Journal of Applied Crystallography

Volume 34, Part 1 (February 2001)

research papers

J. Appl. Cryst. (2001). 34, 20-26 [ doi:10.1107/S0021889800017027 ]

X-ray topographic dislocation contrast visible in reflections orthogonal to the Burgers vectors of axial screw dislocations in hexagonal silicon carbide

W. M. Vetter and M. Dudley

Abstract: Contrast is associated with micropipes in X-ray topographs of SiC crystals obtained with prismatic reflections, representing an apparent violation of the g·b = 0 invisibility criterion. This is explained as a population of basal-plane dislocations with Burgers vectors of the set b = ${\textstyle{1 \over 3}}$ <11 ${\bar{2}}$ 0> that occur in a high density within a few micrometers of the micropipes, below the resolution of X-ray topography. These basal-plane dislocations could be observed under an electron microscope. The presence of the surfaces of the micropipes influences the dislocation images in the topographs taken with prismatic reflections, often resulting in a band of light contrast along the axes of the micropipes.