | 0.0458 (16) | 0.044 (2) | 0.0434 (16) | −0.0039 (14) | 0.0360 (15) | −0.0030 (14) |
Cl2A | 0.071 (2) | 0.0303 (18) | 0.062 (2) | 0.0045 (16) | 0.0527 (19) | 0.0016 (16) |
P1A | 0.0273 (14) | 0.0350 (18) | 0.0323 (15) | 0.0007 (14) | 0.0198 (13) | 0.0005 (15) |
P2A | 0.0342 (16) | 0.040 (2) | 0.0364 (16) | 0.0039 (15) | 0.0254 (14) | 0.0023 (15) |
Pt1B | 0.0335 (2) | 0.0370 (3) | 0.0318 (2) | 0.0018 (2) | 0.0215 (2) | −0.0016 (2) |
Cl1B | 0.057 (2) | 0.055 (2) | 0.0356 (16) | 0.0086 (17) | 0.0267 (16) | 0.0045 (16) |
Cl2B | 0.0542 (19) | 0.037 (2) | 0.0472 (18) | 0.0048 (15) | 0.0307 (16) | 0.0007 (15) |
P1B | 0.0294 (15) | 0.039 (2) | 0.0298 (15) | 0.0009 (14) | 0.0176 (13) | −0.0052 (14) |
P2B | 0.0292 (15) | 0.0313 (18) | 0.0323 (15) | 0.0011 (13) | 0.0207 (13) | −0.0020 (13) |
Pt1A—P1A | 2.227 (4) | P1B—C13B | 1.855 (12) |
Pt1A—P2A | 2.215 (3) | P1B—C16B | 1.844 (14) |
Pt1A—Cl1A | 2.351 (3) | P2B—C19B | 1.847 (12) |
Pt1A—Cl2A | 2.350 (5) | P2B—C22B | 1.836 (13) |
P1A—C13A | 1.848 (12) | P1B—C1B | 1.879 (11) |
P1A—C16A | 1.844 (12) | P2B—C2B | 1.872 (12) |
P2A—C19A | 1.875 (12) | C1B—C2B | 1.672 (16) |
P2A—C22A | 1.831 (14) | C1B—B6B | 1.709 (17) |
P1A—C1A | 1.880 (12) | C1B—B5B | 1.714 (19) |
P2A—C2A | 1.861 (12) | C1B—B4B | 1.738 (17) |
C1A—B4A | 1.692 (18) | C1B—B3B | 1.749 (18) |
C1A—B3A | 1.712 (17) | C2B—B11B | 1.685 (18) |
C1A—B5A | 1.715 (19) | C2B—B3B | 1.724 (18) |
C1A—C2A | 1.716 (16) | C2B—B7B | 1.731 (16) |
C1A—B6A | 1.746 (18) | C2B—B6B | 1.747 (18) |
C2A—B11A | 1.68 (2) | B3B—B4B | 1.74 (2) |
C2A—B7A | 1.707 (18) | B3B—B8B | 1.74 (2) |
C2A—B6A | 1.712 (18) | B3B—B7B | 1.781 (19) |
C2A—B3A | 1.734 (17) | B3B—H3B | 1.1200 |
B3A—B8A | 1.75 (2) | B4B—B8B | 1.742 (19) |
B3A—B7A | 1.75 (2) | B4B—B9B | 1.74 (2) |
B3A—B4A | 1.77 (2) | B4B—B5B | 1.75 (2) |
B3A—H3A | 1.1200 | B4B—H4B | 1.1200 |
B4A—B8A | 1.77 (2) | B5B—B6B | 1.79 (2) |
B4A—B5A | 1.77 (2) | B5B—B9B | 1.81 (2) |
B4A—B9A | 1.78 (2) | B5B—B10B | 1.81 (2) |
B4A—H4A | 1.1200 | B5B—H5B | 1.1200 |
B5A—B10A | 1.75 (2) | B6B—B10B | 1.75 (2) |
B5A—B9A | 1.77 (2) | B6B—B11B | 1.774 (19) |
B5A—B6A | 1.78 (2) | B6B—H6B | 1.1200 |
B5A—H5A | 1.1200 | B7B—B12B | 1.74 (2) |
B6A—B10A | 1.74 (2) | B7B—B8B | 1.75 (2) |
B6A—B11A | 1.74 (2) | B7B—B11B | 1.76 (2) |
B6A—H6A | 1.1200 | B7B—H7B | 1.1200 |
B7A—B8A | 1.74 (2) | B8B—B9B | 1.76 (2) |
B7A—B12A | 1.75 (2) | B8B—B12B | 1.77 (2) |
B7A—B11A | 1.80 (2) | B8B—H8B | 1.1200 |
B7A—H7A | 1.1200 | B9B—B12B | 1.79 (2) |
