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Data were collected from a crystal of CoZnPO-CZP {sodium cobalt–zinc phosphate hydrate, Na6[Co0.2Zn0.8­PO4]6.6H2O} using synchrotron radiation at ELETTRA at the inflection point and `white line' for both the cobalt and zinc K edges, and at 1.45 Å, a wavelength remote from the K edges of both metals. The data were processed using the programs DENZO and SCALEPACK. The CCP4 program suite was used for the scaling of data sets and the subsequent calculation of dispersive difference Fourier maps. Optimal scaling was achieved by using a subset of reflections with little or no contribution from the metal atoms (i.e. which were essentially wavelength independent in their intensities) and using weights based on the σ's to obtain an overall scale factor in each case. Phases were calculated with SHELXL97 based on the refined structure using a much higher resolution and complete Cu Kα data set. An occupancy of 100% by zinc at the two metal-atom sites was assumed. The dispersive difference Fourier map calculated for zinc gave two peaks above the background of similar heights at the expected metal-atom sites. The peak height at the Zn1 site was a little higher than at the Zn2 site. The dispersive difference Fourier map calculated for cobalt gave just one peak above the background, at the Zn1 site, and only a small peak at the Zn2 site, thus indicating that incorporation of cobalt takes place mainly at one site. Refinement of the zinc occupancies using MLPHARE reinforces this con­clusion. The chemical environment of each site is discussed.

Supporting information

cif

Crystallographic Information File (CIF)
Contains datablock hex

hkl

Structure factor file (CIF format)
Contains datablock hex

Computing details top

Data collection: MSC/AFC Diffractometer Control; cell refinement: MSC/AFC Diffractometer Control; data reduction: TEXSAN (MSC, 1995); program(s) used to solve structure: Zabukovic et al.; Rajic et al., 1995; program(s) used to refine structure: SHELXL97 (Sheldrick, 1997); software used to prepare material for publication: TEXSAN (MSC, 1995).

(hex) top
Crystal data top
Na6[Co0.2Zn0.8PO4]6·6(H2O)Dx = 2.792 Mg m3
Mr = 200.06Cu Kα radiation, λ = 1.5418 Å
Hexagonal, P6522Cell parameters from 14 reflections
a = 10.464 (4) Åθ = 15.6–26.1°
c = 15.056 (4) ŵ = 15.01 mm1
V = 1427.6 (6) Å3T = 294 K
Z = 12Prismatic, blue
F(000) = 11690.05 × 0.02 × 0.02 mm
Data collection top
Rigaku AFC5R four circle
diffractometer
637 reflections with I > 2σ(I)
Radiation source: Rigaku rotating anodeRint = 0.059
Graphite monochromatorθmax = 59.9°, θmin = 5.7°
ω–2θ scansh = 1010
Absorption correction: ψ scan
(North,Phillips & Matthews, 1968)
k = 1010
Tmin = 0.592, Tmax = 0.741l = 1616
1733 measured reflections3 standard reflections every 150 reflections
713 independent reflections intensity decay: 1.0%
Refinement top
Refinement on F2Hydrogen site location: inferred from neighbouring sites
Least-squares matrix: fullH atoms treated by a mixture of independent and constrained refinement
R[F2 > 2σ(F2)] = 0.051Calculated w = 1/[σ2(Fo2) + (0.0333P)2 + 20.8883P]
where P = (Fo2 + 2Fc2)/3
wR(F2) = 0.125(Δ/σ)max < 0.001
S = 1.08Δρmax = 0.62 e Å3
713 reflectionsΔρmin = 0.47 e Å3
72 parametersExtinction correction: SHELXL97, Fc*=kFc[1+0.001xFc2λ3/sin(2θ)]-1/4
0 restraintsExtinction coefficient: 0.0020 (2)
Primary atom site location: structure-invariant direct methodsAbsolute structure: Flack H D (1983), Acta Cryst. A39, 876-881
Secondary atom site location: difference Fourier mapAbsolute structure parameter: 0.00 (18)
Special details top

Experimental. The scan width was (0.94 + 0.30tanθ)° with an ω scan speed of 8° per minute (up to 4 scans to achieve I/σ(I) > 10). Stationary background counts were recorded at each end of the scan, and the scan time:background time ratio was 2:1.

