Journal of Applied Crystallography

Volume 27, Part 2 (April 1994)

research papers

 

Measurement of the static disorder contribution to the temperature factor in cubic stabilized ZrO₂

D. N. Argyriou

Abstract: Neutron powder diffraction has been used to measure the temperature factors of both the cation and the anion atoms in 10mol% Y₂O₃-ZrO₂ over the temperature range 15 to 1323 K. The Housley-Hess approach has been used to determine the static disorder term of the temperature factors for both the Zr/Y and O atoms. The static contribution was determined to be 1.04 (6) Å² for Zr/Y and 2.2 (1) Å² for O. From these results, a Debye temperature of 527 (20) K was calculated for this sample.

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