B8A—B12A | 1.74 (2) | B9B—B10B | 1.82 (2) |
B8A—B9A | 1.76 (2) | B9B—H9B | 1.1200 |
B8A—H8A | 1.1200 | B10B—B11B | 1.80 (2) |
B9A—B12A | 1.78 (2) | B10B—B12B | 1.80 (2) |
B9A—B10A | 1.79 (2) | B10B—H10B | 1.1200 |
B9A—H9A | 1.1200 | B11B—B12B | 1.77 (2) |
B10A—B11A | 1.73 (2) | B11B—H11B | 1.1200 |
B10A—B12A | 1.79 (2) | B12B—H12B | 1.1200 |
B10A—H10A | 1.1200 | C13B—C15B | 1.513 (18) |
B11A—B12A | 1.75 (2) | C13B—C14B | 1.528 (16) |
B11A—H11A | 1.1200 | C13B—H13B | 1.0000 |
B12A—H12A | 1.1200 | C14B—H14D | 0.9800 |
C13A—C14A | 1.541 (17) | C14B—H14E | 0.9800 |
C13A—C15A | 1.543 (18) | C14B—H14F | 0.9800 |
C13A—H13A | 1.0000 | C15B—H15D | 0.9800 |
C14A—H14A | 0.9800 | C15B—H15E | 0.9800 |
C14A—H14B | 0.9800 | C15B—H15F | 0.9800 |
C14A—H14C | 0.9800 | C16B—C17B | 1.510 (18) |
C15A—H15A | 0.9800 | C16B—C18B | 1.543 (18) |
C15A—H15B | 0.9800 | C16B—H16B | 1.0000 |
C15A—H15C | 0.9800 | C17B—H17D | 0.9800 |
C16A—C17A | 1.527 (17) | C17B—H17E | 0.9800 |
C16A—C18A | 1.529 (17) | C17B—H17F | 0.9800 |
C16A—H16A | 1.0000 | C18B—H18D | 0.9800 |
C17A—H17A | 0.9800 | C18B—H18E | 0.9800 |
C17A—H17B | 0.9800 | C18B—H18F | 0.9800 |
C17A—H17C | 0.9800 | C19B—C21B | 1.523 (16) |
C18A—H18A | 0.9800 | C19B—C20B | 1.542 (16) |
C18A—H18B | 0.9800 | C19B—H19B | 1.0000 |
C18A—H18C | 0.9800 | C20B—H20D | 0.9800 |
C19A—C21A | 1.512 (19) | C20B—H20E | 0.9800 |
C19A—C20A | 1.537 (17) | C20B—H20F | 0.9800 |
C19A—H19A | 1.0000 | C21B—H21D | 0.9800 |
C20A—H20A | 0.9800 | C21B—H21E | 0.9800 |
C20A—H20B | 0.9800 | C21B—H21F | 0.9800 |
C20A—H20C | 0.9800 | C22B—C23B | 1.538 (17) |
C21A—H21A | 0.9800 | C22B—C24B | 1.546 (17) |
C21A—H21B | 0.9800 | C22B—H22B | 1.0000 |
C21A—H21C | 0.9800 | C23B—H23D | 0.9800 |
C22A—C24A | 1.498 (17) | C23B—H23E | 0.9800 |
C22A—C23A | 1.524 (19) | C23B—H23F | 0.9800 |
C22A—H22A | 1.0000 | C24B—H24D | 0.9800 |
C23A—H23A | 0.9800 | C24B—H24E | 0.9800 |
C23A—H23B | 0.9800 | C24B—H24F | 0.9800 |
C23A—H23C | 0.9800 | C25A—Cl4A | 1.715 (10) |
C24A—H24A | 0.9800 | C25A—Cl3A | 1.718 (10) |
C24A—H24B | 0.9800 | C25A—H25A | 0.9900 |
C24A—H24C | 0.9800 | C25A—H25B | 0.9900 |
Pt1B—P1B | 2.235 (4) | C25B—Cl3B | 1.719 (10) |
Pt1B—P2B | 2.220 (3) | C25B—Cl4B | 1.720 (10) |
Pt1B—Cl1B | 2.348 (3) | C25B—H25C | 0.9900 |
Pt1B—Cl2B | 2.353 (5) | C25B—H25D | 0.9900 |
P1A—Pt1A—Cl1A | 92.47 (11) | H24A—C24A—H24C | 109.5 |
P1A—Pt1A—Cl2A | 178.97 (13) | H24B—C24A—H24C | 109.5 |
P1A—Pt1A—P2A | 93.13 (12) | C16B—P1B—C13B | 109.4 (6) |