Geometry. All e.s.d.'s (except the e.s.d. in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell e.s.d.'s are taken into account individually in the estimation of e.s.d.'s in distances, angles and torsion angles; correlations between e.s.d.'s in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell e.s.d.'s is used for estimating e.s.d.'s involving l.s. planes.

Refinement. Refinement of F2 against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F2, conventional R-factors R are based on F, with F set to zero for negative F2. The threshold expression of F2 > σ(F2) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F2 are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger.

Fractional atomic coordinates and isotropic or equivalent isotropic displacement parameters (Å2) top
xyzUiso*/UeqOcc. (<1)
Zn10.49273 (11)0.50727 (11)0.08330.0160 (6)
Zn20.15823 (11)0.15823 (11)0.08330.0145 (6)
P10.1691 (3)0.4097 (3)0.05934 (18)0.0123 (7)
Na10.6343 (11)0.2974 (11)0.0765 (9)0.044 (3)*0.50
O10.0491 (8)0.2469 (8)0.0535 (5)0.023 (2)
O20.3112 (8)0.4286 (10)0.0181 (5)0.027 (2)
O30.6162 (9)0.4919 (9)0.0088 (6)0.028 (2)*
O40.1966 (8)0.4612 (8)0.1553 (5)0.0200 (19)
Na2A0.091 (4)0.018 (5)0.038 (2)0.137 (12)*0.320 (14)
Na2B0.212 (7)0.185 (8)0.049 (4)0.137 (12)*0.180 (14)
O5A0.414 (4)0.312 (5)0.157 (3)0.168 (14)*0.66 (5)
O5B0.416 (7)0.173 (10)0.064 (8)0.168 (14)*0.34 (5)
Atomic displacement parameters (Å2) top
U11U22U33U12U13U23
Zn10.0161 (8)0.0161 (8)0.0169 (11)0.0090 (9)0.0024 (7)0.0024 (7)
Zn20.0140 (8)0.0140 (8)0.0136 (10)0.0057 (9)0.0014 (7)0.0014 (7)
P10.0077 (13)0.0163 (15)0.0114 (12)0.0048 (12)0.0004 (11)0.0024 (11)
O10.019 (4)0.019 (4)0.027 (5)0.006 (4)0.005 (3)0.006 (4)
O20.010 (4)0.039 (5)0.025 (4)0.007 (4)0.007 (3)0.011 (4)
O40.027 (5)0.022 (4)0.014 (4)0.014 (4)0.001 (3)0.003 (3)
Geometric parameters (Å, º) top
Zn1—O21.920 (7)O2—Na2B2.44 (7)
Zn1—O2i1.920 (7)O2—Na1ii2.604 (15)
Zn1—O31.956 (8)O3—P1xiv1.531 (8)
Zn1—O3i1.956 (8)O3—Na1i2.445 (14)
Zn1—Na13.207 (10)O4—Zn2xii1.969 (7)
Zn1—Na1i3.207 (10)O4—Na1xvi2.257 (14)
Zn1—Na1ii3.663 (12)O4—Na1iii2.488 (13)
Zn1—Na1iii3.663 (12)Na2A—Na2Axv1.18 (6)
Zn2—O11.938 (8)Na2A—Na2Axi1.49 (6)
Zn2—O1iv1.938 (8)Na2A—Na2B1.57 (7)
Zn2—O4ii1.969 (7)Na2A—Na2Bxi1.71 (7)
Zn2—O4v1.969 (7)Na2A—Na2Bxv2.29 (9)
Zn2—Na1vi3.163 (10)Na2A—Na2Aii2.656 (11)
Zn2—Na1vii3.163 (10)Na2A—Na2Axii2.656 (11)
P1—O41.519 (7)Na2A—Na2Bxii2.67 (8)
P1—O21.529 (8)Na2A—O1xv2.91 (4)
P1—O3viii1.531 (8)Na2A—O5B2.97 (7)
P1—O11.532 (8)Na2A—Na2Bii3.62 (8)
P1—Na2B3.08 (7)Na2B—Na2Axi1.71 (7)
P1—Na1ii3.090 (13)Na2B—Na2Bxi1.94 (14)
P1—Na1viii3.359 (12)Na2B—O5Bxi2.07 (9)
Na1—Na1i0.744 (19)Na2B—O5B2.21 (10)
Na1—O4ix2.257 (14)Na2B—Na2Axv2.29 (9)
Na1—O3i2.445 (14)Na2B—O5A2.46 (8)
Na1—O4x2.488 (13)Na2B—Na2Aii2.67 (8)
Na1—O32.493 (14)Na2B—O5Axi2.72 (8)
Na1—O5Axi2.53 (4)Na2B—O5Axvii2.83 (9)
Na1—O2xii2.604 (15)O5A—O5Bxi1.10 (9)
Na1—O5B2.90 (9)O5A—Na1xi2.53 (4)
Na1—P1xii3.090 (13)O5A—Na2Bxi2.72 (8)
Na1—Zn2xiii3.163 (10)O5A—Na2Bxvii2.83 (9)
Na1—P1xiv3.359 (12)O5B—O5Bxi0.9 (2)
O1—Na2B2.61 (7)O5B—O5Axi1.10 (9)
O1—Na2Axv2.91 (4)O5B—Na2Bxi2.07 (9)
O1—Na2A2.97 (4)
O2—Zn1—O2i121.9 (5)Na2Axv—Na2A—Na2Axi168 (4)
O2—Zn1—O398.9 (3)Na2Axv—Na2A—Na2B112 (6)
O2i—Zn1—O3118.0 (4)Na2Axi—Na2A—Na2B68 (3)
O2—Zn1—O3i118.0 (4)Na2Axv—Na2A—Na2Bxi133 (3)
O2i—Zn1—O3i98.9 (3)Na2Axi—Na2A—Na2Bxi58 (3)
O3—Zn1—O3i99.9 (5)Na2B—Na2A—Na2Bxi72 (5)
O2—Zn1—Na1112.8 (3)Na2Axv—Na2A—Na2Bxv39 (4)
O2i—Zn1—Na1125.3 (3)Na2Axi—Na2A—Na2Bxv146 (4)
O3—Zn1—Na151.0 (3)Na2B—Na2A—Na2Bxv142 (4)
O3i—Zn1—Na149.6 (3)Na2Bxi—Na2A—Na2Bxv108 (3)
O2—Zn1—Na1i125.3 (3)Na2Axv—Na2A—Na2Aii167.5 (14)
O2i—Zn1—Na1i112.8 (3)Na2Axi—Na2A—Na2Aii5.1 (16)
O3—Zn1—Na1i49.6 (3)Na2B—Na2A—Na2Aii73 (3)
O3i—Zn1—Na1i51.0 (3)Na2Bxi—Na2A—Na2Aii59 (3)
Na1—Zn1—Na1i13.3 (3)Na2Bxv—Na2A—Na2Aii141 (2)
O2—Zn1—Na1ii42.8 (3)Na2Axv—Na2A—Na2Axii6 (2)
O2i—Zn1—Na1ii93.1 (3)Na2Axi—Na2A—Na2Axii163 (3)
O3—Zn1—Na1ii87.5 (3)Na2B—Na2A—Na2Axii115 (3)
O3i—Zn1—Na1ii160.7 (3)Na2Bxi—Na2A—Na2Axii139 (3)
Na1—Zn1—Na1ii131.9 (4)Na2Bxv—Na2A—Na2Axii39.7 (17)
