Acta Crystallographica Section C

Crystal Structure Communications

Volume 64, Part 8 (August 2008)


inorganic compounds



Acta Cryst. (2008). C64, i69-i70    [ doi:10.1107/S0108270108020398 ]

Tl2CO3 at 3.56 GPa

A. Grzechnik and K. Friese

Abstract: The crystal structure of thallium carbonate, Tl2CO3 (C2/m, Z = 4), is stable at least up to 3.56 GPa, as demonstrated by hydrostatic single-crystal X-ray diffraction measurements in a diamond anvil cell at room temperature. Our results contradict earlier observations from the literature, which found a structural phase transition for this compound at about 2 GPa. Under atmospheric conditions, all atoms except for one O atom reside on the mirror plane in the high-pressure structure. The compression mainly affects the part of the structure where the nonbonded electron lone pairs on the Tl+ cations are located.

Formula: Tl2CO3

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