P2A—Pt1A—Cl1A | 173.27 (12) | C16B—P1B—C1B | 103.3 (6) |
P2A—Pt1A—Cl2A | 86.57 (12) | C13B—P1B—C1B | 104.4 (5) |
Cl1A—Pt1A—Cl2A | 87.78 (12) | C16B—P1B—Pt1B | 119.5 (5) |
C1A—C2A—P2A | 113.2 (7) | C13B—P1B—Pt1B | 111.6 (4) |
C2A—C1A—P1A | 114.4 (8) | C1B—P1B—Pt1B | 107.2 (4) |
P1B—Pt1B—Cl1B | 91.69 (12) | C22B—P2B—C19B | 110.2 (6) |
P1B—Pt1B—Cl2B | 178.93 (13) | C22B—P2B—C2B | 101.5 (5) |
P1B—Pt1B—P2B | 89.95 (12) | C19B—P2B—C2B | 107.5 (5) |
P2B—Pt1B—Cl1B | 174.20 (12) | C22B—P2B—Pt1B | 121.8 (4) |
P2B—Pt1B—Cl2B | 90.98 (12) | C19B—P2B—Pt1B | 107.8 (4) |
Cl1B—Pt1B—Cl2B | 87.33 (12) | C2B—P2B—Pt1B | 107.1 (4) |
C1B—C2B—P2B | 113.3 (7) | C2B—C1B—B6B | 62.2 (7) |
C2B—C1B—P1B | 113.0 (8) | C2B—C1B—B5B | 112.0 (9) |
C16A—P1A—C13A | 107.1 (6) | B6B—C1B—B5B | 63.1 (8) |
C16A—P1A—C1A | 105.7 (5) | C2B—C1B—B4B | 107.9 (8) |
C13A—P1A—C1A | 101.2 (5) | B6B—C1B—B4B | 111.5 (9) |
C16A—P1A—Pt1A | 116.5 (4) | B5B—C1B—B4B | 61.0 (8) |
C13A—P1A—Pt1A | 116.6 (4) | C2B—C1B—B3B | 60.5 (7) |
C1A—P1A—Pt1A | 108.2 (4) | B6B—C1B—B3B | 112.8 (9) |
C22A—P2A—C2A | 108.2 (6) | B5B—C1B—B3B | 111.6 (9) |
C22A—P2A—C19A | 106.6 (6) | B4B—C1B—B3B | 59.9 (7) |
C2A—P2A—C19A | 106.7 (6) | B6B—C1B—P1B | 119.4 (8) |
C22A—P2A—Pt1A | 114.6 (5) | B5B—C1B—P1B | 127.5 (8) |
C2A—P2A—Pt1A | 109.5 (4) | B4B—C1B—P1B | 125.0 (8) |
C19A—P2A—Pt1A | 111.0 (4) | B3B—C1B—P1B | 113.1 (8) |
B4A—C1A—B3A | 62.7 (8) | C1B—C2B—B11B | 110.7 (10) |
B4A—C1A—B5A | 62.8 (8) | C1B—C2B—B3B | 62.0 (7) |
B3A—C1A—B5A | 113.2 (10) | B11B—C2B—B3B | 113.0 (9) |
B4A—C1A—C2A | 110.5 (9) | C1B—C2B—B7B | 111.4 (9) |
B3A—C1A—C2A | 60.8 (7) | B11B—C2B—B7B | 61.9 (8) |
B5A—C1A—C2A | 108.7 (9) | B3B—C2B—B7B | 62.1 (7) |
B4A—C1A—B6A | 113.4 (10) | C1B—C2B—B6B | 60.0 (7) |
B3A—C1A—B6A | 111.5 (9) | B11B—C2B—B6B | 62.2 (8) |
B5A—C1A—B6A | 61.8 (8) | B3B—C2B—B6B | 112.2 (10) |
C2A—C1A—B6A | 59.3 (7) | B7B—C2B—B6B | 112.5 (9) |
B4A—C1A—P1A | 124.4 (8) | B11B—C2B—P2B | 125.4 (8) |
B3A—C1A—P1A | 115.5 (8) | B3B—C2B—P2B | 115.4 (8) |
B5A—C1A—P1A | 126.0 (8) | B7B—C2B—P2B | 124.6 (8) |
B6A—C1A—P1A | 116.9 (8) | B6B—C2B—P2B | 117.4 (7) |
B11A—C2A—B7A | 64.2 (8) | C2B—B3B—B4B | 105.5 (10) |
B11A—C2A—B6A | 61.8 (8) | C2B—B3B—B8B | 105.4 (10) |
B7A—C2A—B6A | 114.5 (10) | B4B—B3B—B8B | 60.0 (8) |
B11A—C2A—C1A | 109.8 (10) | C2B—B3B—C1B | 57.5 (7) |
B7A—C2A—C1A | 109.1 (9) | B4B—B3B—C1B | 59.7 (8) |
B6A—C2A—C1A | 61.2 (7) | B8B—B3B—C1B | 106.3 (10) |
B11A—C2A—B3A | 113.1 (10) | C2B—B3B—B7B | 59.2 (7) |