Na1i—Zn1—Na1ii136.26 (16)Na2Aii—Na2A—Na2Axii161.1 (7)
O2—Zn1—Na1iii93.1 (3)Na2Axv—Na2A—Na2Bxii27.9 (19)
O2i—Zn1—Na1iii42.8 (3)Na2Axi—Na2A—Na2Bxii161.4 (15)
O3—Zn1—Na1iii160.7 (3)Na2B—Na2A—Na2Bxii97 (3)
O3i—Zn1—Na1iii87.5 (3)Na2Bxi—Na2A—Na2Bxii107 (4)
Na1—Zn1—Na1iii136.26 (16)Na2Bxv—Na2A—Na2Bxii45 (3)
Na1i—Zn1—Na1iii131.9 (4)Na2Aii—Na2A—Na2Bxii164.5 (18)
Na1ii—Zn1—Na1iii91.2 (3)Na2Axii—Na2A—Na2Bxii34.3 (16)
O1—Zn2—O1iv112.6 (5)Na2Axv—Na2A—O1xv81 (4)
O1—Zn2—O4ii110.2 (3)Na2Axi—Na2A—O1xv95.2 (15)
O1iv—Zn2—O4ii113.2 (3)Na2B—Na2A—O1xv158 (3)
O1—Zn2—O4v113.2 (3)Na2Bxi—Na2A—O1xv112 (3)
O1iv—Zn2—O4v110.2 (3)Na2Bxv—Na2A—O1xv59 (2)
O4ii—Zn2—O4v96.5 (4)Na2Aii—Na2A—O1xv90.4 (10)
O1—Zn2—Na1vi117.9 (3)Na2Axii—Na2A—O1xv76.2 (9)
O1iv—Zn2—Na1vi129.3 (3)Na2Bxii—Na2A—O1xv101.6 (17)
O4ii—Zn2—Na1vi51.9 (3)Na2Axv—Na2A—O5B105 (3)
O4v—Zn2—Na1vi45.1 (3)Na2Axi—Na2A—O5B84 (2)
O1—Zn2—Na1vii129.3 (3)Na2B—Na2A—O5B46 (3)
O1iv—Zn2—Na1vii117.9 (3)Na2Bxi—Na2A—O5B43 (3)
O4ii—Zn2—Na1vii45.1 (3)Na2Bxv—Na2A—O5B108 (3)
O4v—Zn2—Na1vii51.9 (3)Na2Aii—Na2A—O5B87 (3)
Na1vi—Zn2—Na1vii13.5 (3)Na2Axii—Na2A—O5B111 (3)
O4—P1—O2109.9 (4)Na2Bxii—Na2A—O5B78 (3)
O4—P1—O3viii107.5 (4)O1xv—Na2A—O5B150 (3)
O2—P1—O3viii108.4 (5)Na2Axv—Na2A—O176 (3)
O4—P1—O1110.7 (4)Na2Axi—Na2A—O195 (3)
O2—P1—O1108.9 (5)Na2B—Na2A—O161 (3)
O3viii—P1—O1111.3 (4)Na2Bxi—Na2A—O1133 (3)
O4—P1—Na2B134.6 (13)Na2Bxv—Na2A—O1113.0 (18)
O2—P1—Na2B51.6 (13)Na2Aii—Na2A—O198.3 (10)
O3viii—P1—Na2B117.5 (13)Na2Axii—Na2A—O173.8 (8)
O1—P1—Na2B58.1 (13)Na2Bxii—Na2A—O187.5 (18)
O4—P1—Na1ii119.2 (4)O1xv—Na2A—O1107.7 (11)
O2—P1—Na1ii57.3 (4)O5B—Na2A—O1102 (2)
O3viii—P1—Na1ii51.3 (4)Na2Axv—Na2A—Na2Bii148 (3)
O1—P1—Na1ii129.9 (4)Na2Axi—Na2A—Na2Bii21 (3)
Na2B—P1—Na1ii87.1 (13)Na2B—Na2A—Na2Bii64 (2)
O4—P1—Na1viii109.6 (4)Na2Bxi—Na2A—Na2Bii78 (3)
O2—P1—Na1viii66.7 (4)Na2Bxv—Na2A—Na2Bii153 (3)
O3viii—P1—Na1viii43.9 (4)Na2Aii—Na2A—Na2Bii23.1 (13)
O1—P1—Na1viii138.0 (4)Na2Axii—Na2A—Na2Bii143.2 (17)
Na2B—P1—Na1viii99.5 (13)Na2Bxii—Na2A—Na2Bii159 (2)
Na1ii—P1—Na1viii12.4 (3)O1xv—Na2A—Na2Bii94.6 (14)
Na1i—Na1—O4ix99.3 (12)O5B—Na2A—Na2Bii94 (3)
Na1i—Na1—O3i85.0 (13)O1—Na2A—Na2Bii75.5 (13)
O4ix—Na1—O3i174.8 (6)Na2A—Na2B—Na2Axi54 (3)
Na1i—Na1—O4x63.6 (11)Na2A—Na2B—Na2Bxi57 (3)
O4ix—Na1—O4x76.3 (5)Na2Axi—Na2B—Na2Bxi50 (3)
O3i—Na1—O4x103.3 (5)Na2A—Na2B—O5Bxi121 (5)
Na1i—Na1—O377.7 (12)Na2Axi—Na2B—O5Bxi103 (4)
O4ix—Na1—O3108.9 (6)Na2Bxi—Na2B—O5Bxi67 (3)
O3i—Na1—O374.7 (5)Na2A—Na2B—O5B103 (5)
O4x—Na1—O3141.1 (5)Na2Axi—Na2B—O5B107 (5)
Na1i—Na1—O5Axi164 (3)Na2Bxi—Na2B—O5B59 (3)
O4ix—Na1—O5Axi77.0 (10)O5Bxi—Na2B—O5B25 (6)
O3i—Na1—O5Axi99.6 (10)Na2A—Na2B—Na2Axv29 (3)
O4x—Na1—O5Axi128.7 (13)Na2Axi—Na2B—Na2Axv82 (3)
O3—Na1—O5Axi89.1 (13)Na2Bxi—Na2B—Na2Axv78 (4)
Na1i—Na1—O2xii125 (2)O5Bxi—Na2B—Na2Axv126 (5)
O4ix—Na1—O2xii116.1 (5)O5B—Na2B—Na2Axv101 (4)
O3i—Na1—O2xii58.8 (4)Na2A—Na2B—O2143 (4)
O4x—Na1—O2xii84.5 (4)Na2Axi—Na2B—O2142 (4)
O3—Na1—O2xii122.7 (5)Na2Bxi—Na2B—O2158 (2)
O5Axi—Na1—O2xii69.4 (12)O5Bxi—Na2B—O291 (3)
Na1i—Na1—O5B143 (3)O5B—Na2B—O2101 (4)
O4ix—Na1—O5B79.1 (17)Na2Axv—Na2B—O2118 (3)
O3i—Na1—O5B99.2 (17)Na2A—Na2B—O5A132 (4)
O4x—Na1—O5B147 (2)Na2Axi—Na2B—O5A93 (3)
O3—Na1—O5B68 (2)Na2Bxi—Na2B—O5A75 (3)
O5Axi—Na1—O5B22.0 (16)O5Bxi—Na2B—O5A26 (3)
O2xii—Na1—O5B87.2 (19)O5B—Na2B—O5A51 (4)
Na1i—Na1—P1xii104.9 (18)Na2Axv—Na2B—O5A149 (4)
O4ix—Na1—P1xii145.7 (5)O2—Na2B—O5A85 (2)
O3i—Na1—P1xii29.3 (2)Na2A—Na2B—O187 (3)
O4x—Na1—P1xii92.9 (4)Na2Axi—Na2B—O1103 (3)
O3—Na1—P1xii99.9 (4)Na2Bxi—Na2B—O1143 (2)
O5Axi—Na1—P1xii85.4 (11)O5Bxi—Na2B—O1150 (4)
O2xii—Na1—P1xii29.6 (2)O5B—Na2B—O1147 (4)
O5B—Na1—P1xii95.3 (17)Na2Axv—Na2B—O172.6 (19)
Na1i—Na1—Zn2xiii83.24 (17)O2—Na2B—O158.9 (16)
O4ix—Na1—Zn2xiii38.2 (2)O5A—Na2B—O1138 (3)
O3i—Na1—Zn2xiii140.6 (5)Na2A—Na2B—Na2Aii72 (3)
O4x—Na1—Zn2xiii38.5 (2)Na2Axi—Na2B—Na2Aii18.8 (15)
O3—Na1—Zn2xiii137.9 (5)Na2Bxi—Na2B—Na2Aii57 (3)
O5Axi—Na1—Zn2xiii101.7 (10)O5Bxi—Na2B—Na2Aii94 (4)
O2xii—Na1—Zn2xiii99.0 (4)O5B—Na2B—Na2Aii105 (4)
O5B—Na1—Zn2xiii112.7 (19)Na2Axv—Na2B—Na2Aii100 (3)
P1xii—Na1—Zn2xiii121.3 (4)O2—Na2B—Na2Aii128 (3)
Na1i—Na1—Zn183.34 (17)O5A—Na2B—Na2Aii78 (2)
O4ix—Na1—Zn1145.5 (6)O1—Na2B—Na2Aii108 (2)
O3i—Na1—Zn137.5 (2)Na2A—Na2B—O5Axi87 (3)
O4x—Na1—Zn1132.7 (5)Na2Axi—Na2B—O5Axi111 (4)
O3—Na1—Zn137.6 (2)Na2Bxi—Na2B—O5Axi61 (3)
O5Axi—Na1—Zn191.2 (11)O5Bxi—Na2B—O5Axi48 (4)
O2xii—Na1—Zn188.7 (4)O5B—Na2B—O5Axi23 (3)
O5B—Na1—Zn178.5 (19)Na2Axv—Na2B—O5Axi79 (3)
P1xii—Na1—Zn162.7 (2)O2—Na2B—O5Axi104 (2)
Zn2xiii—Na1—Zn1166.6 (3)O5A—Na2B—O5Axi74 (3)
Na1i—Na1—P1xiv62.8 (17)O1—Na2B—O5Axi131 (3)
O4ix—Na1—P1xiv90.5 (4)Na2Aii—Na2B—O5Axi117 (3)
O3i—Na1—P1xiv94.0 (4)Na2A—Na2B—O5Axvii140 (4)
O4x—Na1—P1xiv121.3 (4)Na2Axi—Na2B—O5Axvii87 (3)
O3—Na1—P1xiv25.2 (2)Na2Bxi—Na2B—O5Axvii102 (4)
O5Axi—Na1—P1xiv101.8 (14)O5Bxi—Na2B—O5Axvii66 (4)
O2xii—Na1—P1xiv147.7 (4)O5B—Na2B—O5Axvii91 (4)
O5B—Na1—P1xiv80 (2)Na2Axv—Na2B—O5Axvii165 (3)
P1xii—Na1—P1xiv122.1 (3)O2—Na2B—O5Axvii67.0 (19)
Zn2xiii—Na1—P1xiv113.3 (3)O5A—Na2B—O5Axvii41 (2)
Zn1—Na1—P1xiv59.82 (19)O1—Na2B—O5Axvii101 (2)
P1—O1—Zn2128.2 (5)Na2Aii—Na2B—O5Axvii68 (2)
P1—O1—Na2B92.1 (16)O5Axi—Na2B—O5Axvii114 (3)
Zn2—O1—Na2B137.0 (15)O5Bxi—O5A—Na2B56 (5)
P1—O1—Na2Axv130.5 (9)O5Bxi—O5A—Na1xi98 (5)
Zn2—O1—Na2Axv99.8 (8)Na2B—O5A—Na1xi152 (3)
Na2B—O1—Na2Axv48.6 (18)O5Bxi—O5A—Na2Bxi51 (5)
P1—O1—Na2A123.5 (8)Na2B—O5A—Na2Bxi44 (3)
Zn2—O1—Na2A107.6 (8)Na1xi—O5A—Na2Bxi113 (2)
Na2B—O1—Na2A31.8 (15)O5Bxi—O5A—Na2Bxvii124 (5)
Na2Axv—O1—Na2A23.1 (11)Na2B—O5A—Na2Bxvii85 (3)
P1—O2—Zn1122.5 (4)Na1xi—O5A—Na2Bxvii105 (2)
P1—O2—Na2B99.0 (16)Na2Bxi—O5A—Na2Bxvii72 (2)
Zn1—O2—Na2B118.2 (16)O5Bxi—O5B—O5Axi170 (10)
P1—O2—Na1ii93.1 (5)O5Bxi—O5B—Na2Bxi86 (7)
Zn1—O2—Na1ii107.1 (4)O5Axi—O5B—Na2Bxi98 (6)
Na2B—O2—Na1ii114.7 (16)O5Bxi—O5B—Na2B69 (6)
P1xiv—O3—Zn1139.6 (6)O5Axi—O5B—Na2B106 (6)
P1xiv—O3—Na1i99.4 (5)Na2Bxi—O5B—Na2B54 (4)
Zn1—O3—Na1i92.9 (4)O5Bxi—O5B—Na1114 (8)
P1xiv—O3—Na1110.9 (5)O5Axi—O5B—Na160 (5)
Zn1—O3—Na191.4 (4)Na2Bxi—O5B—Na1155 (5)
Na1i—O3—Na117.3 (4)Na2B—O5B—Na1118 (4)
P1—O4—Zn2xii119.1 (4)O5Bxi—O5B—Na2A94 (3)
P1—O4—Na1xvi143.8 (5)O5Axi—O5B—Na2A85 (5)
Zn2xii—O4—Na1xvi96.7 (4)Na2Bxi—O5B—Na2A34 (2)
P1—O4—Na1iii144.5 (5)Na2B—O5B—Na2A31 (2)
Zn2xii—O4—Na1iii89.6 (4)Na1—O5B—Na2A125 (4)
Na1xvi—O4—Na1iii17.2 (4)
O2—Zn1—Na1—Na1i161.3 (19)Na2Bxi—Na2A—Na2B—O5A8 (4)
O2i—Zn1—Na1—Na1i21 (2)Na2Bxv—Na2A—Na2B—O5A105 (5)
O3—Zn1—Na1—Na1i78 (2)Na2Aii—Na2A—Na2B—O5A54 (5)
O3i—Zn1—Na1—Na1i90 (2)Na2Axii—Na2A—Na2B—O5A144 (4)
Na1ii—Zn1—Na1—Na1i115.2 (19)Na2Bxii—Na2A—Na2B—O5A113 (5)
Na1iii—Zn1—Na1—Na1i77 (2)O1xv—Na2A—Na2B—O5A98 (9)
O2—Zn1—Na1—O4ix64.6 (8)O5B—Na2A—Na2B—O5A48 (6)
O2i—Zn1—Na1—O4ix117.9 (7)O1—Na2A—Na2B—O5A164 (6)
O3—Zn1—Na1—O4ix18.3 (7)Na2Bii—Na2A—Na2B—O5A77 (5)
O3i—Zn1—Na1—O4ix172.8 (9)Na2Axv—Na2A—Na2B—O158 (2)
Na1i—Zn1—Na1—O4ix97 (2)Na2Axi—Na2A—Na2B—O1109 (3)
Na1ii—Zn1—Na1—O4ix18.4 (10)Na2Bxi—Na2A—Na2B—O1171 (4)
Na1iii—Zn1—Na1—O4ix173.8 (7)Na2Bxv—Na2A—Na2B—O191 (6)
O2—Zn1—Na1—O3i108.2 (5)Na2Aii—Na2A—Na2B—O1109.7 (19)
O2i—Zn1—Na1—O3i69.3 (5)Na2Axii—Na2A—Na2B—O152 (3)
O3—Zn1—Na1—O3i168.9 (3)Na2Bxii—Na2A—Na2B—O183 (2)
Na1i—Zn1—Na1—O3i90 (2)O1xv—Na2A—Na2B—O165 (9)
Na1ii—Zn1—Na1—O3i154.4 (4)O5B—Na2A—Na2B—O1148 (5)
Na1iii—Zn1—Na1—O3i13.4 (4)Na2Bii—Na2A—Na2B—O186.8 (19)
O2—Zn1—Na1—O4x154.6 (6)Na2Axv—Na2A—Na2B—Na2Aii168.0 (10)
O2i—Zn1—Na1—O4x22.9 (8)Na2Axi—Na2A—Na2B—Na2Aii0 (3)
O3—Zn1—Na1—O4x122.5 (7)Na2Bxi—Na2A—Na2B—Na2Aii62 (3)
O3i—Zn1—Na1—O4x46.4 (6)Na2Bxv—Na2A—Na2B—Na2Aii159 (5)
Na1i—Zn1—Na1—O4x44.1 (16)Na2Axii—Na2A—Na2B—Na2Aii162.0 (12)
Na1ii—Zn1—Na1—O4x159.2 (4)Na2Bxii—Na2A—Na2B—Na2Aii167.4 (15)
Na1iii—Zn1—Na1—O4x33.0 (6)O1xv—Na2A—Na2B—Na2Aii44 (9)
O2—Zn1—Na1—O382.9 (4)O5B—Na2A—Na2B—Na2Aii102 (4)
O2i—Zn1—Na1—O399.7 (5)O1—Na2A—Na2B—Na2Aii109.7 (19)
O3i—Zn1—Na1—O3168.9 (3)Na2Bii—Na2A—Na2B—Na2Aii22.9 (10)
Na1i—Zn1—Na1—O378 (2)Na2Axv—Na2A—Na2B—O5Axi73 (3)
Na1ii—Zn1—Na1—O336.7 (5)Na2Axi—Na2A—Na2B—O5Axi119 (3)
Na1iii—Zn1—Na1—O3155.6 (4)Na2Bxi—Na2A—Na2B—O5Axi57 (3)
O2—Zn1—Na1—O5Axi4.0 (13)Na2Bxv—Na2A—Na2B—O5Axi40 (6)