B7A—C2A—B3A | 61.1 (8) | B4B—B3B—B7B | 107.3 (10) |
B6A—C2A—B3A | 112.1 (10) | B8B—B3B—B7B | 59.4 (8) |
C1A—C2A—B3A | 59.5 (7) | C1B—B3B—B7B | 105.5 (10) |
B11A—C2A—P2A | 125.3 (9) | C2B—B3B—H3B | 124.0 |
B7A—C2A—P2A | 126.3 (9) | B4B—B3B—H3B | 122.0 |
B6A—C2A—P2A | 114.2 (8) | B8B—B3B—H3B | 122.6 |
B3A—C2A—P2A | 117.1 (8) | C1B—B3B—H3B | 123.4 |
C1A—B3A—C2A | 59.7 (7) | B7B—B3B—H3B | 122.4 |
C1A—B3A—B8A | 105.1 (10) | C1B—B4B—B3B | 60.4 (8) |
C2A—B3A—B8A | 104.5 (10) | C1B—B4B—B8B | 106.9 (10) |
C1A—B3A—B7A | 107.3 (10) | B3B—B4B—B8B | 60.1 (8) |
C2A—B3A—B7A | 58.7 (8) | C1B—B4B—B9B | 107.2 (10) |
B8A—B3A—B7A | 59.9 (9) | B3B—B4B—B9B | 109.6 (10) |
C1A—B3A—B4A | 58.1 (7) | B8B—B4B—B9B | 60.5 (8) |
C2A—B3A—B4A | 106.1 (10) | C1B—B4B—B5B | 58.8 (8) |
B8A—B3A—B4A | 60.4 (9) | B3B—B4B—B5B | 110.2 (10) |
B7A—B3A—B4A | 109.1 (11) | B8B—B4B—B5B | 110.8 (10) |
C1A—B3A—H3A | 123.2 | B9B—B4B—B5B | 62.3 (8) |
C2A—B3A—H3A | 123.7 | C1B—B4B—H4B | 123.4 |
B8A—B3A—H3A | 123.4 | B3B—B4B—H4B | 120.5 |
B7A—B3A—H3A | 121.2 | B8B—B4B—H4B | 121.3 |
B4A—B3A—H3A | 121.8 | B9B—B4B—H4B | 120.8 |
C1A—B4A—B8A | 105.0 (10) | B5B—B4B—H4B | 119.8 |
C1A—B4A—B3A | 59.2 (8) | C1B—B5B—B4B | 60.2 (8) |
B8A—B4A—B3A | 59.1 (8) | C1B—B5B—B6B | 58.3 (8) |
C1A—B4A—B5A | 59.3 (8) | B4B—B5B—B6B | 107.1 (11) |
B8A—B4A—B5A | 106.8 (11) | C1B—B5B—B9B | 105.4 (10) |
B3A—B4A—B5A | 107.6 (10) | B4B—B5B—B9B | 58.6 (8) |
C1A—B4A—B9A | 106.0 (10) | B6B—B5B—B9B | 106.4 (10) |
B8A—B4A—B9A | 59.6 (9) | C1B—B5B—B10B | 103.9 (10) |
B3A—B4A—B9A | 107.4 (11) | B4B—B5B—B10B | 106.5 (10) |
B5A—B4A—B9A | 59.8 (8) | B6B—B5B—B10B | 58.0 (8) |
C1A—B4A—H4A | 123.6 | B9B—B5B—B10B | 60.4 (8) |
B8A—B4A—H4A | 123.2 | C1B—B5B—H5B | 123.8 |
B3A—B4A—H4A | 121.9 | B4B—B5B—H5B | 122.0 |
B5A—B4A—H4A | 121.9 | B6B—B5B—H5B | 122.9 |
B9A—B4A—H4A | 122.2 | B9B—B5B—H5B | 122.6 |
C1A—B5A—B10A | 105.6 (11) | B10B—B5B—H5B | 123.4 |
C1A—B5A—B9A | 105.3 (11) | C1B—B6B—C2B | 57.8 (7) |
B10A—B5A—B9A | 61.2 (9) | C1B—B6B—B10B | 107.0 (10) |
C1A—B5A—B4A | 58.0 (8) | C2B—B6B—B10B | 105.7 (9) |
B10A—B5A—B4A | 108.6 (11) | C1B—B6B—B11B | 104.8 (10) |
B9A—B5A—B4A | 60.2 (8) | C2B—B6B—B11B | 57.2 (7) |
C1A—B5A—B6A | 59.9 (8) | B10B—B6B—B11B | 61.5 (8) |
B10A—B5A—B6A | 59.1 (9) | C1B—B6B—B5B | 58.6 (8) |
B9A—B5A—B6A | 108.4 (11) | C2B—B6B—B5B | 105.0 (10) |
B4A—B5A—B6A | 108.0 (11) | B10B—B6B—B5B | 61.6 (8) |
C1A—B5A—H5A | 124.2 | B11B—B6B—B5B | 109.4 (10) |
B10A—B5A—H5A | 121.9 | C1B—B6B—H6B | 123.9 |