O2i—Zn1—Na1—O5Axi173.5 (13)Na2Aii—Na2A—Na2B—O5Axi119 (2)
O3—Zn1—Na1—O5Axi86.9 (13)Na2Axii—Na2A—Na2B—O5Axi79 (3)
O3i—Zn1—Na1—O5Axi104.2 (13)Na2Bxii—Na2A—Na2B—O5Axi48 (3)
Na1i—Zn1—Na1—O5Axi165 (3)O1xv—Na2A—Na2B—O5Axi163 (7)
Na1ii—Zn1—Na1—O5Axi50.1 (14)O5B—Na2A—Na2B—O5Axi17 (3)
Na1iii—Zn1—Na1—O5Axi117.6 (13)O1—Na2A—Na2B—O5Axi131 (3)
O2—Zn1—Na1—O2xii73.4 (4)Na2Bii—Na2A—Na2B—O5Axi141.9 (19)
O2i—Zn1—Na1—O2xii104.1 (4)Na2Axv—Na2A—Na2B—O5Axvii162 (5)
O3—Zn1—Na1—O2xii156.3 (5)Na2Axi—Na2A—Na2B—O5Axvii5 (6)
O3i—Zn1—Na1—O2xii34.8 (4)Na2Bxi—Na2A—Na2B—O5Axvii67 (6)
Na1i—Zn1—Na1—O2xii125 (2)Na2Bxv—Na2A—Na2B—O5Axvii165 (3)
Na1ii—Zn1—Na1—O2xii119.5 (4)Na2Aii—Na2A—Na2B—O5Axvii6 (5)
Na1iii—Zn1—Na1—O2xii48.2 (3)Na2Axii—Na2A—Na2B—O5Axvii156 (4)
O2—Zn1—Na1—O5B14 (2)Na2Bxii—Na2A—Na2B—O5Axvii173 (4)
O2i—Zn1—Na1—O5B168 (2)O1xv—Na2A—Na2B—O5Axvii39 (13)
O3—Zn1—Na1—O5B69 (2)O5B—Na2A—Na2B—O5Axvii108 (7)
O3i—Zn1—Na1—O5B122 (2)O1—Na2A—Na2B—O5Axvii104 (6)
Na1i—Zn1—Na1—O5B147 (3)Na2Bii—Na2A—Na2B—O5Axvii17 (5)
Na1ii—Zn1—Na1—O5B32 (2)P1—O2—Na2B—Na2A32 (7)
Na1iii—Zn1—Na1—O5B136 (2)Zn1—O2—Na2B—Na2A103 (6)
O2—Zn1—Na1—P1xii88.1 (3)Na1ii—O2—Na2B—Na2A129 (6)
O2i—Zn1—Na1—P1xii89.3 (4)P1—O2—Na2B—Na2Axi64 (6)
O3—Zn1—Na1—P1xii171.0 (4)Zn1—O2—Na2B—Na2Axi161 (5)
O3i—Zn1—Na1—P1xii20.1 (3)Na1ii—O2—Na2B—Na2Axi34 (6)
Na1i—Zn1—Na1—P1xii111 (2)P1—O2—Na2B—Na2Bxi177 (14)
Na1ii—Zn1—Na1—P1xii134.3 (3)Zn1—O2—Na2B—Na2Bxi48 (15)
Na1iii—Zn1—Na1—P1xii33.4 (2)Na1ii—O2—Na2B—Na2Bxi80 (14)
O2—Zn1—Na1—Zn2xiii161 (2)P1—O2—Na2B—O5Bxi177 (4)
O2i—Zn1—Na1—Zn2xiii21 (2)Zn1—O2—Na2B—O5Bxi48 (4)
O3—Zn1—Na1—Zn2xiii78 (2)Na1ii—O2—Na2B—O5Bxi80 (4)
O3i—Zn1—Na1—Zn2xiii90 (2)P1—O2—Na2B—O5B159 (4)
Na1i—Zn1—Na1—Zn2xiii0.001 (5)Zn1—O2—Na2B—O5B25 (4)
Na1ii—Zn1—Na1—Zn2xiii115.2 (19)Na1ii—O2—Na2B—O5B103 (4)
Na1iii—Zn1—Na1—Zn2xiii77 (2)P1—O2—Na2B—Na2Axv51 (3)
O2—Zn1—Na1—P1xiv99.0 (3)Zn1—O2—Na2B—Na2Axv84 (3)
O2i—Zn1—Na1—P1xiv83.5 (4)Na1ii—O2—Na2B—Na2Axv148 (2)
O3—Zn1—Na1—P1xiv16.1 (3)P1—O2—Na2B—O5A152.0 (18)
O3i—Zn1—Na1—P1xiv152.8 (4)Zn1—O2—Na2B—O5A73 (2)
Na1i—Zn1—Na1—P1xiv62 (2)Na1ii—O2—Na2B—O5A54 (2)
Na1ii—Zn1—Na1—P1xiv52.8 (4)P1—O2—Na2B—O16.6 (11)
Na1iii—Zn1—Na1—P1xiv139.4 (2)Zn1—O2—Na2B—O1127.9 (8)
O4—P1—O1—Zn265.8 (6)Na1ii—O2—Na2B—O1104.2 (10)
O2—P1—O1—Zn2173.2 (5)P1—O2—Na2B—Na2Aii82 (3)
O3viii—P1—O1—Zn253.8 (7)Zn1—O2—Na2B—Na2Aii143 (3)
Na2B—P1—O1—Zn2163.7 (16)Na1ii—O2—Na2B—Na2Aii15 (4)
Na1ii—P1—O1—Zn2110.4 (6)P1—O2—Na2B—O5Axi136 (2)
Na1viii—P1—O1—Zn297.4 (6)Zn1—O2—Na2B—O5Axi2 (3)
O4—P1—O1—Na2B130.5 (15)Na1ii—O2—Na2B—O5Axi126 (2)
O2—P1—O1—Na2B9.5 (15)P1—O2—Na2B—O5Axvii113.7 (13)
O3viii—P1—O1—Na2B110.0 (15)Zn1—O2—Na2B—O5Axvii111.8 (15)
Na1ii—P1—O1—Na2B53.3 (16)Na1ii—O2—Na2B—O5Axvii16.1 (18)
Na1viii—P1—O1—Na2B66.3 (16)P1—O1—Na2B—Na2A172 (3)
O4—P1—O1—Na2Axv97.6 (10)Zn2—O1—Na2B—Na2A27 (4)
O2—P1—O1—Na2Axv23.4 (10)Na2Axv—O1—Na2B—Na2A25 (2)
O3viii—P1—O1—Na2Axv142.8 (9)P1—O1—Na2B—Na2Axi137 (3)
Na2B—P1—O1—Na2Axv32.9 (16)Zn2—O1—Na2B—Na2Axi24 (5)
Na1ii—P1—O1—Na2Axv86.1 (10)Na2Axv—O1—Na2B—Na2Axi77 (4)
Na1viii—P1—O1—Na2Axv99.2 (10)Na2A—O1—Na2B—Na2Axi51 (3)
O4—P1—O1—Na2A125.4 (8)P1—O1—Na2B—Na2Bxi176 (8)
O2—P1—O1—Na2A4.4 (9)Zn2—O1—Na2B—Na2Bxi15 (10)
O3viii—P1—O1—Na2A115.1 (8)Na2Axv—O1—Na2B—Na2Bxi37 (8)
Na2B—P1—O1—Na2A5.1 (17)Na2A—O1—Na2B—Na2Bxi12 (6)
Na1ii—P1—O1—Na2A58.4 (9)P1—O1—Na2B—O5Bxi15 (9)
Na1viii—P1—O1—Na2A71.5 (10)Zn2—O1—Na2B—O5Bxi176 (8)
O1iv—Zn2—O1—P1155.6 (7)Na2Axv—O1—Na2B—O5Bxi132 (10)
O4ii—Zn2—O1—P177.0 (6)Na2A—O1—Na2B—O5Bxi157 (11)
O4v—Zn2—O1—P129.8 (7)P1—O1—Na2B—O5B63 (8)
Na1vi—Zn2—O1—P120.3 (7)Zn2—O1—Na2B—O5B135 (8)
Na1vii—Zn2—O1—P129.0 (8)Na2Axv—O1—Na2B—O5B83 (8)
O1iv—Zn2—O1—Na2B49 (2)Na2A—O1—Na2B—O5B108 (9)
O4ii—Zn2—O1—Na2B79 (2)P1—O1—Na2B—Na2Axv146.7 (15)
O4v—Zn2—O1—Na2B175 (2)Zn2—O1—Na2B—Na2Axv52 (3)
Na1vi—Zn2—O1—Na2B135 (2)Na2A—O1—Na2B—Na2Axv25 (2)
Na1vii—Zn2—O1—Na2B127 (2)P1—O1—Na2B—O26.6 (11)
O1iv—Zn2—O1—Na2Axv11.7 (6)Zn2—O1—Na2B—O2167.7 (10)
O4ii—Zn2—O1—Na2Axv115.7 (7)Na2Axv—O1—Na2B—O2140 (2)
O4v—Zn2—O1—Na2Axv137.5 (7)Na2A—O1—Na2B—O2165 (4)