B9A—B5A—H5A | 121.7 | C2B—B6B—H6B | 124.9 |
B4A—B5A—H5A | 121.7 | B10B—B6B—H6B | 121.0 |
B6A—B5A—H5A | 121.5 | B11B—B6B—H6B | 122.0 |
C2A—B6A—B10A | 104.9 (10) | B5B—B6B—H6B | 121.4 |
C2A—B6A—B11A | 58.3 (8) | C2B—B7B—B12B | 105.4 (10) |
B10A—B6A—B11A | 59.6 (9) | C2B—B7B—B8B | 105.0 (9) |
C2A—B6A—C1A | 59.5 (7) | B12B—B7B—B8B | 60.9 (8) |
B10A—B6A—C1A | 104.7 (10) | C2B—B7B—B11B | 57.8 (7) |
B11A—B6A—C1A | 105.7 (10) | B12B—B7B—B11B | 60.9 (8) |
C2A—B6A—B5A | 106.1 (10) | B8B—B7B—B11B | 108.8 (11) |
B10A—B6A—B5A | 59.6 (9) | C2B—B7B—B3B | 58.8 (7) |
B11A—B6A—B5A | 107.4 (11) | B12B—B7B—B3B | 108.0 (11) |
C1A—B6A—B5A | 58.3 (8) | B8B—B7B—B3B | 59.2 (8) |
C2A—B6A—H6A | 123.4 | B11B—B7B—B3B | 106.9 (10) |
B10A—B6A—H6A | 123.4 | C2B—B7B—H7B | 124.8 |
B11A—B6A—H6A | 122.4 | B12B—B7B—H7B | 121.4 |
C1A—B6A—H6A | 123.6 | B8B—B7B—H7B | 121.9 |
B5A—B6A—H6A | 122.3 | B11B—B7B—H7B | 121.6 |
C2A—B7A—B8A | 105.8 (11) | B3B—B7B—H7B | 122.3 |
C2A—B7A—B3A | 60.2 (8) | B4B—B8B—B3B | 59.9 (8) |
B8A—B7A—B3A | 60.0 (9) | B4B—B8B—B7B | 108.8 (10) |
C2A—B7A—B12A | 104.2 (10) | B3B—B8B—B7B | 61.3 (8) |
B8A—B7A—B12A | 59.5 (9) | B4B—B8B—B9B | 59.8 (8) |
B3A—B7A—B12A | 107.5 (12) | B3B—B8B—B9B | 108.8 (10) |
C2A—B7A—B11A | 57.2 (8) | B7B—B8B—B9B | 109.1 (11) |
B8A—B7A—B11A | 106.2 (11) | B4B—B8B—B12B | 107.9 (10) |
B3A—B7A—B11A | 106.8 (10) | B3B—B8B—B12B | 108.4 (10) |
B12A—B7A—B11A | 59.1 (9) | B7B—B8B—B12B | 59.3 (8) |
C2A—B7A—H7A | 124.1 | B9B—B8B—B12B | 60.9 (8) |
B8A—B7A—H7A | 122.5 | B4B—B8B—H8B | 121.9 |
B3A—B7A—H7A | 121.3 | B3B—B8B—H8B | 121.1 |
B12A—B7A—H7A | 123.0 | B7B—B8B—H8B | 121.0 |
B11A—B7A—H7A | 123.3 | B9B—B8B—H8B | 121.0 |
B12A—B8A—B7A | 60.4 (9) | B12B—B8B—H8B | 121.9 |
B12A—B8A—B3A | 108.4 (12) | B4B—B9B—B8B | 59.7 (8) |
B7A—B8A—B3A | 60.1 (9) | B4B—B9B—B12B | 106.9 (11) |
B12A—B8A—B9A | 61.2 (9) | B8B—B9B—B12B | 59.8 (8) |
B7A—B8A—B9A | 110.2 (11) | B4B—B9B—B5B | 59.1 (8) |
B3A—B8A—B9A | 109.2 (11) | B8B—B9B—B5B | 107.6 (11) |
B12A—B8A—B4A | 109.2 (11) | B12B—B9B—B5B | 107.9 (11) |
B7A—B8A—B4A | 109.5 (11) | B4B—B9B—B10B | 106.6 (10) |
B3A—B8A—B4A | 60.5 (9) | B8B—B9B—B10B | 107.6 (11) |
B9A—B8A—B4A | 60.4 (9) | B12B—B9B—B10B | 60.0 (8) |
B12A—B8A—H8A | 121.2 | B5B—B9B—B10B | 59.9 (8) |
B7A—B8A—H8A | 120.7 | B4B—B9B—H9B | 122.9 |
B3A—B8A—H8A | 121.6 | B8B—B9B—H9B | 121.8 |
B9A—B8A—H8A | 120.4 | B12B—B9B—H9B | 121.9 |
B4A—B8A—H8A | 121.0 | B5B—B9B—H9B | 121.9 |
B8A—B9A—B5A | 107.2 (12) | B10B—B9B—H9B | 122.1 |