Na1vi—Zn2—O1—Na2Axv172.4 (7)P1—O1—Na2B—O5A27 (4)
Na1vii—Zn2—O1—Na2Axv163.7 (7)Zn2—O1—Na2B—O5A135 (4)
O1iv—Zn2—O1—Na2A34.1 (6)Na2Axv—O1—Na2B—O5A173 (6)
O4ii—Zn2—O1—Na2A93.3 (7)Na2A—O1—Na2B—O5A162 (7)
O4v—Zn2—O1—Na2A160.0 (6)P1—O1—Na2B—Na2Aii118 (2)
Na1vi—Zn2—O1—Na2A150.0 (7)Zn2—O1—Na2B—Na2Aii43 (4)
Na1vii—Zn2—O1—Na2A141.2 (7)Na2Axv—O1—Na2B—Na2Aii96 (3)
O4—P1—O2—Zn10.0 (8)Na2A—O1—Na2B—Na2Aii70 (3)
O3viii—P1—O2—Zn1117.3 (6)P1—O1—Na2B—O5Axi88 (4)
O1—P1—O2—Zn1121.5 (6)Zn2—O1—Na2B—O5Axi110 (3)
Na2B—P1—O2—Zn1131.8 (18)Na2Axv—O1—Na2B—O5Axi58 (3)
Na1ii—P1—O2—Zn1112.6 (7)Na2A—O1—Na2B—O5Axi83 (4)
Na1viii—P1—O2—Zn1103.4 (6)P1—O1—Na2B—O5Axvii47.6 (19)
O4—P1—O2—Na2B131.8 (17)Zn2—O1—Na2B—O5Axvii114 (2)
O3viii—P1—O2—Na2B110.9 (17)Na2Axv—O1—Na2B—O5Axvii166 (3)
O1—P1—O2—Na2B10.3 (17)Na2A—O1—Na2B—O5Axvii141 (4)
Na1ii—P1—O2—Na2B115.6 (17)Na2A—Na2B—O5A—O5Bxi74 (8)
Na1viii—P1—O2—Na2B124.8 (17)Na2Axi—Na2B—O5A—O5Bxi115 (7)
O4—P1—O2—Na1ii112.6 (4)Na2Bxi—Na2B—O5A—O5Bxi67 (7)
O3viii—P1—O2—Na1ii4.7 (6)O5B—Na2B—O5A—O5Bxi5 (9)
O1—P1—O2—Na1ii125.9 (4)Na2Axv—Na2B—O5A—O5Bxi36 (9)
Na2B—P1—O2—Na1ii115.6 (17)O2—Na2B—O5A—O5Bxi103 (7)
Na1viii—P1—O2—Na1ii9.2 (4)O1—Na2B—O5A—O5Bxi131 (8)
O2i—Zn1—O2—P150.6 (5)Na2Aii—Na2B—O5A—O5Bxi126 (7)
O3—Zn1—O2—P1178.3 (6)O5Axi—Na2B—O5A—O5Bxi4 (6)
O3i—Zn1—O2—P172.0 (7)O5Axvii—Na2B—O5A—O5Bxi163 (7)
Na1—Zn1—O2—P1127.0 (6)Na2A—Na2B—O5A—Na1xi48 (9)
Na1i—Zn1—O2—P1132.2 (6)Na2Axi—Na2B—O5A—Na1xi89 (6)
Na1ii—Zn1—O2—P1105.2 (8)Na2Bxi—Na2B—O5A—Na1xi42 (6)
Na1iii—Zn1—O2—P116.8 (6)O5Bxi—Na2B—O5A—Na1xi26 (7)
O2i—Zn1—O2—Na2B173.9 (19)O5B—Na2B—O5A—Na1xi21 (6)
O3—Zn1—O2—Na2B54.9 (19)Na2Axv—Na2B—O5A—Na1xi11 (10)
O3i—Zn1—O2—Na2B51.4 (19)O2—Na2B—O5A—Na1xi129 (5)
Na1—Zn1—O2—Na2B3.6 (19)O1—Na2B—O5A—Na1xi157 (3)
Na1i—Zn1—O2—Na2B8.8 (19)Na2Aii—Na2B—O5A—Na1xi100 (5)
Na1ii—Zn1—O2—Na2B131.4 (19)O5Axi—Na2B—O5A—Na1xi22 (5)
Na1iii—Zn1—O2—Na2B140.2 (18)O5Axvii—Na2B—O5A—Na1xi171 (6)
O2i—Zn1—O2—Na1ii54.7 (3)Na2A—Na2B—O5A—Na2Bxi7 (4)
O3—Zn1—O2—Na1ii76.5 (4)Na2Axi—Na2B—O5A—Na2Bxi48 (3)
O3i—Zn1—O2—Na1ii177.2 (4)O5Bxi—Na2B—O5A—Na2Bxi67 (7)
Na1—Zn1—O2—Na1ii127.8 (5)O5B—Na2B—O5A—Na2Bxi62 (4)
Na1i—Zn1—O2—Na1ii122.6 (4)Na2Axv—Na2B—O5A—Na2Bxi31 (6)
Na1iii—Zn1—O2—Na1ii88.4 (5)O2—Na2B—O5A—Na2Bxi170 (4)
O2—Zn1—O3—P1xiv122.4 (8)O1—Na2B—O5A—Na2Bxi162 (6)
O2i—Zn1—O3—P1xiv11.2 (9)Na2Aii—Na2B—O5A—Na2Bxi59 (3)
O3i—Zn1—O3—P1xiv116.9 (9)O5Axi—Na2B—O5A—Na2Bxi64 (3)
Na1—Zn1—O3—P1xiv125.5 (9)O5Axvii—Na2B—O5A—Na2Bxi129 (4)
Na1i—Zn1—O3—P1xiv108.2 (9)Na2A—Na2B—O5A—Na2Bxvii63 (5)
Na1ii—Zn1—O3—P1xiv81.0 (8)Na2Axi—Na2B—O5A—Na2Bxvii22 (3)
Na1iii—Zn1—O3—P1xiv5.4 (16)Na2Bxi—Na2B—O5A—Na2Bxvii70 (3)
O2—Zn1—O3—Na1i129.4 (4)O5Bxi—Na2B—O5A—Na2Bxvii137 (7)
O2i—Zn1—O3—Na1i97.0 (4)O5B—Na2B—O5A—Na2Bxvii132 (4)
O3i—Zn1—O3—Na1i8.7 (2)Na2Axv—Na2B—O5A—Na2Bxvii101 (6)
Na1—Zn1—O3—Na1i17.2 (4)O2—Na2B—O5A—Na2Bxvii120 (3)
Na1ii—Zn1—O3—Na1i170.8 (3)O1—Na2B—O5A—Na2Bxvii92 (5)
Na1iii—Zn1—O3—Na1i102.8 (10)Na2Aii—Na2B—O5A—Na2Bxvii10.9 (13)
O2—Zn1—O3—Na1112.2 (4)O5Axi—Na2B—O5A—Na2Bxvii134 (3)
O2i—Zn1—O3—Na1114.3 (4)O5Axvii—Na2B—O5A—Na2Bxvii59 (3)
O3i—Zn1—O3—Na18.5 (2)Na2A—Na2B—O5B—O5Bxi140 (11)
Na1i—Zn1—O3—Na117.2 (4)Na2Axi—Na2B—O5B—O5Bxi84 (11)
Na1ii—Zn1—O3—Na1153.5 (4)Na2Bxi—Na2B—O5B—O5Bxi101 (12)
Na1iii—Zn1—O3—Na1120.0 (7)Na2Axv—Na2B—O5B—O5Bxi169 (10)
Na1i—Na1—O3—P1xiv50.5 (17)O2—Na2B—O5B—O5Bxi69 (11)
O4ix—Na1—O3—P1xiv45.2 (6)O5A—Na2B—O5B—O5Bxi5 (9)
O3i—Na1—O3—P1xiv138.7 (7)O1—Na2B—O5B—O5Bxi116 (13)
O4x—Na1—O3—P1xiv46.4 (11)Na2Aii—Na2B—O5B—O5Bxi65 (11)
O5Axi—Na1—O3—P1xiv121.1 (11)O5Axi—Na2B—O5B—O5Bxi171 (17)
O2xii—Na1—O3—P1xiv174.2 (5)O5Axvii—Na2B—O5B—O5Bxi2 (11)
O5B—Na1—O3—P1xiv114.5 (18)Na2A—Na2B—O5B—O5Axi49 (8)
P1xii—Na1—O3—P1xiv153.7 (4)Na2Axi—Na2B—O5B—O5Axi104 (7)
Zn2xiii—Na1—O3—P1xiv14.5 (9)Na2Bxi—Na2B—O5B—O5Axi88 (8)
Zn1—Na1—O3—P1xiv145.6 (7)O5Bxi—Na2B—O5B—O5Axi171 (17)
Na1i—Na1—O3—Zn195.1 (16)Na2Axv—Na2B—O5B—O5Axi20 (8)
O4ix—Na1—O3—Zn1169.2 (4)O2—Na2B—O5B—O5Axi102 (7)
O3i—Na1—O3—Zn16.97 (19)O5A—Na2B—O5B—O5Axi176 (8)