B8A—B9A—B4A | 60.0 (9) | B6B—B10B—B11B | 60.0 (8) |
B5A—B9A—B4A | 60.0 (9) | B6B—B10B—B12B | 107.4 (11) |
B8A—B9A—B12A | 58.7 (9) | B11B—B10B—B12B | 58.9 (8) |
B5A—B9A—B12A | 107.0 (12) | B6B—B10B—B5B | 60.4 (8) |
B4A—B9A—B12A | 106.9 (12) | B11B—B10B—B5B | 107.3 (11) |
B8A—B9A—B10A | 106.4 (12) | B12B—B10B—B5B | 106.9 (11) |
B5A—B9A—B10A | 58.8 (9) | B6B—B10B—B9B | 107.8 (11) |
B4A—B9A—B10A | 106.6 (12) | B11B—B10B—B9B | 106.0 (11) |
B12A—B9A—B10A | 60.1 (9) | B12B—B10B—B9B | 59.1 (8) |
B8A—B9A—H9A | 122.6 | B5B—B10B—B9B | 59.7 (8) |
B5A—B9A—H9A | 122.2 | B6B—B10B—H10B | 121.4 |
B4A—B9A—H9A | 122.1 | B11B—B10B—H10B | 122.8 |
B12A—B9A—H9A | 122.4 | B12B—B10B—H10B | 122.6 |
B10A—B9A—H9A | 122.7 | B5B—B10B—H10B | 121.9 |
B11A—B10A—B6A | 60.4 (9) | B9B—B10B—H10B | 122.6 |
B11A—B10A—B5A | 109.4 (13) | C2B—B11B—B7B | 60.3 (8) |
B6A—B10A—B5A | 61.3 (9) | C2B—B11B—B12B | 105.9 (10) |
B11A—B10A—B12A | 59.8 (9) | B7B—B11B—B12B | 59.0 (8) |
B6A—B10A—B12A | 108.0 (12) | C2B—B11B—B6B | 60.6 (7) |
B5A—B10A—B12A | 107.7 (11) | B7B—B11B—B6B | 109.9 (10) |
B11A—B10A—B9A | 108.5 (12) | B12B—B11B—B6B | 107.6 (11) |
B6A—B10A—B9A | 109.3 (12) | C2B—B11B—B10B | 106.0 (10) |
B5A—B10A—B9A | 60.0 (9) | B7B—B11B—B10B | 108.3 (11) |
B12A—B10A—B9A | 59.7 (9) | B12B—B11B—B10B | 60.6 (8) |
B11A—B10A—H10A | 121.2 | B6B—B11B—B10B | 58.5 (8) |
B6A—B10A—H10A | 120.9 | C2B—B11B—H11B | 122.8 |
B5A—B10A—H10A | 121.1 | B7B—B11B—H11B | 120.8 |
B12A—B10A—H10A | 122.4 | B12B—B11B—H11B | 122.7 |
B9A—B10A—H10A | 121.4 | B6B—B11B—H11B | 121.2 |
C2A—B11A—B10A | 106.5 (12) | B10B—B11B—H11B | 122.5 |
C2A—B11A—B6A | 59.9 (8) | B7B—B12B—B8B | 59.8 (8) |
B10A—B11A—B6A | 60.0 (9) | B7B—B12B—B11B | 60.0 (8) |
C2A—B11A—B12A | 105.2 (11) | B8B—B12B—B11B | 107.2 (10) |
B10A—B11A—B12A | 61.7 (9) | B7B—B12B—B9B | 108.2 (11) |
B6A—B11A—B12A | 109.3 (12) | B8B—B12B—B9B | 59.2 (8) |
C2A—B11A—B7A | 58.6 (8) | B11B—B12B—B9B | 108.7 (10) |
B10A—B11A—B7A | 108.7 (12) | B7B—B12B—B10B | 108.9 (10) |
B6A—B11A—B7A | 108.4 (11) | B8B—B12B—B10B | 107.9 (10) |
B12A—B11A—B7A | 59.0 (9) | B11B—B12B—B10B | 60.4 (8) |
C2A—B11A—H11A | 123.9 | B9B—B12B—B10B | 60.9 (8) |
B10A—B11A—H11A | 121.1 | B7B—B12B—H12B | 121.4 |
B6A—B11A—H11A | 120.8 | B8B—B12B—H12B | 122.6 |
B12A—B11A—H11A | 121.9 | B11B—B12B—H12B | 121.7 |
B7A—B11A—H11A | 122.0 | B9B—B12B—H12B | 121.4 |
B8A—B12A—B7A | 60.0 (9) | B10B—B12B—H12B | 120.9 |
B8A—B12A—B11A | 108.8 (13) | C15B—C13B—C14B | 111.2 (10) |
B7A—B12A—B11A | 61.9 (9) | C15B—C13B—P1B | 116.6 (9) |