O4x—Na1—O3—Zn199.3 (9)O1—Na2B—O5B—O5Axi55 (12)
O5Axi—Na1—O3—Zn193.2 (10)Na2Aii—Na2B—O5B—O5Axi124 (7)
O2xii—Na1—O3—Zn128.6 (6)O5Axvii—Na2B—O5B—O5Axi169 (7)
O5B—Na1—O3—Zn199.9 (18)Na2A—Na2B—O5B—Na2Bxi39 (3)
P1xii—Na1—O3—Zn18.1 (4)Na2Axi—Na2B—O5B—Na2Bxi16 (4)
Zn2xiii—Na1—O3—Zn1160.2 (5)O5Bxi—Na2B—O5B—Na2Bxi101 (12)
P1xiv—Na1—O3—Zn1145.6 (7)Na2Axv—Na2B—O5B—Na2Bxi68 (4)
O4ix—Na1—O3—Na1i95.7 (16)O2—Na2B—O5B—Na2Bxi170 (6)
O3i—Na1—O3—Na1i88.1 (17)O5A—Na2B—O5B—Na2Bxi96 (5)
O4x—Na1—O3—Na1i4.2 (11)O1—Na2B—O5B—Na2Bxi143 (10)
O5Axi—Na1—O3—Na1i172 (2)Na2Aii—Na2B—O5B—Na2Bxi36 (4)
O2xii—Na1—O3—Na1i124 (2)O5Axi—Na2B—O5B—Na2Bxi88 (8)
O5B—Na1—O3—Na1i165 (2)O5Axvii—Na2B—O5B—Na2Bxi103 (4)
P1xii—Na1—O3—Na1i103.2 (17)Na2A—Na2B—O5B—Na1113 (5)
Zn2xiii—Na1—O3—Na1i65.1 (14)Na2Axi—Na2B—O5B—Na1168 (4)
Zn1—Na1—O3—Na1i95.1 (16)Na2Bxi—Na2B—O5B—Na1152 (6)
P1xiv—Na1—O3—Na1i50.5 (17)O5Bxi—Na2B—O5B—Na1107 (11)
O2—P1—O4—Zn2xii92.7 (6)Na2Axv—Na2B—O5B—Na184 (5)
O3viii—P1—O4—Zn2xii149.4 (5)O2—Na2B—O5B—Na138 (5)
O1—P1—O4—Zn2xii27.7 (6)O5A—Na2B—O5B—Na1113 (5)
Na2B—P1—O4—Zn2xii37.5 (19)O1—Na2B—O5B—Na19 (11)
Na1ii—P1—O4—Zn2xii155.6 (3)Na2Aii—Na2B—O5B—Na1172 (3)
Na1viii—P1—O4—Zn2xii164.2 (3)O5Axi—Na2B—O5B—Na164 (7)
O2—P1—O4—Na1xvi76.7 (9)O5Axvii—Na2B—O5B—Na1105 (5)
O3viii—P1—O4—Na1xvi41.1 (9)Na2Axi—Na2B—O5B—Na2A56 (4)
O1—P1—O4—Na1xvi162.9 (8)Na2Bxi—Na2B—O5B—Na2A39 (3)
Na2B—P1—O4—Na1xvi132.0 (19)O5Bxi—Na2B—O5B—Na2A140 (11)
Na1ii—P1—O4—Na1xvi13.8 (10)Na2Axv—Na2B—O5B—Na2A29 (3)
Na1viii—P1—O4—Na1xvi5.3 (9)O2—Na2B—O5B—Na2A151 (5)
O2—P1—O4—Na1iii47.3 (9)O5A—Na2B—O5B—Na2A135 (4)
O3viii—P1—O4—Na1iii70.6 (9)O1—Na2B—O5B—Na2A104 (9)
O1—P1—O4—Na1iii167.7 (7)Na2Aii—Na2B—O5B—Na2A75 (4)
Na2B—P1—O4—Na1iii103 (2)O5Axi—Na2B—O5B—Na2A49 (8)
Na1ii—P1—O4—Na1iii15.7 (9)O5Axvii—Na2B—O5B—Na2A142 (5)
Na1viii—P1—O4—Na1iii24.2 (9)Na1i—Na1—O5B—O5Bxi16 (13)
P1—O1—Na2A—Na2Axv116 (3)O4ix—Na1—O5B—O5Bxi107 (11)
Zn2—O1—Na2A—Na2Axv73 (2)O3i—Na1—O5B—O5Bxi78 (10)
Na2B—O1—Na2A—Na2Axv126 (4)O4x—Na1—O5B—O5Bxi149 (9)
P1—O1—Na2A—Na2Axi71.4 (7)O3—Na1—O5B—O5Bxi9 (10)
Zn2—O1—Na2A—Na2Axi99.5 (6)O5Axi—Na1—O5B—O5Bxi171 (15)
Na2B—O1—Na2A—Na2Axi62 (3)O2xii—Na1—O5B—O5Bxi136 (11)
Na2Axv—O1—Na2A—Na2Axi173 (3)P1xii—Na1—O5B—O5Bxi107 (10)
P1—O1—Na2A—Na2B10 (3)Zn2xiii—Na1—O5B—O5Bxi126 (10)
Zn2—O1—Na2A—Na2B161 (3)Zn1—Na1—O5B—O5Bxi47 (10)
Na2Axv—O1—Na2A—Na2B126 (4)P1xiv—Na1—O5B—O5Bxi14 (10)
P1—O1—Na2A—Na2Bxi21 (4)Na1i—Na1—O5B—O5Axi173 (4)
Zn2—O1—Na2A—Na2Bxi150 (3)O4ix—Na1—O5B—O5Axi82 (5)
Na2B—O1—Na2A—Na2Bxi11 (5)O3i—Na1—O5B—O5Axi93 (5)
Na2Axv—O1—Na2A—Na2Bxi137 (4)O4x—Na1—O5B—O5Axi40 (7)
P1—O1—Na2A—Na2Bxv129 (2)O3—Na1—O5B—O5Axi162 (6)
Zn2—O1—Na2A—Na2Bxv61 (2)O2xii—Na1—O5B—O5Axi35 (5)
Na2B—O1—Na2A—Na2Bxv138 (4)P1xii—Na1—O5B—O5Axi64 (5)
Na2Axv—O1—Na2A—Na2Bxv13 (3)Zn2xiii—Na1—O5B—O5Axi64 (6)
P1—O1—Na2A—Na2Aii75.4 (11)Zn1—Na1—O5B—O5Axi124 (6)
Zn2—O1—Na2A—Na2Aii95.4 (11)P1xiv—Na1—O5B—O5Axi175 (6)
Na2B—O1—Na2A—Na2Aii66 (3)Na1i—Na1—O5B—Na2Bxi158 (9)
Na2Axv—O1—Na2A—Na2Aii169 (3)O4ix—Na1—O5B—Na2Bxi111 (11)
P1—O1—Na2A—Na2Axii122.2 (9)O3i—Na1—O5B—Na2Bxi64 (11)
Zn2—O1—Na2A—Na2Axii67.0 (9)O4x—Na1—O5B—Na2Bxi69 (11)
Na2B—O1—Na2A—Na2Axii132 (3)O3—Na1—O5B—Na2Bxi133 (11)
Na2Axv—O1—Na2A—Na2Axii6 (3)O5Axi—Na1—O5B—Na2Bxi29 (8)
P1—O1—Na2A—Na2Bxii90.2 (16)O2xii—Na1—O5B—Na2Bxi6 (11)
Zn2—O1—Na2A—Na2Bxii99.0 (16)P1xii—Na1—O5B—Na2Bxi35 (11)
Na2B—O1—Na2A—Na2Bxii100 (3)Zn2xiii—Na1—O5B—Na2Bxi92 (10)
Na2Axv—O1—Na2A—Na2Bxii26 (3)Zn1—Na1—O5B—Na2Bxi95 (11)
P1—O1—Na2A—O1xv168.5 (7)P1xiv—Na1—O5B—Na2Bxi156 (11)
Zn2—O1—Na2A—O1xv2.3 (10)Na1i—Na1—O5B—Na2B94 (5)
Na2B—O1—Na2A—O1xv159 (3)O4ix—Na1—O5B—Na2B175 (5)
Na2Axv—O1—Na2A—O1xv76 (3)O3i—Na1—O5B—Na2B0 (5)
P1—O1—Na2A—O5B13 (3)O4x—Na1—O5B—Na2B133 (4)
Zn2—O1—Na2A—O5B176 (2)O3—Na1—O5B—Na2B69 (5)
Na2B—O1—Na2A—O5B23 (4)O5Axi—Na1—O5B—Na2B93 (7)
Na2Axv—O1—Na2A—O5B103 (3)O2xii—Na1—O5B—Na2B58 (5)
P1—O1—Na2A—Na2Bii78.3 (14)P1xii—Na1—O5B—Na2B29 (5)
Zn2—O1—Na2A—Na2Bii92.5 (13)Zn2xiii—Na1—O5B—Na2B156 (4)
Na2B—O1—Na2A—Na2Bii69 (3)Zn1—Na1—O5B—Na2B32 (5)