B8A—B12A—B9A | 60.2 (9) | C14B—C13B—P1B | 110.8 (9) |
B7A—B12A—B9A | 109.1 (12) | C15B—C13B—H13B | 105.8 |
B11A—B12A—B9A | 107.9 (12) | C14B—C13B—H13B | 105.8 |
B8A—B12A—B10A | 107.7 (12) | P1B—C13B—H13B | 105.8 |
B7A—B12A—B10A | 108.4 (12) | C13B—C14B—H14D | 109.5 |
B11A—B12A—B10A | 58.5 (9) | C13B—C14B—H14E | 109.5 |
B9A—B12A—B10A | 60.2 (9) | H14D—C14B—H14E | 109.5 |
B8A—B12A—H12A | 121.7 | C13B—C14B—H14F | 109.5 |
B7A—B12A—H12A | 120.6 | H14D—C14B—H14F | 109.5 |
B11A—B12A—H12A | 121.5 | H14E—C14B—H14F | 109.5 |
B9A—B12A—H12A | 121.4 | C13B—C15B—H15D | 109.5 |
B10A—B12A—H12A | 122.4 | C13B—C15B—H15E | 109.5 |
C14A—C13A—C15A | 109.5 (10) | H15D—C15B—H15E | 109.5 |
C14A—C13A—P1A | 111.7 (9) | C13B—C15B—H15F | 109.5 |
C15A—C13A—P1A | 116.3 (8) | H15D—C15B—H15F | 109.5 |
C14A—C13A—H13A | 106.2 | H15E—C15B—H15F | 109.5 |
C15A—C13A—H13A | 106.2 | C17B—C16B—C18B | 108.2 (11) |
P1A—C13A—H13A | 106.2 | C17B—C16B—P1B | 114.5 (10) |
C13A—C14A—H14A | 109.5 | C18B—C16B—P1B | 111.5 (9) |
C13A—C14A—H14B | 109.5 | C17B—C16B—H16B | 107.5 |
H14A—C14A—H14B | 109.5 | C18B—C16B—H16B | 107.5 |
C13A—C14A—H14C | 109.5 | P1B—C16B—H16B | 107.5 |
H14A—C14A—H14C | 109.5 | C16B—C17B—H17D | 109.5 |
H14B—C14A—H14C | 109.5 | C16B—C17B—H17E | 109.5 |
C13A—C15A—H15A | 109.5 | H17D—C17B—H17E | 109.5 |
C13A—C15A—H15B | 109.5 | C16B—C17B—H17F | 109.5 |
H15A—C15A—H15B | 109.5 | H17D—C17B—H17F | 109.5 |
C13A—C15A—H15C | 109.5 | H17E—C17B—H17F | 109.5 |
H15A—C15A—H15C | 109.5 | C16B—C18B—H18D | 109.5 |
H15B—C15A—H15C | 109.5 | C16B—C18B—H18E | 109.5 |
C17A—C16A—C18A | 109.0 (10) | H18D—C18B—H18E | 109.5 |
C17A—C16A—P1A | 112.3 (8) | C16B—C18B—H18F | 109.5 |
C18A—C16A—P1A | 113.7 (9) | H18D—C18B—H18F | 109.5 |
C17A—C16A—H16A | 107.1 | H18E—C18B—H18F | 109.5 |
C18A—C16A—H16A | 107.1 | C21B—C19B—C20B | 111.3 (10) |
P1A—C16A—H16A | 107.1 | C21B—C19B—P2B | 117.7 (8) |
C16A—C17A—H17A | 109.5 | C20B—C19B—P2B | 110.4 (8) |
C16A—C17A—H17B | 109.5 | C21B—C19B—H19B | 105.5 |
H17A—C17A—H17B | 109.5 | C20B—C19B—H19B | 105.5 |
C16A—C17A—H17C | 109.5 | P2B—C19B—H19B | 105.5 |
H17A—C17A—H17C | 109.5 | C19B—C20B—H20D | 109.5 |
H17B—C17A—H17C | 109.5 | C19B—C20B—H20E | 109.5 |
C16A—C18A—H18A | 109.5 | H20D—C20B—H20E | 109.5 |
C16A—C18A—H18B | 109.5 | C19B—C20B—H20F | 109.5 |
H18A—C18A—H18B | 109.5 | H20D—C20B—H20F | 109.5 |
C16A—C18A—H18C | 109.5 | H20E—C20B—H20F | 109.5 |
H18A—C18A—H18C | 109.5 | C19B—C21B—H21D | 109.5 |
H18B—C18A—H18C | 109.5 | C19B—C21B—H21E | 109.5 |
C21A—C19A—C20A | 109.3 (11) | H21D—C21B—H21E | 109.5 |
C21A—C19A—P2A | 114.2 (9) | C19B—C21B—H21F | 109.5 |
C20A—C19A—P2A | 110.1 (9) | H21D—C21B—H21F | 109.5 |
C21A—C19A—H19A | 107.7 | H21E—C21B—H21F | 109.5 |
C20A—C19A—H19A | 107.7 | C23B—C22B—C24B | 108.7 (11) |
P2A—C19A—H19A | 107.7 | C23B—C22B—P2B | 115.0 (8) |
C19A—C20A—H20A | 109.5 | C24B—C22B—P2B | 112.9 (9) |
C19A—C20A—H20B | 109.5 | C23B—C22B—H22B | 106.6 |
H20A—C20A—H20B | 109.5 | C24B—C22B—H22B | 106.6 |
C19A—C20A—H20C | 109.5 | P2B—C22B—H22B | 106.6 |
H20A—C20A—H20C | 109.5 | C22B—C23B—H23D | 109.5 |
H20B—C20A—H20C | 109.5 | C22B—C23B—H23E | 109.5 |
C19A—C21A—H21A | 109.5 | H23D—C23B—H23E | 109.5 |
C19A—C21A—H21B | 109.5 | C22B—C23B—H23F | 109.5 |
H21A—C21A—H21B | 109.5 | H23D—C23B—H23F | 109.5 |
C19A—C21A—H21C | 109.5 | H23E—C23B—H23F | 109.5 |
H21A—C21A—H21C | 109.5 | C22B—C24B—H24D | 109.5 |
H21B—C21A—H21C | 109.5 | C22B—C24B—H24E | 109.5 |
C24A—C22A—C23A | 113.1 (11) | H24D—C24B—H24E | 109.5 |
C24A—C22A—P2A | 113.0 (10) | C22B—C24B—H24F | 109.5 |
C23A—C22A—P2A | 117.0 (10) | H24D—C24B—H24F | 109.5 |
C24A—C22A—H22A | 104.0 | H24E—C24B—H24F | 109.5 |
C23A—C22A—H22A | 104.0 | Cl4A—C25A—Cl3A | 108.5 (9) |
P2A—C22A—H22A | 104.0 | Cl4A—C25A—H25A | 110.0 |
C22A—C23A—H23A | 109.5 | Cl3A—C25A—H25A | 110.0 |
C22A—C23A—H23B | 109.5 | Cl4A—C25A—H25B | 110.0 |
H23A—C23A—H23B | 109.5 | Cl3A—C25A—H25B | 110.0 |
C22A—C23A—H23C | 109.5 | H25A—C25A—H25B | 108.4 |
H23A—C23A—H23C | 109.5 | Cl3B—C25B—Cl4B | 115.1 (12) |
H23B—C23A—H23C | 109.5 | Cl3B—C25B—H25C | 108.5 |
C22A—C24A—H24A | 109.5 | Cl4B—C25B—H25C | 108.5 |
C22A—C24A—H24B | 109.5 | Cl3B—C25B—H25D | 108.5 |
H24A—C24A—H24B | 109.5 | Cl4B—C25B—H25D | 108.5 |
C22A—C24A—H24C | 109.5 | H25C—C25B—H25D | 107.5 |
P1A—C1A—C2A—P2A | −2.0 (10) | P1B—C1B—C2B—P2B | −3.0 (10) |
Cl1A—Pt1A—P1A—C13A | 73.9 (5) | Cl1B—Pt1B—P1B—C13B | 86.8 (4) |
Cl1A—Pt1A—P1A—C16A | −54.2 (4) | Cl1B—Pt1B—P1B—C16B | −42.5 (5) |
Cl2A—Pt1A—P2A—C19A | −73.5 (5) | Cl2B—Pt1B—P2B—C19B | −91.7 (4) |
Cl2A—Pt1A—P2A—C22A | 47.3 (5) | Cl2B—Pt1B—P2B—C22B | 36.9 (5) |
C1A—C2A—P2A—C19A | −110.0 (8) | C1B—C2B—P2B—C19B | −92.8 (8) |
C1A—C2A—P2A—C22A | 135.6 (7) | C1B—C2B—P2B—C22B | 151.5 (8) |
C2A—C1A—P1A—C13A | 116.1 (8) | C2B—C1B—P1B—C13B | 100.6 (8) |
C2A—C1A—P1A—C16A | −132.4 (8) | C2B—C1B—P1B—C16B | −145.1 (8) |
C13A—P1A—P2A—C19A | 6.7 (7) | C13B—P1B—P2B—C19B | 2.9 (5) |
C22A—P2A—P1A—C16A | −5.4 (10) | C22B—P2B—P1B—C16B | 3.4 (12) |