Na2Axv—O1—Na2A—Na2Bii166 (3)P1xiv—Na1—O5B—Na2B93 (5)
Na2Axv—Na2A—Na2B—Na2Axi167 (4)Na1i—Na1—O5B—Na2A130 (4)
Na2Bxi—Na2A—Na2B—Na2Axi62 (3)O4ix—Na1—O5B—Na2A139 (5)
Na2Bxv—Na2A—Na2B—Na2Axi159 (6)O3i—Na1—O5B—Na2A36 (5)
Na2Aii—Na2A—Na2B—Na2Axi0 (3)O4x—Na1—O5B—Na2A97 (4)
Na2Axii—Na2A—Na2B—Na2Axi161 (4)O3—Na1—O5B—Na2A105 (4)
Na2Bxii—Na2A—Na2B—Na2Axi168 (4)O5Axi—Na1—O5B—Na2A57 (5)
O1xv—Na2A—Na2B—Na2Axi44 (8)O2xii—Na1—O5B—Na2A22 (4)
O5B—Na2A—Na2B—Na2Axi102 (5)P1xii—Na1—O5B—Na2A6 (4)
O1—Na2A—Na2B—Na2Axi109 (3)Zn2xiii—Na1—O5B—Na2A121 (4)
Na2Bii—Na2A—Na2B—Na2Axi22 (3)Zn1—Na1—O5B—Na2A67 (4)
Na2Axv—Na2A—Na2B—Na2Bxi130 (4)P1xiv—Na1—O5B—Na2A128 (4)
Na2Axi—Na2A—Na2B—Na2Bxi62 (3)Na2Axv—Na2A—O5B—O5Bxi143 (12)
Na2Bxv—Na2A—Na2B—Na2Bxi97 (6)Na2Axi—Na2A—O5B—O5Bxi29 (12)
Na2Aii—Na2A—Na2B—Na2Bxi62 (3)Na2B—Na2A—O5B—O5Bxi37 (11)
Na2Axii—Na2A—Na2B—Na2Bxi136 (4)Na2Bxi—Na2A—O5B—O5Bxi77 (13)
Na2Bxii—Na2A—Na2B—Na2Bxi106 (4)Na2Bxv—Na2A—O5B—O5Bxi176 (11)
O1xv—Na2A—Na2B—Na2Bxi106 (8)Na2Aii—Na2A—O5B—O5Bxi33 (12)
O5B—Na2A—Na2B—Na2Bxi40 (4)Na2Axii—Na2A—O5B—O5Bxi142 (11)
O1—Na2A—Na2B—Na2Bxi171 (4)Na2Bxii—Na2A—O5B—O5Bxi150 (12)
Na2Bii—Na2A—Na2B—Na2Bxi85 (3)O1xv—Na2A—O5B—O5Bxi118 (11)
Na2Axv—Na2A—Na2B—O5Bxi109 (5)O1—Na2A—O5B—O5Bxi65 (12)
Na2Axi—Na2A—Na2B—O5Bxi84 (5)Na2Bii—Na2A—O5B—O5Bxi11 (12)
Na2Bxi—Na2A—Na2B—O5Bxi22 (5)Na2Axv—Na2A—O5B—O5Axi27 (8)
Na2Bxv—Na2A—Na2B—O5Bxi76 (7)Na2Axi—Na2A—O5B—O5Axi161 (7)
Na2Aii—Na2A—Na2B—O5Bxi83 (5)Na2B—Na2A—O5B—O5Axi133 (8)
Na2Axii—Na2A—Na2B—O5Bxi115 (5)Na2Bxi—Na2A—O5B—O5Axi112 (8)
Na2Bxii—Na2A—Na2B—O5Bxi84 (6)Na2Bxv—Na2A—O5B—O5Axi14 (7)
O1xv—Na2A—Na2B—O5Bxi128 (8)Na2Aii—Na2A—O5B—O5Axi157 (6)
O5B—Na2A—Na2B—O5Bxi18 (7)Na2Axii—Na2A—O5B—O5Axi28 (7)
O1—Na2A—Na2B—O5Bxi167 (6)Na2Bxii—Na2A—O5B—O5Axi20 (6)
Na2Bii—Na2A—Na2B—O5Bxi106 (5)O1xv—Na2A—O5B—O5Axi72 (8)
Na2Axv—Na2A—Na2B—O5B90 (5)O1—Na2A—O5B—O5Axi105 (6)
Na2Axi—Na2A—Na2B—O5B102 (5)Na2Bii—Na2A—O5B—O5Axi179 (6)
Na2Bxi—Na2A—Na2B—O5B40 (4)Na2Axv—Na2A—O5B—Na2Bxi139 (7)
Na2Bxv—Na2A—Na2B—O5B57 (7)Na2Axi—Na2A—O5B—Na2Bxi49 (4)
Na2Aii—Na2A—Na2B—O5B102 (4)Na2B—Na2A—O5B—Na2Bxi114 (6)
Na2Axii—Na2A—Na2B—O5B96 (4)Na2Bxv—Na2A—O5B—Na2Bxi98 (5)
Na2Bxii—Na2A—Na2B—O5B65 (5)Na2Aii—Na2A—O5B—Na2Bxi45 (4)
O1xv—Na2A—Na2B—O5B146 (7)Na2Axii—Na2A—O5B—Na2Bxi140 (5)
O1—Na2A—Na2B—O5B148 (5)Na2Bxii—Na2A—O5B—Na2Bxi133 (5)
Na2Bii—Na2A—Na2B—O5B125 (4)O1xv—Na2A—O5B—Na2Bxi41 (7)
Na2Axi—Na2A—Na2B—Na2Axv167 (4)O1—Na2A—O5B—Na2Bxi143 (4)
Na2Bxi—Na2A—Na2B—Na2Axv130 (4)Na2Bii—Na2A—O5B—Na2Bxi66 (4)
Na2Bxv—Na2A—Na2B—Na2Axv33 (4)Na2Axv—Na2A—O5B—Na2B106 (7)
Na2Aii—Na2A—Na2B—Na2Axv168.0 (10)Na2Axi—Na2A—O5B—Na2B66 (5)
Na2Axii—Na2A—Na2B—Na2Axv6.0 (5)Na2Bxi—Na2A—O5B—Na2B114 (6)
Na2Bxii—Na2A—Na2B—Na2Axv24.7 (15)Na2Bxv—Na2A—O5B—Na2B147 (4)
O1xv—Na2A—Na2B—Na2Axv124 (9)Na2Aii—Na2A—O5B—Na2B70 (4)
O5B—Na2A—Na2B—Na2Axv90 (5)Na2Axii—Na2A—O5B—Na2B105 (5)
O1—Na2A—Na2B—Na2Axv58 (2)Na2Bxii—Na2A—O5B—Na2B113 (5)
Na2Bii—Na2A—Na2B—Na2Axv145.0 (17)O1xv—Na2A—O5B—Na2B155 (5)
Na2Axv—Na2A—Na2B—O237 (7)O1—Na2A—O5B—Na2B28 (4)
Na2Axi—Na2A—Na2B—O2130 (7)Na2Bii—Na2A—O5B—Na2B48 (4)
Na2Bxi—Na2A—Na2B—O2168 (8)Na2Axv—Na2A—O5B—Na120 (7)
Na2Bxv—Na2A—Na2B—O270 (10)Na2Axi—Na2A—O5B—Na1152 (5)
Na2Aii—Na2A—Na2B—O2131 (7)Na2B—Na2A—O5B—Na186 (6)
Na2Axii—Na2A—Na2B—O231 (7)Na2Bxi—Na2A—O5B—Na1159 (7)
Na2Bxii—Na2A—Na2B—O262 (7)Na2Bxv—Na2A—O5B—Na161 (5)
O1xv—Na2A—Na2B—O286 (11)Na2Aii—Na2A—O5B—Na1156 (4)
O5B—Na2A—Na2B—O2127 (8)Na2Axii—Na2A—O5B—Na119 (5)
O1—Na2A—Na2B—O221 (5)Na2Bxii—Na2A—O5B—Na126 (4)
Na2Bii—Na2A—Na2B—O2108 (7)O1xv—Na2A—O5B—Na1119 (4)
Na2Axv—Na2A—Na2B—O5A138 (5)O1—Na2A—O5B—Na158 (5)
Na2Axi—Na2A—Na2B—O5A54 (5)Na2Bii—Na2A—O5B—Na1134 (4)
Symmetry codes: (i) y1, x1, z+1/6; (ii) xy, x, z1/6; (iii) x1, x+y1, z+1/3; (iv) y, x, z+1/6; (v) x, x+y, z+1/3; (vi) y, x1, z+1/6; (vii) x+1, y, z; (viii) xy, y1, z; (ix) xy1, x, z1/6; (x) x1, x+y, z+1/3; (xi) x, xy, z1/6; (xii) y, x+y, z+1/6; (xiii) x1, y, z; (xiv) xy1, y1, z; (xv) xy, y, z; (xvi) y, x+y1, z+1/6; (xvii) y, x, z1/3.
 
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